Engineering Management Support, Inc.: West Lake OU-1

ENGINEERING MANAGEMENT SUPPORT, INC.
West Lake OU-1
STANDARD LEVEL IV
REPORT OF ANALYSIS
WORK ORDER #13-04105-0R
May 16,2013
EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

OAK RIDGE, TN
TABLE OF CONTENTS
DESCRIPTION
SECTION
PAGE
Chain of Custody & pH Check Sheet
0004
II
Sample Acknowledgement
0011
III
Case Narrative
0014
IV
Analytical Results Summary
0018
Analytical Standards
0024
VI
Quality Control Sample Results Summary
0048
VII
Laboratory Technician's Notes
0057
VIII
Analytical Data (Isotopic Uranium)
0088
IX
Analytical Data (Isotopic Thorium)
0202
Analytical Data (Radium-226)
0316
XI
Analytical Data (Radium-228)
0427
XII
Barium-133 Analytical Tracer Data
0445
Last Page Number
0521
STANDARD OPERATING PROCEDURE
MP..001, Rev.12
Effective: 10131112
Page14of14
Sample Receiving
Eberline Services- Oak Ridge Laboratory

LABORATORY DATA SUPPORT CHECKLIST
MP-001-3
1H3'--_0"--4-'-1-'---'Q"-'5~-----
Eberline Services Work Order # _ _
The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial
Initials
Date
Initials
Checklist Items
Sample Log-In
Data Compilation
First Technical Data Review
Second Technical Data Review
Data Entry/Electronic Deliverable
Case Narrative
Electronic Deliverable Proof
Samples 1\.rfalyzed within Holding Time
y,.,?
INn?
Client in Possession of Data

' or Hard Coov
Invoiced by Laboratory
Technical/Clerical Corrections, Signatures Needed, Problems, Etc
Date/Initials
/\
\
Date package approved by:
~ ~'
I
Laboratory Manager
~1( b(~/
Date
'-""
Copy No. _ _ __
Radiochemistry Services
SECTION I
CHAIN OF CUSTODY
&
pH CHECK SHEET
?J-04105
REC'D A,B.J.A,.2013
Chain of Custody Record

Project Name:
!JJ2:it LA ~
Send Report To:~J
ov- I
N!!
Project Number:
\<~o
Sampler (Print Name):"]~ \:) ~,'1\J
Address:
Shipment Method:
Phone:
Sample
lime
Date
P:?:r/0"5-'55
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Matrix
Number ol
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Sample Custodian Remarks (Completed By Laboratory):

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Level Ill
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Laboratory Receiving:
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Airblll Number:
Ook Aklgo, TN 37830

(885) 481-0683 Phone (865} 483-4621 Fax
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Sampler (Print Name):
(EBERh~~~
601ScalbotoRoad
1604
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0
0
0
Routine 0
CCC Seals Present?
24 Hour 0
COC Seals Intact?
1 Week 0
Other _ _
Received Containers Intact?

Temperature?
EBERL-l ...... E
SERVICES
Oak Ridge Laboratory
Internal
Work Order#
Chain of
Custody
Lab Deadline
13-04105
5/7/2013
UUISO - Level 4
Analysis
Water
Sample Matrix
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
Detector Activity
04
05
39
06
45
07
08
45
-
~~
12
13
46
------------14--- - - - --~.--
Ql.O
Ql.O
T'
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Ql.O
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42
11
Location
42
10
Storage
---1-
39
09
Fxns 05, 07, 09, 11, 13, 15, 17 & 19 are DISSOLVED
HP 210 I 270
Sample
Fraction
Comments
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~_-:_:~--=--"it-----_: "" -- -~~--~-~- - -~ j -~fi

19
---------1---
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Prilied: 4/16/2013 11:22AM
""'l\l-
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.
EBERLINE
SERVICES
Internal
Work Order#
13-04105
Chain of
Custody
Lab Deadline
5/7/2013
ThiSO - Level 4
Analysis
Water
Sample Matrix
Comments
Sample
Fraction
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
04
05
06
07
08
09
10
-----
II
HP 210 I 270
Storage
Detector Activity
Location
39
Ql.O
39
Ql.O
45
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45
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42
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14
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16
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Printed: 4/16/2013 11:22AM
f;l:ffHif7
.
EaERol._lNE:
SERVICES
Internal
Work Order#
13-04105
Chain of
Custody
Lab Deadline
5/7/2013
Ra226 - Level 4
Analysis
Water
Sample Matrix
I HP 210 I 270 I
I Detector Activity I
Sample
Fraction
Comments
J~-ll
- ~- - - -~:.~_ -~ 1~-~-~--~ ~ j
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
09
42
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11
37
12
46
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15
4:"''---- --- -+
18
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--
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Printed: 4/16/2013 11:22AM
-mmma
.
EBERLINE
- ---- ----- -- -- . _. -S-ERV_i_c E:"S
Internal
Work Order#
13-04105
Chain of
Custody
Lab Deadline
5/7/2013
Ra228 - Level 4
Analysis
Water
Sample Matrix
I1
Sample
Comments
Fraction
04
05
06
07
08
09
10
---------
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
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---- -- -- --
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12
. - - - - 13
------14
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...
16
17
18
19
------------------- -----------------------------
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HP 210 I 270
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Printed: 4/16!2013 11:22AM
mmms
Page 1 of 1
Printed: 4/16/2013 11:10 AM
E;~!;::RLI N
Internal Work Order
13-04105
Sample Receiving Report
E;
(Volumes, pH, & CPM)
SERVICES
Received By
KCOULSTON
ClientiD
FR
01
02
03
LCS
04
PZ-204-SS TOT/
# Btls
0
0
0
1
BLANK
DUP
Comments
""'
>-Container Numbe'i'
051
PZ-204-SS DIS'
--Coiltalner- Number
Matrix
Storage
WA
WA
WA
Q1.0
Q1.0
Q1.0
WA
Ql.O
HOrl
7
pH-Final--<_7
WA
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9.50
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9.5000
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I-68 TOT,
WA
1
Container Number
071
I-68 DIS I
_pH Orig
7
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;t:
Container-Number
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H:Finat-7
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9.50
Volume L
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Container'NUmber
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Ql.O
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PH Final
WA
Ql.O
COntainer Number
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41
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41
41
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9.5000
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43
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9.50
40
43
WA
37
Volunte' L
18
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41
HOri
37
46
WA
CPM
37
161
42
42
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141
45
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37
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45
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45
9.50
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Received
by: -mJ:.J;ruv ('&,., ~114
Date:
4/lt.~/1'3
MP-001. Rev 5
Effective: 11/22/02
SECTION II
SAMPLE ACKNOWLEDGEMENT
(.;!lent Name
---~-- "--+---- Contract/ PO --Engineering Management Support, Inc .i West Lake OU~l
---------
------~
Project Name
West Lake OU-1
uate Keceived
Project Type
Environmental
Client WO
Sample Oisp
West Lake OU-1
Sample Date
Matrix
Internal Deadline
N
N
N
N
13-04105
I I
05/13/2013
05/14/2013
:E"'>- "':J5
Storage
01
LCS
04/16/13
WA
Ql.O
"'X "'X
02
BLANK
04{16/13
WA
Q1.0
DUP
04!15/13
WA_
01.0
y3
05/07/2013
w
Client tO
28
Lab Deadline
...
,.
!urnar~~!'~-~~ys
04/16/2013
-
lntemallD
Required
I"
04
PZ-204-SS TOT
04/09/13 09:30
WA
Ql.O
05
PZ-204-SS DIS
04/09/13 09:30
WA
Q1.0
06
I-68 TOT
04/09/13 10:44
WA
Ql.O
07
I-68 DIS
04/09/13 10:44
WA
Ql.O
WA
Ql.O
-~
08
D-87 TOT
04/09/13 11:05
09
D-87 DIS
04/09/13 11:05
WA
Ql.O
10
PZ -106-SD TOT
04/09/13 12:00
WA
Ql.O
11
PZ -106-SD DIS
04/09/13 12:00
WA
Ql.O
12
.13
S-82 TOT
' !::1-82 D1S
'
04/09/13 12:27
WA
Ql.O
,~~filflit312:27
, WA
01.0
14
PZ -106-SS TOT
04/09/13 12:56
WA
Ql.O
15
PZ-106-SS DIS
04/09/13 12:56
WA
Q1.0
16
I-9 TOT
04/09/13 13:35
WA
Ql.O
17
I-9 DIS
04/09/13 13:35
WA
Ql.O
18
D-93 TOT
04/09/13 14:28
WA
Q1.0
19
D-93 DIS
04/09/13 14:28
WA
Ql.O
Totals Per Analysis (non QA samples)
16
16
16
16
*~
Invoice
Paul V. Rosasco, P.E
Report Data

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice
Sample Log In Report
Voice: (865) 481-0683

Fax:
(865) 483-4621
. 0
7220 West Jefferson Ave. Su~e 406
Lakewood. CO 80235
Lakewood, CO 80235
303-640-3426
'
Eng.nee!ing Management Support. lr>e
7220 WestJeff<Orson A""nue. Su<te 400
e~
Paul V. Rosasco, P.E.
Engneerlng Managem<!n!Support. Inc
, ; ; .,;; St;;R !..1

N!;;
SERVICES
1:11
'
Voice
303-940-3426
F"
Contact
Lyn Fitzgerald
Voice
303-601-4255
'"
8-<~
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Printed: 4/16/2013 11 :22 AM
STANDARD OPERATING PROCEDURE
MP-001, Rev. 12
Effective_ 10131112
Page 13of 14
Sample Receiving
Eberline Services - Oak Ridge Laboratory

SAMPLE RECEIPT CHECKLIST
13 - 0 4 1 0 5
MP-001-2
WORK ORDER# ___________________
SAMPLE MATRIX/MATRICES:
(CIRCLE ONE OR BOTH)

(AouEouS)
NON-AQUEOUS
(CIRCLE EITHER YES, NO, OR N/A)

WERE SAMPLES
Received in good condition?
If aqueous, properly preserved
(j)
Present on oulside of package?
00
Unbroken on oulside of package?
G)
Present on samples?
C0
Unbroken on samples?
OJ
N/A
WERE CHAIN OF CUSTODY SEALS
Was chain of custody present upon sample receipi?
rv-<
IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS: _______________________________________________________
DATE
Copy No. _______
t.lfllo/13
Radiochemistry Services
SECTION III
CASE NARRATIVE
EBERLINE ANALYTICAL CORPORATION

601 SCARBORO ROAD
OAK RIDGE, TENNESSEE 37830
PHONE (865) 481-0683
FAX (865) 483-4621
EBS-OR-35567
May 16,2013
Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235
CASE NARRATIVE
Work Order# 13-04105-0R
SAMPLE RECEIPT
This work order contains eight water samples received 04/16/2013. All samples were analyzed as total
and dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENTID
LABID
CLIENTID
LAB ID
PZ-204-SS TOT
PZ-204-SS DIS
l-68 TOT
I-68 DIS
D-87 TOT
D-87 DIS
PZ-1 06-SD TOT
PZ-1 06-SD DIS
S-82 TOT
13-041 05-04
13-04105-05
13-04105-06
13-04105-07
13-04105-08
13-04105-09
13-04105-10
13-04105-11
13-04105-12
S-82 DIS
PZ-1 06-SS TOT
PZ-106-SS DIS
I-9 TOT
I-9 DIS
D-93 TOT
D-93 DIS
13-04105-13
13-04105-14
13-04105-15
13-04105-16
13-04105-17
13-04105-18
13-04105-19
ANALYTICAL METHODS
Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was
analyzed using Method EPA 903.0. Radium-228 was analyzed using Method EPA 904.0.
Laboratory qualifiers are as follows:
J-
Indicates a situation where the result minus the error is less than the detection limit but greater
than zero.
U-
Indicates a situation where the result minus the error is less than or equal to zero.
ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.
Page I of3
filS iS
ANALYTICAL RESULTS CONTINUED

ISOTOPIC URANIUM
Samples were filtered to disassociate dissolved and total fractions. All samples were prepared by
removing a representative aliquot followed by mixed acid digestions and dilutions as appropriate.
Uranium was eluted, micro-precipitated and mounted on micro-porous filter media. Sample activities
were then determined by alpha spectroscopy using energy specific regions of interest for Uranium-234,
Uranium-235 and Uranium-238. Chemical recovery was determined by the use of a Uranium-232 tracer.
Activity of the Uranium-232 tracer was determined by alpha spectroscopy using an energy specific region
of interest.
Samples demonstrated acceptable results for all Uranium analyses. Chemical recovery was acceptable for
all samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable
results. Results for the Uranium-234 and Uranium-238 duplicate demonstrated an acceptable relative
percent difference and normalized difference. Results for the Uranium-235 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Uranium-234 and Uranium-238 laboratory control sample demonstrated an
acceptable percent recovery.
ISOTOPIC THORIUM
Samples were filtered to disassociate dissolved and total fractions. All samples were prepared by
removing a representative aliquot followed by mixed acid digestions as appropriate. Thorium was
selectively extracted by ion exchange. Thorium was eluted, micro-precipitated and mounted on microporous filter media. Sample activities were then determined by alpha spectroscopy using energy specific
regions of interest for Thorium-228, Thorium-230 and Thorium-232. Chemical recovery was determined
by the use of a Thorium-229 tracer. Activity of the Thorium-229 tracer was determined by alpha
spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228, Thorium-230 and Thorium-232 method blank demonstrated acceptable
results. Results for the Thorium-228, Thorium-230 and Thorium-232 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Thorium-228, Thorium-230 and Thorium-232 laboratory control sample
demonstrated an acceptable percent recovery.
RADIUM-226
Samples were filtered to disassociate dissolved and total fractions. All samples were prepared by mixed
acid digestions and dilutions as appropriate. This was followed by selective sulfate precipitations of the
Radium. Samples were then mounted by semi-micro-precipitations onto micro-porous filters. Samples
were counted by alpha spectroscopy using an energy specific region of interest for Radium-226.
Chemical recovery was calculated by the use of a Barium-133 tracer, which was determined by HPGe
gamma spectroscopy.
Samples demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated acceptable results. Results for the Radium226 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results
for the Radium-226 laboratory control sample demonstrated an acceptable percent recovery.
Page 2 of3
ANALYTJCAL RESULTS CONTINUED

RADillM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth ofthe Actinium-228 daughter. After ingrowth, Actinium228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were
then counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium133 tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Samples demonstrated acceptable results for all Radium-228 analyses. Chemical recovery was acceptable
for all samples. The Radium-228 method blank demonstrated acceptable results. Results for the Radium228 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results
for the Radium-228 laboratory control sample demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY
I certifY that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
designee to be ace ate as verified by the following signature.
M.R. McDougall
Laboratory Manager
Date: 5!16/2013
Eberline Analytical wants and encourages your feedback regarding our pertOrmancc providing radioanalytical services. Please
visit http://www .eberlineservices.com/client.htm to provide us with feedback on our services.
Page 3 of3
SECTION IV
ANALYTICAL RESULTS SUMMARY

