Академический Документы
Профессиональный Документы
Культура Документы
Preparation Instructions
Dry a portion at 80 °C for 4 hours before use. Use
promptly. Discard unused material.
Product Description Storage/Stability
Molecular Formula: C18H24O2 Store in a sealed vial under argon protected from light
Molecular Weight: 272.38 at room temperature.
This product meets USP specifications (Current through CJH,MAM 02/10-1
USP 32) and is traceable to USP Reference Standard
lot L0C337.
Result
TEST USP 32 SPECIFICATIONS Sigma Reference Standard
Lot 069K5010
Infrared asorption
spectrum KBr dispersion compares to standard compares to standard
<197A>
Ultraviolet absorption compares to standard and absorptivities at
spectrum 50 µg/mL in 280 nm, calculated on the anhydrous basis, do meets requirements
alcohol <197U> not differ by more than 3.0%
Melting range, °C
between 173 °C and 179 °C 176–179 °C
Class 1 <741>
Specific rotation, [α]25
D
1.0
0.8
Absorbace
0.6
0.4
0.2
0.0
200 220 240 260 280 300
Wavelength (nm)