GVHD Lp

Nhm 1

: Ths.Trn Quang Hiu : C09-TP02

: 01.Vng Th Trn 02.Trn Th Ngc Sinh 03.Trn Th Thu Thy(301) 04.Phm Minh Trc 05.Phan Quc Trng 06.Nguyn Trn Minh Trang 07.Phm Th Thy Loan 08.Cao Th Huyn Trinh 1

09/23/11

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

S Lc V Du

Cu Trc,Dinh Dng

nh Hng Ca Cc Tc Nhn n Cht lng du

Thnh phn & Bo qun

Kim Ngim

09/23/11

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Du l gia v cn thit c dng hng ngy mn n thm h p dn,b dng. Du n c tinh lc t ngun gc thc vt, nm th lng trong mi trng bnh thng.

09/23/11

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

C kh nhiu loi du c xp vo loi du n c gm :

Du u phng
Du/cht bo Du/cht bo Du/cht bo Du lc/du Du vng (cha Du phu ng u t DDhoah u/ch ng bo tinh) dngnnh tng/du Du vng (bn tinh) Du liu (cc th)

Du u nnh

Du hng dng

Du m

Du -liu

v..v

Du liu (th)

Du liu (tinh)

Khng bo ha Khng bo ha Khng bo ha Khng bo ha Bo ha im si S dng Khng bo ha n ha bo haa ha Khng Khng bo Khng bo n Bo Bo ha ha im siim si S dng S dng Bo ha n im si S dng n a a a Chin, nu, du Nsalad, lmn u n, tr 18% 49% 33% 231C Khng bo ha Khng bo ha 14% 43% 43% 177C Nu n,u S du thchn Nsalad, dng c trn, chin n Bo ha 20% macgarin 11v 15% 69% 246C im si 24% 61% 241C n a salad, macgarin . vt, macgarin, to N n, n, 14% 43% 43% 232C Nu ugin du chin chn 14% 73% 11% 190C salad, lm macgarin Nu n, du 14% 73% 11% 215C salad, lm macgarin Chin p cho, chin khuy, nu 14% 73% 11% 225C n, du salad, lm macgarin

09/23/11

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Cu trc

Dinh dng

Cht bo ch yu c nhiu trong cc loi du m c mt vai tr c t u c c th biDi vi nh.t cao, khng tan trong nc, tan trong cc dung mi huc nh ether, chlorphorm, benzene, ru nng . ngu n sinh nng Ch t bo thuc nhm cht dinh dng chnh v l ng quan tr cc 1kg cht bo khi c to nn c C, H cho 9 Kcal lGing nh ng:carbonhydrate, du t chy trongt th v O nhng chng 1g ch cha cc nguyn t khc nh P v (trong khi:c tht m hay cht bt ch cho 4Kcal). N. Chng khc vi carbonhydrate chhp n choi mn t hn. cn gip Du m khng ch to cm quan ch d a O v t l n m thc n lu gi trong d dy to cm gic no. 09/23/11 5

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Du m chnh l dung mi tt ha tan cc vitamin A, D, E, K l nhng vitamin c nhiu chc nng quan trng trong c th . Cht bo hay lipid cn tham gia cu to cc t bo v dch th ca cc t chc, c bit l t chc no. Ngoi ra, cht bo cn tham gia vo qu trnh hnh thnh v c u trc ca cc hormone sinh dc, duy tr s mm mi ca ln da
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09/23/11

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

09/23/11

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

HHHH ! ! ! ! !

H !

HHHHHHH O ! ! ! ! ! ! ! !!

H-C-C-C-C-C-C=C-C-C=C-C-C-C-C-C-C-C-C-O-H ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! !

Acid linoleic chui 18C , polyunsaturated fat, mt hai cp H, c hai ni i C=C, l cht bo thng thng cc loi du thc vt.

H HHHH HHHH H HHHH HHH

09/23/11 8

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

09/23/11

Du n ti mu, dc ln c cc vng c n l trong

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Cn ghi r nhng mc sau y: + Thnh phn + Ni sn xut + Ngy sn xut v hn s dng + S l sn xut

Dy chuyn ng chai du

09/23/11

11

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Ni kh ro thong mt . Khng nn chai du di nh nng trc tip hoc gn nhng ni c nhit cao, chai du ang s dng cn c y np kn... thi hn s dng du c lu hn, trnh vic du b oxy ha, c mi i. Khng du s dng vo chai du. Nn du n vo l snh, chai, khng nn vo l bng kim loi nh st, ng, nhm, v chng thng lm cho du b hng, nht l l ng

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

L ng du n phi sch s v kh ro, np kn. Nu c nc trong l hoc nc bn ngoi lt vo, hoc vi khun cng vi khng kh thm nhp vo s lm du n chng hng. C th cho t mui rang nng vo du n theo t l 40 :1 mu i h p th thnh phn nc, lm cho du n ti mu v thm. nhit 10 n 15OC ct gi du n l tt nht, cao nht khng c qu 35 C. Cho mt t ht tiu, hi, qu, gng c kh nng chng oxy ho vo du n, khng nhng ngn nga du n b oxy ho m cn gi c mi thm.

