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SYSTEMS
by Professor P G Kihlstedt, Division of Mineral
Processing, The Royal Institute of Technology,
Stockholm, Sweden.
Synopsis
Particle size distributions for different ores and
grinding systems have been studied with me_as.urements
down to ca 2 When mineral aggregates are ground,
two maxima are normally observed in the mass frequency
curve for the ground product, a coarse grinding maxi-
mum which becomes higher the finer the grinding and
an abrasion maximum.
Three grinding systems have been included in the in-
vestigation, a rod mill- ball mill, a ' ball mill. and
an mill in a closed Parallel with
the full-scale sampling, grinding has been carried out
in a laboratory rod mill - ball mil-l to permit a compa-
rison between the different grinding systems. The
quantities studied have been the energy consumption,
k
80
and the specific s urface . k
80
is t he t heor etical
mesh through which 80% by weight of the material ccan
pass.
Another study has comprised two different
systems with autogenous - pebble mills and has been
designed to show how an open grinding system-with an
autogenous mill influences the mass frequency curves
for the material and for the mineral content of the
ground product.
2
Partikelgro:isenverteilung bei verschiedenen Vermahlungs-
systemen
Man hat Untersuchungen der Partikelgrossenverteilung
bei verschiedenen Erzen und Vermahlungssystemen durch-
geftihrt mit Messungen bis hinab zu ca 2 pro. Bei Zer-
kleinerung von Mineralaggregaten erhalt man gewohnlich
zwei Maxima auf der Massenfrequenzkurve des gemahlenen
Produktes. Einesteils ein groberes mahltechnisches
Maximum, das hoher ist, je feiner die Vermahlung ge-
trieben wird, und anderenteils ein Abntitzungsmaximum.
In einer Untersuchungsserie haben wir drei Vermahlungs-
systeme, St abmtihl e-Kugelmtihle, Kugelmlihle und einfache
Autogenmtihle in geschlossenen Kreisen studiert. Parallel
mit Probeentnahme in vollgrosser Skala haben wir in
dem System S.tabmtihle-Kugelmtihle Vermahlung in Labora-
torieskala durchgeftihrt und damit einen Vergleich
zwischen den verschiedenen Vermahlungssystemen er-
moglicht. Die undersuchten Grossen sind Energiever-
brauch, k
80
, sowie die spezifische Oberflache. k
80
ist
die gedachte Maschenweite, durch die 80 Gewichts-% des
Gutes passieren.
Eine andere Untersuchung umfasst zwei verschiedene
Vermahlungssysteme mit Autogenmlihle-Steinmtihle und soll
beleuchten, wie ein offenes Vermahlungssystem mit
Autogenmtihle die Massenfrequenzkurven des gemahlenen
Produktes in Bezug auf Gut resp. Mineralgehalt beein-
flusst.
Repartition de 1a t aille des particules pour les
differents types de broyages
Des observations sur la repartition de la taille des
particules ont ete effectuees pour des minerais
differents et pour d ~ s procedes de broyage differents,
avec des mesures jusqu'a 2 Lors du broyage d'un
agrgat mineral on obtient norrnalement deux maxima
sur la courbe de frequence des masses du produit
broye. D'une part un maximum du a la technique de
broyage utilisee qui devient de plus en plus haut,
plus le broyage est fin, d'autre part un maximum du
a !'abrasion.
Dans une serie d'observations on a tudi trois sys-
de broyage: concasseur a barre et a boulets,
broyeur a boulets et broyeur simple autogene. Pa-
au d'chantillons a !'chelle
industrielle, on a effectu, en laboratoire, un
broyage dans un concasseur a barre et boulets et rendu
possible une comparison des diffrents procds. Les
etudis sont: la consornrnation d'energie,
k
80
ainsi que la surface specifique. k
80
est la
largeur suppose des mailles d'un grilla9e a travers
lesquelles 80% du poids total du materiau passent.
