NAME : NOR ASHIKIN BINTI ISMAIL CLASS : E12F TITLE : DETERMINATION OF THE RELATIVE MOLECULAR MASS OF AMIDOSULPHURIC ACID

DATA COLLECTION : QUALITATIVE : 1. Colour of methyl orange changes from reddish pink to orange. 2. The colour of amidosulphuric acid is white and in formed of powder. 3. The sodium hydroxide used to neutralize the amidosulphuric acid solution. 4. The end point of the titration has been reached when the colour of methyl orange changes to orange. QUANTITATIVE : 1. Mass of amidosulphuric acid = 2.4964 g 0.0001 g . 2. Volume of amidosulphuric acid in volumetric flask = 250.00 cm 0.15 cm . 3. Volume of amidosulphuric acid in pipette = 25.00 cm 0.03 cm . 4. The molarity of sodium hydroxide used = 0.100 M . 5. Volume of sodium hydroxide in burette = 50.00 cm 0.05 cm . RESULT : Burette reading,(cm) Initial reading 0.05 cm Final reading 0.05 cm Volume of sodium hydroxide used 0.10 cm Trial 1 0.00 25.90 25.90 Trial 2 0.00 26.30 26.30 Trial 3 0.00 26.10 26.10

The chemical equation is : HNSOH + NaOH NaSONH + HO { Based on (www.ibsurvival.com) } Calculation : (1) Average reading for volume of sodium hydroxide used : = = =26.10 cm (2) Number of mole of sodium hydroxide used : = = =0.0026 mol

(3) Number of mole of sodium hydroxide in 250 cm of sodium hydroxide : = =0.026 mol From the equation : 1 mol of amidosulphuric acid : 1 mol of sodium hydroxide 0.026 mol of amidosulphuric : 0.026 mol of sodium acid hydroxide (4) The molar mass of amidosulphuric acid : = = =96.02 g/mol (5) Percentage error,% = = =1.112% Conclusion : The relative molecular mass for amidosulphuric acid in my experiment is 96.02 g/mol.Hence,the percentage error in my experiment is 1.112%.Therefore,the theoretical value for amidosulphuric acid is actually 97.1 g/mol (www.scribd.com./doc/30134263/sulfamic-acid-and-sulda-mates) Limitations and weakness : 1. When the amidosulphuric acid is transfer from its container to the beaker,some of the particles are not transferred because stick and still remains in container.So the molarity of amidosulphuric acid solution is not accurate.To overcome this error,the container should be wash using distilled water and transfer it to the beaker. 2. When the amidosulphuric acid solution is transfer from pipette to the conical flask,some of the solution was fallen down.So the volume of amidosulphuric acid solution is not accurate.To overcome this error,I must carefull and make sure the volume is constant for three of experiment.So the volume of sodium hydroxide used to neutralize the amidosulphuric acid will constant for each trial. 3. There is an error when determining the colour change of methyl orange.Theoretically,the colour of methyl orange will change to orange so I couldnt make sure what is actually orange and overshoot.To overcome this error,a controlled beaker containing methyl orange which colour is orange should be put beside the conical flask. 4. The mixture in the conical flask was not well shake so the reading are not constant.To overcome this error,the mixture in the conical flask must well shake so all reading will become constant. x 100 X 100%