Ahri 700 2012

Appendix D to AHRI Standard 700
2012 Appendix D for Gas Chromatograms for
AHRI Standard
700-2012 Informative
IMPORTANT
SAFETY DISCLAIMER
AHRI does not set safety standards and does not certify or guarantee the safety of any products,
components or systems designed, tested, rated, installed or operated in accordance with this
standard/guideline. It is strongly recommended that products be designed, constructed, assembled,
installed and operated in accordance with nationally recognized safety standards and code requirements
appropriate for products covered by this standard/guideline.
AHRI uses its best efforts to develop standards/guidelines employing state-of-the-art and accepted
industry practices.
AHRI does not certify or guarantee that any tests conducted under its
standards/guidelines will be non-hazardous or free from risk.
Note:
This Appendix supersedes the 2008 version of Appendix D.
FOREWORD
The intent of this normative appendix is to provide figures for the gas chromatograms used with the 2008
Appendix C, Analytical Procedures for AHRI Standard 700 Normative.
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Printed in U. S.A.
Copyright 2012, by Air-Conditioning, Heating and Refrigeration Institute

Registered United States Patent and Trademark Office
LIST OF FIGURES
Figure 1.
Figure 2.
Figure 3.
Figure 4.
Figure 5.
Figure 6.
Figure 7.
Figure 8.
Figure 9.
Figure 10.
Figure 11.
Figure 12.
Figure 13.
Figure 14.
Figure 15.
Figure 16.
Figure 17.
Figure 18.
Figure 19.
Figure 20.
Figure 21.
Figure 22.
Figure 23.
Figure 24.
Figure 25.
Figure 26.
Figure 27.
Figure 28.
Figure 29.
Figure 30.
Figure 31.
Figure 32.
Figure 33.
Figure 34.
Figure 35.
Figure 36.
Figure 37.
Figure 38.
Figure 39.
Figure 40.
Figure 41.
Figure 42.
Gas Chromatogram of Non-Condensable Gas .........................................................2

Gas Chromatogram of R-11 .....................................................................................3
Gas Chromatogram of R-22 (Packed)......................................................................6
Gas Chromatogram of R-22 (Capillary) ..................................................................7
Gas Chromatogram of R-113 .................................................................................10
Gas Chromatogram of R-123 (Packed)..................................................................14
Gas Chromatogram of R-123 (Capillary) ..............................................................15
Gas Chromatogram of R-134a ...............................................................................18
Gas Chromatogram of R-141b ...............................................................................19
Gas Chromatogram of R-142b ...............................................................................20
Gas Chromatogram of R-236fa ..............................................................................24
Gas Chromatogram of R-245fa ..............................................................................25
LIST OF FIGURES (Continued)
Figure 43.
Figure 44.
Figure 45.
Figure 46.
Figure 47.
Figure 48.