Lakewood, CO 80235
Client Sample ID
~~I
!all
......
1,0
Project: West Lake OU-1

SDG: 1304105
Received: 04/16/2013
Matrix: Water
Lab Sample ID
Analvsis Date/Time
Analvte
LCS13-04105-01
LCS13-041 05-01
LCS13-04105-01
LCS13-04105-01
LCS13-041 05-01
LCS13-04105-01
LCS13-04105-01
LCS13-04105-01
13-04105-01
13-04105-01
13-04105-01
13-041 05-01
13-04105-01
13-04105-01
13-04105-01
13-04105-01
05/01/2013 16:18:07
05/09/2013 09:17:01
04/30/201311:48:51
04/30/2013 11 :48:51
04/30/2013 11:48:51
04/29/2013 09:59:25
04/29/2013 09:59:25
04/29/2013 09:59:25
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
BLANK13-04105-02
BLANK13-041 05-02
BLANK13-04105-02
BLANK 13-041 05-02
BLANK13-041 05-02
BLANK13-041 05-02
BLANK 13-041 05-02
BLANK13-041 05-02
13-04105-02
13-04105-02
13-04105-02
13-04105-02
13-04105-02
13-04105-02
13-04105-02
13-04105-02
05/01/2013 16:18:08
05/09/2013 09:17:01
04/30/2013 11 :48:53
04/30/2013 11 :48:53
04/30/2013 11 :48:53
04/29/2013 09:59:26
04/29/2013 09:59:26
04/29/2013 09:59:26
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-106-SS TOT DUP

PZ-106-SS TOT DUP
PZ-204-SS TOT DUP
PZ-204-SS TOT DUP
PZ-204-SS TOT DUP
PZ-204-SS TOT DUP
PZ-204-SS TOT DUP
PZ-204-SS TOT DUP
13-04105-03
13-04105-03
13-04105-03
13-04105-03
13-04105-03
13-04105-03
13-04105-03
13-04105-03
05/01/201316:18:09
05/09/2013 09:17:01
04/30/2013 11 :49:02
04/30/2013 11:49:02
04/30/201311:49:02
04/29/2013 09:59:21
04/29/201309:59:21
04/29/2013"09:59:21
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
. HASL 300,
HASL 300,
HASL 300,
PZ-204-SS TOT
PZ-204-SS TOT
PZ-204-SS TOT
PZ-204-SS TOT
PZ-204-SS TOT
PZ-204-SS TOT
PZ-204-SS TOT
PZ-204-SS TOT
13-04105-04
13-04105-04
13-04105-04
13-04105-04
13-04105-04
13-04105-04
13-04105-04
13-04105-04
05/01/201316:18:10
05/09/2013 09:17:02
04/30/2013 11 :48:59
04/30/2013 11 :48:59
04/30/2013 11 :48:59
04/29/2013 09:59:22
04/29/2013 09:59:22
04/29/2013 09:59:22
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
2J
~EBER!:-:_~~~
Final Report of Analysis

Date: 5/16/2013
Page 1 of 5
Method
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
Result
Error
MDA
10.35
9.90
4.46
4.36
5.17
7.93
0.69
7.57
1.15
1.03
0.69
0.67
0.77
1.02
0.21
0.98
0.23
1.26
0.06
0.06
0.05
0.08
0.08
0.06
0.~
Q~
0.11
Q~
0~
O.U
Q~
Q~
Q~
0.14
0.00
QOO
0.00
0.00
om
OM
0.04
Q~
0.~
Q~
0.00
Q~
om
0.~
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
2.63
0.89
0.31
0.16
0.12
2.92
0.20
1.92
0.49
0.46
0.13
0.09
0.08
0.45
0.10
0.33
0.14
0.88
0.06
0.06
0.06
0.08
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.26
1.16
0.22
0.22
0.08
3.20
0.14
2.47
0.36
0.43
0.11
0.11
0.07
0.51
0.09
0.42
865/481-0683
u
u
u
u
J
0.16
o.n
QOO
0.07
0.00
QOO
0~
0.~
FAX 865/483-4621
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
0.07
0.07

601 SCARBORO ROAD OAK RIDGE, TN 37830
Qualifier
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sample ID
~!I
tl~
!'.l
l?d

SDG: 1304105
Matrix: Water
Lab Sample ID
Analysis Date/Time
Anatvte
PZ-204-SSDIS
PZ-204-SS DIS
PZ-204-SS DIS
PZ-204-SS DIS
PZ-204-SS DIS
PZ-204-SS DIS
PZ-204-SS DIS
PZ-204-SS DIS
13-04105-05
13-04105-05
13-04105-05
13-04105-05
13-04105-05
13-041 05-05
13-04105-05
13-04105-05
05/01/2013 16:18:41
05/09/2013 09:17:09
04/30/2013 11 :49:00
04/30/2013 11 :49:00
04/30/2013 11 :49:00
04/29/2013 09:59:23
04/29/2013 09:59:23
04/29/2013 09:59:23
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
1-68 TOT
1-68 TOT
1-68 TOT
1-68 TOT
1-68 TOT
1-68 TOT
1-68 TOT
1-68 TOT
13-04105-06
13-04105-06
13-04105-06
13-04105-06
13-04105-06
13-04105-06
13-04105-06
13-04105-06
05/01/2013 16:18:42
05/09/2013 09:17:09
04/30/2013 11 :48:55
04/30/2013 11 :48:55
04/30/2013 11 :48:55
04/29/2013 09:59:24
04/29/2013 09:59:24
04/29/2013 09:59:24
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
1-68 DIS
1-68 DIS
1-68 DIS
1-68 DIS
1-68 DIS
1-68 DIS
1-68 DIS
1-68 DIS
13-04105-07
13-04105-07
13-04105-07
13-04105-07
13-04105-07
13-04105-07
13-04105-07
13-04105-07
05/01/2013 16:18:43
05/09/2013 10:57:39
04/30/2013 11 :48:57
04/30/2013 11 :48:57
04/30/201311:48:57
04/29/2013 09:59:59
04/29/2013 09:59:59
04/29/2013 o9:59:59
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
D-87 TOT
D-87TOT
D-87TOT
D-87 TOT
D-87TOT
D-87TOT
D-87 TOT
D-87 TOT
13-04105-08
13-04105-08
13-04105-08
13-041 05-08
13-04105-08
13-04105-08
13-04105-08
13-04105-08
05/01/2013 16:18:44
05/09/2013 10:57:39
04/30/2013 11:48:48
04/30/2013 11 :48:48
04/30/2013 11 :48:48
04/29/2013 10:00:00
04/29/2013 10:00:00
04/29/2013 10:00:00
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
2J
~EBER~~~-~

Date: 5/16/2013
Page 2 of 5
Method
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.87
0.74
0.04
0.10
0.02
3.50
0.13
1.76
0.32
0.47
O.Q7
0.09
0.05
0.51
0.08
0.32
0.22
0.91
0.12
0.11
0.11
0.06
0.05
0.05
on
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
3.34
1.97
2.66
4.14
0.80
2.73
0.24
2.42
0.35
1.16
0.08
0.08
0.08
0.10
0.11
0.12
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.67
1.37
0.00
0.11
0.03
2.58
0.18
2.23
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.33
2.99
0.22
0.40
0.06
0.40
0.03
0.10
OM
0.~
0~
O.D
o.w
0.15
051
OD
865/481-0683
u
J
u
J
014
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
OM
0.00
0.12
012
0~
0.12
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
0.42
0.59
0.13
0.17
0.06
0.20
0.08
0.10
0.21
0.94
0.09
0.09
0.07
0.14
0.17
0.12
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
0~
ow
OM
0.00
0.00
0.00
004
OM

Qualifier
FAX 865/483-4621
u
u

Lakewood, CO 80235
Client Sample ID
Lab Sample ID
Analysis Date/Time
Analvte
D-87 DIS
D-87 DIS
D-87 DIS
D-87 DIS
D-87 DIS
D-87 DIS
D-87 DIS
D-87 DIS
13-041 05-09
13-041 05-09
13-04105-09
13-041 05-09
13-041 05-09
13-04105-09
13-041 05-09
13-04105-09
05/01/2013 16:18:45
05/09/2013 10:57:40
04/30/2013 11 :48:49
04/30/201311:48:49
04/30/2013 11 :48:49
04/29/2013 10:00:01
04/29/2013 10:00:01
04/29/2013 10:00:01
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-106-SD TOT
PZ-106-SD TOT
PZ-106-SD TOT
PZ-106-SD TOT
PZ-1 06-SD TOT
PZ-106-SD TOT
PZ-106-SD TOT
PZ-106-SD TOT
13-04105-10
13-04105-10
13-04105-10
13-04105-10
13-04105-10
13-04105-10
13-04105-10
13-04105-10
05/01/2013
05/09/2013
04/30/2013
04/30/2013
04/30/2013
04/29/2013
04/29/2013
04/29/2013
16:18:46
10:57:41
12:43:33
12:43:33
12:43:33
10:00:02
10:00:02
10:00:02
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-106-SD
PZ-106-SD
PZ-1 06-SD
PZ-106-SD
PZ-106-SD
PZ-106-SD
PZ-106-SD
PZ-1 06-SD
13-04105-11
13-04105-11
13-04105-11
13-04105-11
13-04105-11
13-04105-11
13-04105-11
13-04105-11
05/01/2013 16:19:52
05/09/2013 10:57:44
04/30/2013 12:43:34
04/30/2013 12:43:34
04/30/2013 12:43:34
04/29/2013 10:00:03
04/29/2013 10:00:03
04/29/20131 0:00:03
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04105-12
13-04105-12
13-04105-12
13-04105-12
13-04105-12
13-04105-12
13-04105-12
13-04105-12
05/01/2013 16:19:55
05/09/2013 10:57:44
04/30/2013 12:43:35
04/30/2013 12:43:35
04/30/2013 12:43:35
04/29/2013 10:00:04
04/29/201310:00:04
04/29/2013 10:00:04
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
S-82 TOT
S-82 TOT
S-82 TOT
S-82 TOT
S-82 TOT
S-82 TOT
S-82 TOT
S-82 TOT
~I
!;!~
M
~,..J,,

SDG: 1304105
Matrix: Water
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
2J
~EBER!;:,~~~

Date: 5/16/2013
Page 3 of 5
Method
Result
Error
MDA
0.75
0.95
0.31
OM
0.22
0.93
0.08
0.08
0.08
0.10
0.12
0.12
0.07
0.~
0.11
0.01
0.26
0.02
0.11
QM
QM
0.31
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.04
0.34
0.21
0.13
0.14
0.32
0.06
0.31
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.61
0.89
0.00
0.34
-0.01
0.43
0.03
0.20
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.63
2.04
0.12
0.24
0.11
1.26
0.12
1.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.15
0.00
0.10
0.~
0.11
Q~
OM
0.16
1.14
0.10
0.08
0.09
0.00
0.07
0.07
Q13
0.06
0~
0.11
0.14
1.02
0.14
0.10
0.10
0.08
0.08
0.08
0.13
0.~
ore
Q16
o.ro
Q16
OM
0~
Q17
QY
1~1
0.10
0.13
0.~
0.~
0.41
0.13
0.~
0.12
Q10
0.17
0.17
0.11

665/481-0663
FAX 665/463-4621
Qualifier
u
J
u
J
u
J
J
J
u
u
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
~~
~~
~~
pC~
~~
~~
~~
~~

Lakewood, CO 80235
Client Sample ID
S-82
S-82
S-82
S-82
S-82
S-82
S-82
S-82
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
t!~
M
M
Lab Sample ID Analvsis Date/Time
Analvte
05101/2013
0510912013
0413012013
0413012013
0413012013
0412912013
04/29/2013
04/29/2013
16:19:48
10:57:44
12:43:36
12:43:36
12:43:36
10:00:43
10:00:43
10:00:43
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-106-SS TOT
PZ-106-SS TOT
PZ-1 06-SS TOT
PZ-106-SS TOT
PZ-1 06-SS TOT
PZ-106-SS TOT
PZ-106-SS TOT
PZ-106-SS TOT
13-04105-14
13-04105-14
13-04105-14
13-04105-14
13-04105-14
13-04105-14
13-04105-14
13-04105-14
05/01/201316:19:50
05/09/2013 10:57:45
04/30/2013 12:43:37
04/30/2013 12:43:37
04/30/2013 12:43:37
04/29/2013 10:00:45
04/29/2013 10:00:45
04/29/2013 10:00:45
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 3bo,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-106-SS
PZ-106-SS
PZ-106-SS
PZ-106-SS
PZ-106-SS
PZ-1 06-SS
PZ-106-SS
PZ-106-SS
13-04105-15
13-04105-15
13-04105-15
13-04105-15
13-04105-15
13-04105-15
13-04105-15
13-04105-15
05/01/2013 16:20:04
05/09/2013 10:57:37
04/30/2013 12:43:38
04/30/2013 12:43:38
04/30/2013 12:43:38
04/29/2013 10:00:46
04/29/2013 10:00:46
04/29/2013.10:00:46
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04105-16
13-04105-16
13-04105-16
13-04105-16
13-04105-16
13-04105-16
13-04105-16
13-04105-16
05/01/2013 16:19:58
05/09/2013 10:57:37
04/30/201314:35:06
04/30/2013 14:35:06
04/30/2013 14:35:06
04/29/2013 10:00:48
04/29/2013 10:00:48
04/29/2013 10:00:48
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
~EBERLINE
SERVICES

Date: 511612013
Page4 of 5
Method
13-04105-13
13-04105-13
13-04105-13
13-04105-13
13-04105-13
13-04105-13
13-04105-13
13-04105-13
1-9 TOT
1-9 TOT
I-9TOT
1-9TOT
1-9 TOT
1-9 TOT
I-9TOT
I-9TOT
1:-11

SDG: 1304105
Received: 0411612013
Matrix: Water
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.64
1.17
0.00
0.08
0.00
0.91
0.02
0.81
0.27
0.56
0.03
0.07
0.02
0.32
0.06
0.30
0.16
1.06
0.08
0.06
0.06
0.14
0.12
0.14
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
2.80
0.71
0.04
0.16
0.02
0.59
0.05
0.38
0.53
0.54
0.06
0.10
0.04
0.17
0.05
0.13
0.12
1.07
0.10
0.08
O.Q7
0.05
0.06
0.05
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
3.12
0.51
0.01
0.15
0.01
0.61
0.12
0.34
0.56
0.57
0.05
0.10
0.04
0.17
0.08
0.12
0.13
1.16
0.12
0.09
0.09
0.05
0.05
0.04
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.48
3.81
0.15
0.11
-0.02
0.14
0.00
0.04
0.43
0.78
0.11
0.09
0.03
0.12
0.08
0.07
0.20
1.30
0.13
0.10
0.10
0.11
0.18
0.10

