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LECO Corporation
12
S-144DR
Introduction
Introduction
Introduction
The Introduction chapter contains general information on the
S-144DR Dual Range Sulfur Analyzer including important safety
guidelines and warranty terms. Reference this chapter when looking
for replacement parts, operating supplies, or optional accessories. To
place an order by phone, please call our customer service department
toll-free in the United States at 1-800-292-6141 or 269-985-5496.
Orders may also be sent by fax to 269-982-8977.
Introduction
Illustrations .......................................................................17
Warranty...........................................................................18
Warning and Caution Symbols ............................................ 110
Navigational Buttons ......................................................... 111
Interference to Other Devices ............................................ 112
Declaration of Conformity .................................................. 113
Equipment Packages ......................................................... 114
Options ........................................................................... 115
Components and Accessories ............................................. 116
Specifications................................................................... 119
Definitions....................................................................... 122
Installation
Illustrations .......................................................................22
Analyzer Installation ...........................................................23
Heating Element Installation ................................................25
Combustion System Installation ...........................................29
Sliding Door and Combustion Shelf Installation ..................... 211
Reagent Tube Installation .................................................. 212
Gas Connections .............................................................. 213
Exhaust Tube Connections ................................................. 214
Computer Installation ....................................................... 215
USB Cable Installation....................................................... 217
Introduction
S-144DR
13
Option Installation
Illustrations .......................................................................32
Balance.............................................................................33
Printer ..............................................................................36
System Setup
Illustrations .......................................................................44
Controls and Indicators .......................................................45
Configure Balance Parameters ..............................................46
Data Transmission Parameters .............................................48
Set Furnace Temperature .................................................. 411
Calibrate Furnace Temperature........................................... 412
Software Overview ........................................................... 414
Spreadsheet .................................................................... 419
Menus............................................................................. 432
Using the On-Board Manual ............................................... 434
Operation
First Time Analysis..............................................................53
Methods .......................................................................... 510
Blanks ............................................................................ 516
Standards ....................................................................... 518
Calibration....................................................................... 522
Perform Analysis .............................................................. 528
Recalculate Results ........................................................... 530
User-Defined Field ............................................................ 531
View Sample Data ............................................................ 535
View IR Cell Data ............................................................. 537
Print Result Data .............................................................. 541
Print Display Options......................................................... 544
Transmit Data.................................................................. 548
Export Results ................................................................. 549
14
S-144DR
Introduction
Maintenance
Illustrations .......................................................................62
Periodic Maintenance Schedule .............................................63
Adapter.............................................................................64
Disposable Particle Filters ....................................................65
Fan Filter ..........................................................................67
O-ring...............................................................................68
Reagent Tubes ...................................................................69
Computer System............................................................. 610
Printer ............................................................................ 611
Theory of Operation
Illustrations .......................................................................72
Theory of Operation ............................................................73
Infrared Radiation, Absorption, and Detection.........................74
Comparator Level ...............................................................75
Calibration Curves ..............................................................78
Diagnostics
Diagnostics........................................................................83
Electronic Adjustments
Illustrations .......................................................................92
Security Registration...........................................................93
Software Upgrade...............................................................94
IR Cells Adjustment ............................................................95
Oven Temperature Adjustment.............................................97
10
Service
Service Parts ................................................................... 103
USB/ISA Interface Card Installation .................................... 104
11
Illustrations
12
Schematics
Introduction
S-144DR
15
13
16
Index
S-144DR
Introduction
Illustrations
Figure 1-1 ......... S-144DR System ....................................... 121
Figure 2-1 ......... Facility Requirements ................................. 224
Figure 2-2 ......... Computer Hook-ups ................................... 225
Figure 2-3 ......... Wiring Diagram ......................................... 226
Figure 2-4 ......... Component Installation............................... 227
Figure 2-5 ......... Heating Elements....................................... 228
Figure 2-6 ......... Braided Cable Installation ........................... 229
Figure 2-7 ......... Combustion System Assembly ..................... 230
Figure 2-8 ......... Combustion System ................................... 231
Figure 2-9 ......... Sliding Door And Combustion Shelf .............. 232
Figure 2-10 ....... Reagent Tube Removal ............................... 233
Figure 2-11 ....... Reagent Tube Installation ........................... 233
Figure 3-1 ......... Balance Assembly ...................................... 37
Figure 3-2 ......... Balance Control Panel................................. 37
Figure 4-1 ......... Controls and Indicators............................... 452
Figure 4-2 ......... Furnace Temperature Adjustment ................ 453
Figure 4-3 ......... Dual Furnace Controller Card....................... 454
Figure 6-1 ......... Component Installation............................... 612
Figure 6-2 ......... Reagent Tube Removal ............................... 613
Figure 6-3 ......... Reagent Tubes .......................................... 613
Figure 7-1 ......... Analytical Flow Diagram.............................. 712
Figure 9-1 ......... Adjustment Locations ................................. 99
Figure 9-2 ......... Oven Heater Control Card ........................... 910
Figure 11-1 ....... Left Side View ........................................... 11-3
Figure 11-2 ....... Right Side View ......................................... 11-4
Figure 11-3 ....... 616-040 Inlet Gas Assembly........................ 11-5
Figure 11-4 ....... 606-616 High Sulfur IR Cell......................... 11-6
Figure 11-5 ....... 782-067 Low Sulfur IR Cell ......................... 11-7
Figure 11-6 ....... Vacuum Pump ........................................... 11-8
Figure 12-1 ....... 150-851 Cabinet SchematicsPage 1 of 3..... 124
Figure 12-2 ....... 150-851 Cabinet SchematicsPage 2 of 3..... 125
Figure 12-3 ....... 150-851 Cabinet SchematicsPage 3 of 3..... 126
Introduction
S-144DR
17
Warranty
Equipment manufactured by LECO Corporation, St. Joseph,
Michigan is warranted free from defect in material and
workmanship for a period of six months from the date of
installation. Equipment not manufactured by LECO is covered to
the extent of warranty provided by the original manufacturer
and this warranty does not cover any equipment, new or used,
purchased from anyone other than LECO Corporation. All
replacement parts shall be covered under warranty for a period
of thirty days from date of purchase. LECO makes no other
representation or warranty of any other kind, expressed
or implied, with respect to the goods sold hereunder,
whether as to merchantability, fitness for purpose, or
otherwise.
Expendable items such as crucibles, combustion tubes,
chemicals, and items of like nature are not covered by this
warranty.
LECO's sole obligation under this warranty shall be to repair or
replace any part or parts which, to our satisfaction, prove to be
defective upon return prepaid to LECO Corporation, St. Joseph,
Michigan. This obligation does not include labor to install
replacement parts, nor does it cover any failure due to
accident, abuse, neglect, or use in disregard of instructions
furnished by LECO. In no event shall damages for defective
goods exceed the purchase price of the goods, and LECO shall
not be liable for incidental or consequential damages
whatsoever.
All claims in regard to the parts or equipment must be made
within ten (10) days after Purchaser learns of the facts upon
which the claim is based. Authorization must be obtained from
LECO prior to returning any other parts. This warranty is voided
by failure to comply with these notice requirements.
18
S-144DR
Introduction
Notice
The warranty on LECO equipment remains valid only
when genuine LECO replacement parts are employed.
Since LECO has no control over the quality or purity of
consumable products not manufactured by LECO, the
specifications for accuracy of results using LECO instruments
are not guaranteed unless genuine LECO consumables are
employed in conjunction with LECO instruments. If purchaser
defaults in making payment for any parts or equipment, this
warranty shall be void and shall not apply to such parts and
equipment. No late payment or cure of default in payment shall
extend the warranty period provided herein.
LECO Corporation is not responsible for damage to any
associated instruments, equipment, or apparatus nor will LECO
be held liable for loss of profit or other special damages
resulting from abuse, neglect, or use in disregard of
instructions. The Buyer, their employees, agents, and
successors in interest assume all risks and liabilities for the
operation, use, and/or misuse of the product(s) described
herein and agree to indemnify, hold harmless, and defend the
seller from any and all claims and actions arising from any
cause whatsoever, including seller's negligence for personal
injury incurred in connection with the use of said product(s)
and any and all damages proximately resulting therefrom.
Caution
The instrument should be operated only by technically qualified
individuals who have fully read and understand these
instructions. The instrument should be operated only in
accordance with these instructions.
The operator should follow all of the warnings and cautions set
forth in the manual and the operator should follow and employ
all applicable standard laboratory safety procedures.
LECO is a registered trademark of LECO Corporation.
Windows is a registered trademark of Microsoft Corporation.
Excel is a registered trademark of Microsoft Corporation.
Windows 2000 is a trademark of Microsoft Corporation.
Windows 98 is a trademark of Microsoft Corporation.
Windows 95 is a trademark of Microsoft Corporation.
Windows 3.1 is a trademark of Microsoft Corporation.
Introduction
S-144DR
19
WARNING
WARNING
!
CAUTION
110
S-144DR
Introduction
Navigational Buttons
The following buttons may be found throughout the onboard
manual. These buttons indicate when additional information is
available. While in the topic, click the buttons to access the
information.
Introduction
S-144DR
111
112
S-144DR
Introduction
Declaration of Conformity
Introduction
S-144DR
113
Equipment Packages
Notes
S-144DR Package
S-144DR Dual Range Sulfur Analyzer
1
606-000-300
200-618
Instruction Manual
259-014
Software Kit
606-000-071
Component Pack
607-755*
616-079
Accessory Pack
618-798
USB Cable
620-804
Ground Strap
S-144DRPC Package
S-144DR Dual Range Sulfur Analyzer with Computer System
1
606-000-300
200-618
Instruction Manual
259-014
Software Kit
606-000-071
Component Pack
607-755*
616-079
Accessory Pack
686-227-2GH
PC Tower Assembly
701-557
618-798
USB Cable
620-804
Ground Strap
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
114
S-144DR
Introduction
Options
To place an order by phone, please call our customer service
department toll-free in the United States at 1-800-292-6141
or 269-985-5496. Orders may also be sent by fax to 269-9828977.