2012 APPENDIX D TO AHRI STANDARD 700-2012
Gas Chromatogram Figures

Section 1. Purpose
The purpose of this normative appendix is to provide figures for the gas chromatograms used with the 2008
Appendix C, Analytical Procedures for AHRI Standard 700 Normative.
Section 2. Definitions
Note for all figures:
2.1
Ret. Time = Retention Time
2.2
Comp. = Component
0.44
6.0
5.5
5.0
4.5
Response - MilliVolts
4.0
3.5
3.0
2.5
Air
0.5
2.05 C=0.0
1.0
1.75 C=0.0
1.5
1.33 C=0.0
0.67 C=0.04 CO2
2.0
0.0
0.0
1.0
2.0
Run Time = 5.791479 minutes
Ret. Time
0.44
0.67
1.33
1.75
2.05
3.0
4.0
Time - Minutes
5.0
7.0
Data Sampling Rate = 5.001601 points/sec
Component
Air
CO2
Figure 1. Gas Chromatogram of Non-Condensable Gas
6.0
8.0
10.68
100
10
Ret. Time
4.33
4.48
6.13
7.61
8.02
8.69
9.13
10.68
11.74
12.37
13.98
15.13
17.11
18.13
18.98
20.09
24.22
27.23
15
Time - Minutes
20
27.23 R112
24.22 TCE
20.09 3M7100#2
18.98 CCL4
18.13 R140a
10
13.98 CHCL3
SBN
R11
20
7.61
30
SBN
40
R133a
8.02
R21
CH2CL2
9.13
R114/ACETONE
50
8.69
6.13 R12
60
4.33 4.48 R22
70
15.13 R113
11.74 R123a
12.37 R123
80
17.11 3
90
25
30
Data Sampling Rate = 5 points/sec
Component
R22
R12
R133a
R21
CH2CL2
R114/ACETONE
R11
R123a
R123
CHCL3
R113
3M7100#1
R140a
CCL4
3M7100#2
TCE
R112
Figure 2. Gas Chromatogram of R-11
12.53
100
90
80
25.18 N-PENTANE
21.20 R123
23.41 MEK
24.11
R113
24.38
2-BUT.
2-BUT-T
18.66
SBN
20.53
SBN
10.75
19.50 R11
13.37 R142b
11.02
C3H6
7.54 R152a
8.07 R134a
R12
2.63
10
8.67 R22
3.23 CH4
20
3.96 R23
30
7.87 R40
40
R115
50
14.83 R124
15.47 R133a
R21
16.10
16.52
ISOB.
SUM+
17.45 R114R114A
SUM18.01 N-BUTANE
60
4.63 C2H4
5.28 C2H6
5.87
R13
6.16
6.69 R143a
70
0
0
Run Time = 30 minutes
Ret. Time
2.63
3.23
3.96
4.63
5.28
5.87
6.16
6.69
7.54
7.87
8.07
8.67
10.75
11.02
12.53
13.37
14.83
15.47
16.10
16.52
17.45
18.01
18.66
19.50
20.53
Component
CH4
R23
C2H4
C2H6
R13
10
12
14
Time - Minutes
16
18
22
24
26
Ret. Time
21.20
23.41
24.11
24.38
25.18
R143a
R152a
R40
R134a
R22
C3H6
R115
R12
R142b
R124
R133a
R21
ISOB.
R114R114A
N-BUTANE
2-BUT-T
R11

4
20
Component
R123
MEK
R113
2-BUT.
N-PENTANE
28
30
6.32
240
220
200
160
140
20
0
Ret. Time
3.69
4.47
6.05
6.32
9.53
10.48
11.01
12.99
14.65
19.38
21.76
14
16
18
21.76 R11
19.38 R114R114a
14.65 R12
SBN
12.99 R115
10.48 R22
11.01 R13B1
10
12
Time - Minutes
SBN
R13
INT-
40
INT+
60
9.53 R125
3.69 R14
80
SBN
100
6.05 R116
120
4.47 R23
180
20
22
24
Component
R14
R23
R116
R13
R125
R22
R13B1
R115
R12
R114R114a
R11
8.47
75
70
65
60
55
24.11 R113
18.67 2-BUT-T
SBN
19.50
R11
19.94
20.54 R123a
21.20 R123
10
12.73 R12
13.41 R142b
15
10.77 11.02 C3H6 R115
20
SBN
3.23 CH4
3.97 R23R32
4.63 C2H4
5.28 C2H6
5.87 R13
25
6.69 R143a
30
R22
35
7.53 R152a
R125
8.05 R134a
40
14.84 R124
15.48 R133a
R21
16.11
16.53
ISOB.
17.46 SUM+
R114R114a
18.01 SUM- N-BUTANE
45
7.76
50
0
0
Ret. Time
3.23
3.97
4.63
5.28
5.87
6.69
7.53
7.76
8.05
8.47
10.77
11.02
12.73
13.41
14.84
15.48
16.11
16.53
17.46
18.01
18.67
19.50
19.94
20.54
21.20
10
12
14
16
Time - Minutes
18
20
24
26
Component
CH4
R23R32
C2H4
C2H6
R13
R143a
R152a
R125
R134a
R22
C3H6
R115
R12
R142b
R124
R133a
R21
ISOB.
R114R114a
N-BUTANE
2-BUT-T
R11
R123a
R123
Figure 5. Gas Chromatogram of R-22 (Packed)

