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Cold Process Soap Making for Beginners!

SEPTEMBER 14, 2012By Tiffany | offbeat & inspiredin BATH & BODY,CRAFTS, DIY, GIFT IDEAS, HEALTH &
FITNESS, TUTORIALSTags: BATH,BEGINNER, BODY,COLD PROCESS,HANDMADE,HOMEMADE, HOW TO, INSTRUCTIONS,NATURAL, ORGANIC,POSTADAY, RECIPE,SOAP, TUTORIAL,VEGAN44 COMMENTS

About 2 years ago I went on a skincare health kick. I dont remember exactly what set it off, but it was probably after watching some doomsday documentary about the monsters living in our moisturizers. Im pretty gullible when it comes to stuff like that, but I figure its better to be safe than sorry! I started off by cross-checking almost every bath & body product I was using on EWGs Skin Deep Cosmetics Database. This is a great resource if you have a favorite product and want to know its potential hazard rating. I only felt comfortable using products with a rating lower than 4. As helpful as this was, I started feeling less trusting of the companies behind the labels. The cosmetics industry does have certain standards to live up to, but you can never know for sure if a label is completely honest! I know this mindset can send me off the deep end where I move into a tree house and eat leaves for the rest of my life, so in the interest of REALISM, I decided to take on a new hobby: SOAP MAKING!

The idea of knowing exactly what was going into my most frequently used bath product was definitely appealing, to say the least. I set out on a mission to create a moisturizing, cleansing, fragrant, all natural soap with quality ingredients. It also doesnt hurt that quality handmade soaps make WONDERFUL gifts! There are a few different methods of soap making, but the one I ended up loving was Cold Process (CP). This method has a short prep time and a long cure time. The cure time (4-6 weeks) is frustrating if youre in a hurry to use your soap, but a long cure is necessary to produce the best quality. Making a batch of Cold Process Soap takes 1-2 hours initially and then an additional 4-6 weeks before you should use or gift it. This is how long it takes for the water to completely evaporate, resulting in a harder, longer lasting bar of soap. One misconception about CP cure time is that the soap is unsafe to use within the 4-6 week time frame because it hasnt saponified yet. Saponification is the chemical reaction between fats, lye & water that produces the substance we call soap! It actually only takes about 2 days for saponification to complete. So technically, you can use your soap after 2 days, but it will be very soft and will most likely fall apart in the shower. Aging your soap is definitely encouraged! The long wait was annoying at first, but it allowed me to walk away from the project for a while, thus avoiding burnout (which I am 100% prone to) AND giving me something to look forward to! Researching a topic like this can be extremely tedious, so Im hoping to save budding CP soapers a little bit of trouble by consolidating everything I learned into this post. By the end, you will be equipped to try your first batch of CP soap! A word of warning: CP soaping requires the use of lye (Sodium Hydroxide), which is a caustic substance that can cause severe burns if its inhaled or makes contact with skin. Its EXTREMELY important to do all of your soap making in a well-ventilated room while using rubber gloves, goggles and a surgical mask. Its also wise to wear long sleeves so that if any splashing occurs, your arms are protected. In this giant tutorial Ill be covering the following topics:

Supplies Formulating Your Own Recipe Beginners Test Recipe Cold Process Instructions

Lets get started!

Supplies
Note: any supplies that make contact with lye should be devoted to soap making! Dont use them for cooking once youve used them for soaping! Rubber Gloves Plastic Goggles Surgical Mask Stick Blender (aka Immersion Blender you can get one of these for $20-$30) Candy or Oil Thermometer Tupperware Measuring Pitcher (with a lip for pouring, and a lid) Heat-Proof Stirring Spoons Measuring Cups & Measuring Spoons 1 Large Microwaveable Bowl 1 Small Bowl Electric Scale that measures ounces and grams Soap Mold(s) you can order some cute ones from The Sage, one of my favorite suppliers!