865/481-0683
FAX 865/483-4621
Qualifier
u
J
u
u
u
J
u
u
u
u
J
u
J
u
J
u
u
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sample ID
tlill
ll!il
I,;~
Lab Sample ID

SDG: 1304105
Matrix: Water
Analvsis Date/Time
Analvte
Method
1-9 DIS
1-9 DIS
1-9 DIS
1-9 DIS
1-9 DIS
1-9 DIS
1-9 DIS
1-9 DIS
13-04105-17
13-04105-17
13-04105-17
13-04105-17
13-04105-17
13-04105-17
13-04105-17
13-04105-17
05/01/2013
05/09/2013
04/30/2013
04/30/2013
04/30/2013
04/29/2013
04/29/2013
04/29/2013
16:20:01
10:57:37
14:35:07
14:35:07
14:35:07
10:00:50
10:00:50
10:00:50
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
D-93 TOT
D-93 TOT
D-93 TOT
D-93 TOT
D-93 TOT
D-93 TOT
D-93 TOT
D-93 TOT
13-04105-18
13-04105-18
13-04105-18
13-04105-18
13-04105-18
13-04105-18
13-04105-18
13-04105-18
05/02/2013 05:32:48
05/09/2013 10:57:37
04/30/2013 14:35:03
04/30/2013 14:35:03
04/30/201314:35:03
04/29/2013 10:00:51
04/29/201310:00:51
04/29/2013 10:00:51
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
D-93
D-93
D-93
D-93
D-93
D-93
D-93
D-93
13-04105-19
13-04105-19
13-04105-19
13-04105-19
13-04105-19
13-04105-19
13-04105-19
13-04105-19
05/02/2013 05:32:49
05/09/2013 11 :22:40
04/30/2013 14:35:04
04/30/2013 14:35:04
04/30/2013 14:35:04
04/29/2013 10:00:53
04/29/2013.10:00:53
04/29/2013 10:00:53
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
EBERLINE
SERVICES

Date: 5/16/2013
Page 5 of 5
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.67
1.49
-0.01
0.15
0.10
0.20
0.10
0.19
0.29
0.60
0.11
0.15
0.12
0.12
0.09
0.11
0.20
1.12
0.28
0.18
0.16
O.D7
0.09
0.07
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
3.02
4.79
0.16
0.09
0.01
0.39
0.03
0.16
0.71
0.74
0.11
0.08
0.04
0.16
0.05
0.12
0.31
1.12
0.13
0.09
0.09
0.09
0.10
0.15
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.93
2.89
0.05
0.16
0.03
0.30
0.04
0.15
0.48
0.59
0.06
0.09
0.04
0.14
0.06
0.10
0.21
0.97
0.09
0.05
0.06
0.08
0.09
O.D7

865/481-0683
FAX 865/483-4621
Qualifier
u
u
u
J
J
J
u
u
J
u
u
u
J
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
SECTIONV
ANALYTICAL STANDARDS
U.-8
QA/QG REVIEWED CERTIFICATE OF CALIBRATION

bq(lnitialsJ&C ALPHA STANDARD SOLUTION
Date
Radionuclide:
Half Life:
(4.468
Catalog No.:
Source No.:
TMA EBERLINE
Customer:
OR2778
P.O.No.:
Reference Date:
Januruy 1 1995
12:00 PST.
Contained Radioactivity: (Total U) 8.016 ~Ci
Contained Radioactivity: (Total U) 297 kBq
U-238NAT
0.005) x 10'9 years

7338
479-50
Description of Solution
a. Mass of solution:
b. Chemical form:
65.2896 g in a 50 ml flame sealed ampoule

Uranyl Nitrate in H20
None
Approximately 1.3202
c. Carrier content:
d. Density:
Radioimpurities
' '---.
.------.
.-,;,.
g/ml@
wc.
,.
Refer to attached technical data sheet
'~
'
Radioactive Daughters
Refer to attached technical data sheet
Radionuclide Concentration
(Total U) 0.1228
Method of Calibration
i!Cilg.
Activity calculations are based upon known specific activity and mass.
">>.
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
3.0%
0.0%
2.0%
3.6%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
;
See reverse side for Leak Test(s) applied to this source.

Notes
loi {-i'
:,,,:-. ..>,
1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Vtrginja S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance prognqn to eE.tablish and maintain implicit traceability for a riumber of nuclides,
based on th~ blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
,;-
:-.
Date Signed
ISOTOPE PRODUCTS LABORATORIES
3017 N. SAN FERNANDO BLVD.
.. ~
..
BURBANK, CALIFORNIA
91504
8188437000
8188436168
FAX
. ,.
(.,
.. , ..
,.
-..
QUALITY CONTROL PROGRAM

IVIP.009
Rev.S; 11/01/03
Title:
Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DI/.UT/ON RECERTIFICATION
MP009
Radionucllde .
Certified Activity~'.'"",:a::'o.u='~'"'e"'e""+~ooi:-IJ.LCi
.
Certified Concentration
J.LCi per gram
Ampoule /Solution Gross
Empty Ampoule
Solution Net
Total Activity In Ampoule
Reference Datel.
:.;.-. .,
97,6400
32:5020
65.1380
8.0160
>11111'995 O:ocil
Weight, Grams
Weight, Grams
Weight, Grams
J.LCI
Chemical Com osition of Standard Solution
Dilution Solvent Used

Dilute to a volume otl i
Certified Total Activity ofl
a;0160IJ.LCI
1000:00
P. M
.... H.NO
. . . 3. /
. . ..
. .
'
Imilliliters
Which Eauals
1.780E+07Idpm at the date listed above
This activity concentration Is based on the original

And after dilution the activity of this solution isl 1.77955E+04Idpm/mh.lerence date listed above; All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date: I September6, 2013
Date: --==;:.;.;;;...;;.;.;=.
9/26/2012 0:00
Date:
--'lf-/.::;.u:ot/.:....1"2...;;;.....__
iillll26
~I;;BEF;!+INE;; I QUALITY CONTROL PROGRAM

MP-009
ERVICES
Rev.s; 11/01103
nte: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES- OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009
Solution Reference #IIPl'47~50-'- ';.:: ..._
Principal Radionuclide
Half Life, Years
~''H~ 238(J I
j. ''4:468E'>osl
.. ..
Radionuclide of Interest! '~~: 21:f'l!lt) .1

Parent Solution Conc.1 1:7796E+04.Jdpmlml
Reference Date
Chemical Coml!ositlon of Standard Solution
IUranWNitiatii lr(1 \Ill HN.03. .
Date I
9/6/2012 0:00 I
Solution #F ._.,_ ... u,aa:.... c. :1
Half Life, Da~s
. 1.632E+12I
I
'I
-1/1t1995
o:oo 1
.,'.
Dilution Instructions:
l1MHN03 .
SECONDARY VOLUMETRIC DILUTION

.. :.
,:"4:0000 ml
Vol. Parent Solution:
Total Activity: 7.1182E+04 dpm
Final Volume: .-.1000;00 ml
Final Activity Concentration:!
This activity concentration is based on the original

reference date listed above. All activities are
corrected to the date and time of analysis by the
labor: tory data processing software.
NOTES:
Isotopic Distribution as:
U238 Atom % 48.239
U-235 Atom % = 2.25
U-234 Atom % =49.601
All values +/ 3.6%
7.1182E+01idpmlml
U-238 71.182 dpmlml X 0.48249 = 34.345 dpm/mt

U-235 71.182 dpmtm!X 0.0225 1.602 dpm/ml
U-238 71.182 dpmlml X 0.49501 35.238 dpm/ml
Expiration Date: September 6,
Isotopic ratios from manufacturer's data sheet
\,~.
Verified & Approved By
QCApproval
2oi3 I
f\
~
.
~d!WtAlll
Date:
9/26/2012 0:00
Date:
~U6trZ-
t\i-827
RECORD COPY
Tracer Solution for Environmental Analysis & Disequilibrium Studies
Product Description & Measurement Certificate
Description
Principal radionuclide:
Daughter Nuclide:
uranium 232 (U-232)

Th-228
Measurement
Reference date:
Radioactive concentration U-232
which is equivalent to
Product code: UDPl 0050

Batch Number: '12/232/67
01 March 2000
6. 739E+03 becquerels per gram of solution
1.821E-O.l microcuries per gram of solution
5.35! ga"'OAiilS
Volume of solution
Total activity ofU-232
which is equivalent to
5.035 millilitres
3.61E+04 becquerels
9.76E-01 microcuries
Method of measurement (see reverse of this certificate)

Systematic uncertainty: 0.5%
Random uncertainty is: 0.7%
Overall uncertainty in the radioactive concentration quoted above: 1.7%
Overall uncertainty is defined on the reverse of this certificate.
Accuracy
Radionuc/idic
Purity
Any radioactive impurities measured are listed below, expressed as percentages

of the activity of the principle radio nuclide at the reference date .
Th-228 and daughter activity removed 2 Feb 2000
U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 113/00
~ne
Isotopic
isotopic composition, exprP-ssed as atom per cent at the reference date .
Purity
,-<ot measured
Chemical
Composition
Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution bas been produced 'carrier free'.
Physical
Data
Recommended half life of uranium 232: 6.980E+01 years

Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.0%
Branching ratio for alpha emission: 100%
Calculated specific activity of uranium 232: 8.167E+05 Bq per microgram U-232.
Remarks
For safety information and notes to ensure correct usage by all persons handling this radio'IC!ive Tracer
solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and
approved to ISO 9001.
Approved
Signatory
Project Ref. AE231S
Roger Wiltshire
Prepared and characteried in the UK, for world wide distribution by Isotrak, AEA Technology, QSA.
Trkcert.wps I 0103/00
AEA Techn,Jlogy is the trading name of AEA Technology !{li-E; 2 8
~EBERLINE I

MP.OD9
Se:RV!Ce::G
Rev.B; 11/01/03
Title:

PRIMARY DILUTION RECERTIFICATION
MP009
SOLUTION REFERENCE #IAEA!Ame..Sham.921232167
Half Life, Years
.. . . ""~U1
I
7:2cioE+o1l
CURRENT DATE I . 12/13/2012 0;001

I SOLUTION #I ~ < .U~1o. I
Half Life, Da~s
2.630E+04I
I . .. . .. .
Radionuclide, .. . . :cp~u. ~
Certified Activity ...9.760.Eo,01 ~tCI
Certified Concentration ~tCi per gram
..
Reference Date!. ..31112cio:o O:Ool
. .,,.,..,., ,.,"r,. .""'

~I
Empty Ampoule . .. . Weight, Grams

Solution Net . . Weight, Grams
Total Activity in Ampoule
0.9760 ~tCI
Chemical Composition of Standard Solution

l""j.l,(N03)e.in?Mi:iN03i.> :
<. .
<;.. .
;1
..
.. :...' . -:; ~ .: :-:- - : ;:._:,_'.
I2MHNo
. ' - . 3-- '
_:-
-_
Dilute to a volume otl >1000.00 /I milliliters
Certified Total Activity of I
.. 0.9760I~tCI
Which Eauals
. . 2.167E+06Idpm at the date listed above

And after dilution the activity of this solution Is I2.167E+03Idpmlml reference date listed above. All activities are corrected
to the date and time of analysls by the laboratory data
Expiration Date: I December 7, 2013 I

QC Approval
~~';,
o~hit IUAJr
r\
'V
Date;
Date:
12113/2012 0;00
'siP7
Rev.6; 11/01/03
Title: Radioactive Ref&rence Standarde Solutions & Records

DateI
12/7/~12 0:001
. -- . .
' - I
1#1
Half LifE '8VS
I
Half Life. ears
7
II
...
Radlonucllde of lnteres1f_::. <'~'~ir-:-\ 1

Parent Solution Cone.! <2.167E+03 ldpm/ml
Reference Date! :- ' -. 3i1/20oo":o:ool
.. Instructions:
IDilluticm

Vol. Parent Solution:
10.0000 ml
Total Activity: - 2.1670E+04 dpm
Final Volume:
"1000:00 ml
-. 2.1e70E+01ldpmlml

laboratory data processing software.
NOTES:
Expiration Date:! December 7, 2013 I
~
\ _..!,t\...:..,:-i==
0 ~t=::;_-:-r.,.p'<----.!'--
QC
r~ /hlAJ A(~--._\
Date: _ _1~21:!..:1:.:;:3/~2:.:;:0.:,:12::..;0~:~00~
Date:-"""
l::l.J/d.,s,/u,=_t:l-_ _
I I
lnitia~
RTIF'ICATE OF CALffiRATI~t~
CJ\
LPHA. STANDARD SOLUTION" \}"' '\ ~~~\\\\\\
Radionuclide
Th-230
Half Life:
(7 .54 0.03) x 10"4 yeatS
Catalog No.:
7230
Source No.:
388-116
b. Chemical form:
c. Carrier content:
d. Density:
TMA EBEruli\\\~~~' \.~
Customer:
P.O.No.:
Tf4944
Reference Date:
November 1 1991
ConlaiDed Radioactivity:
1.036
5.0042
Th(N03)4 in O.lN HN03
None added
1.0016
,~~..
12:00 PST.
j<Ci.
grams.
gram/ml @ 20"C.
Radioimpurities
See attached technical data sheet
See attached technical data sheet
0.207
jLCi/gram.
Weighed aliquots of the solution were assayed using a liquid scintillation counter.
Uncertainty .of Measurement

a. Systematic uncertainty in instrument calibration:
b. Raodom uncertainty in assay:
c. Random uncertaintY in weighing(s):
2.0%
0.5%
0.2%
2.7%
NIST Traceability
This calibration is implicitly traceable to the National Institote of Standards and Teclmology.
Notes
1. Nuclear data were taken from "Table of Isotopes, Seventh Edition, edited by Virginia S. Shirley.
2. IPL participates in an NIST measurement assunmce program to establish and maintain implicit
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatory Guide 4.15)

1800 No. Keystone Street.,
Burbank, California 91504
818 843 - 7000
lfo E
~
13 E RLI N.<;:
SS:R\I'ICfi
I QUALITY CONTROL
PROGRAM
MP-oo9
Rev.B; 11/01/03
Title:

MP-009
Solution Reference #IIPL 3S8il16 :,:
Principal Radlonuclide
Half Life, Years
. ,.,_:~ti:.. .:::l
Date!
3/4/20130:001
Solution #j/:;.: ::.:Th01b>' .:>.:-1
Half Life, Days
I.
2.754E"c07l
Reference DateFY
'''11)~11991::1J\pol
I 7i54oE+O~I
Radionuclide of Interest!: ~.Ortitiriiim'-'i

Parent Solution Conc.r. ':Z.30E+03','.1dpm/ml
of:
-~\-.:'/
>''. . . \~_;,_:,-:,,.:. . . .. ,
.I
,_._..,_,:,_