Notes
529-204-250
Combustion Boat
620-630-110
620-632
Printer Cartridge
751-300-150
789-431
Accessory Pack
Introduction
S-144DR
115
159-145-131
Software Pack
203-505-267
Registration Form
190-742
Screw
501-241
Vacuum Grease
606-298
606-319
Lead Wire
606-320
606-321
606-323
Back Insulator
606-324
Shelf
606-601
608-898
Receptacle Cover
613-564
614-694
Combustion Shelf
616-015
616-027
Bottom Guide
616-062
Combustion Door
616-068
O-ring
616-070
616-084
616-086
616-089
618-798
620-804
Wire Connector
762-458
Connector
765-978
783-897
O-ring
116
S-144DR
Introduction
501-171
502-085
502-435
503-032
529-204
Combustion Boat
606-327
Reagent Tube
606-403
616-063
Boat Puller
616-068
O-ring
763-265
772-520
O-ring
773-320
O-ring
783-897
O-ring
203-913
Paper
620-630
DeskJet Printer
700-689
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
Introduction
S-144DR
117
609-787
Component Pack
611-119
Receptacle Strip
618-980
Mouse Pad
686-994
PC Tower
501-081
10
501-171
529-204-250
Combustion Boat
606-327
Reagent Tube
616-068
O-ring
616-070
616-086
616-089
768-980
Tube Filter
772-520
O-ring
773-320
O-ring
783-897
O-ring
118
S-144DR
Introduction
Specifications
Range (at 350 mg)* ........................... 5 ppm or 0.0005% to 26%
Precision ............................................ 1% RSD or 2.5 ppm
(whichever is greater)
Readability......................................... 1 ppm
Calibration ......................................... Single-point; Multi-point
(linear, quadratic, cubic polynomial)
Analysis Time..................................... 90 seconds (nominal)
Sample Size ....................................... 350 mg for coal (nominal)
Balance Readability and Range........... 0.0001 to 120 g
Detection Method ............................... Infrared
Chemical Reagent .............................. Anhydrous Magnesium Perchlorate
Gas Required...................................... Oxygen, 99.5% pure, 40 psi (2.76 bars),
3.5 lpm (nominal)
Regulator ........................................... CGA-540, 0 to 125 psi, 7/8-inch Male RH
Furnace.............................................. 400o to 1450oC, 1350oC (nominal)
External PC (optional).......................... Pentium 333 MHz (min.)
256 MB RAM (min.)
2 GB Hard Drive (min.)
1 USB Port and 1 USB Port (min.)
Microsoft Windows2000
Monitor (optional)................................ 15 inch (38 cm) monitor
SVGA (min.)
Electrical Power Requirements
S-144DR.............................................. 230V~ (10%), 50/60Hz,
12A (idle), 19A (max.)
Computer ............................................ 115/230V~ (10%), 50/60Hz,
40W (typical), 220W (max.)
Monitor................................................ 90 to 264V~ (10%), 50/60Hz,
110w (max.)
Balance ............................................... 120V~ (10%), 60Hz, 16W (max.)
Printer................................................. 120V~ (10%), 60Hz, 12W (max.)
Introduction
S-144DR
119
Dimensions
S-144DR
Height ................................................. 24.00 inches (61.0 cm)
Width .................................................. 21.50 inches (55.0 cm)
Depth.................................................. 22.00 inches (56.0 cm)
Weight ................................................ 150 pounds (68 kg)
Computer
Height ................................................. 17.00 inches (43.2 cm)
Width .................................................. 7.50 inches (19.0 cm)
Depth.................................................. 17.00 inches (43.2 cm)
Weight ................................................ 29 pounds (13.2 kg)
Monitor
Height ................................................. 14.50 inches (37.0 cm)
Width .................................................. 14.00 inches (35.6 cm)
Depth.................................................. 16.00 inches (40.6 cm)
Weight ................................................ 35 pounds (15.9 kg)
Total Shipping Weight ........................ 240 pounds (108 kg)
120
S-144DR
Introduction
Figure 1-1
S-144DR System
Introduction
S-144DR
121
Definitions
#Shows the numeric sequence in which the sample was
added to the sample pane. An asterisk indicates the currently
selected sample. (Columns, page 422)
Add SampleCreates a new entry in the sample pane. (Using
the Toolbar, page 430)
AnalyzeStarts the analysis for the first unanalyzed sample.
(Using the Toolbar, page 430)
Baud RateControls the number of bits per seconds being
transmitted. (Configure Balance Parameters, page 46, Data
Transmission Parameters, page 48)
CalibrationAllows the calibration parameters to be accessed
and configured. (Using the Toolbar, page 430)
Data BitsA way of measuring the amount of data transmitted.
(Configure Balance Parameters, page 46, Data Transmission
Parameters, page 48)
DateDisplays the date the sample was analyzed. The date is
taken from the CPU system clock and cannot be manually
edited in the sample pane. The date and time can be set using
the Windows control panel. (Columns, page 422)
DescriptionDisplays any additional descriptions that have
been added to identify the sample. (Columns, page 422)
DiagnosticsDisplays the current conditions of the cells. (Using
the Toolbar, page 430)
HelpAccess the onboard help topics. (Using the Toolbar, page
430)
High Sulfur AreaDisplays the total milligrams of sulfur in the
sample as measured in the high sulfur cell before calibration.
(Columns, page 422)
High SulfurDisplays the concentration of the sample as
measured by the high sulfur cell. (Columns, page 422)
High Sulfur PeakDisplays the peak voltage read by the high
sulfur cell. (Columns, page 422)
High Sulfur TimeDisplays the amount of time the sample was
analyzed by the high sulfur cell. (Columns, page 422)
Low SulfurDisplays the concentration of the sample as
measured by the low sulfur cell. (Columns, page 422)
Low Sulfur AreaDisplays the total milligrams of sulfur in the
sample as measured in the low sulfur cell before calibration.
(Columns, page 422)
122
S-144DR
Introduction
Introduction
S-144DR
123
124
S-144DR
Introduction
Installation
n
I
s
lio
ta
The Installation chapter guides you through the hardware setup
and connection of the S-144DR Dual Range Sulfur Analyzer. For
software information, refer to System Setup, page 41.
Illustrations .......................................................................22
Analyzer Installation ...........................................................23
International Installation ................................................ 24
Heating Element Installation ................................................25
Combustion System Installation ...........................................29
Sliding Door and Combustion Shelf Installation ..................... 211
Reagent Tube Installation .................................................. 212
Gas Connections .............................................................. 213
Exhaust Tube Connections ................................................. 214
Computer Installation ....................................................... 215
Minimum Requirements ................................................ 216
USB Cable Installation....................................................... 217
Ground Strap Installation .................................................. 218
Software ......................................................................... 219
Installation ................................................................. 219
Start Up ..................................................................... 220
Setup Information ............................................................ 221
Import Setup .............................................................. 221
Export Setup .............................................................. 223
Installation
S-144DR
21
Illustrations
Figure 2-1 ......... Facility Requirements ................................. 224
Figure 2-2 ......... Computer Hook-ups ................................... 225
Figure 2-3 ......... Wiring Diagram ......................................... 226
Figure 2-4 ......... Component Installation............................... 227
Figure 2-5 ......... Heating Elements....................................... 228
Figure 2-6 ......... Braided Cable Installation ........................... 229
Figure 2-7 ......... Combustion System Assembly ..................... 230
Figure 2-8 ......... Combustion System ................................... 231
Figure 2-9 ......... Sliding Door And Combustion Shelf .............. 232
Figure 2-10 ....... Reagent Tube Removal ............................... 233
Figure 2-11 ....... Reagent Tube Installation ........................... 233
22
S-144DR
Installation
Analyzer Installation
WARNING
Note
Installation
1.
2.
3.
4.
S-144DR
23
International Installation
For international installation, a HAR approved line cord for use
in the end country must be obtained. This product requires a
disconnect device that may either be the plug of the power cord
or a disconnect device installed at the installation site if the
equipment is permanently wired.
When the plug on the power supply cord is intended to serve as
the disconnect device, the socket/outlet must be installed near
the equipment and shall be easily accessible. When the wiring
is permanently connected, a disconnect device (such as a
circuit breaker or switch) must be lockable, installed near the
equipment, and be easily accessible.
24
S-144DR
Installation
WARNING
WARNING
!
CAUTION
!
CAUTION
Installation
S-144DR
25
1.
WARNING
WARNING
2.
3.
4.
5.
B.
C.
6.
7.
8.
9.
10. Insert the four heating elements in the four holes in the
furnace. The heating elements are properly positioned
when approximately 1/4 inch of the darker portion of each
rod is visible in front of the combustion area (figure 2-5,
page 228).
26
S-144DR
Installation
Note
11. From the front of the furnace, curl one end of the braided
cable around the upper left heating element (figure 2-6,
page 229).
12. Using the clamp expansion tool, install a clamp onto the
heating element over the braided cable.
13. Curl the other end of the cable around the lower bottom
heating element and clamp it in place. The braided cable
must not be taut.
Note
14. Repeat steps 11-13 for the right two heating elements.
15. From the back of the furnace, curl the free end of the left
braided cable, already connected to the instrument,
around the lower left heating element and clamp it in
place.
16. Curl the free end of the right braided cable, already
connected to the instrument, around the lower right
heating element and clamp it in place.
17. Curl one end of the remaining braided cable around the
upper left heating element and clamp it in place.
18. Curl the other end of the braided cable around the upper
right heating element and clamp it in place.
19. Set the lower front ceramic insulator into the slots
provided on the left and right of the furnace. Slide the
square down in place (figure 2-5, page 228).
20. Place the ceramic insulator with the notch on top of the
first square (figure 2-5, page 228).
21. Insert the back ceramic insulator through the slot in the
top of the instrument and into the slots provided on the
left and right sides of the furnace (figure 2-5, page 228).
Installation
S-144DR
27
22. Reinstall the rear access panel (figure 2-4, page 227).
23. Reinstall the cover to the slot located on top of the
instrument.
Notes
28
S-144DR
Installation
WARNING
WARNING
Note
Installation
1.
2.
3.
Be sure that the face of the front flange is flush with the
face of the inner combustion tube. If it is not, the
combustion tube will break when installed.
4.
5.
Insert the boat stop into the end of the inner combustion
tube (figure 2-7, page 230).
6.
S-144DR
29
7.
Place the outer combustion tube over the boat stop and
inner combustion tube. The combustion tube is properly
positioned when the o-ring is centered on the flanged lip of
the adapter block (figure 2-7, page 230).
8.
9.
10. Place the entire assembly in the furnace and secure the
adapter block assembly with the two thumbscrews (figure
2-8, page 231).
210
S-144DR
Installation
Note
Installation
1.
2.
3.
4.
5.
B.
6.
7.
8.
9.
S-144DR
211
212
B.
C.
2.
3.
4.
S-144DR
Installation
Gas Connections
Installation
1.
2.
S-144DR
213
Note
214
1.
2.
S-144DR
Installation
Computer Installation
An IBM compatible personal computer (PC) and monitor are
required to control the instrument and are included in the
equipment package. If the computer system is not supplied by
LECO, the computer used must meet the minimum
requirements, page 216, for additional information.
!
CAUTION
1.
2.
3.
4.
Installation
A.
B.
B.
C.
S-144DR
215
5.
6.
Note
B.
C.
7.
8.
9.
Minimum Requirements
216
CPUPentium 333MHz
RAM256 MB
Operating SystemWindows2000
Hard Drive2 GB
S-144DR
Installation
!
CAUTION
WARNING
Installation
1.
2.
Locate the USB cable (universal serial bus) and plug one
end to the USB connector on the rear of the computer.
3.
Plug the other end to the USB connector on the rear of the
instrument into the USB/ISA interface card, page 104.
Refer to figure 11-1, page 11-3, for additional information.
S-144DR
217
!
CAUTION
WARNING
WARNING
218
Remove the second screw and washer from the right along
the bottom of the instrument back panel. Leave the
washer on the screw.
3.
4.
Reinstall the screw and washer with the ground strap into
the back panel.
5.
B.
Slide the ring lug on the free end of the ground strap
onto the screw.