6
22
28
30
17.87
20
18
22.46 R31
SKIM
27.97 R113
17.40 R12
14.51
10
20.67 R40
12
13.46 R23/R115
R22
14
26.72 R21
14.40 R143A R32
16
0
12
14
Ret. Time
13.46
14.40
14.51
17.40
17.87
20.67
22.46
26.72
27.97
16
18
20
Time - Minutes
22
24
26
28
30
Component
R23/R115
R143A
R32
R12
R22
R40
R31
R21
R113
Figure 6. Gas Chromatogram of R-22 (Capillary)
4.33
4.69
10.0
9.0
7.0
8
Time - Minutes
10
Ret. Time
4.04
4.33
4.69
7.17
8.16
11.17
11.63
14.99
12
14
16
Component
R14
R23
R116
R13
R22
R13B1
R12
14.99 R12
11.17 R22
R23
3.0
11.63 R13B1
INT-
4.0
PW-
4.04
5.0
8.16 R13
7.17 R116
R14
6.0
INT+
8.0
18
20.07
13.47
6.6
6.4
6.0
5.8
5.6
4.6
12
14
16
R-141b
R-31
23.30 R-40
R-1270
R-22
4.8
R-12
5.0
R-134A
12.67 R-23
5.2
SBN
5.4
R-32
6.2
18
20
22
24
26
28
30
32
34
Time - Minutes
Ret. Time
12.67
13.47
20.07
23.30
Component
R-23
R-32
R-22
R-40
17.72 R123
18.23
20
18
10
12
14
16
18
Time - Minutes
22
29.05 PCE
25.41
24
26
28
30
Component
R115
R1113
R12
R22
R114
R216ba
R133a
1112a
318mbb
R11
C-316
R123a
R123
R113
R225
CCL4
R122
R112
TCE
PCE
Figure 9. Chromatogram of R-113
10
25.02
23.70 CCL4
SBN
20
Ret. Time
11.51
12.12
12.29
12.41
12.92
14.07
14.31
15.25
15.74
16.42
17.04
17.51
17.72
18.23
18.78
19.35
23.70
23.90
25.02
25.14
25.41
29.05
25.14 R112
TCE
R122
R113
18.78
17.04
19.35 R225
16.42 R11
SUM+
C-316
SUM17.51 R123a
R216ba
15.25 1112a
15.74 318mbb
14.07
11.51 R115
10
14.31
12
12.29 12.41 R12 R22
12.92 R114
14
R133a
12.12 R1113
16
23.90
32
Ret. Time
0.92
1.97
3.37
4.22
5.90
6.63
7.33
7.58
8.51
9.12
9.77
10.31
12.25
13.93
14.62
14.78
15.24
15.95
16.26
16.55
17.33
17.90
18.54
19.78
20.64
21.65
22.32
23.15
25.23
25.69
31.35
33.58
34.26
Component
R23
R13
R152a
R134a
R22
R1301
R115
R12
R124a
R124
R133a
R217ba
R114/R114a
R133aB1
R11
R1112a/R123a
R123
R113
R113a
R122
TCE

11
14.16
15.35
R1113
R124
11.54
8.18
50
9.08
17.83 R114/R114A
45
40
30
20
SKIM
10
12
14
PW+
SKIM
R115
R22
7.85
R125
5.29 R116
10
3.93 R23
3.24 R14
15
19.79 R11
13.18 R12
25
6.08 R13
35
16
18
20
22
24
26
28
Time - Minutes
Ret. Time
3.24
3.93
5.29
6.08
7.85
8.18
9.08
11.54
13.18
14.16
15.35
17.83
19.79
Component
R14
R23
R116
R13
R125
R22
R115
R12
R1113
R124
R114/R114A
R11
12
30
7.14
4.92
200
180
8.02
160
9.26 R22
120
6.24 R13
100
80
60
18.62
R152a
R143a
R116
20
4.12 R23
40
3.36
140
0
0
10
12
14
16
18
20
Time - Minutes
Ret. Time
3.36
4.12
4.92
6.24
7.14
8.02
9.26
18.62
21.65
22.32
23.15
25.23
25.69
31.35
33.58
34.26
Component
R23
R116
R13
R143a
R152a
R22
R1112a/R123a
R123
R113
R113a
R122
TCE
Figure 12. Gas Chromatogram of R116
13
Figure 13. Gas Chromatogram of R-123 (Packed)
14
43.98 44
24
1111
R123b1
47.69
43.42
47.36
43.13
R123b
R123a
45.74
42.22 R21
40.02 124B1
40.68 R11
39.21 1112
37.96
22
46.10 R30
R141b
133a
33.16 R124
34.31 216ba
36.97 1326
38.25
31.63 1122
29.04 1336mzz R22
32.44 R124a
34.73
30.08 R114
29.24
26.50 1225zc
27.10 1113
10
27.41 27.62 R12
12
23.49
14
R113
1112a
16
46.62
18
43.63
24.24 1132a
20
26
28
30
32
34
36
38
40
42
44
46
48
50
Time - Minutes
Ret. Time
23.49
24.24
26.50
27.10
27.41
27.62
29.04
29.24
30.08
31.63
32.44
33.16
34.31
34.73
36.97
37.96
38.25
39.21
40.02
Component
1132a
1225zc
1113
R12
1336mzz
R22
R114
1122
R124a
R124
216ba
Ret. Time
40.68
42.22
43.13
43.42
43.63
43.98
44.16
45.74
46.10
46.62
47.36
47.69
Component
R11
R21
R141b
R113
R123b
R123a
R123
R30
R123b1
1111
1326
133a
1112a
1112
124B1
Figure 14. Gas Chromatogram of R-123 (Capillary)
15
14.03
100
90
26.28
27.12
24.18 R113
21.26 R123
20.58
15.46 R133a
17.48 17.67 R114 1318-C
18.87
19.55 R11
10
11.13 R115
20
7.86
3.30
4.00 R23
30
8.77 R22
9.43 R31
6.76 R143a
40
12.23
12.74 R12
13.37
13.60 1113
R124a
R124 SKIM
50
SBN
60
7.62 R152a R125
70
16.44 1318-T
8.16 R134a
80
0
0
10
12
14
Time - Minutes
16
18
20
24
26
28
Ret. Time Component