Vol. Parent Solution: ;:<.<:Ao;oooo ml

Total Activity: . 2.2999E+04 dpm
Final Volume: ;-:-:;. .'':':::_:-:.':1.0.00~00 mi
2.2999E+01ldpmlml

NOTES:
('
1'-~~ _j
r-
Recertified
QCApproval
~"'~-=,L"".;JDtt NIAA
Expiration Date:!
Date:
Date:
Date:
'
March 4, 2014
3/21/2013 0:00
j~t l'3~{:w\(p

MP~09
Rev.e; 11/01/03
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES OAK RIDGE I

"", ''"',
MP009
CURRENT DATE ..
RadionuclideU"~tioiium<
Reference Date! i
0:001
d1iW199to:bol
Certified Activity .Sf;p~6Et00 ~tCI

Certified Concentration F"".:o:-:;.<->i ~tCI per gram
<
Ampoule ISolutlon Gross,. 9o266.0 Weight, Grams

Empty Ampoule < "4Jl2t8 Weight, Grams
Solution Net . 4.6442 Weight, Grams
Total Activity In Ampoule . 1~0360 ~tCI
IDiilution Instructions:
Dilute to a volume of! <tooo:oo :. ]milliliters
Certified Total Activity of!
'1.0360I~CI
Which Eauals I
2:300E+oeldpm at the date listed above
And after dilution the activity of this solution Is I2.300E+o3ldpmfml

reference date listed above. All activities are corrected
to tho date and time of analysis by 1he laboratory data
processfn9 software.
Expiration Date: I
Recertified By
QCApproval
~ ~['
'-~ ~AAJ
Date:
"\
Date:
~
"March 4, 2014 I
3121/2013 0:00
"f~LcJ
I
Jh-8
CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION
Radionuclide:
Th-232
Half Life: . (1.405 0.006) x 10'10 years
Catalog No.:
7232
Source No.:
435-104-2
b. Chemical form:
c. Carrier content:
d. Density:
TMAEBERLINE
Customer:
VH1632
P.O.No.:
November 1 1993.
12:00 PST.
Reference Date:
Contained Radioactivity:
(Th-232) 0.0933
,c;.
(Th-232) 3.45
kBq.
I !.9712 g (iri a 10 mJ flame sealed ampoule)
Th(N03)4 iri water

None added
APProx. l. 21
g/ml@ 20C.
None detected (other than daughters).
Radioimpurities
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212, Po-212, Tl-208 .
(Th-232) 0.00779
p.Ci/g.
Activity calculations are based upon known specific activity and mass.
a. Systematic uncertairity in instrument calibration:
b. Random uncertainty in assay:
c. Rlmdom uncertainty in weighing(s):.
3.0%
0.0%
2.0%
3.6%
NIST Traceability
This calibration is implicitly traceable to the Nationallnstitute of Standards and Technology.
Leak Test(s)
Notes
1. Nuclear da~ :~e~ .iaken from n"rabte. Of' Radioactive Isotopes"; edited by Virgilua S. ShirtCy, '1986.
2. lPL panicip~tes hi an NIST measurement BSSUrance program lO establish and maintain implicit traceability foe a number of nucli~.
based on the blind assay (and later NIST oerlification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
QUALITY CONTROL
/lfpv, 16- I
1 9 "$
Date Signed
1800 North Keystone Street
818 843 - 7000

MP.009
Rev.8; 1/10/03
Title: Radioaclive Reference standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY

MP009
Certified Acltivilty
Certified Co11centf11tion
G1!2!Zfr2
IDilution Instructions:
per gram
Dilute to a volume ofli'WNtOOo:oo:,!'?lmllllllters
ICEtrtil~ed Total Activity ofl'
.co:o933I11Ci
Which Eauals 1: ;: ..:2.07:tE+o5ldpm at the date listed above
And after dilution the ar;tivity of this ~;olutlon i~>l'2;071E+:o2ldpm/ml
This activity ccncentralion Is based on tile original

to tile date and time of analysis by tile laboratory data
Expiration Date:
Date:
I,. Octoller9,'2013 I
10/9/2012 O:oo
----'==-""'-==
(EBERI,.._{bl_~ I QUALITY CONTROL PROGRAM

MP-009
~~RVICE$
Rev.8; 1110/03
TIUe: Radioactive Reference Standarde Solutions & Records

MP..Q09
Solution Reference #IIPL435'1D+2 .
Half Life, Years
:"'".a.~th I
'1:4o5E"'10l
Datel. 1119/2012 0:00 I

Solution #I '. Th-6b .
I
Half life, Da)!S
5:132E..12I
I . .
Radionuclide of Interest!
Parent Solution Conc.l
22
~&2J2th
z:o7E+oz
..J
Reference Date
I . >1111i1sea.o:ooj
'ldpm/ml
Chemical COI!lf>C!llitlon of Standard Solution
1Th(N03)4 in1%HNQ3
'
. . ..
'I
j1% NitriciAeid
I~
1.C
f!dpm
Vol. Parent
Total
Final
Final ACtivity Concentration:!
.......
1.0356E.+02Idpm/ml

NOTES:
Expiration Date:
Verified & Approved
B~
QCApprovai
~A
v \T
\J
u
-...
l/j""
Date:
Date:
I . October 9, 2013 I
1119/2012 0:00
ll I"'
/1-z._
1
' !!'
Isotope Products
Laboratories
An Eckert & Ziegler Company
lJ,-f(J
24937 Avenue Tibbitts

Valencia, California 91355
Tel 6613091010
Fax 6612578303
ALPHA STANDARD SOLUTION
Th-229
7340 160 years
7229
867-54
Radionuclide:
Half-life:
Catalog No.:
Source No.:
Physical
A.
B.
C.
D.
Description:
Mass of solution:
Chemical form:
Carrier content:
Density:
Customer:
P.O.No.:
Reference Date:
(Th-229 only)
EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST
1.013
J.tCi
37.48
kBq
5.0147 gin 5 ml ftame-sealed ampoule

Th(N03 ) 4 in 0.1 M HN0 3
10~g Th/ml
1.0016 g/ml @ 20C.
Radioimpurities:
None detected (daughters in equilibrium)

Radionuclide Concentration:
0.2020
~Ci/g,
7.474
kBq/g
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in ~Ci/g was determined
using gamma ray spectrometry.

Peak energy used for integration:
193.5 keV
Branching ratio used:
0.0441 gammas per decay
Uncertainty of Measurement:
A. Type A (random) uncertainty:

B. Type B (systematic) uncertainty:
C. Uncertainty in aliquot weighing:
D. Total uncertainty at the 99% confidence level:
0.7%
3.0%
0.0%
3.1%
Notes:
- See reverse side for leak test(s) performed on this source.
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference
Materials (As in NRC Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.
Quality 'Control
Date Signed
IPL Ref. No.:
867-54
- - - - - - - - - - - - - - - - - - IS09001CERriFIED - - - - - - - - - - - - - - - - - Medical Imaging Laboratory

lndustr.ial Gauging Laboratory
24937 Avenue Tibbitts
Valencia, California 91355
~ E !0!.,; R h~t;t!r.i I

MP-009
Rev.S; 1/10/03
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES -OAK RIDGE LABORATORY

MP009
SOLUTION REFERENCE #nPL 867'54 ..-~-. .
Princ1Dal Radionuclide
Half Life, Years
: :~'Tti".l
7.3.ilot=+o3l
CURRENT DATE I .
11/9/2012 0:001
SOLUTION #I '""ThAB.c: >" I
Half Life, Daxs
2.681E+06j
Radionuclide I,:.... #"iii . I

Certified Activity c J:013E+OO f'CI
Certified Concentration ,:..:. . ""
per gram
Reference Datal
::~
<.
111fii2oo2o:ooj
,..c1
Ampoule ISolutlon Gross

Empty Ampoule
Solution Net
Total Activity In Ampoule
8.7752 Weight, Grams

. 3.7591 Weight, Grams
5.0161 Weight, Grams
1.0130 ,..ct
Chemical ComPOSition of Standard Solution
. "I
l""':fn(NQ3)4 irj o,1IVI HN03 :

Dilute to a volume of
Certified Total Activity of
jO.fiVI HN03
I.
< .
1ooo.oo milliliters
1.0130jjlCi
Which Eauals
2;249E+06jdpm at the date listed above

And after dilution the activity of this solution Is 1 2.249E+03jdpmfml reference date listed above. All activities are corrected
Expiration Date:

QC Approval
~
4:~<)!1 AA1) \JA) N
.....__...
Date:
Date:
October 9, 2013
11/9/2012 0:00
ulrz/rz
...
't ;
~EE;!ERL,!NE I QUALITY CONTROL PROGRAM

MP-609
SE:RVI<;CS
Rev. 7; 9/29199
nue: Radioactive Reference stalldal'<ls SOlutions & Recol'<ls

MP-009
Solution Reference #IIPL86J;,s4: . .
Principal Radlonuctide
Half Life, Years
22"Th
7.34oE+o3l
Date I
11/9/2012 0:00 I
---.. Th,18a . I
Solution #I
Half Life, Da:t:s
2.681E+osl
Radionucllde of lnteres1 .~:.

Parent Solution Cone. 2.25E+03 .jdpmlml
Reference Date

ITH<IIIOsJ4 'tri 0.1 M:HN03
> .
>
I ::
.,,1si2oo2o:ool
:. I
jo.1MHNo:
... . ..
.
- . -- 3 ..

Vol. Parent Solution: .... 10.0000 ml

Total ActiVIty: . 2.2490E+04 dpm
Final Volume:
' 1000.00 ml
2.2490E+01ldpmlml

NOTES:
Expiration Date:!
'
~.~
QCApprovai~
"
'-'
October 9, 2013
Date:
11/9/2012 0:00
Date:
!llt&2-I I
j}ational .3Jn!{titute of
~tanbati.l.{
&
~ecbnologp
([erttftcate
.
.'/.
. .
..
::
-_
_,i_!}.;
Standard Reference Material4251C

Barium-13;3 Radioactivity ,Standard
This Standard Referencel'v,fat~rial ,(SRM) consists of radioactive barium-133. cbloride,,llonc!adioactive barium
chloride, and hydrochloric acid dissolved in 5 mL of distilled water. The solution is contain~ ill a flamesealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionizatiori'i:ilambers and
soliq-state gamma-ray,spectrometry.SY~tems.
Radiological Hazard
s:R:M
'a
The
iriopoule contains barium-133 with total activity of approximateiy 2.5 MBq. Barium-133 decays
by electron capture and during tJ:!e decay pro,.,ss X-rays and gan)llla:~ays with l,'nl'rgies from 4. to 400 ke V are
emitted. Most of these photons escape from the SRM ampoule and can represent a radiatirn hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given ill note [a]*.
Appropriate shielding 11ndlor distance shoulq be ~.ed to .l)linimiziO. personnel exposure_, .The .SRM ~hould be
.)"'e<;i only by pyrsons qualified to han<;lie radioactiv~ materiaL

Chemical Hazard
The SRM ampoule ~ntain,s,hydrqch!oric acid (HO) with a con<,:entration pf 1 mole pyr Iiter,,orwater. 'Jhe
solution is corrosive and represents a health hazard if it comes in contact with,eyes or. skin, Jf the ampoule
is to be opened to transfer the solution,.the recommended procedure is given on page 2. The ampoule should
be opyned. ouly by persons qualified to handle both radioactive material and strong a.9id solution.
..
Storage and Handling
-;
The SRM should be stored and used at a temperature between 5 and 65 c. The solution in an unopyned
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the innpoule is a dangerous
good (hazardous materia!) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall techoical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standar<! Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
October 1994
Sll,l4 4251C,p~ge.l.of 6..
Thomas E. Gills, Chief

Standard Reference Materials Program
*Notes and r~ferences_ are_ ':"lll: pages-~ and 6.

QCP-009
Rev.B; 11/10103
ntle: Racfloactive Reference standards Solutions & Records

QCP009-1
SOLUTION
Certified Acltivi1tv If~,

Certified Colnce,ntr.aticm
JDI,Iution Instructions:
Dilute to a volume ofF~:'\::J.OOO:OO{A'':imtfllllters
Certified Total Activity of!
66.5577hCi
Which Eauals
L 1A78E+ll8!dpm at the date listed above
And after dilution the activity of this solution isi1.478E+05Idpm/ml

reference date listed above. All actiVities are corrected
tothedateandlimeof analysis by the laboratory data
Expiration Date: I Septenil:ler 20;>2013J
Date: ---':::..::.!.'-!!:.-9127/12
Date:
----'"1-'/
'l-::.'1-'11.;.;'Z:;;__
J;:J,E!J;;_F;l Ll N
e:
~ICE&

QCP-009
Rev.6; 11/10/03
TIUe: Radioactive ReferencE~ Standards Solutions & Reeords

QCP.0091A
Solution Reference #INISTSRM4251C '
Princioal Radionuclide
Half Life, Years
I
j . 1.04SE+01l
9/20/12
1
'Ba"6a
I
Half Life, Da~s
I
.
3.828E+03I
Date!
Solution#!
.. ,,.sa .
Radionuclide of lnteresj : '!ilea

Parent Solution Cone. .. l.48E1-05 : dpm/ml
Reference Date!
Chemical Comeosition of Standard Solution

.-. '
jl~BaCI,in 1M Hcl ..
. .: . < S/1/1993 o:ool
j1MHCI
-.-,
.... "':
,,

Vol. Parent Solution: .. ... '25:0000 ml
Total Activity:
3.6950E+06. dpm
Final Volume: ,:-:: '1000:00 ml
3.8950E+03ldpm/ml

NOTES:
Expiration Date: September 20, 2013
'
oc Approval
:-'SaJtA..J~1A
.~
\....) "
Date:
9/27112
Date:
'l{z.'1[rz..
Radionuclide:
Half Life:
Catalog No.:
Source No.:
Ra-226
1600 7 years
7226
453-26
b. Chemical fonn:
c. Carrier content:
d. Density:
Customer:
TMA EBERLlNE
VH1888
P,O.No.:
12:00 PST.
Reference Date:
February 1 1994
Contained Radioactivity: (Ra-226) 1.001 JCi.
Contained Radioactivity: (Ra-226)
37.0 kBq.
5.1864 g (in a 5 ml Flame Sealed Ampoule).