Une autre observation est basee sur deux procdes
differents avec broyeur a pierres et
destinee a montrer comment un de broyage ouvert
avec broyeur influe sur la courbe de freque nce
des masses du produit broye pour le produit et pour
la teneur des minerales.
Introduction
In a series of earlier lectures and articles /l-5/ I have
described studies of the particle size distributions,
specific surfaces and effects on subsequent mineral
dressing processes resulting from different methods
of grinding mineral raw materials. These studies have
shown how Rittinger's and Bond's laws have been found
to agree in the measurement of particle size distribu-
tion and specific surfaces. It has also been found
3
4
that this is due to the mechanical strength properties
of the crystalline structure of minerals. The normal
three-dimensional minerals, when ground, eventually
acquire a lattice structure in the 0.1-1.0 particle
size range which is so strong that no further crushing
can be produced by the disintegrative forces available
in an ordinary mill. This particle size represents, so
to speak, a barrier against which the particle size
distribution is squeezed up by further grinding.
ACk
61og k
/'
I I
I I
:
\
\
:
'
.....
-
TOlAL SCliO
/ \
"'
1\
-
1--
/
\
90
80
70
60
50
.:.o
30
/
J/
-
--
GALEN.A
2'J
10
0
1)0
120
110
100
90
81)
70
60
50
4'J
)0
20
1'J
0
1/
..........
,\
'I
I
..... _
2 ) 4 5 6 s 10 20 30 40 6C 80100
,-,
I
: I
\
! I
TOTAL SOL 10
: I
\
:f
If
\
1
-\
/
'
.\
//
'"'\l
\
fj
.)1
\I\
\
\
\ \
\
\
,_
200 400 6001ro k um
2 ) 4 5 6 8 10 200 3001.00 600 BOO k
Fig. 1. Mass frequency curves for particle size
20 30 40 5060 8010C
distributions of total solid and galena after rod mill
grinding and after teritiary grinding with small balls.
Finely disseminated complex massive pyrite ore with
galena.
The procedure is illustrated in Fig. 1. /3/ Here we
see two stages in the grinding of a solid pyrite ore
from Canada which contains galena and other minerals.
The mass frequency diagrams show the particle distri-
bution of the total material and of the galena at diffe-
rent sizes after rod mill grinding (at the top) and
after the third grinding step and final classification
(at the bottom). Three peaks can be seen in the case
of this ore. The first and coarsest is a peak related
to the grinding process. The second, which in final
grinding coincides with the grinding peak, marks the
liberation _df galena crystals from their settings in
the ore matrix. The third peak, at about 3 pro, is an
abrasion peak that occurs with ores and some methods
of grinding. It is evident that progressively finer
grinding concentrates the particle size distribution
into an ever-narrower range.
In this lecture I propose to show the corresponding
particle size distributions for a number of ores of
different types ground by different methods.
Some particle size distributions
By way of additional background to our view of diffe-
rent particle size distributions and their implications,
I will show you in Fig. 2 /5/ the mass frequency curves
for the feed to three large European flotation plants
for complex sulphide ore. The grinding layout in these
three plants is of standard type, with a rod mill and
one or two ball mills in series plus hydrocyclone
classification. The finenesses differ, as can be seen
5
6
~ Ck
~ logk
150
~
I
7
I
I
I
\
c k
80
39 ~ m
\
\
'
v-
1\. B k
80
1.1 ~ m
/ ~
\
k.
140
130
120
110
100
90
eo
70
&)
I
~ v
\ 1\.
~
\A k
60
135 um
50
40
30
20
10
~
~
~
/ v f-....
//
v ./
v
v
J
/
i""'oo.,
r--... It
7_.
........
r--
t>C
r-
l,.;'
~
~
v
\
\
~
~ ~ \
\
\
\
i\
\
\
\
' 1\
1\ 1\
\
0
1
s 10 50 100 200 ~ m ( k )
Fig. 2. Mass frequency curves. Feed to flotation at
three European flotation mills. Estimated quantity of
particles per m
3
.
