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Code: 9A10601 B.Tech III Year II Semester (R09) Regular & Supplementary Examinations, April/May 2013 ANALYTICAL INSTRUMENTATION (Electronics & Instrumentation Engineering) Time: 3 hours Max. Marks: 70 Answer any FIVE questions All questions carry equal marks ***** 1 (a) (b) (a) (b) What is pH value? Describe the working of a pH meter. Explain about silica analyzer. Explain fundamental law of photometry. Derive Lambert-Beers law. Explain industrial analyzer circuits. Explain the basic principle and application of chromatography and describe the sample injection system and detection systems of gas chromatography. Write short notes on: Magnetic force type oxygen analyzer. Magnetic wind type oxygen analyzer. Write about different infrared radiation sources and detectors. (a) (b) (a) (b) What are the basic differences between atomic emission and atomic absorption spectroscopy? Explain the principle and constructional details of flame photometer. Discuss the constructional details of NMR spectrophotometer. Distinguish between the resonances of absorption and dispersion type of NMR spectroscopy. Write short notes on: Ionization chamber. Solid state detectors. *****

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Code: 9A10601

B.Tech III Year II Semester (R09) Regular & Supplementary Examinations, April/May 2013 ANALYTICAL INSTRUMENTATION (Electronics & Instrumentation Engineering) Time: 3 hours Max. Marks: 70 Answer any FIVE questions All questions carry equal marks ***** 1 (a) (b) (a) (b) Explain any one electrical method for pH measurements. Explain about sodium analyzer. Describe the working of a gas analyzer. Explain about CO monitor analyzer. With the help of a neat schematic diagram, explain the principle of operation of a liquid chromatography. Discuss in detail about oxygen analyzer. (a) (b) (a) (b) List any five sources of errors in a spectrophotometer and explain how they are over come. Explain UV and visible absorption spectroscopy. Explain the principle and operation of atomic emission spectrophotometer. Why is source modulation often employed in atomic absorption spectroscopy? Describe one particular technique of such spectroscopic analysis and explain its operation. Explain about mass spectrophotometers. Explain the theory of non-magnetic resonance and electron spin resonance. Explain any two types of nuclear radiation detectors. *****

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Code: 9A10601

B.Tech III Year II Semester (R09) Regular & Supplementary Examinations, April/May 2013 ANALYTICAL INSTRUMENTATION (Electronics & Instrumentation Engineering) Time: 3 hours Max. Marks: 70 Answer any FIVE questions All questions carry equal marks ***** 1 (a) (b) Explain about electrical conductivity meters. Explain hydrogen electrode pH measurement and mention its advantages and disadvantages. Write short notes on: NOx analyzer. H2S analyzer system. With the help of a neat schematic diagram, explain the principle of operation of a gas chromatography. Explain paramagnetic type oxygen analyzer and its sampling systems. (a) (b) Explain in detail single beam spectrophotometers. Briefly discuss about the relative merits and demerits of single beam and double beam instruments. Explain Fourier transform IR spectrometer with neat diagram. Explain about flame emission spectrophotometer. Give the constructional details and working of ESR spectrophotometer. Write short notes on: Proportional counter. GM counters. *****

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Code: 9A10601

B.Tech III Year II Semester (R09) Regular & Supplementary Examinations, April/May 2013 ANALYTICAL INSTRUMENTATION (Electronics & Instrumentation Engineering) Time: 3 hours Max. Marks: 70 Answer any FIVE questions All questions carry equal marks ***** 1 (a) (b) 2 3 4 5 (a) (b) (a) (b) Write short notes on: Hydrogen analyzer. Sampling systems. Explain in detail about H2S analyzer system and sampling technique. Describe the sample injection systems and detection systems of chromatography. Explain with neat diagram of oxygen analyzer detectors and sampling systems. Explain about VIS spectrophotometers. Explain in detail a double beam IR spectrometer. What are its advantages over single beam? What is spectroscopy? Explain and distinguish absorption and emission spectroscopy. Discuss about online calorific value measurement. Discuss the functioning of an ESR spectrometer; indicate some of its application areas. How does it differ from NMR? (a) (b) Describe with neat schematic, the construction and working of proportional counter. Describe the constructional details of GM counter and explain the basic principle of this counter. How will you measure the radiation using this counter? *****