Mold Tips: If you want a more rustic looking hand-cut bar of soap, purchase one of the loaf molds rather than the individual cavity molds. If you go the loaf route, youll need a sharp knife or soap cutting tool. I made my own loaf mold, if anyone wants a tutorial on this please let me know in the comments! If you dont want to purchase a mold right away, just devote a 912 or 99 inch baking pan to soaping, and be sure to line it with parchment before pouring! Parchment Paper (if youre using a loaf mold) Lye (Sodium Hydroxide) you can order Sodium Hydroxide from a few places, but the prices do vary a bit 12 oz. Canola Oil (test recipe ingredient) 8 oz. Coconut Oil (test recipe ingredient) You can get this in small quantities at the grocery store, but for larger

depending on the location and the quality. Here is one of the best deals I could find: The Lye Guy

quantities I order here, from the Fixed Oils section of TheSage.com. You can find pretty much all of your Base Oils here. 8 oz. Olive Oil (test recipe ingredient) 1.6 oz. Orange Essential Oil (optional test recipe ingredient use this if you want to scent & color your soap!) I

order mine here, from the Essential Oils section!

Formulating Your Own Recipe


Choosing Your Base Oils
CP soap is made by combining fats (base oils, aka fixed oils or carrier oils) and Lye Solution (Lye + a liquid of choice, well use water for our test recipe). The Base Oils you choose will determine the qualities of your soap. For example, using Coconut Oil will produce a very bubbly, cleansing lather and a very hard bar of soap, but too much Coconut Oil

will make your soap too drying. Youll want to balance out the coconut with a more moisturizing base like Olive Oil. There are dozens of Base Oils to choose from, but understanding the chemical reaction that produces a quality soap can get complicated, so until we all earn our Ph.D.s in chemistry, pre-made charts are our best friends! This chart is extremely helpful. It explains the fatty acid properties of Base Oils and what they each contribute to a bar of soap. They also recommend percentages of use in soap recipes. For example, next to Coconut Oil, they tell you not to use more than 30-35%, because using more than that will dry you out. You can compose an entire recipe using this chart! For our test recipe, I chose to use 42% Canola Oil, 29% Coconut Oil and 29% Olive Oil. This will produce a creamy, stable lather. I converted the percentages to ounces based on the capacity of the mold Im using.

Calculating Your Lye Solution


Now that weve chosen our Base Oils, its time to calculate our Lye Solution. Again, Im not a chemist, so I rely on a super handy Lye Calculator to do the hard work for me! There are a few out there, but I always use this one from TheSage.com. You can save your recipes here, or just use this page to create your formula. I prefer to write everything down on paper but either way, make sure you record all your amounts. First youre going to select the unit of weight measurement (in our case, ounces), then choose the type of lye youre using. For CP soap, you will always be using Sodium Hydroxide (NaOH). Next, enter your liquid of choice. Well be using water for our test recipe, but its possible to use other liquids such as goats milk, coffee, tea, etc. Further down the page you will see a list of Base Oils. Find your oils and enter the number of ounces youll be using next to each, then click Calculate Lye. The next page will tell you how many ounces of water you need in your Lye Solution. They give a small range for the water amount, so I usually pick a number that falls in the middle of the range. On the right-hand side it will show the total weight of your oils and a chart with 2 columns: % excess fatand Lye Amount. Here is where you can choose how much you want to superfat your soap. Without superfatting, your Base Oils will be cancelled out by your Lye Solution during saponification. This means many of the moisturizing benefits of the oils you used wont survive the chemical reaction. Superfatting is when your Base Oil to Lye Solution ratio is imbalanced just enough that a percentage of your oils will remain intact during saponification. This allows your soap to maintain the properties of those oils. If you go lower on the % excess fat column, you will have a dryer, harsher soap. If you go too high, your bar will be very moisturizing but it will also spoil faster because of the excess oil. I always stay between 5% and 7%. The number to the right of the % excess fat you choose shows exactly how many ounces of lye you need in your Lye Solution. Write down the water and lye amounts and thats the formula for your Lye Solution based on the oils you entered.

