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III B.Tech I Semester Supplementary Examinations, February 2007
MASS TRANSFER AND SEPARATION
(Bio-Technology)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
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1. Obtain an expression for the steady state Equimolal counter diffusion of two gases
starting from fundamentals? [16]
2. (a) Distinguish between Eddy and Molecular Diffusion?
(b) Explain Penetration Theory versus Two Film Theory? [8+8]
3. A liquid mixture containing 40 mole% n-Heptane and 60 mole% n-Octane is sub-
jected to differential distillation at atmospheric pressure with 60 mole% of the liquid
distilled. Compute the composition of the composited distillate and the residue.
Take relative volatility α =2.16. [16]
4. A rectification column is fed 100 kg mol/h of a mixture of 50 mol% Benzene and 50
mol% Toluene at 101.32 Kpa abs pressure. The feed is liquid at the boiling point.
The distillate is to contain 90 mol% Benzene and the bottoms 10 mol% Benzene.
The reflux ratio is 4.52:1. Calculate the kg mol/h distillate, kg mol/h bottoms and
the number of theoretical trays needed using Mc Cabe Thiele Method. [16]
5. (a) What is a plait point?
(b) Draw the flow diagram for continuous counter current multistage extraction
operation. [6+10]
6. Soyabean flakes containing 22 wt% oil are to be leached in a counter current multi-
stage to contain 0.8 kg oil/ 100 kg inert solid. Using fresh and pure hexane solvent.
For every 1000 kg soyabeans, 1000 kg Hexane is used. Experiments give the fol-
lowing retention of solution with the solids in the underflow, where N is kg inert
solid/ kg solution retained and YA is wt. fraction of oil in solution.
N 1.73 1.52 1.43
YA 0 0.20 0.30
Calculate the exit flows and compositions and the number of theoretical stages
required? [16]
7. The equilibrium adsorption of Acetone vapour on an activated carbon at 300 C and
1 atm is given by the following data
gm adsorbed / gm carbon 0 0.1 0.2 0.3 0.35 0.38
Partial pressure of Acetone mm Hg 0 2 12 42 92 120
The vapour pressure of Acetone at 350 C is 283 mm Hg. A one liter flask contains air
and Acetone vapour at 1 atm and 300 C with a relative saturation of the vapour of
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Code No: RR312301 Set No. 1
35%. Two grams of fresh activated carbon is introduced into the flask and the flask
is sealed. Calculate the final vapour concentration at 300 C and the final pressure.
Neglect the adsorption of air. [16]
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Code No: RR312301 Set No. 2
III B.Tech I Semester Supplementary Examinations, February 2007
MASS TRANSFER AND SEPARATION
(Bio-Technology)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
⋆⋆⋆⋆⋆
1. Obtain an expression for the steady state Equimolal counter diffusion of two gases
starting from fundamentals? [16]
3. An equimolar mixture of A and B is flash distilled such that 65% of the feed is in
product distillate of the total moles fed. Compute the composition of the distillate
and residue. Vapour liquid equilibrium data is as follows.
X (mole) % 8 10 20 30 40 50 70 80 95
Y (mole) % 37 42 58 67 73 78 87 96 98
(a) If 100 kg of feed solution is extracted in a single stage with 150 kg of solvent.
(b) If 100 kg of feed solution is extracted in three theoretical stages using 50 kg
of fresh solvent in each stage. [8+8]
6. Crushed oil seeds containing 55% oil (by weight) is to be extracted at the rate
of 4000 kg/hr using 100 kg/min of n-hexane containing 5% oil (by weight) as the
solvent. A counter current two stage extraction system is employed. The oil seeds
will retain 1 kg of solution per kg of oil free cake. Estimate the percent recovery of
oil obtained under the above conditions? [16]
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Code No: RR312301 Set No. 2
the membrane and its concentration on the other side is C2 = 0.50×10−2 kgmol/m3 .
The mass transfer coefficient KC1 is large and can be considered as infinite and
KC2 =2.02 ×10−5 kmol/m2 s mol fraction. Calculate the flux and the concentrations
at the membrane interfaces? [16]
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Code No: RR312301 Set No. 3
III B.Tech I Semester Supplementary Examinations, February 2007
MASS TRANSFER AND SEPARATION
(Bio-Technology)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
⋆⋆⋆⋆⋆
1. Obtain an expression for the steady state Equimolal counter diffusion of two gases
starting from fundamentals? [16]
2. Prove (or) show the following relationships starting with the equation.
(a) Convert K′C to KY and KG .
(b) Convert KL to Kx and K′ x .
(c) Convert KG to KY and KC . [6+5+5]
3. A liquid feed consisting of 1200 kg moles of mixture containing 30% Naphthalene
and 70% Dipropylene Glycol is differentially distilled at 100 mm Hg pressure and
final distillate contains 55% of Naphthalene. The VLE data are
X 8.4 11.6 2.8 50.6 68.7 80.6 88
Y 22.3 41.1 62.9 74.8 80.2 84.4 88
(a) Determine the amount of distillate.
(b) Determine the concentration of Naphthalene in residue and distillate? [8+8]
4. A rectification column is fed 100 kg mol/h of a mixture of 50 mol% Benzene and 50
mol% Toluene at 101.32 Kpa abs pressure. The feed is liquid at the boiling point.
The distillate is to contain 90 mol% Benzene and the bottoms 10 mol% Benzene.
The reflux ratio is 4.52:1. Calculate the kg mol/h distillate, kg mol/h bottoms and
the number of theoretical trays needed using Mc Cabe Thiele Method. [16]
5. Explain the following co-ordinate systems?
(a) Rectangular co-ordinate system.
(b) Triangular co-ordinate system.
(c) Rectangular co-ordinate system on solvent free basis. [5+5+6]
6. Soyabean flakes containing 22 wt% oil are to be leached in a counter current multi-
stage to contain 0.8 kg oil/ 100 kg inert solid. Using fresh and pure hexane solvent.
For every 1000 kg soyabeans, 1000 kg Hexane is used. Experiments give the fol-
lowing retention of solution with the solids in the underflow, where N is kg inert
solid/ kg solution retained and YA is wt. fraction of oil in solution.
N 1.73 1.52 1.43
YA 0 0.20 0.30
Calculate the exit flows and compositions and the number of theoretical stages
required? [16]
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Code No: RR312301 Set No. 3
7. Discuss about fixed bed adsorption and its application in food industry. [16]
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Code No: RR312301 Set No. 4
III B.Tech I Semester Supplementary Examinations, February 2007
MASS TRANSFER AND SEPARATION
(Bio-Technology)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
⋆⋆⋆⋆⋆
1. Obtain an expression for the steady state Equimolal counter diffusion of two gases
starting from fundamentals? [16]
5. With the help of neat sketches, explain briefly the various types of commercial
extraction equipment. [16]
8. Explain:
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Code No: RR312301 Set No. 4
(a) Effects of pressure ratio and separation factor on recovery.
(b) Effects of process flow patterns on separation and area. [8+8]
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