3.30
4.00 R23
6.76 R143a
7.62 R152a
7.86 R125
8.16 R134a
8.77 R22
9.43 R31
11.13 R115
12.23
12.74 R12
13.37
13.60 1113
14.03 R124a
14.49 R124
15.46 R133a
16.44 1318-T
17.48 R114
17.67 1318-C
18.87
19.55 R11
20.58
21.26 R123
24.18 R113
26.28
27.12
16
22
30
19.10
16.47
12.51
7.71
8.46
100
9.98
23.52 R123
90
27.04 R113
29.71
28.08
26.34
24.61
22.69
22.39
21.10
SUM18.07
R115
R22
7.20
R143a
R125
10
5.91 R116
3.45 CH4
20
4.40 R23\R32
30
6.78 R13
40
15.16 1113
15.71 R124a
R124
17.12 R133a
14.23 R12
50
19.75 SUM-
60
4.03
Response - Picoamps
70
19.30 R114\R114a
10.48 R1301
80
0
0
10
Ret. Time Component

3.45 CH4
4.03
4.40 R23\R32
5.91 R116
6.78 R13
7.20
7.71 R143a
8.46 R125
9.98 R22
10.48 R1301
12.51 R115
14.23 R12
15.16 1113
15.71 R124a
16.47 R124
17.12 R133a
18.07
19.10
19.30 R114\R114a
19.75
21.10
22.39
22.69
23.52 R123
24.61
15
Time - Minutes
20
25
30
Ret. Time Component

26.34
27.04 R113
28.08
29.71
17
Run Time = 33.99667
Data Sampling Rate = 20
Ret. Time Component

13.01 R115
13.59 R143a
13.89 R125
15.34 R245CB
15.47 R134a
17.14 R161
17.25 R152a
17.73 R12
18.60 R134
20.07 R22
22.76 R114/R114a
23.27 R40
23.60 1122
24.87 R124
25.22
25.46 1140
25.88 R31
26.76 1131-t
28.31 R133a
30.87 1131-c
33.07 R123
Figure 17. Gas Chromatogram of R-134a
18
31.53
364
16
132b
18
25.17 1130a
16.32
20
24.43
29.03 150a
27.42
27.06
34.11
33.78
31.14
R140a
32.02
32.54
29.57
27.84
28.58
26.33 1121-t
25.76
23.89
R141b
24.88 25.09
22.55
26.44
21.21
21.80 392 ISOMERS
19.28 1363mz
19.03
R142b
17.48
17.10
14.41 R12
15.85 1131a
151a
10
20.86
12
20.17 365mfc
12.89 R143a
14
0
12
14
16
18
20
Ret. Time Component