C.
S-144DR
Installation
Software
The S-144DR software can be loaded once the hardware
components have been properly set up. The Windows
operating system and S-144DR software is initially installed by
LECO. Use this procedure to install the S-144DR software when
a PC is not purchased from LECO.
A major portion of the analyzer's functions are defined and
controlled by a software program. Periodically, software version
updates that enhance operation are available from LECO. An
identification system for program changes called 'Program
Version' is used in the S-144DR Analyzer and other LECO
instruments. For software update of the program, refer to
Software Upgrades.
A three-digit number identifies program version levels. The first
generation of a program is version '1.00'. Each time a program
is changed, the version number is increased.
Note
Installation
Note
Installation
1.
2.
3.
4.
5.
S-144DR
219
Note
Start Up
220
1.
2.
3.
S-144DR
Installation
Setup Information
LECO provides a Setup Information disk containing the furnace
calibration for the instrument and a calibrated method. The
setup disk should be used to initially set up the S-144DR
system. Typically, the information on the setup disk will not be
used again after the initial setup.
Import Setup
The import setup information feature can be used to import
setup information from another file or disk into the S-144DR
software.
Notes
1.
2.
Installation
S-144DR
221
B.
3.
222
Locate and select the file. Click Open. The system loads
the setup information into the S-144DR software.
S-144DR
Installation
Export Setup
The S-144DR allows setup information to be exported to a disk
or alternate file location.
1.
2.
Installation
B.
S-144DR
223
REGULATOR
KEYBOARD
MOUSE
H/P PRINTER
(OPTIONAL)
OXYGEN
TANK
TO POWER
SOURCE
OXYGEN
CONNECTOR
EXHAUST
ANALYZER
J101
MEASURE
EXHAUST
ALARM
RELAY
COMPUTER
(OPTIONAL)
REAR ACCESS
PANEL
MONITOR
(OPTIONAL)
BALANCE
(OPTIONAL)
40 PSI
2.76 BAR
OXYGEN INLET
RESET
OXYGEN
INLET
TO POWER
SOURCE
Note
WARNING
High Voltage
To avo id elect ric sh ock, dis conn ect the linecord be fore servici ng.
OVEN FAN
OVEN HEATER
USB
CABLE
TO POWER
SOURCE
TO POWER
SOURCE
TO POWER
SOURCE
BALANCE
INTERFACE
CABLE
Figure 2-1
Facility Requirements
224
S-144DR
Installation
MONITOR
(VIDEO PORT)
MOUSE
(SERIAL PORT)
KEYBOARD
(SERIAL PORT)
PRINTER
(USB PORT)
ANALYZER
(USB PORT)
BALANCE
(COM1 PORT)
COM2 PORT
Figure 2-2
Computer Hook-ups
Installation
S-144DR
225
DETERMINATOR
POWER CORD
BLACK
POWER
220 VAC
WHITE
NEUTRAL
0 VAC
GREEN
GROUND
CHASSIS
(CABINET)
GROUND
POWER
115 VAC
GROUND
POWER
230 VAC
115 VAC
WHITE
GREEN
BLACK
WHITE
GREEN G
RED
RED *
X
BLACK
CHASSIS
(CABINET)
GROUND
765-978 RECEPTACLE
Figure 2-3
Wiring Diagram
226
S-144DR
Installation
614-687
REAR ACCESS
PANEL
616-051
PURGE TUBE
616-035
ADAPTER
BLOCK
ASSEMBLY
606-316
ADAPTER
606-327
REAGENT
TUBE
(2-REQ'D)
Figure 2-4
Component Installation
Installation
S-144DR
227
606-323
REAR CERAMIC
INSULATOR
616-084
TOP FRONT
CERAMIC
INSULATOR
606-321
LOWER FRONT
CERAMIC
INSULATOR
606-601
HEATING
ELEMENTS
(4/SET)
Figure 2-5
Heating Elements
228
S-144DR
Installation
CLAMP
HEATING
ELEMENT
CABLE
CABLE
HEATING
ELEMENT
CLAMP
EXPANSION
TOOL
BRAIDED
CABLE
(2 REQUIRED)
0.125 TYP
BRAIDED
CABLE
BRAIDED
CABLE
WITH CLIP
(2 REQUIRED)
STANDOFF
(2 REQUIRED)
Figure 2-6
Braided Cable Installation
Installation
S-144DR
229
616-012
FRONT FLANGE
616-068
INNER COMBUSTION
TUBE O-RING
606-307
FITTING
616-070
INNER COMBUSTION
TUBE
616-035
ADAPTER BLOCK
ASSEMBLY
616-013
COMPRESSION
FLANGE
616-086
BOAT STOP
783-897
OUTER COMBUSTION
TUBE O-RING
FLAT SIDES
TOWARD SLOTS
REAR VIEW OF
ADAPTER BLOCK
616-089
OUTER COMBUSTION
TUBE
616-013
COMPRESSION
FLANGE
190-742
SCREW
(8 REQ'D)
Figure 2-7
Combustion System Assembly
230
S-144DR
Installation
616-009
SLOT COVER
616-051
PURGE TUBE
616-015
UPPER DOOR
GUIDE
COMBUSTION
SYSTEM
ASSEMBLY
606-298
THUMBSCREW
AND SPACER
(2 REQD)
Figure 2-8
Combustion System
Installation
S-144DR
231
616-062
SLIDING
DOOR
ASSEMBLY
606-324
SHELF
616-027
LOWER DOOR
GUIDE
614-694
COMBUSTION
SHELF
606-316
ADAPTER
Figure 2-9
Sliding Door And Combustion Shelf
232
S-144DR
Installation
TUBE
Figure 2-10
Reagent Tube Removal
773-320
O-RING
(2 REQ'D)
606-327
REAGENT TUBE
(2 REQ'D)
501-171
ANHYDRONE
(4 3/4 IN.)
501-081
GLASS WOOL
(1/2 IN.)
772-520
O-RING
(2 REQ'D)
Figure 2-11
Reagent Tube Installation
Installation
S-144DR
233
234
S-144DR
Installation
Option Installation
O
p
tio
n
I
ta
s
lio
n
The Option Installation chapter gives information about and
explains how to install optional accessories and kit packages.
Illustrations .......................................................................32
Balance.............................................................................33
Balance Installation ....................................................... 33
Reset Balance ............................................................... 34
Set Data Output Parameters ........................................... 35
Printer ..............................................................................36
Option Installation
S-144DR
31
Illustrations
Figure 3-1 ......... Balance Assembly ...................................... 37
Figure 3-2 ......... Balance Control Panel................................. 37
32
S-144DR
Option Installation
Balance
The S-144DR is capable of being interfaced to an electronic
balance so that sample weights may be electronically
transferred. The optional balance offered is the Sartorius
AC121S. Refer to Options, page 115, for part number and
ordering information.
Balance Installation
Option Installation
1.
2.
3.
4.
5.
S-144DR
33
Reset Balance
The balance must be activated in the Windows software to
properly accept the balance's data. Refer to Configure Balance
Parameters, page 46, for activation information. The electronic
balance has its own setup menu. The serial communications are
preset. Refer to the balance manual should any of these
parameters need to be changed or reset.
34
1.
2.
3.
4.
5.
6.
Press Tare.
7.
8.
S-144DR
Option Installation
Option Installation
1.
2.
3.
4.
5.
6.
7.
Press Tare.
8.
9.
S-144DR
35
Printer
The S-144DR is designed to directly interface with the DeskJet
printer offered by LECO. Although other printers may work,
LECO does not recommend nor support these printers.
Notes
36
S-144DR
Option Installation
MENU ACCESS
SWITCH
HOLE PLUG
Figure 3-1
Balance Assembly
TOGGLE
POWER ON
CLEAR
FUNCTION
INFORMATION
I/O
F1
TARE
i
CF
TARE
TARE
F2
Figure 3-2
Balance Control Panel
Option Installation
S-144DR
37
38
S-144DR
Option Installation
System Setup
S
s
y
m
te
S
tu
e
p
The System Setup chapter explains how to set the operating
parameters for a specific application or set of applications. These
procedures should be done before any samples are analyzed for
the first time per application.
System Setup
S-144DR
41
S-144DR
System Setup
System Setup
S-144DR
43
Illustrations
Figure 4-1 ......... Controls and Indicators............................... 452
Figure 4-2 ......... Furnace Temperature Adjustment ................ 453
Figure 4-3 ......... Dual Furnace Controller Card....................... 454
44
S-144DR
System Setup
Note
System Setup
S-144DR
45
Notes
1.
2.
3.
4.
46
S-144DR
System Setup
B.
C.
D.
E.
Balance Definitions
Baud RateControls the number of bits per seconds being
transmitted.
ParityThe way the computer checks that the information
being transmitted fits a specific code expression.
Selections: Odd, Even, or None.
Data BitsA way of measuring the amount of data transmitted.
Stop BitsControls the delays between bits of transmitting
data.
PortSerial port to which the balance is connected.
System Setup
S-144DR
47
48
1.
2.
3.
4.
S-144DR
System Setup
5.
6.
Notes
System Setup
Select format.
A.
B.
C.
B.
S-144DR
49
1)
2)
3)
4)
5)
7.
8.
9.
410
S-144DR
System Setup
Note
System Setup
1.
2.
3.
4.
S-144DR
411
Note
Note
1.
2.
3.
412
S-144DR
System Setup
Notes
Note
4.
5.
6.
7.
8.
9.
WARNING
System Setup
S-144DR
413
Software Overview
Before operating the S-144DR software, it is necessary to be
comfortable with the Microsoft Windows operating system.
Main Window
The S-144DR main window displays the toolbar and menu
commands used to calibrate and run an analysis. The S-144DR
main window also displays the sample data collected during the
analysis and the status bar used to monitor the current
condition of the program.
414
S-144DR
System Setup
Executing Commands
There are several different ways to execute the commands and
routines in the S-144DR software: menu commands, shortcut
keys, and mouse-activated buttons.
Menu CommandsAre activated by selecting the menu with the
mouse and then clicking the command on that menu.
Shortcut KeysThese are keyboard keys used to activate the
command. No clicking with the mouse is needed when using
shortcut keys.
Keyboard Key CombinationsUsed to activate a menu and
execute a command. The underlined letter in the menu
command indicates the letter on the keyboard that is used to
activate the command.
Example
Pressing the ALT key and the S key opens the Samples
menu, then pressing the A key executes the Analyze
command.
System Setup
S-144DR
415
Note
416
S-144DR
System Setup
The OK button saves entries in the dialog box and may use
the entries to perform a function.
The Cancel button closes the dialog box without saving the
entries or performing the function.
System Setup
S-144DR
417
Using Help
The S-144DR includes an Onboard Help system designed to
help answer questions while you are using the program.
Information explaining menu commands, dialog boxes, terms,
definitions, how to perform various tasks, etc. is available by
pressing the F1 key, clicking the Help button on the toolbar, or
by selecting the Help Topics from the Help menu. Refer to
Using the On-board Manual, page 434, for additional
information.