Ra(N03)2 in 1 N HN03
None added
1.0318
Radioimpurities
gtml2oc.
None delecied(other than daughters)
Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.
(Ra-221\)
0.1929
~Ci/g.
Weighed aliquots of the solution were assayed using gannna spectrometry:
Energy peak(s) integraied IIDder: 186 keV.
Branching ratio(s) used:
0.0351
gamma rays per decay.
a. Systematic IJDcertainty in instrument calibration:
b. Random nncertainty in assay:
c. Random uncertainty in weighing(s):
d. TotalllDcertainty at the 99% confidence level:
3.4%
3.1%
0.2%
.4.6%.
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)

Notes
1. Nuclear data wore _takCn "from "Table of Radioa~ve lsotopCs", edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement 8ssurance program to establish and maintain implicit traceability for a num~r of nuclides,
-oased on-tlftfl)liiiini8Bii)'(ii:Dd.1litef N1ST-certifil;fiiti0ii)""Of'S1iiH1800 ReteteilC(fMiiteriiilS\AHii NRC ltegmaroryGmde-4; fS); .... - ---
QUALITY CONTROL
fiA..
Ewbank, California 91504
818 843 -7000
'I
199/f
Date Signed
~EE;IERLINE I

MP009
SERVIC~~
Rev.S; 11/01/03
Title: Radioactive Reference Standard Solutions & Records

MP009
. 11/9/2012 0:001
CURRENT DATE!
SOLUTION #I : . "Ra~s; . I
I
Half Life, Da~
5.844e+osl
SOLUTION REFERENCE #IIPL453-26 ..

Prlnciflal Radionuclide
Half Life, Years
2
' " ~Radiuin 1
(aooe+osl
I
Reference Date I
Radionuclide }~."R~diurrr"
Certified Activity >1 :o.o.1
..CI
Certified Concentration I ....... ~tCi per gram
e+oo
... , .. , 21111s94
o:oo I
..
. . .. : .. Weight, Grams
~ -~~~~~r~
.
Weight, Grams
Am,.., Empty
,...... Ampoule .
Solution Net
Total Activity in Ampoule
1.0010
Chemical Comeositlon of Standard

Solution
..
j~Ra(N03J2injMHNo 3
-,_-:::,
~tCI
Dilute to a volume otl . '1000:00 .

Certified Total Activity otl, 1;001 Ol~tCI
j1MHN03
.I
'
Imilliliters
Which Eauals
. 2.222E+06Idpm at the date listed above
And after dilution the activity of this solution lsi 2.222E+03Idpmlml

Expiration Date:

QCApproval
J::atj;J
L
-l0
November 9, 2013
11/912012
Date:
Date:
rr
J,z..LIZ_
~E:_E:R!.,INE
I QUALITYCONTROLPROGRAM
~
ecRvoco:s.
MP 009
Rev.8; 11/01/03
T!tie:
Radioacffve Reference Standards Solutions & Records

IDilutictn Instructions:
Dilution Solve.nt Used

NOTES:
Final Activity Concentration:k :..)<1.4440E+01ldpmlml

Expiration Date: November 9, 20131
Date:
Date:
''
1119/2012 0:00
frz./,z_
I
RA-\\
ANALYTICS
1380 Seaboard Industrial Blvd.

Atlanta, Georgia 30318 U.S.A.
Phone (404) 352-8677
Fax (404) 352-2837
Standard Radionuclide Source
62680-416
Ra-228 5 mL Liquid in Flame Sealed Vial
This
standard
radionuclide
source
was
prepared
gravimetrically from a calibrated master solution.
The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
CALIBRATION DATE:
Ra-228
2.585 E3
5.75 years
November 7, 2001 12:00 EST
TOTAL UNCERTAINTY*:
4.0%
ACTIVITY (dps) :
HALF-LIFE:
SYSTEMATIC:
RANDOM:
3.0%
1. 0%
*99% Confidence Level

Impurities: y-impurities (other than decay products) <0.1%
5.07198 grams 0.1M HCl solution with 50
P 0 NUMBER
~g/g
Ba carrier.
9508, Item 1 (Part #4339A)
SOURCE PREPARED BY:
Q A APPROVED:
":,~m'"'

MP-009
Rev.a; 1/10/03
TIUe: Radioactive Reference Standards Solutions & Records

RECERTIFICATION
MP009
SOLUTION
Certified Activity
Certified Concentration
IDilution Instructions:
Dilute to a volume ofl:tf~;.';Wii!OO;'Ol):\\fiiilmllllllters
Which Eauals
I: c:".fi1 ;SStE+o5ldpm at the date listed above
And after dilution the activity of this solution lsF4i"551E+J)2!dpmfml

Expiration Date:!> /Aptil12i'-20.13::<
-~~
Date: _ _...;:4::..11~6::..11:.::2:-_
Date:-------
Z--;;;_
Date: --<4'-1-/..._ffe""/u..I...
SECTION VI
QUALITY CONTROL SAMPLE RESULTS SUMMARY
Eberline Services
Analysis Control Chart
Printed: 4/29/2013 2:14PM

Page 1 of2
Wo
Analysis
Run
Activity Units
13-04105
UUISO
pCi
Ali uot Units
Client Name
Laboratory Control Sample

