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acid and a strong base Volume of 1M NaOH added for the reaction, (V) / 0.05 cm3 0.00 5.00 10.00 15.00 20.00 21.00 22.00 23.00 24.00 25.00 26.00 27.00 28.00 29.00 30.00 35.00 40.00 45.00 50.00 pH of the solution 0.62 0.62 0.67 0.79 0.99 1.10 1.21 1.36 1.63 2.42 11.08 11.42 11.59 11.71 11.80 12.00 12.14 12.20 12.24 Reaction 1M Hydrochloric acid and 1M sodium hydroxide Observation A colourless solution was formed when colourless sodium hydroxide solution was titrated to colourless hydrochloric acid.
pH
NaCl + H2O
Lim You Sie. Text for PRE-U STPM Chemistry. Selangor: Pearson Malaysia Sdn. Bhd, 2003. (p. 179)
EXPERIMENT 2 Reaction of a strong acid and a weak base Volume of 1M NH3 added for the reaction, (V) / 0.05 cm3 0.00 5.00 10.00 15.00 20.00 21.00 22.00 23.00 24.00 25.00 26.00 27.00 28.00 29.00 30.00 35.00 40.00 45.00 50.00 pH of the solution 0.02 0.02 0.11 0.22 0.35 0.36 0.36 0.39 0.41 0.45 0.49 0.52 0.57 0.60 0.63 0.80 1.02 1.44 7.83 Reaction 1M Hydrochloric acid and 1M ammonia Observation A colourless solution was formed when colourless ammonia solution was titrated to colourless hydrochloric acid.
Thus, by considering methyl orange (pKln 3.7) and phenolphthalein (pKln 9.0)2, only methyl orange is suitable for indicators.
Ibid.
EXPERIMENT 3 Reaction of a weak acid and a strong base Volume of 1M NaOH added for the reaction, (V) / 0.05 cm3 0.00 5.00 10.00 15.00 20.00 21.00 22.00 23.00 24.00 25.00 26.00 27.00 28.00 29.00 30.00 35.00 40.00 45.00 50.00 pH of the solution 2.68 4.03 4.42 4.73 5.08 5.17 5.28 5.41 5.58 5.84 6.45 11.26 11.59 11.75 11.85 12.09 12.20 12.27 12.31 Reaction 1M Ethanoic acid and 1M sodium hydroxide Observation A colourless solution was formed when colourless sodium hydroxide solution was titrated to colourless ethanoic acid.
pH
Thus, by considering methyl orange (pKln 3.7) and phenolphthalein (pKln 9.0)3, only phenolphthalein is suitable for indicators.
Ibid.
EXPERIMENT 4 Reaction of a weak acid and a weak base Volume of 1M NH3 added for the reaction, (V) / 0.05 cm3 0.00 5.00 10.00 15.00 20.00 21.00 22.00 23.00 24.00 25.00 26.00 27.00 28.00 29.00 30.00 35.00 40.00 45.00 50.00 pH of the solution 2.56 3.72 4.09 4.34 4.54 4.58 4.63 4.67 4.70 4.74 4.78 4.80 4.86 4.88 4.90 5.11 5.40 5.91 7.85 Reaction 1M Ethanoic acid and 1M ammonia Observation A colourless solution was formed when colourless sodium hydroxide solution was titrated to colourless hydrochloric acid.
CH3COONa + H2O