Pressing the Shift and F1 keys, clicking the What's This? button
on the toolbar, or clicking the What's This? command from the
Help menu changes the cursor to a question mark. Clicking on
an item in the program with the question mark cursor accesses
Help information about that item.
Clicking the question mark located in the upper right corner of
a dialog box ( ) also changes the cursor to a question mark
allowing help to be accessed for any part of the dialog box.
Example
418
S-144DR
System Setup
Spreadsheet
The S-144DR software allows the operator to configure the
spreadsheet for a specific application or the operator's
preference. It also provides instructions for navigation and
explanations for usage.
Sample Pane
The sample pane spreadsheet grid records and tracks data for
individual samples. Listing the sample data in a spreadsheet
grid allows for greater versatility in entering and displaying the
sample data.
Notes
System Setup
S-144DR
419
Samples
Selecting samples in the sample pane and then selecting the
Add Sample or Delete Sample command from the samples
menu can add and delete samples.
Notes
Add a Sample
1.
2.
Delete a Sample
420
1.
2.
3.
S-144DR
System Setup
Entering Text
Text can be entered and replaced right in the sample pane,
making any additional steps for entering data unnecessary.
Clicking once on text in the spreadsheet grid activates replace
mode. In replace mode, text is replaced by typing something
new.
Double clicking on the text activates edit mode. In edit mode, a
cursor is displayed to indicate where text will be entered or
edited as you type.
Sample types and method names can be entered by selecting
them from the drop-down list or typing in the names. Double
clicking on these fields or clicking once on the arrow displays
the drop-down list so an entry can be selected.
Note
System Setup
S-144DR
421
Columns
The columns that are displayed in the sample pane can be
selected and organized by clicking the Columns command on
the View menu and accessing the Columns dialog box.
Select the columns to display in the sample pane by using the
Add and Remove buttons to create a list of desired column
titles in the Displayed Columns field. The C-144 stores the data
for all of the columns listed in both the Available Columns and
Displayed Columns fields, but only shows the data for the
columns listed in the Displayed Columns field. Refer to Column
Definitions, page 424, for additional information.
Columns can also be locked in place in the sample pane to
prevent them from scrolling out of view. The number entered in
the Locked Columns field indicates the number of fields that
stay visible when using the scroll bars to move through the
sample pane.
Example
422
S-144DR
System Setup
Resize Columns
Columns can be sized for easy viewing and organization of the
sample data. The grid cells can be resized by selecting one side
of the column title frame and dragging the frame to the desired
size. Double clicking on the divider line between the columns
sizes the column to the largest entry.
User-Defined Fields
Whenever a user-defined field is added, page 423, a column
matching the user-defined field name is displayed at the right
of the spreadsheet.
The user-defined fields can be formatted. Refer to Format
Columns, page 426, for additional information.
If the user-defined field is needed for previously analyzed
samples, the results can be recalculated for the new userdefined field. Refer to Recalculate Results, page 530, for
additional information.
System Setup
S-144DR
423
Columns Definitions
#Shows the numeric sequence in which the sample was
added to the sample pane. An asterisk indicates the currently
selected sample.
NameList the sample name. If running a standard, the
standard name can be selected from the available drop-down
list.
DescriptionDisplays any additional descriptions that have
been added to identify the sample.
MethodAllows the name of the method to be specified. The
method name can be selected from the available drop-down
list.
WeightAllows the total weight, in grams, of the sample to be
entered.
SulfurList the percentage of sulfur in the sample as
determined by the analysis.
Moisture %Allows the percentage of moisture in the sample
to be entered. The S-144DR system compensates for the
moisture value by removing this percentage from the total
weight of the sample before calculating the analysis results.
OperatorAllows the name of the system operator to be
recorded.
DateDisplays the date the sample was analyzed. The date is
taken from the CPU system clock and cannot be manually
edited in the sample pane. The date and time can be set using
the Windows control panel.
Sulfur AreaDisplays the total measured milligrams of sulfur in
the sample before calibration.
Sulfur PeakDisplays the peak voltage read by the sulfur cell.
Sulfur TimeDisplays the amount of time the sample was
analyzed by the sulfur cell.
Low SulfurDisplays the concentration of the sample as
measured by the low sulfur cell.
High SulfurDisplays the concentration of the sample as
measured by the high sulfur cell.
Low Sulfur PeakDisplays the peak voltage read by the low
sulfur cell.
Low Sulfur AreaDisplays the total milligrams of sulfur in the
sample as measured in the low sulfur cell before calibration.
Low Sulfur TimeDisplays the amount of time the sample was
analyzed by the low sulfur cell.
High Sulfur PeakDisplays the peak voltage read by the high
sulfur cell.
424
S-144DR
System Setup
System Setup
S-144DR
425
Format Columns
Format Columns lets the user specify the type of unit to be
used when displaying the result data and where the unit should
be displayed on the sample pane.
1.
2.
A.
426
S-144DR
System Setup
3.
Note
System Setup
B.
C.
D.
E.
S-144DR
427
Format Codes
The numeric format of the result data can be specified by
entering a formatting code. The following types of codes can be
used to format the data output results.
Picture Format CodeIndicates the decimal and comma
placement.
Format Code
#,###.##
Translation
2,333.24
S4
Translation
3.432+002
428
Format Code
F3
Translation
124000000
Format Code
F4
Translation
0.00023
S-144DR
System Setup
From the View menu, click Status Bar. A check indicates the
status bar is displayed.
System Setup
S-144DR
429
430
S-144DR
System Setup
Menu References
The following table provides the corresponding menu locations
of the toolbar buttons.
Sample Menu
F3
Add Sample
F4
Analyze
F7
Tools Menu
F5
Methods
F6
Standards
F8
Diagnostics
F9
Calibrate
Help Menu
System Setup
F1
Help
F10
What's This?
S-144DR
431
Menus
The following are the choices on the Menu bar in the software.
Clicking on any of these will open another set of menu choices.
Samples Menu
AddCreates a new entry in the sample pane.
DeleteDelete a sample removes a selected sample, with
sample data, from the spreadsheet.
AnalyzeDisplays the sample login screen to login and analyze
a sample or standard.
RecalculateAfter an analysis is complete, recalculate results
can be used adjust the results based on a new calibration,
blank, or sample weight.
PropertiesDisplays the sample property including name,
description, method, operator, moisture, and weight.
PrintThe print command accesses the Report Settings dialog
box to print selected sample results on the system printer.
Print PreviewThe print preview command accesses the Report
Settings dialog box to preview how selected samples would
print on the system printer.
TransmitTransmits the selected analyzed samples, with a
data format, to a host computer.
ExportUsed to export sample data to another storage location
such as a floppy diskette.
ExitUsed to exit the software application program and return
to the Windows Operating System.
Edit Menu
CopyUsed to copy data from an entire row in the spreadsheet
to the clipboard.
PasteUsed to paste data from the clipboard to a selected row
in the spreadsheet.
432
S-144DR
System Setup
View Menu
ToolbarToggles the toolbar off or on.
Status BarToggles the status bar off or on.
ColumnsAccesses the Columns dialog box. Refer to Columns,
page 422, for additional information.
Tools Menu
MethodsUsed to create a method for analysis. Refer to
Methods, page 5-10, for additional information.
StandardsUsed to enter standards into the calibration
standards list. Refer to Standards, page 5-18, for additional
information.
OptionsAccesses the Options dialog box. Refer to either
Configure Balance Parameter, page 46, or Data Transmission
Parameters, page 48, for additional information.
DiagnosticsAccesses the Diagnostics dialog box. Refer to
Diagnostics, page 8-3, for additional information.
Set BlankUsed to automatically calculate and set the Blank at
1 gram values for the samples selected in the sample grid.
Refer to Blank, page 516, for additional information.
CalibrateSets the accuracy of the instrument to that of known
calibration standard samples.
Calibrate FurnaceSets the accuracy of the Furnace Calibration
dialog box. Refer to Calibrate Furnace Temperature, page 411,
for additional information.
Export Setup InformationUsed to export sample data to
another storage location like a floppy disk.
Import Setup InformationUsed to import sample data from
another software application.
Validate DatabaseUsed to recover missing database
information. Validating the database ensures that any item
referenced by another item is included in the database.
Select LanguagePermits the user to select the language of the
software. The on-board manual will remain in English.
Help Menu
Help TopicsAccesses the on-board instruction manual.
What's This?Provides additional information about an item
when available.
AboutContains information about the software version
number, and the computer and registration numbers.
System Setup
S-144DR
433
434
S-144DR
System Setup
System Setup
1.
2.
3.
S-144DR
435
Navigation Pane
On the left side of the screen is the Navigation pane. It contains
the navigational tabs such as the Contents, Index, Search, and
Favorites tabs. The Navigation pane can also be hidden from
view.
Hide/Show
On the toolbar, click Hide or Show to close or display the
Navigation pane.
Note
436
S-144DR
System Setup
Resize
To resize the Navigation or Topic pane, point to the divider
between the two panes. When the pointer changes to a doubleheaded arrow, drag the divider right or left.
Change Height/Width
To change the height or width of the on-board manual, point to
the top, bottom, left, or right edge of the on-board manual.
When the pointer changes to a double-headed arrow, drag the
edge.
Reposition
To reposition the on-board manual on your screen, click the
title bar and drag the Viewer to a new position.
System Setup
S-144DR
437
Topics
The on-board manual is composed of numerous topics. Each
topic contains information designated to a particular area or
process.
Find a Topic
Click the contents entry or search results entry to display the
corresponding topic. In the Navigation pane, click one of the
following tabs.
Contents
To browse through the table of contents, click the Contents tab.
The table of contents is an expandable list of important topics.
Index
To locate a topic related to a word contained in the on-board
manual, click the Index tab then type the word.
Search
To locate every occurrence of a word or phrase that may be
contained in the on-board manual, click the Search tab then
type the word.
438
S-144DR
System Setup
Copy a Topic
Note
System Setup
1.
If you want to copy only part of a topic, select the text you
want to copy, right-click, and then click Copy.
2.
3.
4.
5.
S-144DR
439
Print a Topic
1.
2.
Current topic
3.
440
A.
B.
C.
B.
1)
2)
S-144DR
System Setup
C.
D.
System Setup
1.
2.
3.
4.
5.
S-144DR
441
Searches
There are many different ways to perform searches within the
on-board manual. This section explains how to utilize the
search capabilities.
Example
Note
442
Search For
Example
Results
sample OR standard
S-144DR
System Setup
Basic Rules
The basic rules for formulating queries are as follows.
1.
2.
3.
4.
Example
Results
A single word
select
Topics that contain the word "select." (You will also find its
grammatical variations, such as "selector" and "selection.")
A phrase
"new operator"
or
new operator
Topics that contain the literal phrase "new operator" and all its
grammatical variations.
Without the quotation marks, the query is equivalent to specifying
"new AND operator," which will find topics containing both of the
individual words, instead of the phrase.
Wildcard
expressions
ESC*
or
80?86
Note
System Setup
S-144DR
443
Note
1.
2.
3.
Click List Topics, select the topic you want, then click
Display.
Notes
444
1.
2.
If you are viewing a long topic, only the first 500 instances
of a search word or phrase will be highlighted.