Analyte
N~rmalized
Difference
LCS
Measured
I
I
CSU
Measured
'
!
1
LCS
Expected
Uncert.
Expected
Known
Known
Error
Result
CSU
standard
ID
7.93E+OO
1.17E+OO
U-Sa
7.57E+OO
1.12E+OO
U-Sa
[3.44E+01l3.60E+OO I 5.13E-01
Standard
ACT (dpm)
Standard
Error
Standard
Added (g)
U-234
0.36
97.36%
14.71%
I 100.00%
U-23S
0.64
95.30%
14.SO%
I 100.00%
~---~~~~;.,
3.60%
r-,
18.15E+OO . 2.93E-01
7.94E+OO
I 2.86E-01
3.52E+01
3.60E+OO
5.13E-01
Matrix Spike
Analyte
Nonnalized
Difference
-+
Expected
MS Result
!
I
Expected
MS Uncert
Sample
Result
Sample
CSU
, Nonnalized
I Difference
Standard
ACT (dpm)
it:!!!lt
~~~'
RPD
Original
Result
Original
csu
Replicate
Result
Replicate
csu
LCS R_eJative
BiaS
LCS%R
LCSND
MS%R
MSND
Ull
RepRPD
RepND
NA
OK
OK
U-234
0.73
9.10
3.20E+OO
5.5SE-01
2.92E+OO
4.93E-01
0.97
OK
OK
U-23S
1.S4
24.95
2.47E+OO
4.5SE-01
1.92E+OO
3.62E-01
0.95
OK
OK
NA
U-235
0.71
29.73
1.45E-01 I 9.31E-02
1.95E-01
1.03E-01
OK
OK
NA
Version
Standard
Added (g)
QCSummary
ti:l
Standard
Error%
l-----+-------+-------+---------------+-------+ ------+-----+--------l
Replicate Sample
Analyte
Standard
ID
OK
Eberline Services
Printed: 4/29/2013 2:14PM

Page 2 of 2
Analysis
Activity .ld!:li~-~
UUISO
pCi
______
--~ ________ __6!!9_!:!t_l!!:!~s
Client Nam'!:.
Replicate Sample RPD
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
-------~------1
25.00
20 00
90.00
15.00
J.-----------
80.00
10.00
10 oo
,,,.
U-~~
U-238
Lower Error
Upper Error
79.05
115.68
%R
76.90
113.70
95.30
80
100
120
~-
80
100
120
LCL
Mean
UCL
----
5.00
0.00 +-----~c=-,-------,-----=
UL;j4
u-238
27.28
9.89
E~c
~'~
CL
'""
0.0<
9.10
""
24.
--
':'.'
_,
Normalized Difference
~-------------
3.00
2.50
+-------------------------+------------------------------
2.00
+---
1.50
1.00
0.00
l.'
10~1
~~
l,l'l
1:'.11
U-:2~
I
r-
U-238
UCL
Version
,---
+--------------i
+---------------i
0.501
~---
No Matrix Spike
3.50
0
L':C:::S::N;;;Dc---0.36
0.64
o.Oo
3
REP ND
MS NO
0.73
1.84
0.00
- O.OC
3
O.OC
U-235
38.32
21.15
29.73
35
--
Eberline Services
Printed: 5/1/201310:08 AM
Page 1 of2
wo
-Aillilfysis
Ruo
Activi~ Units
13-04105
ThiSO
pCi
~uotUnits
Client Name

Normalized
Difference
Analyte
LCS
Measured
csu
Measured
LCS
Expected
Uncert.
Expected
8.03E-01
5.49E+OO
1.48E-01
4.36E+OO
8.64E-01
Th-1b
2.35E+01
2.70E+OO
5.18E-01
4.80E+OO
1.73E-01
5.17E+OO
8.96E-01
Th-8b
1.04E+02
3.60E+OO
1.03E-01
100.00%
3.60%
I 4.80E+oo
TH-230
2.53
79.52%
19.79%
100.00%
2.70%
Em"
17.31%
100.00%
3.60%
Standard
Added (g)
4.46E+OO
18.03%
107.69%
Standard
Error
1.73E-01
92.72%
0.80
Standard
ACT(dpm)
II
0.84
TH-232
Standard
csu
TH-228
Known
Result
Known
ID
Th-8b
I 1.04E+02
3.60E+OO 11.03E-01
Matrix Spike
Anafyte
Expected
MS Uncert
Normalized
Difference
Actual
MSResult
Sample
Result
Sample
QCSummary
Replicate Sample
l<lU
~
!..)'1
1\'...Ji,
3.15E-01
1.35E-01
0.93
OK
1.11E-01
1.64E-01
9.41E-02
0.80
7.10E-02
1.16E-01
7.74E-02
1.08
Replicate
Result
34.83
2.21E-01
1.09E-01
0.79
30.21
2.23E-01
0.69
38.12
7.88E-02
1.06
TH-230
TH-232
Version
LCS%R
csu
TH-228
II
LCS Relative
Bias
Original
RPD
csu
Original
Result
Normalized
Difference
Analyte
Standard
Added(g)
csu
Replicate
LCSND
M5%R
RepRPD
RepND
OK
NA
OK
OK
OK
NA
OK
OK
OK
NA
OK
MSND
Eberline Services
Printed: 5111201310:08 AM
Page 2 of 2
Wo
AnalYSiS
Roo
Activity Units
13-04105
ThiSO
pCi
AliQUOt Units
Client Name
120.00
40.00
- - - - - - - - - - - - - - -+UCL
35.00
110.00
30.00
100.00
20.00
lower Error
UJ?:J?:Br Error
%R
LCL
Mean
UCL
15.00
------r-------LCL
80.00
---
1l.- -----
25.00
90.00
70.00
_t ______ i
LCS % Recovery
130.00
l
TH-228
71.09
114.36
92.72
80
100
120
TH-230
57.03
102.01
79.52
80
100
120
10.00
5.00
TH-232
86.78
128.60
107.69
80
100
120
o.oot---~==----,-----c;;c-;;:;::-----,----==:----,
TH-228
I
TH-230
I
TH-232
I
42.76
38.22
I
52.64
lowerError
26.91
22.20
I
23.60
Uooer Error
30.21
38-.12
34.83
RPD
35
35
35
CL
3.50~--------------------------
3.00
2.50
+--------------------------t-------r--r--------------------
+-----1
1.50 +-----1
2.00
1.00
0.50
0.00
S~1
til
n'~~~
Version
+-----l
No Matrix Spike
Eberline Services
Printed: 5/212013 10:07 AM

Page 1 of2
wo
Analysfs
13-04105
Ra226
"""
Activltv Units
Aliquot Units
pCi
Client Name

Analyte
RA-226
Normalized
Difference
0.09
I
I
LCS
Measured
I1
CSU
Measured
LCS
Expected
Uncert.
Expected
101.12%
23.90%
100.00%
4.60%
Known
1.02E+01
Kno=--1
Result
CSU
Error
4.71E-01
I 1.04E+01
Standard
10
Standard
ACT (dpm)
2.47E+OO
Ra-5b
4.41E+01
Sample
Aliquot
Standard
Standard
ACT(dpm)
Standard
Error
I 4.60E+OO
Standard
Added (g)
I 5.16E-01
Matrix Spike
Analyte
Nonnalized
Difference
MSActual
%Rec
Exp"""'
MSResult
Expected
MSUncert
Actual
MSResult
Actual
MSCSU
Sample
Resuh
Sample
csu
RA-226
~i!l
til
w....~
Version
Nonnalized
Difference
RPD
0.32
6.44
Original
Result
Standard
Error%
Standard
Added(g)
RepRPD
RepND
OK
OK
QCSummary
Replicate Sample
Analyte
ID
Original
csu
2.80E+OO I 7.95E-01
Replicate
Result
Replicate
csu
LCS Relative
Bias
LCS%R
LCSND
2.63E+OO
7.41E-01
1.01
OK
OK
MS%R
MSND
Printed: 5/21201310:07 AM
Eberline Services
Page 2 of 2
wo
Analysis
Run
Activity Units
13-04105
Ra226
pCi
Al.~_uot
Units
Client Name
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
25.00
20.00
90.00
15.00
80.00
10.00
1o.oo
RA-226
lower Error
Upper Error
129.62
%R
101.12
ooo
RA-226
72.62
80
100
120
LCL
---Mean
UCL
5.00
1
-
Lower Error
UPPer Error
RPD
-Cl
7.36
5.53
6.44
35
3.50,-------------------------
s.ooj----2.50+------------------------2.00+------------------------1.50
+---------------------------
1.00+------------------------0.50+-------------------------
aw
ll'l
t..
Version
No Matrix Spike
Eberline Services
Printed: 5/9/2013 2:27PM

Page 1 of2
wo
Aria-lysis
R""
Activity Units
13-04105
Ra228
pCi
AliB_L,!OI
U~its
Client Name

Analyte
RA-228
Nonnalized
Difference
1--
csu
LCS
Measured
110.59%
o.75
I
'
Measured
LCS
Expected
24.93%
100.00%
I
'
Uncert.
Expected
Known
5.10%
8.96E+OO
Known
Error
4.57E-01
Result
I 9.90E+OO
csu
Standard
10
2.47E+OO
Ra-11
3.90E+01
sample
Aliquot
Standard
Standard
ACT(dpm)
Standard
ACT (dpm)
Standard
Error
I 5.10E+OO
Standard
Added {g)
5.10E01
Matrix Spike
Ana/yte
NomJalized
Difference
MSActua/
%Rec
Exp.cr.d
Expected
Actual
MS Result
MS Uncert
MSResult
Actual
MSCSU
Sample
Result
Sample
csu
RA-228
~il
1!:!~
IJl
tl1
Version
Normalized
Difference
RPD
0.46
22.08
Original
Standard
Error%
Standard
Added(g)
RepRPD
RepND
NA
OK
QCSummary
Replicate Sample
Analyte
ID
Original
Result
csu
7.14E-01
5.63E01
Replicate
Result
csu
LCS Relative
Bias
LCS%R
LCSND
8.91E-01
S.OOE-01
1.11
OK
OK
Replicate
MS%R
MSND
Printed: 5/9/2013 2:27PM
Eberline Services
Page 2 of 2
wo
Analysis
Ron
Activitv Units
13-04105
Ra228
pCi
AliQuot Units
Client Name
: Engineering Management Support, Inc.
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
25.00
20.00
90.00
15.00
80.00
10.00
7o.oo
RA-228
lower Error
Upper Error
%R
80.56
140.63
110.59
-lCl
Mean
UCL
80
100
120
5.00
o.oo
-
__:-____l:!P.per Error
RA-228
lower Error I
RPD
29.40
14.76
22.08
3.50.,--------------------------3.00
----------------
2.50+-------------------------2.00+------------------------1.50 +---------------~-----------
G:u
~.!It
tJ1
Version
No Matrix Spike
SECTION VII
LABORATORY TECHNICIAN'S NOTES
tllli!57
ISOUNOTES
Printed: 4/24/2013 12:22 PM
Page 1 of 1
}!J ~B~R.bJ_N I;:

~

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com
SERVICES
Work Order Analysis Notes
Date
04/24/13 12:22
Dept
PREP
User
JBARNARO
Internal Work Order
Analysis Code
Run Number
13-04105
UUISO
1
Notes
ALIQUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
Printed: 4/26/2013 5:24 PM
~
#
Page 1 of 1
~. 1=)_1;;_R_h-~~c~
Date
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04105
UUISO
1
Dept
User
04/24/13 12:22
PREP
JBARNARO
AU QUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
Notes
04/26/13 17:24
CHEM
JDEMELAS
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 mi8N HCl; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCl, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI- 0.1 N NH4l, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCl; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
Printed: 4/29/2013 7:11AM
Page 1 of 1

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Date
Dept
User
lntemat Work Order

Analysis Code
Run Number
13-04105
UUISO
1
Notes
04/24/13 12:22
PREP
JBARNARD
ALIQUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
04/26/13 17:24
CHEM
JDEMELAS
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 mi8N HCl; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI- 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of O.SN HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
04/29/13 07:11
CHEM
RMARTZ
ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET
SIT IN ICE BATH FOR ONE HOUR. SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.
Eberline Analytical
Printed: 4/29/2013 7:11AM

Page 1 of 1
Internal Work Order
SERVICES
Analysis Code
Run
UUISO
Reagents Used in an Analysis
Reagent
ID
13-04105
E a w;;;::_RL t!'-1 E
Reagent
Concentration
Reagent
Name
1
Analyst
ID
Date
Recorded
013624P
Nitric Acid
Reagent Grade
JBARNARD
4/24/2013 I
013666P
Anion Exchange Resin
Reagent Grade
JDEMELAS
4/26/2013
013794S
HCI - HF
6.5N - 0.04N
JDEMELAS
4/26/2013
013675001
Hydrochloric Acid
O.SN
JDEMELAS
013791S
Hydrochloric Acid
013675P
Hydrochloric Acid
0138025
SN
JDEMELAS
4/26/2013
-4/26/2013
Reagent Grade
JDEMELAS
14/26/2013
HCI- NH41
SN - 0.1M
JDEMELAS
4/26/2013
0137345
Hydrochloric Acid
6.5N
JDEMELA5
4/26/2013
0132465
Carbon substrate
Solution
RMARTZ
4/29/2013
012809P
Ethyl Alcohol
Reagent Grade
RMARTZ
4/29/2013
013221P
Hydrofluoric Acid
Reagent Grade
RMARTZ
4/29/2013
0131915
Neodymium Carrier
1 mg/ml
RMARTZ
4/29/2013
013434P
Titanous Chloride
Reagent Grade
RMARTZ
4/29/2013
--
---
,,,-_
~.
'
..... \ ,..._
. ..
..
--
--
:-
--
- -- -
-- -- -
- -
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--
--
II
~frd
(l---&~ . _,.,- !-&.
~- fl o-r F'
i
I
12
c:?,df/1
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7
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nr-.........
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lfrt6
l,A'/
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uI
<1 I'2.1. rf) 'I~ s...t.. VV\._'b" "' ~
L/i/J,u!
ltd
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lA?
-~~<.:u l
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l.
ISOTHNOTES
Page 1 of 1
Printed: 4/24/2013 12:22 PM
j!P E;J? E:: FL'=J 1'-l_E::

~
SERVICES
#
1
Date
Dept
04/24/1312:22
PREP
User
JBARNARO

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04105
ThiSO
1
Notes
AU QUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
Page 1 of 1
Printed: 4/29/2013 6:11PM
~
E: E:J E:: .R L.. I Ni:::;
~

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865:481.0683
SERVICES
User
lntemal Work Order
13-04105
Analysis Code
Run Number
Date
Dept
04/24/13 12:22
PREP
JBARNARD
ALIQUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS~ ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
04/29/13 18:11
CHEM
JDEMELAS
Added concentrated HN03 to sample beakers and heated to dryness; Added 20 ml 8N HN03 to samples and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with so ml SN HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml SN HN03; Centrifuged rinsates and loaded onto columns: Rinsed columns with 40 ml SN HN03; Eluted
Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15ml. Set samples aside for later nrecinitation and filterinn.
Notes
!Y-68
Printed: 4/30/2013 5:38AM
Page 1 of 1

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Date
Dept
User
!
I
Internal Work Order
Analysis Code
Run Number
13-04105
ThiSO
1
Notes
ALl QUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
"" "-t -Ada-ecTconcentrated-HN03tosamp'ie-beake;:sand-fieatecTto-dr~/ness;Aaaea:zamiaN-Hr;k:>-3tosam-p'ies"an;T
04/30/13
OSSB-
CHEM
RMARTZ
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; Eluted
Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15m I. Set samples aside for later pre!pitation and filtering.
ADDED 0.75 ML 0.1MG/ML CERIUM CARRIER & 1 ML HF TO C-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOl & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES FROM C- TUBES,
REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.
Eberline Analytical
Printed: 4/30/2013 5:39AM