12.89 R143a
14.41 R12
15.85 1131a
16.32 R142b
17.10
17.48
19.03
19.28 1363mz
20.17 365mfc
20.86 151a
21.21
21.80 392 ISOMERS
22.55
23.89
24.43 R141b
24.88
25.09
25.17 1130a
25.76
26.33 1121-t
26.44
27.06 364
27.42 132b
27.84
28.58
29.03 150a
22
24
Time - Minutes
26
28
30
32
34
36
Ret. Time Component

29.57
31.14
31.53 R140a
32.02
32.54
33.78
34.11
Figure 18. Gas Chromatogram of R-141b
19
24.10
23.12
11.87
12.20
20
15.20
12
12
14
Ret. Time
11.87
12.20
13.40
13.65
14.07
15.03
15.20
16.68
19.33
20.31
21.63
23.12
24.10
32.02
32.54
33.78
34.11
16
18
Time - Minutes
20
22
24
26
Component
1132a
R143a
R152a
R12
R22
1131a
R142b
R160
R11
R141b
1130a
Figure 19. Gas Chromatogram of R-142b
20
1130a
R141b
R142b
1132a
R143a
INT+
19.33
16.68 SBN
21.63 R11
10
13.65 R12
14
14.07 R22
13.40 R152a
16
20.31 R160
15.03 1131a
18
7.05
200
8.16
21.06 365mfc
18.84 N-BUTANE
17.32 ISOB.
16.30 R133a
15.68 R124
14.47 1113
11.85 R115/C3H8
9.39 R22
R152a
S4K3IM
R1
a
3.35
20
INT+
40
5.60 C2H6/1132a
60
4.11 R23R32
3.78 R41
80
4.87 C2H4
8.77
100
13.49 R12
120
INT-
140
14.17 R142b
8.42 R40/R125
160
20.36 R141b
R134a
180
0
4
Ret. Time
3.35
3.78
4.11
4.87
5.60
7.05
8.16
8.42
8.77
9.39
11.85
13.49
14.17
14.47
15.68
16.30
17.32
18.84
20.36
21.06
10
12
Time - Minutes
14
16
18
20
22
24
Component
R41
R23R32
C2H4
C2H6/1132a
R143a
R152a
R40/R125
R134a
R22
R115/C3H8
R12
R142b
1113
R124
R133a
ISOB.
N-BUTANE
R141b
365mfc
21
6.34
50
45
40
15.18
13.55
SBN
R152a
5.40
10
10.63
2.60 CH4
15
3.74 C2H4
8.68
20
13.95 N-BUTANE
8.97
25
12.90 ISOB.
C3H6
C3H8
5.70 R161
30
4.26 C2H6
35
0
0
8
10
Time - Minutes
12
14
18
Ret. Time Component

2.60 CH4
3.74 C2H4
4.26 C2H6
5.40
5.70 R161
6.34 R152a
8.68 C3H6
8.97 C3H8
10.63
12.90 ISOB.
13.55
13.95 N-BUTANE
15.18
22
16
20
10.56
75
70
12.96
65
13.33 1216
60
55
16.20
16.97
17.42
R218
8.79
9.38
15
245cb
11.77 CF8S
20
10
13.93 C-318
25
20.80
30
20.20
35
18.01 C5F10
40
18.67
15.37 R227ea
45
14.43
14.84
50
0
10
12
14
Ret. Time Component