S-144DR
System Setup
Example
System Setup
1.
Click the Search tab, type the word or phrase you want to
find, and then select the Match Similar Words check
box.
2.
Click List Topics, select the topic you want, and then click
Display.
S-144DR
445
Full-Text Search
1.
2.
3.
Click List Topics, select the topic you want, then click
Display.
Notes
446
1.
2.
3.
Click
4.
Click List Topics, select the topic you want, and then click
Display.
5.
S-144DR
System Setup
Nested Expressions
Nested expressions allow you to create complex searches for
information.
Example
Basic Rules
The basic rules for searching topics using nested expressions
are as follows.
Example
System Setup
1.
2.
3.
S-144DR
447
Notes
448
1.
2.
3.
Click List Topics, select the topic you want, then click
Display.
S-144DR
System Setup
Shortcuts
There are both shortcut keys and shortcut menu commands
that can be used in the on-board manual. This section gives a
detailed explanation to the different ways and areas in which
these shortcuts are used.
Shortcut Keys
The following keyboard shortcuts can be used for navigation in
the on-board manual. There are different shortcut keys for
different areas: the on-board manual, the Contents tab, the
Search tab, and the Favorites tab.
Notes
On-Board Manual
To
Press
ALT + F4
ALT + Tab
ALT + O
Print a topic.
F5 or
ALT + O then press R
F6
Tab
System Setup
S-144DR
449
Contents Tab
To
Press
ALT + C
Plus Sign and Minus Sign or Left Arrow and Right Arrow
Select a topic
Enter
Search Tab
To
Press
ALT + S
Start a search.
ALT + L
ALT + D
ALT + U
ALT + M
ALT + R
Note
If the Match Similar Words check box was used in the last
search, it will still be selected.
Favorites Tab
To
Press
ALT + I
ALT + A
ALT + D
ALT + R
450
S-144DR
System Setup
Description
Closes all books or folders. This command only works if the Contents
tab is displayed.
Note
System Setup
S-144DR
451
COMBUSTION
SHELF
765-537
PURGE FLOW
FLOWMETER
778-494
MEASURE FLOW
FLOWMETER
606-327
REAGENT TUBES
(2 REQD)
614-523
CIRCUIT BREAKER
Figure 4-1
Controls and Indicators
452
S-144DR
System Setup
666-121-110
DUAL FURNACE
CONTROLLER
CARD ASSEMBLY
POTENTIOMETER
SET POINT
Figure 4-2
Furnace Temperature Adjustment
System Setup
S-144DR
453
R2
R3
R1
10
U12
C39 TP6
R10
R11
R12
C23
C19
C16
1
2
C59
C29
C22
C28
R38
19
20
C36
C15
C14
U9
C35
R37
C18
C17
U8
TP4
R48
U13
C41
C42
R43
1
TB2
TP5
R47
C38
10
R33
C37 R34
U11
U7
CR4 C34
C31 LED2
TP2
TP3 C32
C30
C33
U10
C26
R32 R24
C27 R25
U6
R31 R23
C25
TP1
C43
R19
C21
LED1
R22
U5
R41
R42
U4
C20
R20
R21
CR3
R26
R28 R27
R29 C24
Q1
C12
R16
R18
666-121-110
DUAL FURNACE
CONTROLLER II
CARD
J121A
R46
C11
C7
R8
C8
R9
R30
CR2
R17
C6
C10
R15
CR1
R14
C9
R13
R7
U3
R44
R45
C4
TB1
U2
C40 R35
R40 R39 CR5
J121
C1
U1
C13
C2
C3
R4
R5
R6
C5
R3
R2
Figure 4-3
Dual Furnace Controller Card
454
S-144DR
System Setup
5 Operation
Operation
Operation
S-144DR
51
52
S-144DR
Operation
Note
Operation
B.
C.
S-144DR
53
2.
Note
B.
C.
54
S-144DR
Operation
Note
Operation
E.
F.
H.
I.
S-144DR
55
J.
Example
Notes
3.
Notes
Login a conditioner.
4.
56
A.
B.
C.
D.
Analyze a conditioner.
A.
B.
S-144DR
Operation
Note
5.
Note
Operation
B.
C.
D.
S-144DR
57
E.
6.
Notes
Analyze a standard.
A.
B.
7.
58
S-144DR
Operation
8.
Operation
B.
C.
Perform an analysis.
A.
B.
S-144DR
59
Methods
A method is a set of analytical parameters used to control the
instrument during analysis and calculation of the final result.
Before analysis, a method must be created or the default
method used.
Create a Method
The S-144DR software offers the feature of creating methods to
be used for carbon analysis. The maximum and minimum
integration times, the comparator levels, and the blank analysis
value are stored in each method.
510
1.
2.
3.
S-144DR
Operation
Note
Note
Operation
4.
5.
6.
7.
8.
9.
S-144DR
511
Example
Notes
512
S-144DR
Operation
Edit a Method
The S-144DR allows existing methods to be edited before
beginning an analysis.
Operation
1.
2.
3.
S-144DR
513
Print a Method
The S-144DR allows existing methods to be printed before
beginning an analysis.
514
1.
2.
3.
4.
Click OK.
S-144DR
Operation
Delete a Method
The S-144DR allows existing methods to be deleted before
beginning an analysis.
Operation
1.
2.
3.
4.
Click OK.
S-144DR
515
Blanks
A blank is an analysis, which is used to establish the level of
background signal observed when no sample is present in the
combustion boat.
Add a Blank
1.
2.
3.
4.
Analyze a Blank
516
1.
2.
S-144DR
Operation
Set Blank
Operation
1.
2.
3.
S-144DR
517
Standards
Standards are certified reference materials with known
concentrations and uncertainty levels.
Add Standard
Any samples that are to be used for calibration must have a
defined standard for that sample type.
Note
518
1.
2.
S-144DR
Operation
Note
Operation
3.
4.
S-144DR
519
Print Standard
Standards can be printed from the system printer.
520
1.
2.
3.
4.
Click OK.
S-144DR
Operation
Delete Standard
Standards that are no longer applicable can be deleted.
1.
2.
3.
4.
Operation
S-144DR
521
Calibration
A valid calibration of the system should be performed before
running any unknown samples. Instrument drift is possible and
a current calibration is necessary to calculate accurate results.
The calibration results are used to compensate for differences
between the total sulfur area measured and the actual sulfur
area.
In order for a calibration procedure to be complete, standards
for each calibration sample must be set up, a calibration
analysis must be run, and a calibration curve must be created.
Calibration Analysis
Notes
!
CAUTION
1.
Note
522
S-144DR
Operation
A.
B.
Note
2.
Note
Note
Operation
2)
Weigh the sample first then press the Print key on the
balance to add the new sample. If all the samples
listed have a weight entry, pressing the print key on
the balance automatically adds a new sample and
enters the measured weight.
3.
4.
S-144DR
523
5.
WARNING
Notes
524
S-144DR
Operation
Calibration Curve
When the system is finished analyzing the known samples, a
calibration curve comparing the measured raw sulfur areas and
the corrected sulfur areas (calculated by multiplying the weight
of the sample by the standard percentage of sulfur) can be
created. The calibration curve is then used to calculate the
corrected sulfur area of the unknown samples.
Notes
Operation
1.
2.
S-144DR
525
3.
Note
Notes
526
Only the points that saturated the low sulfur cell are used
when calibrating the high sulfur cell.
4.
5.
B.
C.
6.
S-144DR
Operation
Operation
7.
8.
S-144DR
527
Perform Analysis
Be sure that the analyzer hardware and software has been
setup and that the analyzer has reached the set temperature
before beginning an analysis. Standards must be set up for all
sample types used for calibrating the system.
!
CAUTION
Note
1.
Add the sample and the sample weight. There are two
ways to add samples and their weights.
B.
Note
528
2)
S-144DR
Operation
Note
2.
3.
4.
5.
WARNING
Note
Operation
6.
Notes
S-144DR
529
Recalculate Results
If the calibration or moisture values have changed for a
sample, the analysis results can be recalculated using the new
values.
530
1.
2.
S-144DR
Operation
User-Defined Field
User-Defined Fields allows the operator to enter a formula in
order to perform custom calculations using pre-determined
functions or to define a column for text only. After a UserDefined Field has been added, it is displayed in the spreadsheet
and sample login screen.
Operation
1.
2.
3.
B.
C.
S-144DR
531
Examples
(2.786+(8.8831*@sulfur())-(2.143-@moisture())
(8.8831*@sulfur())/@moisture()
@sulfur*0.25
4.
5.
Note
532
B.
C.
B.
C.
S-144DR
Operation
Operation
6.
7.
S-144DR
533
2.
3.
4.
5.
Available Functions
@Name ()
Text Only
@Description()
Text Only
@Method()
Text Only
@Weight()
Numeric Only
@Sulfur()
Numeric Only
@Moisture()
Numeric Only
534
S-144DR
Operation
Operation
S-144DR
535
536
S-144DR
Operation
Operation
1.
2.
S-144DR
537
3.
Note
Like the analysis data, the IR cell data can be viewed for a
single sample or for multiple samples.
538
S-144DR
Operation
General Tab
The general tab displays the sample information listed in the
sample pane. If multiple samples are selected, fields containing
varying information are left blank.
Example
Operation
S-144DR
539
The View Data option is available when viewing cell data for a
single sample. Clicking the View Data button displays a list of
voltages recorded by that cell and the intervals at which they
were recorded.
The Saturated box indicates if the cell was or was not saturated
during analysis. A check mark indicates that the cell was
saturated.
540
S-144DR
Operation
Print Preview
To view the printout before sending it to the printer, select
Print Preview from the Samples menu.
Print Setup
To select the printer, paper size, paper size, paper source, and
page orientation for a printout, select Print Setup from the
Samples menu.
Operation
S-144DR
541
Print Data
542
1.
2.
3.
4.
5.
S-144DR
Operation
Operation
6.
7.
8.
9.
Click OK to print.
S-144DR
543
544
1.
2.
3.
A.
B.
C.
D.
S-144DR
Operation
Example
4.
Operation
A.
B.
C.
D.
E.
S-144DR
545
F.
5.
A.
546
2)
3)
4)
S-144DR
Operation
B.
Example
5)
6)
7)
2)
Example
6.
Notes
Operation
S-144DR
547
Transmit Data
Result data can be transmitted to a receiving application or to a
file to be used with other applications.
Make sure the transmission parameters have been entered so
the data can be sent in a format that the receiving application
understands. Refer to Data Transmission Parameters, page
48, for additional information.
548
1.
2.
3.
4.
S-144DR
Operation
Export Results
The S-144DR allows result data to be selected for export to
another file or applications. It also allows the fields, unit
formats, and statistics to be specified when exporting the data.
Information other than what is listed in the sample pane can be
exported.
Operation
1.
2.
3.
A.
B.
S-144DR
549
4.
5.
550
A.
B.
C.
S-144DR
Operation
6.
Note
Operation
A.
B.
C.
D.
S-144DR
551
Validate Database
The validate database feature recovers missing database
information. Validating the database ensures that any item
referenced by another item is included in the database.