Page 1 of 1
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RA-226 NOTES
Printed: 4/24/2013 12:21 PM
Page 1 of 1
}!J!;::: .:;u;:;~_BJ,..JN E:
~
SERVICES
Date
Dept
04/24/13 12:21
PREP
User
JBARNARD

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04105
Ra226
1
Notes
ALIQUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSDRIED FRACTION 6 DOWN AND DIGESTED DUE TO SAMPLE BEING DIRTY PH'D SAMPLES
PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND
CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS
t\Hi175
Printed: 4/30/2013 1:36PM
~
#
Page 1 of 1
E;__B 1;;;--~--b~-~c-~
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Date
04124113 12:21
04130113 13:36
--
''
'
Dept
User
PREP
JBARNARD
CHEM
TSMITH
'
13-04105
Internal Work Order
Ra226
Analysis Code
Run Number
I'
-----
Notes
ALIQUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSDRIED FRACTION 6 DOWN AND DIGESTED DUE TO SAMPLE BEING DIRTY- PH'D SAMPLESPRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND
--Followed steps 12.1 to 12.8 in AP-006 rev. 12. { Sringe filtered samples. Precipitated and filtered sam piSs,
obtained final weights, and took to count room )
Printed: 5/1/2013 10:51 AM

Page 1 of 1
Eberline Analytical
13-04105
}!JEBERLINE
SERVICES
Ra226
013575P
Ammonium Sulfate
Reagent Grade
JBARNARO
4/24/2013
012766014
Barium Carrier
1 mg/ml
JBARNARO
4/24/2013
012729007
Lead Carrier
166 mg/ml
JBARNARO
4/24/2013
013624P
Nitric Acid
Reagent Grade
JBARNARO
4/24/2013
013416P
Perchloric Acid
Reagent Grade
JBARNARO
4/24/2013
009098P
Sulfuric Acid
Reagent Grade
JBARNARO
4/24/2013
013788S
EOTA
0.25M
TSMITH
4/26/2013
011383P
Acetic Acid
Reagent Grade
TSMITH
4/30/2013
013751001
Ammonium Sulfate
200 mg/ml
TSMITH
4/30/2013
'
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RA-228 NOTES
GtiH31
Printed: 4/24/2013 12:21 PM
~
#
1
Page 1 of 1
~--~-t;;;B_hl-~c~
Date
04124/13 12:21
Dept
PREP
User
JBARNARD
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04105
Ra228
1
Notes
ALIQUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSDRIED FRACTION 6 DOWN AND DIGESTED DUE TO SAMPLE BEING DIRTY- PH'D SAMPLESPRECIPITATED WITH BAAND PB CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND
"\":::)
1 ~~~
Printed: 5/8/2013 7:41 PM
Page 1 of 1
j!J EE:IE:RLINE
~
SERVICES
Internal Work Order
Analysis Code
Run Number
13-04105
Ra228
1
Notes
Date
Dept
04/24/13 12:21
PREP
JBARNARD
04/26/13 11:44
CHEM
TSMITH
05/02/13 13:12
PREP
LWALKER
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
05/08/13 19:41
PREP
LWALKER
FOLLOWED STEPS 12.1 TO 12.7 IN AP-007 REV 17 (CHEMICAL CLEANUP FOR RA 228)
User

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
AU QUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSDRIED FRACTION 6 DOWN AND DIGESTED DUE TO SAMPLE BEING DIRTY- PH'D SAMPLESPRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND
Dissolved samples from prep in EDTA.
Page 1 of 1
Printed: 5/9/2013 8:07AM
~ E a 1::~ biN 1::::

S!O:RVIC!O:S

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
lntemal Work Order
Analysis Code
Run Number
13-04105
Ra228
1
Notes
Date
Dept
04/24/13 12:21
PREP
JBARNARD
04/26/13 11 :44
CHEM
TSMITH
05/02/13 13:12
PREP
LWALKER
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
05/08/13 19:41
PREP
LWALKER
FOLLOWED STEPS 12.1 TO 12.71N AP-007 REV 17 (CHEMICAL CLEANUP FOR RA 228)
05/09/13 08:07
CHEM
TSMITH
Followed steps 12.7 to 12.15 in AP-007 rev. 17. (Precipitated samples, hot bathed, centrifuged, and
discarded svpernate. Dissolved precip, precipitated samples, hot bathed, centrifuged, and discarded
supernate. Dissolved precip, precipitated and filtered samples, obtained final weights, covered with aluminum
foil and took to count roo~
User
ALIQUOTED AND FILTERED SAMPLES FOR DISSOLVED FRACTIONS- ADDEo SPIKES AND TRACERSDRIED FRACTION 6 DOWN AND DIGESTED DUE TO SAMPLE BEING DIRTY- PH'D SAMPLESPRECIPITATED WITH BAAND PB CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND
Dissolved samples from prep in EDTA
tiHll84
Eberline Analytical
Printed:
5/9/2Ql~
8:55AM
Page 1 of 1
I(
Internal Work Order
13-04105
~~J:JERLINE
SERVICES
I
I
. Analysis Code
Ra228
R~n
1
.
Reagent
ID
--
Reagent
Name
Reagent
Concentration
Analyst
.
10
Date
___ Recorded
013376P
Ammonium Hydroxide
Reagent Grade
JBARNARO
4/24/2013
013575001
Ammonium Sulfate
200 mg/ml
JBARNARO
4/24/2013
012766014
Barium Carrier
1 mgjml
JBARNARO
4/24/2013
012729007
Lead Carrier
166 mg/ml
JBARNARO
4/24/2013
013624P
Nitric Acid
Reagent Grade
JBARNARO
4/24/2013
013416P
Perchloric Acid
Reagent Grade
JBARNARO
4/24/2013
009098P
Sulfuric Acid
Reagent Grade
JBARNARO
4/24/2013
011504022
Ammonium Sulfide
2%
LWALKER
5/8/2013
012729008
Lead Carrier
1.5 mg/ml
LWALKER
5/8/2013
013797P
Nitric Acid
Reagent Grade
LWALKER
5/8/2013
013690S
Sodium Hydroxide
10M
LWALKER
5/8/2013
013801S
Yttrium Carrier
9 mgjml
LWALKER
5/8/2013
012717004
Ammonium Oxalate
5%
TSMITH
5/9/2013
013624003
Nitric Acid
1N
TSMITH
5/9/2013
013686S
Nitric Acid
6N
TSMITH
5/9/2013
013690S
Sodium Hydroxide
10M
TSMITH
5/9/2013
Sodium Hydroxide
18M
TSMITH
5/9/2013
~13065004
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SECTION VIII
ANALYTICAL DATA (ISOTOPIC URANIUM)
Eberline Services
Analysis Sheet
13-04105
Printed: 4/29/2013 7:11AM

Page 1 of 3
UUISO
Run 1
Work Order
Sample
Desc
Analysis Code
01
~ LCS
Run
02
MBL
Client
ID
Login
CPM
Sample
Date
Sample
Aliquot
i ~0~4~ 6/~~00:00_ __1_:_0~00~0~E+OO
LCS __
BLANK
04/16/13 00:00
1.0000E+OO
39
04/09/13 09:30
1.0000E+OO
39
04/09/13 09:30---
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Date Received
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5/7f2013
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42
. 04/09.
!~3__11 05.
_2_:_0~?~E+O~
42
04/09/13 11:05
1.0000E+OO
_:j-04ffi9/1312:0o -
1.0000E+OO
__
1
i
04/09/13 10'44
1.0000E+OO
+_
D-87 DIS
WA
10
TRG
PZ-106-SDTOT
1
37
TRG ;
PZ-106-SDDIS
37
--o4to9t1312:o~~r-1.ooooE+oo
46 -
46
04/09/1312:27
'
1.0000E+OO
11
-- 12
T~G .. ------__ -~~82 TOT
13
' TRG
15
TRG
16
! TRG .
17
TRG--t
S-82 DIS
o4to~~~7 J.~~~1~oooo8oo
U-1 Oa
---------1
-
TracerAct(dpmlg)
19.094
-Carrier - -
1------
1.0000E+OO
--- --,
1-68 TO~
_D--~7 TOT
04/09/13 09:30
TRG
U-232
Radiometric Sol#
--
----
'
09
lnstru~~ Type ---AI~ha spe~~roscopy
1-c-a-rr-ie-rc_o_n_c-(m_g_tm_l_l
TRG I
TRG:
39
-
-NAsNs-3o5oModified
Radiometric Tracer
-;~0-000E+OO
--
------
TRG
----
PZ-204-SS DIS
We~t_Lake OU-1
P-z~204-SS TOT
DO
---
----~-----
P~lect
PZ-204-SS TOT
--~---
--
PZ-106-SS DIS
'
41
04/09/1312:56
1.0000E+OO
1-9 TOT
'
43
04/09/13 13:35 !
1.000QE.;:"oo!
1-9 DIS
--
43
- 04/09/1313:35
40
04/09/13 14:28
1.0000E+OO
---~-------
-------
19
---
TRG
-~----:-
D-93 DIS
-
--
1.0000E+001
--~----1
1:!~
~
til
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
13-04105
Printed: 4/29/2013 7:11AM

Page 2 of 3
UUISO
Run 1
Internal
Fraction
01
Sample
Desc
Tracer
Aliquot(g)
Lcs
0.6088
Tracer Total
ACT(dpm)
-11.6
Radiometric
Tracer (pCi)
'I
: -~:~ ::: .. ::: '
,,.,:L
03
04
! DO
o7 --~
08
TRG
1
~-~~~: 1----;~~0.6007
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I
0.6002-
TRG
TRG
::1
____,__
I
I
-~--
Grav Filter
Final (g)
i ----.... -+
1
_
_
Grav Filter
Net(g)
__l
---
Grav
%Rec
Mean
%Rec
SAF
1*
f--
----
:: rG L~
tOt
t!!!i
SAF
2.
f- ---
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11.4 ,
11.5[_ - - -
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m
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j
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nn"
14
o.ool
'
Grav Filter
Tare (g)
Radiometric I Grav Carrier

% Rec
Added (ml)
Eberline Services
Analysis Sheet
13-04105
Printed: 4/29/2013 7:11AM

Page 3 of 3
UUISO
Run 1
01
I
Rough Prep
Sample
Desc
Internal
Fraction
LCS
02__ )--MBL 1----
~:-
' DUP
04
1----
DO
Rough Prep
By
Date
08
: :
,_11
12
04/24/13 12:02
I
I JBARNARD I
JBARN.ARD'
I 04/24/13 12:02
--
Sep t1
Date/Time
..
-I
I----~
'
JBARNARD
Sep t1
By
--
'
--
--~--
___ L_~-
\lARD
-
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04/24/13 12:02
j_
i JBARNARD
::::: :::: ~:::::1--------+-_-.
T~G_--------~-+---1-~~/24/13--1~:~-~ARNARD
-+--- '
:
I
~;G
04/24/1312:02 JBARNARD
~-F
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~~
-1
I
I
-~24/131;o;tJ-BARNARor-
___j_ 04/24/1312:0~-1
JBARNARD
..----_1I:~:::::::: 1~:::::
:: I :::
,_1_9--~--!-T-RG
Sep to
By
04/24/13 12:02 JBAR~-~A:RtD

'
04/24/13 12:02 ! JBARNARD
TRG
Sep to
Date/Time
---------+04/24/1312:02 I JBARN~RD
_.
TRG
'
=t~ 04/24/131~:02
05 ___ TRG
06
TRG
07
Prep
By
Prep
Date
+---+----J
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pCi/1
7.93E+OO
1.02E+OO
8.42E-02
-~--LMBL
BLANK
pCi/1
2.34E-02
3.80E-02
6.53E-02
DUP
PZ-204-SS TOT
pCi/1
2.92E+OO
4.47E-01
7.58E-02
DO
PZ-204-SS TOT
pCi/1
3.20E+OO
5.09E-01
5.70E-02
OK
PZ-204-SS DIS
pCi/1
3.50E+OO
5.12E01 1
S.SOE-02
OK
01
U-234
02
U-234
03
U-234
04
U-234
LCS
_________ L~--
+---I
=t~
Results
Error Estimate
MDA
LCS
Known
8.15E+OO
LCS
%R
LCS
Flag
97.36
OK
RPD
MDA
Blank
Flag
Flag
Flag
OK
OK
NA
OK
-
1-68 TOT
pCi/1
2.73E+OO
S.SSE-01
1.02E-01
OK
07
U-234
TRG
1-68 DIS
pCi/1
2.58E+OO
4.98E-01
8.85E-02
OK
08
U-234
TRG
D-87 TOT
pCi/1
4.00E-01
2.03E-01
1.40E-01
OK
09
U-234
TRG
D-87 DIS
pCi/1
2.60E-01
1.49E-01
9.82E-02
OK
10
U-234
TRG
PZ-106-SD TOT
pCI/1
3.18E-01
1.33E-01
7.38E-02
OK
11
U-234
TRG
PZ-106-SD DIS
pCi/1
4.31E-01
1.61E-01
8.27E-02
OK
12
U-234
TRG
S82TOT
pCI/1
1.26E+OO
4.10E-01
1.69E-01
OK
13
U-234
TRG
S-82 DIS
pCI/1
9.07E-01
3.16E-01
1.40E-01
OK
-t:
0
14
U-234
TRG
PZ-106-SS TOT
pCI/1
5.92E-01
1.70E-01
4.59E-02
OK
"'c".
15
U-234
TRG
PZ-106-SS DIS
pCI/1
6.05E-01
1.69E-01
5.11E-02
OK
.."'.
E
16
U-234
TRG
1-9 TOT
pCi/1
1.36E-01
1.17E-01
1.15E-01
OK
17
U-234
TRG
1-9 DIS
pCI/1
2.04E-01
1.20E-01
7.21E-02
OK
"'
18
U-234
TRG
D-93 TOT
pCi/1
3.90E-01
1.62E-01
9.28E-02
OK
c
c
19
U-234
TRG
D-93 DIS
pCI/1
2.99E-01
1.35E-01
7.65E-02
OK
:;;
c
-~
c,
w
1<!1
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OK
- - ------
TRG
Units
U-234
c.
c.
Activity
06
::J
.5
-!!!
Client
Identification
! Sample
/ Desc
05
Printed: 4/29/2013 2:14PM

Page 1 of 3
Work Order: 13-04105-UUIS0-1
Nuclide
Fraction
"'"'
Preliminary Data Report & Analytical Calculations
Eberline Services
~
~
~
0:
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0
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Sample
Date
01
U-234
LCS
04116113 00:00
02
U-234
MBL
04116113 00:00
J
!
Sample
Aliquot
Radiometric
%Rec
Gr."
Mean
%Rec
% Rec
SAF
128.31
0.00
0.00
125.47
0.00
0.00
1.00E+OO
130.78
0.00
0.00
1.00E+OO
-~+--1.00E+OO
i'
U-234
DUP
04109113 09:30
04
U-234
DO
04109113 09:30
1.00E+OO
112.88
0.00
0.00
C/)
05
U-234
TRG
04109113 09:30
1.00E+OO
135.45
0.00
o.oo
::J
::J
06
U-234
TRG
04109113 10:44
1.00E+OO
79.68
0.00
0.00
07
U-234
TRG
0410911310:44
1.00E+OO
95.31
0.00
0.00
08
U-234
TRG
0410911311:05
1.00E+OO
74.32
0.00
0.00
09
U-234
TRG
04109113 11:05
1.00E+OO
75.58
0.00
0.00
10
U-234
TRG
04109113 12:00
1.00E+OO
116.98
0.00
0.00
11
U-234
TRG
04109113 12:00
1.00E+OO
111.20
0.00
0.00
12
U-234
TRG
04109113 12:27
1.00E+OO
50.S2
0.00
0.00
13
U-234
TRG
04109113 12:27
1.00E+OO
62.54
0.00
0.00
14
U-234
TRG
0410911312:56
1.00E+OO
130.05
0.00
0.00
-"
15
U-234
TRG
0410911312:56
1.00E+OO
136.18
0.00
0.00
16
U-234
TRG
04109113 13:35
1.00E+OO
62.09
0.00
0.00
"'c
"'
c
"'
;:
17
U-234
TRG
0410911313:35
1.00E+OO
80.90
0.00
0.00
18
U-234
TRG
04109113 14:28
1.00E+OO
86.60
0.00
0.00
"c
19
U-234
TRG
0410911314:28
1.00E+OO
98.70
0.00
0.00
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Sept1
Date/Time
Date/Time
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Sample
Desc
'f"'"
Printed: 4/29/2013 2:14PM

Page 2 of3
Nuclide
Lab
Fraction
ill
;:
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Halflife
Lab
Fraction
Nuclide
Sample
Desc
Counting
DatefTime
01
U-234
LCS
04/29/13 09:59
U-234
MBL
04/29/13 09:59
A_Spec
U-234
DUP
04/29/13 09:59
04
U-234
DO
05
U-234
06
(days)
Detect
A_Spec
0:
-!:0
0
-~
~
..
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i!
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19.4
A_Spec
1Alpha_010
170.02 2.83 E+02
1.00 E-02
19.7
04/29/13 09:59
A_Spec
Alpha_011
170.02 2.69 E+02
2.00 E-03
19.7
TRG
04/29/13 09:59
A_Spec
Alpha_D13
170.02 3.33 E+02
3.00 E-03
18.7
U-234
TRG
04/29/13 09:59
A_Spec
Alpha_014
170 1.51 E+02
4.00 E-03
18.5
07
U-234
TRG
04/29/13 09:59
A_Spec
Alpha_018