3.42
5.63
8.79
9.38
10.56
11.77
12.96
13.33
13.93
14.43
14.84
15.37
16.20
16.97
17.42
18.01
18.67
20.20
20.80
16
18
Time - Minutes
20
22
24
26
28
30
R218
CF8S
245cb
1216
C-318
R227ea
C5F10
23
Figure 23. Gas Chromatogram of R-236fa
24
25.89
50
45
40
R-133a
33.38 R-123
30
R-123a
R-30
33.49
R-141b
R-11
31.18
30.99
30.58 R-1235
29.46 R-1224 Isom1
R-226
10
26.65 R-1234
15
R-1233
20
R-113
R-1224 Isom2
25
R-245fa
35
0
21
22
23
24
Ret. Time
25.89
26.65
29.46
30.58
30.99
31.18
33.38
33.49
25
26
27
Time - Minutes
28
29
30
31
32
33
34
35
Component
R-245fa
R-1234
R-1224 Isom1
R-1235
R-1224 Isom2
R-133a
R-123
R-113
Figure 24. Gas Chromatogram of R245fa
25
18.62
11.68
5.53
100
17.12
90
80
60
50
29.68
26.48
24.12
19.73
20.35
C3H6
8.63
10
C2H6
3.23 CH4
20
ISOB.
11.40 C3H8
30
N-BUTANE
40
SBN
70
0
0
Ret. Time
3.23
5.53
8.63
11.40
11.68
17.12
18.62
19.73
20.35
24.12
26.48
29.68
24.11
10
12
14
Time - Minutes
16
18
20
24
26
28
Component
CH4
C2H6
C3H8
C3H6
ISOB.
N-BUTANE
R113
26
22
30
19.99
240
11.46
9.59
220
200
10.61 R134a
140
120
100
19.33 R124a
17.80 R12
160
80
10
Ret. Time
9.59
10.61
11.46
17.80
19.33
19.99
SBN
SBN
15
Time - Minutes
SBN
SBN
R124
20
R22
R152a
40
INT+
60
INT-
180
20
25
30
Component
R152a
R134a
R22
R12
R124a
R124
27
11.48
R22
15.89
9.96
240
R125
220
200
180
160
140
120
100
80
20
0
10
12
Time - Minutes
14
16
18
20
22
24
Ret. Time Component

9.96 R125
11.48 R22
15
28
SBN
SBN
SBN
R290
INT-
40
INT+
60
26
14.40
15.82
R290
240
R218
11.32
220
200
160
140
120
100
80
R22
20
0
10
Ret. Time
11.32
14.40
15.82
15
Time - Minutes
SBN
SBN
SBN
40
INT+
60
INT-
180
20
25
30
Component
R22
R218
R290
29
240
220
200
10.01
10.59 R134a
8.27
160
120
100
17.79 R12
15.83 R115
140
11.64 R22
180
80
20
0
Ret. Time
8.27
10.01
10.59
11.64
15.83
17.79
10
12
Time - Minutes
14
16
18
SBN
20
22
24
Component
R143a
R125
R134a
R22
R115
R12
30
SBN
SBN
R125
R143a
INT-
40
INT+
60
26
11.34
750
700
18.55
650
21.40 R600a
600
550
450
400
350
300
250
200
150
10
Ret. Time
11.34
18.55
21.40
R142b
SBN
R22
50
INT+
100
INT-
500
15
Time - Minutes
20
25
30
Component
R22
R142b
R600a
31
700
9.97
10.47
4.38
750
650
600
550
500
450
400
350
300
250
10
Ret. Time
4.38
9.97
10.47
11.54
15.76
15
Time - Minutes
SBN
R125
R134a
INT+
R32
50
INT-
100
11.54 R22
150
15.76 R115
200
20
25
Component
R32
R125
R134a
R22
R115
32
30
700
11.40
8.22
750
650
600
550
10.10 R125
450
400
350
300
SBN
150
10
Ret. Time
8.22
10.10
11.40
15.79
17.76
15.79
R22
R143a
50
INT+
100
15
Time - Minutes
SBN
200
SBN
17.76 R12
R115
250
INT-
500
20
25
30
Component
R143a
R125
R22
R115
R12
33
700
19.97
11.33
750
18.50
650
600
550
450
400
350
SBN
17.76
150
10
Ret. Time
11.33
17.76
18.50
19.30
19.97
R142b
R22
INT+
50
INT-
100
15
Time - Minutes
R124
200
SBN
R12
250
R124a
300
19.30
500
20
25
Component
R22
R12
R142b
R124a
R124
34
30
4.36
750
700
9.97
650
600
550
450
400
350
300
250
10
Ret. Time
4.02
4.36
9.97
11.56
15.78
15
Time - Minutes
SBN
11.56 R22
50
R125
100
INT+
4.02 R41
R 32
150
15.78 R115
200
INT-
500
20
25
30
Component
R41
R32
R125
R22
R115
35
11.28
750
700
9.49 R152a
650
600
550
450
400
350
15.41 1270
500
300
250
200
10
Ret. Time
9.49
11.28
15.41
17.76
17.76
R22
INT+
50
INT-
100
15
Time - Minutes
SBN
SBN
150
20
25
Component
R152a
R22
1270
36
30
11.30
750
700
18.51
650
600
550
450
400
350
14.34 R218
300
250
200
150
10
Ret. Time
11.30
14.34
18.51
SBN
15
Time - Minutes
R142b
SBN
R22
50
INT+
100
INT-
500
20
25
30
Component
R22
R218
R142b
37
10.48
750
700
650
21.39 R600a
600
14.34 R218
550
500
450
400
350
300
250
200
150
10
Ret. Time
10.48
14.34
21.39
15
Time - Minutes
SBN
SBN
R134a
INT+
50
INT-
100
20
25
Component
R134a
R218
R600a
38
30
700
19.93
11.33
750
18.47
650
600
550
450
21.40 R600a
400
350
19.28 R124a
300
250
200
150
10
Ret. Time
11.33
18.47
19.28
19.93
21.40
R124
SBN
15
Time - Minutes
R142b
SBN
R22
50
INT+
100
INT-
500
20
25
30
Component
R22
R142b
R124a
R124
R600a
39
22.80
240
19.94
10.53
220
19.30 R124a
200
180
160
140
120
100
80
Ret. Time
10.53
19.30
19.94
22.80
10
12
Time - Minutes
14
16
20
N-BUTANE
22
24
Component
R134a
R124a
R124
N-BUTANE
40
SBN
18
R124
20
0
SBN
R134a
INT-
40
INT+
60
26
9.89
10.50
750
700
650
22.79 R600
600
550
450
400
350
300
250
200
Ret. Time
9.89
10.50
12.10
15.79
20.03
21.40
22.21
22.79
21.40
20
22.21
20.03
15
Time - Minutes
SBN
10
SBN
12.10
R125
R134a
50
INT+
100
15.79
150
INT-
500
25
30
Component
R125
R134a
R600
41
21.51
9.92
10.68
R134a
500
R125
450
400
300
22.90
INT+
50
INT-
100
SBN
15.91 R115
150
R600a
200
SBN
SBN SBN SBN SBN