Note
552
1.
2.
3.
S-144DR
Operation
Operation
S-144DR
553
Maintenance
M
in
a
te
c
The Maintenance chapter includes procedures that should be
performed on a regular basis to keep your S-144DR Dual Range
Sulfur Analyzer operating up to specifications. Periodic
maintenance is an important part of extending the life of your
instrument and minimizing downtime.
Illustrations .......................................................................62
Periodic Maintenance Schedule .............................................63
Adapter.............................................................................64
Disposable Particle Filters ....................................................65
Front Disposable Particle Filter......................................... 65
Internal Disposable Particle Filter ..................................... 66
Fan Filter ..........................................................................67
O-ring...............................................................................68
Reagent Tubes ...................................................................69
Computer System............................................................. 610
Printer ............................................................................ 611
Maintenance
S-144DR
61
Illustrations
Figure 6-1 ......... Component Installation............................... 612
Figure 6-2 ......... Reagent Tube Removal ............................... 613
Figure 6-3 ......... Reagent Tubes .......................................... 613
62
S-144DR
Maintenance
Replacement
and Maintenance
Inspection and
Cleaning Schedule
Adapter
Daily
Refer to page 64.
Weekly
Refer to page 65.
Fan Filter
Daily
Refer to page 67.
O-ring
Weekly
Refer to page 68.
Reagent Tubes
Weekly
Refer to page 69.
Computer System
Weekly
Refer to page 610.
Printer
Weekly
Refer to page 611.
Maintenance
S-144DR
63
Adapter
1.
64
B.
C.
2.
Unscrew adapter.
3.
4.
5.
S-144DR
Maintenance
Note
1.
Note
B.
C.
2.
3.
4.
Maintenance
S-144DR
65
Note
Note
66
1.
2.
3.
Slide the disposable particle filter out of the nut and pull it
out a few inches from the instrument.
4.
5.
6.
7.
S-144DR
Maintenance
Fan Filter
The fan filter, located on the back of the furnace, needs to be
inspected daily and cleaned when dirt is visible.
Note
Maintenance
1.
Remove the blank plastic box containing the fan filter from
the back of the instrument.
2.
Separate the sides of the plastic box and remove the fan
filter.
3.
4.
Rinse clean under running water then gently shake out any
excess water.
5.
6.
S-144DR
67
O-ring
The o-rings, located around the top of the reagent tubes,
should be cleaned and greased when replacing reagent
materials.
1.
2.
Note
3.
Note
68
B.
C.
4.
5.
S-144DR
Maintenance
Reagent Tubes
Repack the reagent tubes with anhydrone whenever the
reagent becomes caked or moist (from moisture being released
from samples).
1.
Maintenance
B.
C.
2.
3.
4.
5.
S-144DR
69
Computer System
Maintain the computer system by cleaning the system once a
week or as needed to maintain usability of the system and
eliminate static charge build up.
Note
1.
2.
3.
610
Monitor
1)
Wipe the screen using a soft cloth or an antistatic wipe designed for electronics.
2)
B.
C.
Mouse
1)
2)
S-144DR
Maintenance
Printer
Maintain the printer by cleaning the printer once a week or as
needed to maintain usability of the system and eliminate static
charge build up.
Note
Maintenance
1.
2.
3.
4.
5.
S-144DR
611
606-316
ADAPTER
606-327
REAGENT
TUBE
(2 REQ'D)
Figure 6-1
Component Installation
612
S-144DR
Maintenance
TUBE
Figure 6-2
Reagent Tube Removal
773-320
O-RING
(2 REQ'D)
606-327
REAGENT TUBE
(2 REQ'D)
501-171
ANHYDRONE
(4 3/4 IN.)
501-081
GLASS WOOL
(1/2 IN.)
772-520
O-RING
(2 REQ'D)
Figure 6-3
Reagent Tubes
Maintenance
S-144DR
613
614
S-144DR
Maintenance
Theory of Operation
T
h
o
e
ry
fO
p
ra
e
tio
n
The Theory of Operation chapter provides a technical description of
how the instrument operates and the stages of operation that
generate reliable results. Learn how precision and accuracy are
directly related to the initial calibration and changes in standard
concentrations.
Illustrations .......................................................................72
Theory of Operation ............................................................73
Infrared Radiation, Absorption, and Detection.........................74
Comparator Level ...............................................................75
Calibration Curves ..............................................................78
Curves and Intercepts .................................................... 78
Intercepts ............................................................... 78
Linear Calibration Curve ............................................ 79
Calibrating with a Linear Curve .............................. 79
Quadratic Calibration Curve ..................................... 710
Calibrating with a Quadratic Curve ....................... 710
Cubic Calibration Curve ........................................... 711
Calibrating with a Cubic Curve ............................. 711
Theory of Operation
S-144DR
71
Illustrations
Figure 7-1 ......... Analytical Flow Diagram.............................. 712
72
S-144DR
Theory of Operation
Theory of Operation
The S-144DR Sulfur Analyzer is a software controlled
instrument designed to determine the sulfur content in a wide
variety of organic materials such as coal, coke, and oils, as well
as some inorganic materials such as soil, cement, and
limestone by combustion and non-dispersive infrared detection.
Analysis begins as a sample (0.350 g nominal) is weighed into
a combustion boat. When Analyze is selected from the Samples
menu, the sample is placed in a pure oxygen environment
typically regulated at 1350oC. The combination of furnace
temperature and oxygen flow causes the sample to combust.
All sample materials contained in the combustion boat go
through an oxidative-reduction process that causes sulfurbearing compounds to break down and free the sulfur. The
sulfur forms SO2. (The design of the combustion system
prevents the atmosphere from entering the combustion zone.)
Sample gases are first swept through the boat stop to the back
of the inner combustion tube, then forward between the inner
and outer combustion tubes, allowing the sample gases to
remain in the high temperature zone for a longer period and
permit efficient oxidation.
From the combustion system, the gases flow through two
anhydrone tubes to remove moisture, through a flow controller
that sets the flow of sample gases to 3.5 l/min, and then
through the infrared detection cell.
The sulfur IR cell measures the concentration of sulfur dioxide
gas. The instrument converts these values to a percentage/ppm
value, using an equation preset in the software that takes into
account the sample weight, calibration, and known moisture
value.
Theory of Operation
S-144DR
73
74
S-144DR
Theory of Operation
Comparator Level
Note
Theory of Operation
S-144DR
75
START OF
ANALYSIS
COMPARATOR
LEVELEND OF ANALYSIS
DETECTOR OUTPUT
COLLECTED
START OF
ANALYSIS
COMPARATOR
LEVELEND OF ANALYSIS
DETECTOR OUTPUT
COLLECTED
2.
3.
76
S-144DR
Theory of Operation
DETECTOR
OUTPUT
COLLECTED
SIGNIFICANT
DETECTOR
OUTPUT
EXCLUDED
COMPARATOR LEVEL
(SET TOO LOW)
INSIGNIFICANT
DETECTOR
OUTPUT
DETECTOR
OUTPUT
COLLECTED
Theory of Operation
S-144DR
77
Calibration Curves
When the analyze flow passes through the IR cell, the response
of the cell is not linear. A programmed equation linearizes the
response, permitting a linear measure of milligrams of
sulfur/second. By measuring the signal over time, a curve with
an area representing the total sulfur present in a sample can be
displayed.
An integration of this area is performed to determine the sulfur
measured. Calibration compensates for differences between the
total sulfur measured and the actual sulfur concentration, as
discussed in Curves and Intercepts.
Intercepts
A fixed or regressed intercept can be used when calibrating the
instrument.
If a fixed intercept is chosen, the intercept must be entered. To
determine this value, perform three to five analyses using
empty boats (blank samples) then average the values. The
curves will start at the point on the Y-axis entered.
If the regressed intercept is used, enough blank samples should
be analyzed to allow a ratio of one blank for every three
standards chosen for calibration. If this ratio is maintained, the
computer calculates the intercept before graphing the chosen
standards.
78
S-144DR
Theory of Operation
Note
Theory of Operation
1.
2.
3.
S-144DR
79
Note
710
1.
2.
3.
S-144DR
Theory of Operation
Note
Theory of Operation
1.
2.
3.
S-144DR
711
2 WAY
SOLENOID
PARTICLE
FILTER
COMBUSTION
FURNACE
PS
SV1
PURGE
0
1350 C
15 PSI
PRESSURE
SWITCH
ADJUSTABLE
FLOWMETER
3.5 lpm
40 PSI
O2
ADJUSTABLE
FLOW
CONTROLLER
STOP
COMBUSTION
BOAT
PRESSURE
SWITCH
PS
15 PSI
2.5 lpm
ANHYDRONE
REAGENT
TUBE
10-20 MESH
BYPASS
So2
24 V VACUUM PARTICLE
FILTER
PUMP
ASSEMBLY
7 IN
BYPASS
OVEN - 48 C
FLOWMETER
2.5 lpm
EXHAUST
Figure 7-1
Analytical Flow Diagram
712
S-144DR
Theory of Operation
Diagnostics
D
g
ia
n
o
tic
s
The Diagnostics chapter explains how to monitor and check the
operation of the instrument hardware. This can help the operator
or service technician determine if the instrument is operating
properly.
Diagnostics........................................................................83
Diagnostics
S-144DR
81
82
S-144DR
Diagnostics
Diagnostics
The S-144DR allows the IR cells, oven temperature, furnace
temperature, and incoming pressure to be monitored by the
diagnostics portion of the software. The Diagnostics dialog box
also allows the Alarm Relay and Oxygen Inlet Pump to be
turned on and off for testing purposes.
Notes
Diagnostics
1.
2.
Click the Alarm Relay check box to turn on and off the
alarm relay. A checkmark indicates that the option is
activated.
3.
4.
S-144DR
83
84
S-144DR
Diagnostics
Electronic Adjustments
E
tro
c
le
n
iA
d
ju
tm
s
n
e
ts
The Electronic Adjustments chapter explains how to update your
system with the latest version of the software and guides you
through necessary electronic adjustment to obtain proper operation
of the S-144DR Dual Range Sulfur Analyzer.
Illustrations .......................................................................92
Security Registration...........................................................93
Software Upgrade...............................................................94
IR Cells Adjustment ............................................................95
Oven Temperature Adjustment.............................................97
Electronic Adjustments
S-144DR
91
Illustrations
Figure 9-1 ......... Adjustment Locations ................................. 99
Figure 9-2 ......... Oven Heater Control Card ........................... 910
92
S-144DR
Electronic Adjustment
Security Registration
A security registration number needs to be entered after a
software upgrade has been installed. If the system is new, a
LECO technician has already entered the registration number.
Note
Electronic Adjustments
S-144DR
93
Software Upgrade
A major portion of the S-144DR's functions are defined and
controlled by a software program that may be updated. Most
updates do not affect the physical design of the determinator,
but can improve performance and make operation easier.
Therefore, an identification system for program changes called
'Program Version' is used in the S-144DR Dual Range Sulfur
Analyzer and other LECO instruments.
A three-digit number identifies program version levels. The first
generation of a program is version '1.00'. Each time a program
is changed, the version number is increased.