A:5 X 10
15
, B:20 X 10
15
, C:50 X 10
15
from the values of k
80
quoted for each end product.
k
80
is defined as the imaginary screen aperture through
which 80% by weight of the material will pass.
As we see, each curve has two peaks: a grinding peak
that grows higher the farther the grinding is carried,
and an abrasion peak. The particle size distribution
is determined down to about 2 ~ and tends to stop at
about 1 pro. Determination of the exact distribution
in this range calls for special methods and apparatus
which were not available in the present case.
An interesting point is that these particle size de-
terminations can be used to compute ' the number of
particles produced by each method of grinding. The
result works out at something of the order of five
to fifty times ten-to-the-fifteenth particles per
cubic metre of solid material.
The central mineral processing research organisation
in Sweden has been engaged since 1969 on a programme
of sampling and measurement in full-scale operational
plants to investigate how different grinding systems
CONE CRUSHER
fU)
t.41LL
SYSTEM I
ILL
SYSTEM ][
RAKE CLASSIFIER
SYSTEM m
FIG 3
GRQJNO
PROD.
GROUND
PROO.JCT
Fig. 3. Three simplified principle grinding systems
compared by individual laboratory tests.
7
8
work with reference to the properties of the ground
product as well as operating costs and energy consump-
tion. Let us look at some results from three principle
systems.
System I is a standard layout comprising fine crushing,
rod mill and ball mill in a closed circuit with a
hydrocyclone. The ore is a gangue-dominated complex
sulphide ore.
System II is an older layout, with closed fine crushing
circuit followed by ball mill in a closed circuit with
a scraper classifier. The ore is sulphide-bearing,
gangue-dominated skarn iron ore.
System III is an autogenous grinding system with run-
of-the-mine material fed straight to the mill, which
works in a closed circuit with a hydrocyclone. The
ore is a gangue-dominated magnetite ore of skarn type.
To obtain a comparison between the systems, ore samples
were taken as well as samples of products from the
circuits. The former were subjected to standardised
grinding on a laboratory scale in Bond rod and ball
mills. The net energy input was determined, and the
products were analysed for particle size distribution
and specific surface.
System I showed much the same results on both full
and laboratory scale as regards energy input, particle
size distribution (Fig. 4) and specific surface. The
energy input to k
80
= 108 ~ m was about 8.8 kilowatt-
hours per ton in the laboratory and 9.9 kWh/ton in
full-scale operation.
Fig. 4. Mass frequency curves of ground products.
Grinding system I.
Specific surface at k
80
=108 ~ wa s 10 000 square
centimetres per cubic centimetre in the lab and
9 500 cm
2
/cm
3
i n the f ul l -scale plant.
Figure 4 shows how the pyrite content of the ore
distorts the particle size distribution to some extent
in full-scale operation due to the effect of the closed
circuit through the hydrocyclone; in the laboratory
the material was ground in an open circuit.
System II showed less favourable figures for energy
input and specific surface in full-scale operation.
Energy input to k
80
= 75 ~ m was 8.8 kWh/ton in the lab
9
10
and 17.0 kWh/ton in the full-scale plant.
Specific surface at k
80
=75 ~ w a s 7 000 cm
2
;cm
3
in the
lab and 8 700 cm
2
/cm
3
in actual operation.
A Ck
A log k
tSO
100
so
0
1
~
v
,
II
5 10
""'"'
L A ~
v
TOTAL
v
'Jr-..
lli
~
~
PLANT
TOTAL
\
50 100 500 1000 &Jm
Fig. 5. Mass frequency curves of ground products.
Grinding system II.
Figure 5 shows the particle size distributions for
both laboratory-scale and full-scale grinding. The
full-scale curve is somewhat flatter.
System III showed a higher energy input and specific
surface for grinding to the same value of k
80
as well
as a much flatter particle size distribution curve.
Energy input to k
80
=120 ~ w a s 10.1 kWh/ton in the lab
and 17.5 kWh/ton in the full-scale plant.
Specific surface at