SBN
250
SBN
350
0
0
10
Ret. Time
9.92
10.68
15.91
21.51
22.90
15
Time - Minutes
20
25
Component
R125
R134a
R115
R600a
42
30
10.07
300
280
17.76
260
240
220
180
10
Ret. Time
4.39
7.04
8.17
10.07
10.68
11.56
15.72
17.76
18.50
20.02
21.02
22.23
24.15
26.01
28.98
15
Time - Minutes
28.98 R113
26.01 R123
24.15 R11
22.23 R114/R114a
21.02 R21
20.02 R124
18.50 R142b
SKIM
R12
R152a
20
15.72 R115
8.17 R143a
4.39 R32
60
INT+
80
40
7.04 R13
100
SKIM
120
SBN
10.68 R134a
140
11.56 R22
160
INT-
200
20
25
30
Component
R32
R13
R143a
R152a
R134a
R22
R115
R12
R142b
R124
R21
R114/R114a
R11
R123
R113
43
10.80
500
15.99
450
400
10
Ret. Time
4.35
6.02
7.00
8.11
9.49
9.98
10.40
10.80
15.99
17.75
18.45
20.03
21.02
22.21
24.11
26.01
28.89
20
25
28.89 R113
30
Component
R32
R13
R143a
R152a
R125
R134a
R22
R115
R12
R142b
R124
R21
R114/R114a
R11
R123
R113
44
24.11 R11
21.02 R21
20.03 R124
SKIM
15
Time - Minutes
SBN
7.00 R13
8.11 R143a
6.02
INT+
50
INT-
100
4.35 R32
150
R115
200
17.75 R12
18.45 R142b
250
26.01 R123
22.21 R114/R114a
300
9.49 R152a
9.98
R125
10.40
R134a
R22
350
4.32
500
6.98
450
400
300
250
200
10
15
Time - Minutes
SBN
SBN
50
R13
100
3.63 3.84 INT+

R23
150
INT-
350
20
25
30
Ret. Time Component

3.63
3.84
4.32 R23
6.98 R13
45
240
10.34
8.56
220
200
180
160
140
120
100
20
0
Ret. Time
8.56
9.89
10.34
12.07
16.11
18.03
10
12
Time - Minutes
14
18.03 R12
16
18
20
22
24
Component
R143a
R125
R12
46
SBN
SBN
R115
16.11
12.07
R143a
INT-
40
INT+
60
9.89 R125
80
26
4.33
500
6.03
450
400
300
250
200
INT+
150
10
15
Time - Minutes
SBN
SBN
R116
R23
50
3.85
100
INT-
350
20
25
30
Ret. Time Component