Notes
94
1.
2.
3.
4.
5.
6.
7.
S-144DR
Electronic Adjustment
IR Cells Adjustment
The S-144DR allows the IR cells output range to be adjusted.
The cell output range is 7.500 to 9.500 VDC. An alarm occurs if
this range is exceeded. If the alarm occurs, the cells need to be
adjusted. The Zero adjustment should be set at 0.001 VDC.
WARNING
Note
1.
2.
3.
4.
Electronic Adjustments
S-144DR
95
Note
5.
Note
Note
96
6.
7.
Note
The J152 connector goes to the low sulfur cell; J152A goes
to the high sulfur cell.
S-144DR
Electronic Adjustment
WARNING
Note
1.
2.
3.
4.
5.
Electronic Adjustments
S-144DR
97
6.
7.
8.
9.
98
S-144DR
Electronic Adjustment
GAIN
GAIN
ZERO
ADJUST
GAIN
ZERO
ADJUST
ZERO
ADJUST
OVEN HEATER
CONTROL CARD
J152A
J152
Figure 9-1
Adjustment Locations
Electronic Adjustments
S-144DR
99
910
S-144DR
R4
TEMP
TP3
U1
U2
R2
R1
J224C
J224B
J224A
R7
C6
C3
C1R8
J224
R9
C2
U3
C7
C5
R5
R3
R6
R12
C4
U4
U5
TP2
GND
COPYRIGHT C 1997
ALL RIGHTS RESERVED
LECO CORPORATION
ST, JOSEPH, MI U.S.A.
K1
R14
TEST
TP1
CR1
TP1
R10
R11
TP2
R14
TP3
Figure 9-2
Oven Heater Control Card
Electronic Adjustment
10 Service
Service
Service
S-144DR
101
102
S-144DR
Service
Service Parts
Note
606-224
Thermocouples
606-601-110
609-399
616-036
Fan (Oven)
616-038
616-155
772-455
Pressure Switches
777-594-101
781-434
782-746
Service
S-144DR
103
!
CAUTION
WARNING
104
1.
2.
3.
Insert the USB/ISA interface card into the top slot of the
electronic chassis (figure 11-1, page 11-3). The USB/ISA
interface card should snap into place.
4.
S-144DR
Service
11
Illustrations
lu
I
s
io
tra
n
Illustrations
S-144DR
11-1
11-2
S-144DR
Illustrations
666-147-101
TC/IR PWR SUPPLY
CARD
777-759
IR OVEN
INTERFACE
CARD
777-504
CHOPPER MOTOR
CARD
666-001
8 POS. SOLENOID
INTERFACE
CARD
666-355
USB
INTERFACE
CARD
603-880
RELAY
777-710-120
A/D CARD
(16 BIT)
777-694
A/D CARD
(12 BIT)
777-695-110
DIGITAL I/O
CARD
778-492
FLOW
CONTROLLER
782-067
LOW SULFUR
IR CELL
ASSEMBLY
606-616
HIGH SULFUR
IR CELL
ASSEMBLY
666-224-110
OVEN HEATER
CARD
778-494
FLOWMETER
616-036
OVEN FAN
ASSEMBLY
765-537
FLOWMETER
666-121-110
FURNACE CONTROL
CARD
Figure 11-1
Left Side View
Illustrations
S-144DR
11-3
616-037
FURNACE
ASSEMBLY
772-455
PRESSURE
SWITCH
(616-040
INLET
GAS ASSY)
606-649
SOLENOID
VALVE
768-980
PARTICLE
FILTER
616-065
RELAY
607-157
RELAY
606-327
REAGENT TUBE
(2 REQ'D)
768-980
PARTICLE FILTER
(PART OF 606-270
LOWER ANHYDRONE
BLOCK ASSEMBLY)
782-746
20 AMP LINE
602-699
FILTER
CURRENT
TRANSFORMER
608-604
POWER SUPPLY
CARD
616-041
VACUUM PUMP
ASSEMBLY
614-523
CIRCUIT
666-014
BREAKER
POWER
DISTRIBUTION
CARD
Figure 11-2
Right Side View
11-4
S-144DR
Illustrations
Figure 11-3
616-040 Inlet Gas Assembly
Illustrations
S-144DR
11-5
Figure 11-4
606-616 High Sulfur IR Cell
11-6
S-144DR
Illustrations
772-560
MOTOR
190-295
SCREW
(4 REQ'D)
781-943
IR SOURCE
PLATE
190-174
SCREW
(2 REQ'D)
190-247
SCREW
(2 REQ'D)
772-809
BLOCK AND
WINDOWS ASSEMBLY
190-866
SCREW
768-944
O-RING
781-987
SOURCE END
CAP
783-037
MOUNT
782-065
IR DETECTOR
ASSEMBLY
782-697
GASKET
768-974
CHOPPER MOTOR
BLADE
190-766
SCREW
781-942
IR SOURCE &
REFLECTOR
190-227
SCREW
(4 REQD)
193-006
WASHER
(4 REQ'D)
190-227
SCREW
(4 REQ'D)
193-104
WASHER
783-038
STANDOFF
(4 REQ'D)
777-817
CARD
783-040
COVER
ASSEMBLY
781-637
SEAL PREAMP
CARD
781-638
SEAL
BACKING
Figure 11-5
782-067 Low Sulfur IR Cell
Illustrations
S-144DR
11-7
783-040
PREAMP
COVER
193-006
WASHER
(4 REQD)
190-227
SCREW
(4 REQD)
783-037
MOUNT
783-038
HEX SPACER
(4 REQD)
770-838
THERMAL
RESISTOR
777-817
PREAMP
CARD
193-104
WASHER
190-227
SCREW
(4 REQD)
781-637
PREAMP CARD
SEAL
781-638
BACKING SEAL
190-601
SCREW
(4 REQD)
782-056
TUBE CELL BODY
ASSEMBLY
781-990
O-RING
(3 REQD)
190-820
SCREW
(3 REQD)
772-806
PLATE
(2 REQD)
190-766
SCREW
768-944
O-RING
772-561
IR SOURCE
REFLECTOR
PLATE
781-941
SOURCE
END CAP
190-295
SCREW
(4 REQD)
781-949
GUARD
FEEDTHRU
190-247
SCREW
(2 REQD)
772-560
CHOPPER MOTOR
781-943
SOURCE
PLATE
190-174
SCREW
(2 REQD)
781-945
CYLINDER
781-942
IR SOURCE
ASSEMBLY
190-766
SCREW
190-866
SET SCREW
768-974
CHOPPER BLADE
781-991-010
SOURCE
BLOCK
777-066
TUBE BODY
772-520
0-RING
(2 REQD)
775-795
SPACER
(2 REQD)
12
772-804
GOLD PLATED
GLASS TUBE
772-557
TUBE
(2 REQD)
781-849-010
DETECTOR
BLOCK
782-697
INNER
GASKET
190-820
SCREW
(3 REQD)
193-006
STAR WASHER
(4 REQD)
606-208
BRACKET
190-227
SCREW
(4 REQD)
774-571
PUMP
772-458
FITTING
(2 REQD)
194-056
NUT
(8 REQD)
781-677
MOUNT
(4 REQD)
615-981
BRACKET
616-075
STRAP ASSEMBLY
775-133
FOAM TAPE
(3 REQD)
Figure 11-6
Vacuum Pump
11-8
S-144DR
Illustrations
12
Schematics
S
h
c
m
e
s
tic
a
Schematics
S-144DR
12-1
Illustrations
Figure 12-1 ....... 150-851 Cabinet SchematicsPage 1 of 3..... 124
Figure 12-2 ....... 150-851 Cabinet SchematicsPage 2 of 3..... 125
Figure 12-3 ....... 150-851 Cabinet SchematicsPage 3 of 3..... 126
12-2
S-144DR
Schematics
Heaters
Motors
Relay
K1............................................. Relay.............................................................603-880
Resistor
R1............................................. 5K.................................................................769-171
Switches
Circuit Breakers
Filters
Thermocouple
Solenoid Valves
Transformer
T1 ............................................. Transformer ...................................................602-699-010
Schematics
S-144DR
12-3
Figure 12-1
150-851 Cabinet SchematicsPage 1 of 3
124
S-144DR
Schematics
Figure 12-2
150-851 Cabinet SchematicsPage 2 of 3
Schematics
S-144DR
125
Figure 12-3
150-851 Cabinet SchematicsPage 3 of 3
126
S-144DR
Schematics
13 Index
Index
A
About
Examples................................................................... 41
Help Menu ............................................................... 433
Absorption.................................................................... 74
Access, On-Board Manual ............................................. 435
Accessories................................................................. 116
Accessory Pack .................................................. 117, 118
Adapter........................................................................ 64
Add
Sample ................................................................... 420
Toolbar...................................................... 122, 430
Samples Menu.......................................................... 432
Standard ................................................................. 518
User-Defined Field .................................................... 531
Adjust
Furnace Temperature ................................................ 453
IR Cells ..................................................................... 95
Oven Temperature ...................................................... 97
Adjustment, Locations.................................................... 99
Advanced Full-Text Search............................................ 446
Analysis
Calibration ............................................................... 522
First Time .................................................................. 53
Perform................................................................... 528
Time ....................................................................... 119
Analytical Flow Diagram ............................................... 712
Analyze
Samples Menu.......................................................... 432
Toolbar .......................................................... 122, 430
Installation ................................................................ 23
Available Functions, User-Defined Fields ......................... 534
Index
S-144DR
131
B
Back, Toolbar.............................................................. 439
Balance........................................................................ 33
Configure, Parameters ................................................. 46
Control Panel ............................................................. 37
Definitions ................................................................. 47
Illustration................................................................. 37
Installation ................................................................ 33
Range ..................................................................... 119
Readability .............................................................. 119
Reset ........................................................................ 34
Basic Rules
Nested Expressions ................................................... 447
Search Topics........................................................... 443
Baud Rate
Balance ............................................................ 122, 47
Data Transmit ................................................. 122, 410
Blanks ........................................................................5-16
Braided Cable
Illustration............................................................... 229
Installation .............................................................. 229
Buttons ...................................................................... 111
Move, Columns......................................................... 422
C
Cabinet Schematics ......................................................12-3
Calibrate
Cubic Curve ............................................................. 711
Furnace Temperature ................................................ 412
Furnace, Tools Menu ................................................. 433
Quadratic Curve ....................................................... 710
Tools Menu .............................................................. 433
Calibration.................................................................. 522
Analysis .................................................................. 522
Curve...................................................................... 525
Curves ...................................................................... 78
Cubic ................................................................. 711
Linear .................................................................. 79
Quadratic............................................................ 710
Linear Curve .............................................................. 79
Specification ............................................................ 119
Toolbar .......................................................... 122, 430
Card, Oven Heater Control ............................................ 910
Caution
Operator ................................................................... 19
Symbols .................................................................. 110
132
S-144DR
Index
Cell
Adjustment ................................................................ 95
High Sulfur ...............................................................11-6
Low Sulfur ................................................................11-7
View Data................................................................ 537
Change
Height, On-Board Manual ........................................... 437
Size, On-Board Manual .............................................. 437
Width, On-Board Manual ............................................ 437
Check Boxes, Dialog Box .............................................. 417
Chemical Reagent........................................................ 119
Circuit Breaker .............................................................. 45
Codes, Format ............................................................ 428
Columns..................................................................... 422
Definitions ............................................................... 424
Format .................................................................... 426
Resize ..................................................................... 423
View Menu ............................................................... 433
Combustion
Shelf
Illustration .......................................................... 232
Installation ......................................................... 211
System
Illustration ................................................. 230, 231
Installation ........................................................... 29
Command Buttons, Dialog Box ...................................... 417
Commands
Execute ................................................................... 415
Menu Shortcuts ........................................................ 451
Comparator Level .......................................................... 75
Component
Installation ..................................................... 227, 612
Pack ....................................................................... 116
Components ............................................................... 116
Computer
Dimensions .............................................................. 120
Illustration............................................................... 225
Installation .............................................................. 215
Maintenance ............................................................ 610
Specification ............................................................ 119
Configure, Balance, Parameters ....................................... 46
Conformity, Declaration................................................ 113
Index
S-144DR
133
Connect
Exhaust Tube ........................................................... 214
Gas ........................................................................ 213
Contents
Find Topic................................................................ 438
Navigation Pane ....................................................... 436
Tab, Shortcuts.......................................................... 450
Control Panel, Balance ................................................... 37
Controller Card............................................................ 454
Controls ....................................................................... 45
Illustration............................................................... 452
Copy
Edit Menu ................................................................ 432
Topic ...................................................................... 439
Create, Method ........................................................... 510
Cubic
Calibration Curve ...................................................... 711
Curve, Calibrating ..................................................... 711
Curve
Cubic ...................................................................... 711
Linear ....................................................................... 79
Quadratic ................................................................ 710
Curves
Calibration ........................................................ 525, 78
Intercepts.................................................................. 78
Customize, On-Board Manual ........................................ 437
D
Data
Bits
Balance ....................................................... 122, 47
Data Transmit ............................................ 122, 410
Output Parameters, Set ............................................... 35
Print Results ................................................... 541, 542
Transmit.................................................................. 548
Definitions .......................................................... 410
Parameters ........................................................... 48
View
IR Cell ................................................................ 537
Sample............................................................... 535
Database, Validate....................................................... 552
Date, Columns .......................................... 122, 424, 425
Declaration of Conformity ............................................. 113
Define, Search Terms................................................... 442
134
S-144DR
Index
Index
S-144DR
135
Export
Results.................................................................... 549
Samples Menu.......................................................... 432
Setup...................................................................... 223
Information, Tools Menu ....................................... 433
Expressions, Nested..................................................... 447
F
Facility Requirements ................................................... 224