Adding Scents, Colors & Exfoliants


These are the last ingredients to go into your soap. As youre creating your own original recipes, always remember to write down the exact amounts of everything youre using. When you create that magical batch of soap with the perfect color and scent, you really want to be able to replicate it! I cant tell you how many times I rushed through a batch and miraculously nailed it, only to realize I never wrote down how much Cocoa Powder I used to get that delicious color! FRUSTRATING! Anyway, the theme here is natural, so for scenting my soaps I only use Essential Oils (EO). You can look into using Fragrance Oils but Ive never worked with them in my recipes, so I cant give a formula for those. The formula for Essential Oils goes roughly like this: 0.7 ounces per pound of Base Oils for most Essential Oils 0.9 ounces per pound of Base Oils for Citrus Oils 0.4 ounces per pound of Base Oils for more pervasive oils like mints and spices

The per pound of Base Oils is referring to the total weight of your oils. For our test recipe, the total weight is 28 ounces, or 1 lb. 12 oz. (16 oz. in a pound). If you make a batch and find the scent too weak or too strong using this formula, you can make slight adjustments for future batches. For colors, keep it natural! Some great natural Colorants are dried ground herbs, clays, Essential Oils (like orange), cocoa powder and spices (be sure theyre not skin irritants!). When it comes to coloring your soap batch, youll have to do a bit of trial and error. There is no formula for this, so just have your Colorant on hand and be sure to write down the exact amount you end up using. Add Colorants with measuring cups or measuring spoons. This makes it easier to keep track of your amounts. Colors can change a bit during the curing process, so you cant be sure how vibrant or dull your coloring will be until the 4-6 week cure time is over. This doesnt really bother me though because the natural ingredients result in natural-looking tones and they dont need to be very specific. For Exfoliants you can add as much or as little as you want. Whenever I add Exfoliants like seeds or oatmeal, I go by how it looks and what I want the bar to be used for. For example, a foot massage bar would have a coarse Exfoliant in a high concentration. A more gentle body massage bar would have a finely ground Exfoliant at a lower concentration.

Beginners Test Recipe


Orange Olive Soap
Heres a basic recipe with Base Oils you can get at the grocery store! To practice with the Lye Calculator, plug in the 3 Base Oil amounts and see how I got the water & lye amounts and total oil weight from the calculation page. Also see how I calculated the amount of Orange EO based on the total weight of the Base Oils: Base Oils: Canola Oil 12 oz. Coconut Oil 8 oz. Olive Oil 8 oz. Total Base Oil Weight: 28 oz. or 1 lb. 12 oz. which means, since were using a Citrus Oil (referring back to the Essential Oils formulas, a Citrus Oil should be added at .9 oz. per pound of Base Oils) this recipe will call for about 1.6 oz. of Orange EO. Lye Solution: Water 8.5 oz. Lye 3.99 oz. Essential Oils (EO): (to add at trace the stage of mixing where your soap reaches a thin pudding-like consistency) Orange 1.6 oz

Cold Process Instructions


There are 3 steps of preparation to complete before the curing process begins: Step 1 Making your Lye Solution & Melting Down your Base Oils Get your measuring pitcher (with the lid nearby), put on rubber gloves, goggles & mask, and make sure youre wearing long sleeves. Put the pitcher on a scale, and set the scale to 0 ounces. Add water until you reach the correct weight according to your recipe. Once the water is measured, reset the scale back to 0 ounces and slowly sprinkle the lye into the water until you reach the correct weight. The mixture will heat up rapidly to about 200 degrees F. Stir with a heat-proof spoon for a good 30 seconds so that the lye is fully dissolved and doesnt cake up on the bottom of

your pitcher. DONT inhale directly over the pitcher, as the fumes can burn your throat & sinuses. Once youve stirred enough, put the lid on your pitcher and place it somewhere it can cool down safely. If you have kids or pets in the house, put the pitcher somewhere it wont get knocked over. Check the solution with your thermometer about 30 minutes later by placing the probe in the center of the liquid. The temperature youre looking for is between 100 and 125 degrees F. It can take anywhere from 30 minutes to 2 hours to reach this temp, depending on how much Lye Solution youre working with.