3.85
4.33 R23
6.03 R116
47
11.33
500
14.44
450
400
350
300
250
200
150
10
15
Time - Minutes
SBN
SBN
R218
R22
INT+
50
INT-
100
20
25
Ret. Time Component

11.33 R22
14.44 R218
32.02
32.54
33.78
34.11
48
30
24.12
20.37
18.51
11.72
500
17.10
450
400
26.46 N-PENTANE
300
250
200
ISOPENTANE
21.65
NEOPENTANE
19.35
16.23
ISOBUTANE
17.64
18.16
N-BUTANE
50
R290
100
7.19
5.63 C2H6
150
3.38 CH4
350
0
0
Ret. Time
3.38
5.63
7.19
11.72
16.23
17.10
17.64
18.16
18.51
19.35
20.37
21.65
24.12
26.46
10
12
14
Time - Minutes
16
18
20
22
24
26
28
30
Component
CH4
C2H6
R290
ISOBUTANE
N-BUTANE
NEOPENTANE
ISOPENTANE
N-PENTANE
49

Ahri 700 2012

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Ahri 700 2012

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Appendix D to AHRI Standard 700

2012 Appendix D for Gas Chromatograms for

Price $10.00 (Members) $20.00 (Non-Members)

Copyright 2012, by Air-Conditioning, Heating and Refrigeration Institute

Gas Chromatogram of Non-Condensable Gas .........................................................2

LIST OF FIGURES (Continued)

Gas Chromatogram of R-502 .................................................................................44

2012 APPENDIX D TO AHRI STANDARD 700-2012

Gas Chromatogram Figures

Ret. Time = Retention Time

2012 APPENDIX D TO AHRI STANDARD 700-2012

0.67 C=0.04 CO2

Run Time = 5.791479 minutes

Data Sampling Rate = 5.001601 points/sec

Figure 1. Gas Chromatogram of Non-Condensable Gas

2012 APPENDIX D TO AHRI STANDARD 700-2012

Run Time = 32.99667 minutes

4.33 4.48 R22

Data Sampling Rate = 5 points/sec

Figure 2. Gas Chromatogram of R-11

2012 APPENDIX D TO AHRI STANDARD 700-2012

Run Time = 30 minutes

Data Sampling Rate = 5 points/sec

Figure 3. Gas Chromatogram of R-12

2012 APPENDIX D TO AHRI STANDARD 700-2012

Run Time = 24 minutes

Data Sampling Rate = 5 points/sec

Figure 4. Gas Chromatogram of R-13

2012 APPENDIX D TO AHRI STANDARD 700-2012

10.77 11.02 C3H6 R115

Run Time = 30 minutes

Data Sampling Rate = 5 points/sec

Figure 5. Gas Chromatogram of R-22 (Packed)

2012 APPENDIX D TO AHRI STANDARD 700-2012

14.40 R143A R32

Run Time = 31 minutes

Data Sampling Rate = 20 points/sec

Figure 6. Gas Chromatogram of R-22 (Capillary)

2012 APPENDIX D TO AHRI STANDARD 700-2012

Run Time = 18 minutes

Data Sampling Rate = 5 points/sec

Figure 7. Gas Chromatogram of R-23

2012 APPENDIX D TO AHRI STANDARD 700-2012

Run Time = 34.99917 minutes

Data Sampling Rate = 20 points/sec

Figure 8. Gas Chromatogram of R-32

Data Sampling Rate = 20 points/sec

Figure 9. Chromatogram of R-113

Run Time = 30.27 minutes

2012 APPENDIX D TO AHRI STANDARD 700-2012

2012 APPENDIX D TO AHRI STANDARD 700-2012

Figure 10. Gas Chromatogram of R-114

2012 APPENDIX D TO AHRI STANDARD 700-2012

Run Time = 30 minutes

Data Sampling Rate = 5 points/sec

Figure 11. Gas Chromatogram of R-115

2012 APPENDIX D TO AHRI STANDARD 700-2012

Run Time = 20 minutes

Data Sampling Rate = 5 points/sec

Figure 12. Gas Chromatogram of R116

2012 APPENDIX D TO AHRI STANDARD 700-2012

Figure 13. Gas Chromatogram of R-123 (Packed)