Академический Документы
Профессиональный Документы
Культура Документы
Date: 08/20/10
ALMIRANEZ, Kristan
CA!R", A#$rin
K%AN, E&ene&er
E'peri(ent C)
*#ui$i+ation
I, A-stra.t
An experiment to characterize the fluidization behavior of sand in water was
done. The process started by preparing 500 mesh sand particles and determining
its porosity. In the experiment, water was allowed to flow in an upward direction.
low rate was increased by !00cm
"
#min and pressure head loss and velocities were
recorded for every interval. $%uilibrium head loss was computed using the data
gathered. $%uation proposed by &ichard and 'a(i was used to get the empiric
exponent x. The terminal velocity needed for the calculation of x is computed using
the )to(e*s +aw. ,sing the empiric exponent x, the length of the expanded bed was
computed.
II, "-/e.ti&e
The main ob-ective of this experiment is to characterize the fluidization behavior
of sand in water.
III, Re0eren.es
.!/ 0c1abe 2., et. Al., Unit Operations of Chemical Engineering, 3
th
ed., 4ew
5or(6 0c7raw89ill, Inc., :005
.:/ ;erry, &obert 9 and 7reen, <., Perrys Chemical Engineers Handbook, 3
th
ed.,
0c7raw89ill, Inc.
."/ www.wi(ipedia.com
I1, E2uip(ent
;re8sieve sand =d
s
> 0.5 mm and approximately 0.5? (g@
$lectronic balance
508m+ bea(er =:pcs@
Thermometer =0.! deg 1 calibration@
;ermeability and luidization apparatus
1, !3eor4
luidization, as a unit operation, is the measure of the ability of a granular media
to flow =fluidize@. It is the condition where there is suspension of particles in a fluid
media. In li%uid fluidization of granular media, the li%uid initially passes up through
the porous bed of grains, such that the upward force exerted by the li%uid is less
than the downward weight of the grains. The bed is said to be fluidized when the
grains are supported by the li%uid drag that ta(es place when the upward force
e%uals the weight of the granular media in the li%uid. ;art of the <arcy*s +aw and
Aonezy81arman $%*n applies =head loss B flow rate@ for this condition.
,pward force C pressure difference x area
C
gh
e
A
<ownward force C weight of particles in li%uid
C A+
e
=!8
e
@=
s8
@g
$%uilibrium
gh
e
A C A+
e
=!8
e
@=
s8
@g
h
e
C +=!8
@
( )
S
888888888 e%n. !
where6 h
e
C e%uilibrium head loss
+
e
C expanded length of the fluidized bed
e
C porosity of the fluidized bed
e
C density of the grains
A C plan area of the fluidized bed
&elationship between hindered setting velocity =D
h
@and concentration of
grains =c volume#volume@ is given by the e%uation proposed by &ichard and 'a(i,
and others6
D
h
C D
t
=!8c@
n
where6 D
t
C terminal settling velocity of a
single grain
At e%uilibrium in the fluidized bed6 D
h
C D
a
, and =!8c@C
e
, thus,
e
C
n
t
a
V
V
/ 1
,
_
)ince =!8
@ C +
e
=!8
e
@, and !#n C x
( )
x
t
a
e
V
V
L
L
,
_
1
1
88888888888 e%n. :
1I, "peratin5 pro.e$ure
The operation and procedure conducted for the experiment is divided into three
parts6 preliminary operation, experimental procedure and shutdown.
or the preliminary operation, start8up and preparation of the media in the
column were performed. In the start8up, the manometers and valves were chec(ed
for functionality. A steady state condition of the apparatus was obtained by allowing
a constant flow of the water from the water source to the head tan( overflow and
column. The air and water in the column were allowed to escape by opening valve
="@. The upward flow rate in the column was observed and air at the top of the
column was released through the air8release screw =E@ in the capping piece. The
flow was reversed to be able to chec( the downward flow in the column by closing
valve =:@ and opening valve =!@ and drain valve =?@. Air in the column and tubes was
released by further flushing in and up or down flow direction and releasing air in the
column by opening air8release screw =E@.
The manometer was then chec(ed for accurate measurements. Inlet valve =!@
was closed and manometer valves =5, F, 3, and G@ were opened. Air bubbles trapped
in the tubes of the manometers were chec(ed and removed by applying pressure
by opening and closing valve =!@ allowing air to escape through the air8release plug
at the top of the water manometer. 0anometer were read zero at about mid scale
while valves =!, :@ were open and valves =", ?@ closed.
or the preparation of the media and filling column, the media was pre8sieved to
a uniform size fraction. The media was weighed in dry state to determine mass and
to provide a permeable bed about "00mm deep in the column or about 0.5?(g of
sand. Dalves =!,:,",?,5,F,3,G @ were closed and air8release screw =E@ and open valve
=?@ were opened. The ;erspex column was removed from the apparatus by opening
the top8capping piece and the two screws at the side. The media was poured in the
column and wetted thoroughly with water. The water was then drained and the
column was inserted bac( to the apparatus.
or the experimental procedure, the valves were set for up flow through the
column with manometer valves closed and valve =5,F,3,G@ open. The ;erspex
column is tapped gently with a pencil to lightly consolidate the media. The drain
tube from valve ="@ is inserted into a bea(er and a thermometer is placed in it to
determine the temperature of the water leaving. The level of the media surface =+@
is read and the water and mercury manometers are set to a HzeroI reading. Dalves
=:@ and ="@ re opened to admit water through the column in a down flow direction.
About seven settings of flow rate =J@ are read with manometer levels noted for each
flow rate. )ince there are only low pressure drops, the manometer reading is ta(en
from the water manometer. After seven readings of increasing flow, another set of
readings are ta(en with decreasing flow rate bac( to zero.
or the shutdown operation, water in the ;erspex column and water manometer
is drained. 2or(ing section is cleaned by removing any sand that accumulated in
the sieve and at the wor( place. The water supply to the constant head tan( is
disconnected.
1I, Data an$ Resu#ts
In this experiment, flow rates, pressure and temperature readings, and
lengths are necessary for the understanding of the concept of fluidization. This was
gathered during experimentation and was tabulated and presented in table F.!.
Table F.! low rate, velocity, manometer, expanded length, mm water, and
temperature reading
*#o6
rate, 7
8../(in9
1e#o.it4,
1a
8((/s9
Mano(e
ter
8((:59
Mano(e
ter
8((:59
E'pan$
e$
Len5t3,
Le 8((9
3ei53t o0
6ater, ((
!,
;C
0 0.0000 ?: ?: GG GG :G
!00 !.?FEF ?? 53 !0? !:G :3
:00 :.E"E! 55 ?F !!0 !E0 :3
"00 ?.?0G3 53 ?G !"5 ""0 :3
?00 5.G3G" 5E 5! !50 500 :G
500 3."?3E ?0 "! !F0 500 :G
F00 G.G!3? ?" "" !E0 500 "0
300 !0.:G30 ?5 "F ::0 500 "!
350 !!.0:!G ?3 "G :"0 500 ":
The velocity of the li%uid is necessary for future calculation. It was calculated
by dividing the volumetric flow rate by the area of the column for it is constant. It is
shown in e%uation Fa.
$%uation Fa6 for %C!00cc#min
( )
s
mm
s cm
mm
mm
cm
A
q
u 4696 . 1
60
min 1
1
10
38
4
min
100 3
2
3
,
_
<ensity of the solid media was determined using the concept of volume
displacement using a graduated cylinder filled with water. 1omputation is presented
in e%uation Fb.
$%uation Fb6
3
2220 22 . 2
0 . 4 9 . 4
2
m
kg
mL
g
mL mL
g
V V
m
i f
p
p
;orosity is also a ma-or player in this experiment for it affects everything. It
was computed using again the volume displacement method. It is presented in
$%uation Fc.
$%uation Fc6
40 . 0
5 . 5
9 . 4 1 . 7
+solid void
V
$%uation proposed by &ichard and 'a(i, e%uation 3b, will be used to get the
empiric exponent x.
$%uation 3b6
( )
x
t
a
e
V
V
L
L
,
_
1
1
+inearized form of $%uation 3b6
( )
,
_
1
]
1
t
a
e
e
V
V
x
L
L L
ln
1
ln
The terminal velocity is needed for the calculation of x. It is computed using the
)to(e*s +aw, e%uation 3c.
$%uation 3c6
( )
( )
s
mm
gr
V
f P
t
4975 . 166
001 . 18
00025 . 81 . 9 998 2200
18
2
2
Tabulating y,
( )
1
]
1
e
e
L
L L 1
ln
vs. x,
,
_
t
a
V
V
ln
6
Table 3.: the tabulated data for linearization.
8Le<L81<
=99/Le 1a/1t
#n8Le<L81<
=99/Le
#n81a/1
t9
0.F0GGGGGG
E !.5 80.?EF!!E?3F
0.?05?F
5
0.F?G : 80.?""GF?5G"
0.FE"!?
3
0.F3 :.5 80.?00?335F3
0.E!F:E
!
0.3::!05:F
" " 80.":55G?"53
!.0EGF!
:
0.3F ".5 80.:3??"FG?F
!.:5:3F
"
0.330?"?3G
" ".35 80.:F0G00:3!
!.":!35
F
;lotting
( )
1
]
1
e
e
L
L L 1
ln
vs.
,
_
t
a
V
V
ln
6
igure 3."
;lot of the linearized form of $%uation 3b
rom the linearization of $%uation 3b, the resulting e%uation of the line is
yC".??"3x8!.G:?F, where the slope =empiric exponent@, m =x@, is e%ual to ".??"3.
,sing $%uation 3b and the computed empiric exponent x, the expansion length
of the bed, +e is6
( )
mm
mm
L
e
80 . 52
4975 . 166
9391 . 2
1
4 . 1 88
,
_