ABSTRACT

The purpose of the experiment is to determine that the saponification of the ethyl
acetate with the sodium hydroxide is a first order reaction referred to the ethyl acetate
using the initial velocity method.
The procedure is to measure the value of conductivity NaOH and Na-acetat,
making the solvent Na-acetat 0.03 M as much as 200 ml and 10 L NaOH 0.03 M, to
measure the value of conductivity Na-acetat and NaOH with to immerse electrode
indicator into that solvent, and washing clean to the electrode indicator every doneusing
with aquades. And then to look for the value of conductivity reaction product and to look
for order reaction NaOH with ethyl acetate, are making the solvent ethyl acetate 0.03 M
as much as 10 L, washing clean the all instrument of the reactan with the reagent tank
good for yet and after the experiment to the substitute solvent of the variable, put the 10 L
solvent ethyl acetate into the reagent tank, put the 1.6 L NaOH into the reactan with the
direct to electrode indicator immersing all, run the SACED-QRIA program and setting
the time of capture (clock icon), select the name of the file data will be saving with the
press disk icon and finally press the play icon, to load the receive solvent ethyl acetate as
much as 1 L into the reactor with to run the pomp and rotameter scale and then turn on
the stirrer system, wait until to measure the value of conductivity reaction to constant and
then turn off the operation with the press stop symbol and cast the reactor using the valve
of the product reactor outlet from the reactor and then cleaning with aquades. Repeat
more steps with concentration of the new ethyl acetate where ethyl acetate before the
solventing as 10 L back and with still NaOH concentracion.
From all this experiment to get in the value orde reaction with : experiment 1
(NaOH 0.03 M + ethyl acetate 0.03 M) and experiment 2 (NaOH 0.03 M + ethyl acetate
0.027 M) are 0.8431. And then for the experiment 2 (NaOH 0.03 M + ethyl acetate 0.027
M) and experiment 3 (NaOH 0.03 M + ethyl acetate 0.0243 M) are 1.5693 and
experiment 3 (NaOH 0.03 M + ethyl acetate 0.0243 M) and experiment 4 (NaOH 0.03 M
+ ethyl acetate 0.02187 M) are 1.5813. Experiment 4 (NaOH 0.03 M + ethyl acetate
0.02187 M) and experiment 5 (NaOH 0.03 M + ethyl acetate 0.01968 M) are 1.6613. The
value of the all order reaction of the safonification to the ethyl acetate are 1.41375.

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