While the Lye Solution is cooling, get a big microwaveable bowl and measure your Base Oils on the scale the same way you measured your Lye Solution. When youre done measuring, melt down the oils in the microwave. Because a lot of the Base Oils youll use in CP soap will be solid at room temperature, the melting process can take up to 15 minutes. I usually just do 2 minutes at a time on high heat in the microwave, and stir to finish melting. You want to avoid over-heating the oils. Your Base Oil temperature should be between 100 and 125 degrees F when you mix it with the Lye Solution. Make sure the oils bowl has enough room for you to add in your Lye Solution and any other Essential Oils or Exfoliants. While youre waiting for your Base Oils and Lye Solution to finish cooling, line your mold with parchment paper or plastic wrap. Some molds dont require lining before pouring, so check with the manufacturer of the mold you purchased.

Once your mold is lined, measure your Essential Oil(s) on the scale in a small bowl and set aside. This is also the time youd want to prep any other additives youre going to be using like oats, seeds, etc. Step 2 Combine the Base Oils, Lye Solution & Essential Oils/Colorants/Exfoliants and Pour

Once the Lye Solution and your Base Oil temperatures drop below 125 degrees F, slowly pour your Lye Solution into the bowl of melted oils. Mix with the stick blender on a low setting, keeping the blender near the bottom of the bowl. You dont want to splash the soap mixture out of the bowl, since saponification has not taken place yet and the solution is still caustic. The mixture will become cloudy and then start to thicken. After about 3-5 minutes of mixing, what youre looking for is trace (pictured above on the right). This is when the solution reaches a runny pudding-like consistency. If you lift the blender out of the soap and it leaves marks on the surface, youve reached trace. Now youre ready to add your Essential Oils. Mix in the EO with the stick blender until it is fully incorporated, then add your Colorant and distribute evenly with the blender. In the Beginners Test Recipe, our Orange Oil will provide both scent and color, so you can skip adding a Colorant in this case. Lastly, add your Exfoliant (optional). If youre using something like oats and you want the chunks to stay whole, you will want to stir them in by hand using a heat-proof spoon. If youre using something tiny like seeds or ground oats, you can use the stick blender. Try to work quickly during these last steps because once trace has been reached, your mixture will be hardening more rapidly. Now youre ready to pour.

Remember to keep track of the Colorant & Exfoliant amounts you end up using so that you can replicate the recipe later. Once the soap has been poured, you want to tap the bottom of your mold against the countertop to let any bubbles escape. Next, you can smooth the surface with the back of your spoon, cover the mold with plastic wrap and let it sit for 24 hours in a cool, dry place. To clean your supplies, first rinse and wipe down the pitcher and spoon you used for the Lye Solution and set them someplace to dry. Then you can rinse and wipe down the rest of your bowls before the soap residue starts to harden. Once your bowls have been thoroughly rinsed you can run them through the dishwasher, but this isnt really necessary since the soap residue you rinsed off cleaned the bowls.

Step 3 De-Mold Your Soaps and Let Them Cure! The next day you can de-mold the soaps and space them out on a cookie sheet to cure for at least 4 weeks. If you used a loaf mold, you need to cut the soaps before putting them on the cookie sheet. The more surface area of each bar is exposed, the better the cure will be. I usually put a label on the sheet with the recipe I used & the date I stored them so I dont forget. Remember, a long cure means a top quality bar of soap!

Well thats it! If you made it this far, CONGRATS and welcome to CP soaping! I look forward to hearing about your own soap-making endeavors! If you have any questions or anything to share, please leave a comment! Share this: