HUNTER COLLEGE CHEMISTRY DEPARTMENT Spring 2014 Syllab ! C"#$% 121 L&' E!!#n(ial! )* Organi+ C"#$i!

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Lab Coordinator: Dr. Jacopo Samson Room HN1320 Hunter Campus; Emai : !samson"#unter.cun$.edu Lab %ec#nicians: &abrie a So otc#i and &eor'e So otc#i Emai s: 'so otc"#unter.cun$.edu and 'so otc#"#unter.cun$.edu Section: ( ) Da$: Tuesday ) %ime: 8:10 11:00am ) Lab Room: W 203 *nstructor: Fei Mock Emai : #unterc#em121"'mai .com ) +,,ice Hours: Tuesday after class LA& MANUAL: H. Hart - L. Craine. Laborator$ /anua : +r'anic C#emistr$. 0 S#ort Course. 13t# Ed. LECTURE TE,T&OO-: J. /c/urra$. 12undamenta s o, +r'anic C#emistr$1. 3t# Edition LEARNING O&.ECTI/ES: 1. 4er,orm sa,e $. e,,icient $ and in a 5er$ or'ani6e manner. t#e basic tec#ni7ues ,or t#e separation. puri,ication. ana $sis and c#aracteri6ation o, or'anic compounds. 2. 8nderstand t#e main ob!ecti5e o, eac# e9periment. 3. C ear $ record. or'ani6e. ana $6e and report t#e resu ts o, t#eir e9periments. (. Learn to ta:e 'ood e9perimenta notes and co ect data and ;rite accurate and comp ete aborator$ reports inc udin' interpreti5e e5a uation. <. Communicate t#e concepts and resu ts o, t#eir aborator$ e9periments t#rou'# e,,ecti5e ;ritin' and ora communication s:i s. =. >no; t#e proper procedures and re'u ations ,or sa,e #and in' and use o, c#emica s and can ,o o; t#e proper procedures and re'u ations ,or sa,e #and in' ;#en usin' c#emica ?See 7ui6 on Sa,et$@ GRADING POLICY Aour ,ina 'rade is based on t#e ,o o;in' e ements: 1. 4re Lab E9ercisesB and a procedure out ine o, eac# e9periment 2. Lab ReportB 3. 4o;er 4oint ?44%@ 4resentation ?'roups o, 3 or ( ;it# 10 min. presentation and < min. o, CD0 session@B (. Lab per,ormance ?participation. de9terit$ in #and in' e7uipment. team;or:@ <. Sa,et$ 7ui6: a sa,et$ 7ui6 ;i be 'i5en in t#e 2nd ;ee: o, c ass and based on t#e ,o o;in' 5ideo: "((p'001i$#)%+)$02130440 B0ssi'ned b$ $our instructor Gra5#5 #l#$#n( Cui6 Lab 4er,ormance E9periment ReportsBB 44% 4resentation TOTAL 666 Pr# lab #7#r+i!#! 100 Lab R#p)r(! 300 P)in(! 20 E0 (00 100 200

BB%#e o;est 'rade ;i be dropped

LA&ORATORY POLICY 0 ce p#ones. pa'ers. CD p a$ers. /43 p a$ers. etc.. must be turned o,, ;#i e in t#e c ass. 0n$ students ;#o disrupt t#e c ass ;i be as:ed to ea5e. 0cademic Dis#onest$: Hunter Co e'e re'ards acts o, academic dis#onest$ ?e.'.. p a'iarism. c#eatin' on e9aminations. obtainin' un,air ad5anta'e. and ,a si,ication o, records and o,,icia documents@ as serious o,,enses a'ainst t#e 5a ues o, inte ectua #onest$. %#e co e'e is committed to en,orcin' t#e C8NA 4o ic$ on 0cademic *nte'rit$ and ;i pursue cases o, academic dis#onest$ accordin' to t#e Hunter Co e'e 0cademic *nte'rit$ 4rocedures. *n t#e ,irst da$ o, ab $ou ;i be re7uire to #a5e t#e ,o o;in' items: F Lab /anua ?a5ai ab e at t#e Hunter Co e'e boo:store@ F Sa,et$ & asses 8MUST &E 9)rn a( ALL TIMES in ("# Lab)ra()ry:; Lab per,ormance score is a measure o, #o; ;e prepared $ou are be,ore eac# e9periment. ;#et#er $ou read and understood t#e materia . and ;#et#er $ou are ab e to ;or: e,,icient $. sa,e $ and ,o o; aborator$ procedures responsib $. Aou ;i #a5e a c#ance to earn up to < points per e9periments based on $our ab per,ormance. Aour ,ina 'rade ;i be based on t#e 'rade sca eDs$stem set b$ t#e Re'istrar. 2or sa,et$ reasons la(#n#!! i! n)( ()l#ra(#5. *, $ou arri5e ate. $ou are not a o;ed to attend t#e ab. T"#r# ar# NO $a<# p ,or missed abs or e9ams. Aou ma$ on $ miss +NE E9periment. ;#ic# ;i be t#e o;est 'rade dropped. I$p)r(an( n)(#' Ge,ore ea5in' t#e ab. CLEAN YOUR &ENCH.

DATE 01D2ED201(

E,PERIMENT C"#+<=In

02D0(D201( 02D11D201( 02D1ED201( 02D2<D201( 03D0(D201( 03D11D201( 03D1ED201( 03D2<D201( 0(D01D201( 0(D0ED201( 0(D2JD201( 0<D0=D201( 0<D13D201(

E7p%1: /e tin' 4oint Determination E7p% 2: Recr$sta i6ation E7p%3: /o ecu ar /ode s: 4art 1 E7p%3: /o ecu ar /ode s: 4art 2 E7p% >: Disti ation E7p% 4: *so ation o, natura products E7p% 2: C#romato'rap#$ E7p% 1>: 0 :$ Ha ides E7p% 14: 0 co#o s and 4#eno s E7p% 14: 0 de#$des - >etones E7p% 21: S$nt#esis o, 0spirin PPT Pr#!#n(a(i)n C"#+<=O (

TOPICS CO/ERED0COMMENTS C#ec: *n; Discussion o, po icies; Sa,et$ /atters; Hideo tape s#o;n. S$ abus to be #anded out. Read pa'es 4a'es H*** to I*** 4ure 8rea and Cinnamic 0cid; 2 /i9tures and 1 8n:no;n 0cetani ide in ;ater as so 5ent ?macro sca e procedure on $@ 4rior to ab Read pa'es: (1)(3 - <1)=3 in /c/urra$ 4rior to ab read pa'es: (1)(3 - <1)=3 in /c/urra$ Simp e Disti ation and 2ractionation o, mi9 %o ueneDHe9ane 4uri,ication. dr$in' and me tin' point determination. +n $ Ca,,eine *nstructor demonstrates part G. Students do on $ part D. TOPICS for PPT Presentation will be assigned 4rior to ab read pa'es: 223)22J - 23()233 in /c/urra$ ) 213= 21? @ 224=222% +n $ parts G-C ;i be done. Read pa'es 2<3)2=2 in /c/urra$ ) Pri)r () lab +n $ parts: 1. 3. <. E 241=24? @ 221=22A Read C#apters: J.( - J.< o, /c/urra$ ) Pri)r () lab +n $ parts: 02. G2 and C2 to be done. 21A=2?2% Read pa'es: 3(()3(= in /c/urra$. ) Pri)r () lab >23=>2? 2ina e5a uation %eac#er E5a uation. C#ec:)+ut