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Mayonnaise

Khoai ty chin

Bnh ngt

Trong mi g 100 g Mayonnaise th a t bo * 100 bnh khoai t tyc c cha c 23 i 79 g chcht bo ch 35 gg cht t *100g ng bo Mo: Thay th qu mayonnaise tc k c th nc tn ng u nnhmt vi vt, bn hy bo ho cc thnh ph dinh d ng hay Mo: Ct mua loi bnh ngt t ch n ung ca bn nu bn khng Mo: Khi cc dm Balsamic v hm lng dtng sa chua i hoc phomt ilmnt sa s ch bo thay cchncgin m n trn sa lt,sc khe lnh mnh ng kca bn. phm. m s mu th cn hay tng cho tim gn kemn bng ng t. trong n La ch bngc s (khng vi b), bnh qumn chng thay th v n c c bnh m la th en nguyn h Thay th cc n ging cht bo cmnnn b mayonnaise trn gin. n m thayt.th hn n l hm l n hn ch t hloi cc loi khoai chin mn bngccni tho mtm kim cc mnt n nh mn. Ho c b lo cng nn c, tiu en v m lt c chua.

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

1.

TCVN 26271993 TCVN 63512010 TCVN 63521998 TCVN 61212010 TCVN 78682008 TCVN 26421993

Du thc vt-Phng php xc nh mu sc, mi v trong Du, m ng vt v thc vt-Xc nh hm lng tro

2.

3.

Du, m ng vt v thc vt-Xc nh hm lng ng, st, niken-Phng php quang ph hp th nguyn t dng l graphi Du, m ng vt v thc vt-Xc nh tr s peroxit

4.

5.

Du, m ng vt v thc vt- Este metyl axit bo _ Xc nh hm lng este v este metyl axit linolenic Du thc vt-Phng php xc nh nht
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6.
09/23/11

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Mu sc : Xc nh mu sc bng phng php cm quan: Rt du vo cc thy tinh ( ng knh 50 mm, cao 100 mm), chiu cao ca lp du khng c thp hn 50 mm, quan st trn nn trng. Dng cc t thch hp din t nh mu vng nht, vng, vng sm, vng vi nh xanh l cy, sm, da ch, Xc nh mu sc bng thang mu it tiu chun: Ch s mu c biu th bng s miligam it t do c trong 100ml dung dch

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

STT

S ml dung dch iot tiu chun 10.0 9.0 8.0 7.0 6.0 5.0 4.5

S ml nc ct

Ch th mu

1 2 3 4 5 6 7
09/23/11

0 1.0 2.0 3.0 4.0 5.0 5.5

100 90 80 70 60 50 45

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Tin hnh th : du c khuy u v lc sch vo ng so mu . Tin hnh so snh vi thang mu di nh sng ban ngy hay nh sng ca bng n in . Ch s mu ca du l ch s mu ca ng chun c mu sc gn ging nht .

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Xc nh mi: xc nh mi ca du , pht mt lp du mng ln mt knh hoc xoa vo lng bn tay ri tin hnh ngi nh gi . nhn bit mi d dng hn , cho 300ml du vo cc thy tinh , lm nng n 50oC , dng a thy tinh khuy nhanh v tin hnh th . Khi cn thit em so snh vi mu du c phm cht tt

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Phng php do thi gian chy qua ng mao qun: Tin hnh th: Cho mu th vo nhnh B kp nht k theo ph ng th ng ng v ngm trong my iu nhit nhit qui nh trong 20 pht. Sau , dung p lc ht v y cho du i qua mao qu n vo bu nh mc sao cho mc du cao hn mc chun trn mt t. Sau du chy t do t bu nh mc sang nhnh B v dung ng h o giy tnh thi gian. Thi gian bt u k t lc mt khum ca du ri kh i vch chun trn v cui cng l khi du va ch y h t qua vch chun di. Trong thi gian th, cn gi nhit cho my iu nhit khng thay i. Tin hnh th 3 ln ly gi tr trung bnh. Ra sch nht k v tin hnh th nh trn xc nh th i gian chy qua nc ct.
09/23/11 22

Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Nhit 0C

d=1/4

5 10 15 16 18 20 24 25 28 30 35 40
09/23/11

0.99999 0.99973 0.99913 0.99897 0.99862 0.99823 0.99780 0.99757 0.99626 0.99567 0.99406 0.99224

nht centipo az 1.516 1.306 1.141 1.116 1.060 1.005 0.960 0.894 0.836 0.802 0.721 0.653

Nhit 0C

d=1/4

15 50 55 60 65 70 75 80 85 90 95 100

0.99024 0.98870 0.98573 0.98324 0.98059 0.97781 0.97489 0.97183 0.96865 0.96534 0.96192 0.95838

nht centipo az 0.596 0.550 0.507 0.470 0.436 0.406 0.379 0.356 0.334 0.315 0.298 0.282
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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Phng php o vn tc ca vin bi : Tin hnh th : mu th kh ht nc v lc sch qua natri sunfat khan vo ng th sao cho khng to bt kh ( nu c th t nht ) . Th vin bi c kch thc tng ng qua ng vo ng th . Dng thi k o thi gian ri ca vin bi bt u lc im di ca vien bi chm vo vch th 2 v thi gian cui cng lc im ny chm vo vch th 5 ca ng . Th ln lt 5 vin bi , ly trung bnh cng ca 5 ln thi gian o c , lm thi gian cn xc nh . Theo trnh t nh trn , tin hnh xc nh nht ca cht lng tiu chun .

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Cch tin hnh : Chun b thit b Bt my o quang ph hp th nguyn t v my hiu ch nh nn deteri . Theo hng dn ca nh sn xut , iu chnh cng ca n , khe h , di bc sng v khuch i . di bc sng thch hp cho tng kim loi:ng l 324,7mm; St l 302,1mm; Niken l 232,0mm T u ha v tr ca l graphit trong my o quang ph p th nguyn t v cho chy trng trnh iu khin d theo bng 1

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Xc nh

Giai on

Nhit trong l 0C

Thi gian tng , giy

Thi gian duy tr , giy

Lu lng kh trong l ml/pht 300 50 300 50

ng

1 2 1 2

900 2700 1200 2700

50 1 50 1

30 5 30 5

St , niken

Bng 1- Chng trnh hot ng ca l nguyn t ha graphit

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

xc nh hm lng ca ng v niken s dng mt ng graphit khng ph pyrolitic . xc nh hm lng ca st , s dng mt ng c ph niobi bn trong chc chn rng ton b lng st c xc nh . Trc mi ln bm mu , x l u pipet trc bng cch ht vo ri b i 20l nheptan . X l trc mu th v dung dch chun b . Cho tt c mu th , du long v cc dung dch chun lm vic vo t sy 600C t nht l 15 pht trc khhi xc nh . Nu hm lng ca kim loi trong cht bo c bit nm ngoi phm vi a ra , pha long chng vi dung dch du long . Lc k tt c cc mu th v cc dung dich trc khi phn tch . Xc nh . ng mu trng graphit . Du long dng cho mu trng . Chun ha thit b . Phn tch mu th . Cc mu th lng 400C . Cc mu th c 400C . Dng th chun .
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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Nguyn tc : Ha tan phn mu th trong n-hexan v chit ch t chng oxy ha ny bng axetonitryl. Nhn bit cc cht chng oxy ha ny bng sc k lp mng. Cch tin hnh: Phn ly mu th : ly mt phn mu th khong t 7.5g n 10g t cc mu th nghim Chit cc cht chng oxi ha : Sc k v nhn bit
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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

Tm quan trng ca du : C th ngi c nui dng bi cc cht khc nhau, trong vic b sung cht bo ng vai tr quan trng duy tr c th v tng kh nng khng.

Tuy rng hu ht cc ph n u "s" cht bo, nhng thc ra vn l mt trong 4 nhm cht cn thit cho c th. Vn l bn cn chn la v dung np cht bo th no ph hp vi nhu cu m khng nh hng n cuc sng.

09/23/11

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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

C rt nhiu phng php kim nghim du nhng cc phng php trn c chn v n thng dng v d dng thc hin Thng qua cc phng php kim nghim du n : + C th xc nh c thnh phn ha hc ca cc loi du tt hoc h hng v cc cht c trong du +ng thi c th loi b cc cht c hi trong du trnh cc ng c trong thc phm + Gip ngi tiu dng c th la chn , s dng du ng cch . Tuy nhin bn cnh nhng u im cng c nh ng hn ch nh phi c cng ngh hin i , chi ph tn km , mt nhiu th i gian , .
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Phng Php Kim Nghim Du

Ths.Trn Quang Hiu

09/23/11

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