Fan Filter...................................................................... 67
Favorite Topics List ...................................................... 441
Favorites
Navigation Pane ....................................................... 436
Tab, Shortcuts.......................................................... 450
Fields, User-Defined..................................................... 423
Filter, Disposable Particle................................................ 65
Front ........................................................................ 65
Internal..................................................................... 66
Filter, Fan..................................................................... 67
Find, Topic ................................................................. 438
Using Toolbar Buttons ............................................... 439
First Time Analysis......................................................... 53
Flow Diagram.............................................................. 712
Format Code
Picture .................................................................... 428
Scientific, Figures ..................................................... 428
Scientific, Notation.................................................... 428
Format
Codes ..................................................................... 428
Columns .................................................................. 426
Forward, Toolbar ......................................................... 439
Front, Disposable Particle Filter........................................ 65
Full-Text Search .......................................................... 446
Advanced ................................................................ 446
Functions, User-Defined Fields....................................... 534
Furnace
Calibrate Temperature............................................... 412
Controller Card ......................................................... 454
Set Temperature ...................................................... 411
Specification ............................................................ 119
Temperature Adjustment ........................................... 453
136
S-144DR
Index
G
Gas
Connections ............................................................. 213
Required ................................................................. 119
General Tab, IR Cell Data ............................................. 539
Ground Strap Installation.............................................. 218
H
Hazardous Material Pack............................................... 117
Heater Control Card ..................................................... 910
Heating Element
Illustration............................................................... 228
Installation ................................................................ 25
Height, On-Board Manual.............................................. 437
Help
Menu ............................................................. 431, 433
Toolbar .......................................................... 122, 430
Topics, Help Menu..................................................... 433
Use......................................................................... 418
Hide
Navigation Pane ....................................................... 436
Toolbar ................................................................... 439
High, Sulfur
Area, Columns................................................. 122, 425
Columns ......................................................... 122, 424
Peak, Columns ................................................ 122, 424
Tab, IR Cell.............................................................. 540
Time, Columns ................................................ 122, 425
Highlight Words in Topics.............................................. 444
Home, Toolbar ............................................................ 439
I
Illustrations List ............................................................ 17
Import, Setup ............................................................. 221
Information, Tools Menu ............................................ 433
Index
Find Topic................................................................ 438
Navigation Pane ....................................................... 436
Indicators..................................................................... 45
Illustration............................................................... 452
Infrared Radiation ......................................................... 74
Inlet Gas, Illustration ....................................................11-5
Index
S-144DR
137
Install
Analyzer ....................................................................23
Balance ..................................................................... 33
Braided Cable........................................................... 229
Combustion
Shelf .................................................................. 211
System................................................................. 29
Components ................................................... 227, 612
Computer ................................................................ 215
Ground Strap ........................................................... 218
Heating Element ......................................................... 25
Internationally............................................................ 24
Reagent Tube........................................................... 212
Sliding Door ............................................................. 211
Software ................................................................. 219
USB
Cable ................................................................. 217
Interface Card ..................................................... 104
Intercepts .................................................................... 78
Interference to Other Devices........................................ 112
Internal, Disposable Particle Filter .................................... 66
International Installation ................................................ 24
IR Cell
Adjustment ................................................................ 95
Sulfur
High....................................................................11-6
Low ....................................................................11-7
View Data................................................................ 537
K
Keyboard Key Combinations.......................................... 415
Keys, Shortcut ............................................................ 449
L
LECO, Toolbar ............................................................. 439
Linear
Calibration Curve ........................................................ 79
Curve, Calibrating ....................................................... 79
Low, Sulfur
Area, Columns................................................. 122, 424
Columns ......................................................... 122, 424
Peak, Columns ................................................ 123, 424
Tab, IR Cell.............................................................. 540
Time, Columns ................................................ 123, 424
138
S-144DR
Index
M
Main, Software Window ................................................ 414
Maintenance Schedule.................................................... 63
Measure Flow Flowmeter ................................................ 45
Menu
Commands .............................................................. 415
Edit ........................................................................ 432
Help............................................................... 431, 433
References............................................................... 431
Sample ................................................................... 431
Samples .................................................................. 432
Shortcut Commands.................................................. 451
Tools ............................................................. 431, 433
View ....................................................................... 433
Menus........................................................................ 432
Method
Columns ......................................................... 123, 424
Create..................................................................... 510
Delete ..................................................................... 515
Edit ........................................................................ 513
Print ....................................................................... 514
Methods ..................................................................... 510
Toolbar .......................................................... 123, 430
Tools Menu .............................................................. 433
Minimum Requirements ................................................ 216
Moisture, Percent, Columns.................................. 123, 424
Monitor
Dimensions .............................................................. 120
Specification ............................................................ 119
Mouse, Use................................................................. 415
Mouse-Activated Buttons .............................................. 415
Move Buttons, Columns ................................................ 422
N
Name, Columns.................................................. 123, 424
Navigation Pane .......................................................... 436
Tabs ....................................................................... 436
Navigational Buttons .................................................... 111
Nested Expressions...................................................... 447
Notice, Warranty ........................................................... 19
Index
S-144DR
139
O
On-Board Manual
Access .................................................................... 435
Customize ............................................................... 437
Shortcuts................................................................. 449
Use......................................................................... 434
Operator, Columns ............................................. 123, 424
Options ...................................................................... 115
Toolbar ................................................................... 439
Tools Menu .............................................................. 433
O-ring, Reagent Tube..................................................... 68
Output Parameters, Set.................................................. 35
Oven
Heater Control Card .................................................. 910
Temperature, Adjustment ............................................ 97
P
Pane
Navigation ............................................................... 436
Sample ................................................................... 419
Parameters
Configure, Balance ...................................................... 46
Data Transmit ............................................................ 48
Set Data Output ......................................................... 35
Parity
Balance ............................................................ 123, 47
Data Transmit ................................................. 123, 410
Particle Filter ................................................................ 65
Front ........................................................................ 65
Internal..................................................................... 66
Paste, Edit Menu ......................................................... 432
PC
Illustration............................................................... 225
Installation .............................................................. 215
Tower Kit................................................................. 118
Perform Analysis ......................................................... 528
Periodic Maintenance Schedule ........................................ 63
Phrases, Search .......................................................... 443
Picture Format Code .................................................... 428
Port
Balance ............................................................ 123, 47
Data Transmit ................................................. 123, 410
Precision .................................................................... 119
1310
S-144DR
Index
Index
S-144DR
1311
1312
S-144DR
Index
Search
Advanced Full-Text ................................................... 446
Define Terms ........................................................... 442
Find Topic................................................................ 438
Full-Text.................................................................. 446
Navigation Pane ....................................................... 436
Phrases ................................................................... 443
Previous Results ....................................................... 448
Tab, Shortcuts.......................................................... 450
Titles ...................................................................... 444
Topics ..................................................................... 443
Words ..................................................................... 443
Searches, On-Board Manual .......................................... 442
Security, Registration..................................................... 93
Select, Language, Tools Menu ....................................... 433
Service Parts .............................................................. 103
Set
Data Output Parameters .............................................. 35
Furnace Temperature ................................................ 411
Setup
Export..................................................................... 223
Import .................................................................... 221
Information ............................................................. 221
Shipping Weight .......................................................... 120
Shortcut
Keys .............................................................. 415, 449
Menu Commands ...................................................... 451
Shortcuts ................................................................... 449
Show, Navigation Pane................................................. 436
Size, Change, On-Board Manual..................................... 437
Sliding Door
Illustration............................................................... 232
Installation .............................................................. 211
Software
Installation .............................................................. 219
Kit .......................................................................... 116
Overview ........................................................ 219, 414
Start Up .................................................................. 220
Upgrade .................................................................... 94
Specifications.............................................................. 119
Spreadsheet ............................................................... 419
Index
S-144DR
1313
1314
S-144DR
Index
Index
S-144DR
1315
W
Warning Symbols ........................................................ 110
Warranty...................................................................... 18
Weight
Columns ......................................................... 124, 424
Specifications .......................................................... 120
What's This
Help Menu ............................................................... 433
Toolbar .......................................................... 124, 430
Width, On-Board Manual............................................... 437
Window, Main Software ................................................ 414
Wiring Diagram ........................................................... 226
Word
Highlight ................................................................. 444
Search .................................................................... 443
Similar to Search Term .............................................. 445
1316
S-144DR
Index
Index
S-144DR
1317