170.02 1.64 E+02
4.00 E-03
17.8
08
U-234
TRG
04/29/1310:00
A_Spec
Alpha_022
170 1.71 E+01
5.00 E-03
15.3
09
U-234
TRG
04/29/13 10:00
A_Spec
Alpha_024
170.02 1.27 E+01
2.00 E-03
17.1
10
U-234
TRG
04/29/13 10:00
A_Spec
Alpha_025
170 2.43 E+01
4.00 E-03
17.4
11
U-234
TRG
04/29/13 10:00
A_Spec
Alpha_027
170 3.11 E+01
5.00 E-03
17.3
12
U-234
TRG
04/29/13 10:00
A_Spec
Alpha_029
170 4.70 E+01
6.00 E-03
19.5
13
U-234
TRG
04/29/1310:00
A_Spec
Alpha_033
170 3.90 E+01
0.00 E+OO
18.2
t:
0
14
U-234
TRG
04/29/13 10:00
A_Spec
Alpha_034
170 5.38 E+01
1.00 E-03
18.6
"'"c:
15
U-234
TRG
04/29/13 10:00
A_Spec
Alpha_035
170 5.67 E+01
2.00 E-03
18.3
"
"'"
16
U-234
TRG
04/29/1310:00
A_Spec
Alpha_037
170 5.66 E+OO
2.00 E-03
17.8
c:
17
U-234
TRG
04/29/1310:00
A_Spec
Alpha_040
170 1.18 E+01
1.00 E-03
19
"'c:
18
U-234
TRG
04/29/13 10:00
A_Spec
Alpha_041
170 2.51 E+01
5.00 E-03
19.8
"c:
19
U-234
TRG
04/29/1310:00
A_Spec
Alpha_042
170 2.05 E+01
3.00 E-03
18.5
03
en
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5.00 E-03
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170 2.15 E+OO
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Alpha_004
02
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17.5
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170.02 6.69 E+02
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Printed: 4/29/2013 2:14PM

Page 3 of3
+-
Eberline Services
0:
Printed: 4/29/2013 2:14PM

Page 1 of 3
Lab
Fraction
Nuclide
Sample
Desc
Client
Activity
Identification
Units
01
U-238
LCS
LCS
pCill
02
U-238
MBL
BLANK
pCi/1
1.99E-02
3.04E-02
4.53E-02
03
U-238
DUP
PZ-204-SS TOT
pCI/1
1.92E+OO
3.35E-01
6.77E-02
04
U-238
DO
PZ204-SS TOT
pCI/1
2.47E+OO
4.23E01
4.95E-02
OK
05
U-238
TRG
PZ-204-SS DIS
pCill
1.76E+OO
3.18E-01
5.48E02
OK
06
U-238
TRG
1-68 TOT
pCi/1
2.42E+OO
5.11E-01
1.18E-01
OK
07
U-238
TRG
1-68 DIS
pCi/1
2.23E+OD
4.53E-01
1.25E-01
OK
08
U-238
TRG
D-87TOT
pCi/1
1.04E-01
1.04E-01
1.22E-01
OK
09
U-238
TRG
D-87 DIS
pCi/1
1.09E-01
1.00E-01
1.15E-01
OK
10
U-238
TRG
PZ-106-SD TOT
pCi/1
3.08E-01
1.30E-01
6.23E-02
OK
11
U-238
TRG
PZ-106-SD DIS
pCi/1
1.97E-01
1.07E-01
7.76E02
OK
12
U-238
TRG
S-82TOT
pCill
1.09E+OO
3.73E-01
1.11E-01
OK
<.i
13
U-238
TRG
S-82 DIS
pCi/1
8.11E-01
2.96E-01
1.39E-01
OK
14
U-238
TRG
PZ-106-SS TOT
pCI/1
3.80E-01
1.33E-01
5.24E-02
OK
15
U-238
TRG
PZ-106-SS DIS
pCi/1
3.38E-01
1.23E-01
4.44E-02
OK
16
U-238
TRG
1-9 TOT
pCi/1
4.37E-02
6.70E-02
9.97E-02
OK
17
U-238
TRG
1-9 DIS
pCi/1
1.86E-01
1.14E-01
7.18E-02
OK
.".,
Ol
18
U-238
TRG
D-93 TOT
pCi/1
1.56E-01
1.17E-01
1.50E-01
OK
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w
"
"
19
U-238
TRG
D-93 DIS
pCi/1
1.55E-01
9.62E-02
6.94E-02
OK
Results
7.57E+OO
Error Estimate
9.81E-01
MDA
6.19E02
LCS
Known
7.94E+OO
LCS
%R
LCS
Flag
95.30
OK
RPD
MDA
Flag
Flag
Blank
Flag
OK
OK
OK
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04/16/13 00:00
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04/16/13 00:00
03 '
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U-238
DUP
U-238
DO
U-238
TRG
04/09/13 09:30
1.00E+OO
135.45
0.00
0.00
06
U-238
TRG
04/09/1310:44
1.00E+OO
79.68
0.00
0.00
07
U-238
TRG
04/09/13 10:44
1.00E+OO
95.31
0.00
0.00
08
U-238
TRG
04/09/13 11:05
1.00E+OO
74.32
0.00
0.00
09
U-238
TRG
04/09/13 11 :05
1.00E+OO
75.58
0.00
0.00
10
U-238
TRG
04/09/1312:00
1.00E+OO
116.98
0.00
0.00
11
U238
TRG
04/09/1312:00
1.00E+o0
111.20
0.00
0.00
12
U238
TRG
04/09/13 12:27
1.00E+OO
50.92
0.00
0.00
13
U-238
TRG
04/09/1312:27
1.00E+OO
62.54
0.00
0.00
-t:
0
14
U-238
TRG
04/09/1312:56
1.00E+OO
130.05
0.00
0.00
-"
15
U-238
TRG
04/09/13 12:56
1.00E+OO
136.18
0.00
0.00
16
U-238
TRG
04/09/1313:35
1.00E+OO
62.09
0.00
0.00
17
U-238
TRG
04/09/1313:35
1.00E+OO
80.90
0.00
0.00
"'"
18
U-238
TRG
04/09/13 14:28
1.00E+OO
86.60
0.00
0.00
c;,
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19
U-238
TRG
04/09/13 14:28
1.00E+OO
98.70
0.00
0.00
Nuclide
SAF
128.31
0.00
0.00
1.00E+OO
125.47
0.00
0.00
04/09/13 09:30
1.00E+OO
130.78
0.00
0.00
04/09/13 09:30
1.00E+OO
112.88
0.00
0.00
-------
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1.00E+OO
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U-238
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Sample
Date
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Sample
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Sample
Lb
Fraction
Printed: 4/29/2013 2:14PM

Page 2 of 3
--
Eberline Services
0:
.g
0
'-'
-~
..
~
"2
0
-!;
.,
-E
"ill
~
Desc
Counting
DatefTime
01
U-238
LCS
04/29/13 09:59
A_Spec
Alpha_003
170.02 6.41 E+02
3.00 E-03
17.5
02
U-238
, MBL
04/29/13 09:59
A_Spec
Alpha_004
170 1.83 E+OO
1.00 E-03
19.4
03
U-238
DUP
04/29/13 09:59
A_Spec
Alpha_010
170.02 1.87 E+02
7.00 E-03
19.7
04
U-238
DO
04/29/13 09:59
A_Spec
Alpha_011
170.02 2.08 E+02
1.00 E-03
19.7
C/)
05
U-238
TRG
04/29/13 09:59
A_Spec
Alpha_013
170.02 1.68 E+02
3.00 E-03
18.7
::::>
::::>
06
U-238
TRG
04/29/13 09:59
A_Spec
Alpha_014
170 1.35 E+02
7.00 E-03
18.5
07
U-238
TRG
04/29/13 09:59
A_Spec
Alpha_018
170.02 1.43 E+02
1.30 E-02
17.8
08
U-238
TRG
04/29/13 10:00
A_Spec
Alpha_022
170 4.49 E+OO
3.00 E-03
15.3
09
U-238
TRG
04/29/13 10:00
A_Spec
Alpha_024
170.02 5.32 E+OO
4.00 E-03
17.1
10
U-238
TRG
04/29/13 10:00
A_ Spec
Alpha_025
170 2.37 E+01
2.00 E-03
17.4
11
U-238
TRG
04/29/13 10:00
A_ Spec
Alpha_027
170 1.43 E+01
4.00 E-03
17.3
12
U-238
TRG
04/29/1310:00
A_Spec
Alpha_029
170 4.08 E+01
1.00 E-03
19.5
13
U-238
TRG
04/29113 10:00
A_Spec
Alpha_033
170 3.50 E+01
0.00 E+OO
18.2
14
U-238
TRG
04/29/13 10:00
A_Spec
Alpha_D34
170 3.47 E+01
2.00 E-03
18.6
15
U-238
TRG
04/29/13 10:00
A_Spec
Alpha_035
170 3.18 E+01
1.00 E-03
18.3
16
U-238
TRG
04/29/13 10:00
A_Spec
Alpha_037
170 1.83 E+OO
1.00 E-03
17.8
"'c
17
U-238
TRG
04/29/1310:00
A_Spec
Alpha_040
170 1.08 E+01
1.00 E-03
19
Cl
18
U-238
TRG
04/29/1310:00
A_Spec
Alpha_041
170 1.01 E+01
2.30 E-02
19.8
19
U-238
TRG
04/29/1310:00
A_Spec
Alpha_042
170 1.07 E+01
2.00 E-03
18.5
"r'"'
'
..;
-r0
a.
a.
-.
"'".c
E
"'
....
;;,
c
t:
c
c
UJ
t:EI
!Jll
,~,ot.~
----t-
Halflife
(days)
Detect
I'
Carrier
Count
Time
Counts
Bkg
CPM
Eff
'
Cl
:;:

I Sample
Lb
Fraction
Printed: 4/29/2013 2:14PM

Page 3 of 3
Nuclide
<(
----
Eberline Services
(
~I
0
.~
"
'
i!
~
~
-~
"'
~
Sample
Client
Activity
Oesc
Identification
Units
LCS
LCS
pCi/1
Lab
Fraction
Nuclide
01
U-235
02
U-235
03
U-235
04
U-235
DO
05
U-235
06
Results
6.92E-01
Error Estimate
2.11E-01
MDA
LCS
Known
LCS
LCS
RPD
MDA
%R
Flag
Flag
Flag
OK
6.59E-02
8.48E-02
pCi/1
1.95E-01
1.02E-01
7.18E-02
PZ-204-SS TOT
pCi/1
1.45E-01
9.25E-02
6.14E-02
OK
TRG
PZ-204-SS DIS
pCi/1
1.27E-01
8.13E-02
5.40E-02
OK
U-235
TRG
1-68 TOT
pCi/1
2.37E-01
1.48E-01
1.06E-01
OK
07
U-235
TRG
l-68 DIS
pCi/1
1.77E-01
1.23E-01
1.16E-01
OK
08
U-235
TRG
D-87 TOT
pCill
3.31E-02
8.27E-02
1.72E-01
OK
09
U-235
TRG
D-87 DIS
pCi/1
1.67E-02
5.11E-02
1.21E-01
OK
10
U-235
TRG
PZ-106-SD TOT
pCi/1
6.18E-02
6.38E-02
6.73E-02
OK
11
U-235
TRG
PZ-106-SD DIS
pCi/1
2.83E-02
4.80E-02
8.15E-02
OK
12
U-235
TRG
S-82 TOT
pCi/1
1.15E-01
1.32E-01
1.74E-01
OK
c.i
.E
13
U-235
TRG
S-82 DIS
pCUI
2.38E-02
5.72E-02
1.20E-01
OK
14
U-235
TRG
PZ-106-5S TOT
pCi/1
4.97E-02
5.38E-02
6.49E-02
OK
"'"c
15
U-235
TRG
PZ-106-5S DIS
pCi/1
1.16E-01
7.85E-02
5.50E-02
OK
"
E
..
16
U-235
TRG
1-9 TOT
pCi/1
O.OOE+OO
8.20E-02
1.77E-01
OK
17
U-235
TRG
1-9 DIS
pCI/1
1.03E-01
9.45E-02
8.89E-02
OK
"'c
18
U-235
TRG
D-93 TOT
pCi/1
2.85E-02
5.42E-02
1.00E-01
OK
"
;;,
c
w
19
U-235
TRG
D-93 DIS
pCI/1
4.48E-02
6.21E-02
9.43E-02
OK
-r-
en
-::::>
::::>
Q,
Q,
""'
MBL
BLANK
CUP
PZ-204-SS TOT
NA
OK
--
:;;
~
Ill!!
1'1-.li
u~
01.)
Blank
Flag
OK
8.24E-02
6.70E-02
ill
pCi/1
,___
{l
Printed: 4/29/2013 2:14PM

Page 1 of 3
OK
Eberline Services
(
0
0:
.g
0
'-'
-!!!
~
~
""
-e0'
-!:
~
~
0
-~
"'
Radiometric
"'oRee
Nuclide
Sample
Desc
Sample
Date
01 i
02
U-235
LCS
04/16/13 00:00
1.00E+OO
128.31
0.00
0.00
U-235
MBL
04/16/13 00:00
1.00E+OO
125.47
0.00
0.00
U-235
DUP
04/09/13 09:30
1.00E+OO
130.78
0.00
0.00
U-235
DO
04/09/13 09:30
1.00E+OO
112.88
o.oo
0.00
05
U-235
TRG
04/09/13 09:30
1.00E+OO
135.45
0.00
0.00
06
U-235
TRG
04/09/1310:44
1.00E+OO
79.68
o.oo
0.00
07
U-235
TRG
04/09/13 10:44
1.00E+OO
95.31
0.00
0.00
08
U-235
TRG
04/09/13 11 :05
1.00E+OO
74.32
o.oo
0.00
09
U-235
TRG
04/09/13 11:05
1.00E+OO
75.58
0.00
0.00
10
U-235
TRG
04/09/13 12:00
1.00E+OO
116.98
0.00
0.00
11
U-235
TRG
04/09/1312:00
1.00E+OO
111.20
0.00
0.00
12
U-235
TRG
04/09/13 12:27
1.00E+OO
50.92
0.00
0.00
13
U-235
TRG
04/09/1312:27
1.00E+OO
62.54
0.00
0.00
14
U-235
TRG
04/09/1312:56
1.00E+OO
130.05
0.00
0.00
15
U-235
TRG
04/09/1312:56
1.00E+OO
136.18
0.00
0.00
..:;;.
16
U-235
TRG
04/09/13 13:35
1.00E+OO
62.09
0.00
0.00
17
U-235
TRG
04/09/1313:35
1.00E+OO
80.90
0.00
0.00
"'
18
U-235
TRG
04/09/13 14:28
1.00E+OO
86.60
0.00
0.00
"
c,
c
w
"c
19
U-235
"l""'
~----J
03 I
'-----r
04 ,
. .
Mean
%Rec
Grav
%Rec
SAF
(/)
::J
::J
.;
,:
0
c.
c.
:I
"'c
~
~<I
t,o
1.0
Sep t1
Date!Time
"E
""'
--
..
--
I
!
'i:
1<11
Sep tO
OateiTime
-- f---
.E
"
'-'
Sample
Aliquot
--t---
Printed: 4/29/2013 2:14PM

Page 2 of 3
Lb
Fraction
ill
TRG
04/09/13 14:28
1.00E+OO
98.70
0.00
0.00
I
Eberline Services
(
~
~
0:
"'0
0
-~
1i;
~
<>:
'
~
-!!
-~
.,
Lab
Fraction
01
U-235
02
U-235
03
U-235
04
U-235
Printed: 4/29/2013 2:14PM

Page 3 of 3
[ Sample
1
/ LCS
DUP
DO
--r;~;
'
Count
Counts
Bkg
Eff
Carrier
A_Spec
Alpha_003
170.02 4.73 E+01
4.00 E-03
17.5
A_Spec
Alpha_004
170 4.98 E+OO
6.00 E-03
19.4
04/29/13 09:59
A_Spec
Alpha_010
170.02 1.53 E+01
19.7
04/29/13 09:59
A_Spec
Alpha_011
170.02 9.83 E+OO
4.00 E-03
1.00 E-03
19.7
04/29/13 09:59
A_ Spec
Alpha_013
170.02 9.83 E+OO
1.00 E-03
18.7
Time
04/29/13 09:59
---~--
j---
!
(days)
CPM
---- .....
r~BL-
Halflife
04/29/13 09:59
~- -
Counting
DatefTime
Detect
Oesc
'
---
en
05
U-235
::J
::J
06
U-235
+--TRG
04/29/13 09:59
A_Spec
Alpha_014
170 1.07 E+01
2.00 E-03
18.5
07
U-235
TRG
04/29/13 09:59
A_Spec
Alpha_018
170.02 9.15 E+OO
5.00 E-03
17.8
08
U-235
TRG
04/29/13 10:00
A_Spec
Alpha_022
170 1.15 E+OO
5.00 E-03
15.3
09
U-235
TRG
04/29/13 10:00
A_Spec
Alpha_024
2.00 E-03
17.1
10
U-235
TRG
04/29/1310:00
A_Spec
Alpha_025
170 3.83 E+OO
1.00 E-03
17.4
11
U-235
TRG
04/29/1310:00
A_Spec
Alpha_027
170 1.66 E+OO
2.00 E-03
17.3
12
U-235
TRG
04/29/13 10:00
A_Spec
Alpha_029
170 3.49 E+OO
3.00 E-03
19.5
.E
13
U-235
TRG
04/29/1310:00
A_Spec
Alpha_033
170 8.30 E-01
1.00 E-03
18.2
t:
0
14
U-235
TRG
04/29/13 10:00
A_Spec
Alpha_034
170 3.66 E+OO
2.00 E-03
18.6
-"
15
U-235
TRG
04/29/13 10:00
A_ Spec
Alpha_035
170 8.83 E+OO
1.00 E-03
18.3
16
U-235
TRG
04/29/1310:00
A_Spec
Alpha_037
170 1.00 E+OO
0.00 E+OO
17.8
17
U-235
TRG
04/29/13 10:00
A_Spec
Alpha_040
170 4.83 E+OO
1.00 E-03
19
18
U-235
TRG
04/29/13 10:00
A_Spec
Alpha_041
170 1.49 E+OO
3.00 E-03
19.8
"c
19
U-235
TRG
04/29/1310:00
A_Spec
Alpha_042
170 2.49 E+OO
3.00 E-03
18.5
'
ill
.;
c.
c.
~
"'c
Nuclide
"
"c
:;;
"
170.02 6.60 E-01
Cl
Cl
-~
"
c;,
c
w
~-
l:l!l
1-"""'
l:l!l
tii!
-~-
Count Room Report

Client: Engineering Management Su
13-04105-UUIS0-1 (pCi/1) in WA
Tracer ID: U-10a
./"'-
Sample
Aliquot
Tracer
Aliquot (g)
Printed: 4129/2013 7:11AM
Page 1 of 1
"(
\.,--;
Tracer
ACT (dpm)
Radiometric
Tracer (pCi)
SAF
1*
Radiometric
% Rec
SAF
2.
1.0000
\(fl-o
896
172
S-82 DIS
____[
I
04/09/13 12:27
1.0000
0.5661
10.8091
o.oo
----
11.3953
0.00 I
11.3896
114278
1
1
11.3476 :
11.39531
11.3590
---
IW!
~~
!<!I
~-
j _ _ _ j__________ ,
ooo
0.00
-------1--=--::-::1
Eberline Services
Code
LCS & Matrix Spikes
U-234
---U-238
Activity
dpm!g
Sol#
_j
U-Sa
U-Sa
LCS
Solution
Date
35.240
34.350
-~
Approx
Addition
Volume
Used(g)
0.5001
o.5oo
TeChn1
Date
UUISO
Isotope
Page 1 of 1
Printed: 4/24/201312:02 PM
Spike and Tracer Worksheet
MS
LCSD
Volume
Used(g)
Volume
Used{g)
0.51321
o.5132
LCS
MSD
Volume
Used{g)
Known
pCi
fraction
Sol#
Isotope
~U-232
02
1---oJ
U-232
I
I
U-232
0.6300
U-10a
19.0941 4/24/2013
0.6041
0.6300
0~ 608!3 g
0. E035 '3
19.094 4/24/2013
0.6007
0.6300
-0.604i 9
19.094 4/24/2013
0.6027
0.6300
-0~6007
-0,6027 '3
-~3. 5969 ;
U-10a
U-10a
07
U:2321
U-10a
08
U-232
.
'
BE
U-232
09
10
0.6300
-e1. 5996
U-10a
19.094 4/24/2013
0.60021
0.6300
-tZI. 601212 '3
U-10a
19.094 4/24/2013
0.5968
-0.5968 g
-0.5962 '3
-0.5965 s
U-232
U-10a
19.094 4/24/2013 .. 0.5965
0.6300
U-232
U-10a
0.6300
13
U-232
U-10a
19.094 4/24/2013 . 0.5969

19.094 4/24/2013
0.5661
U-232
19.094 4/24/2013
0.5968
0.6300 I
15
U-232
J-
U-10a
U-10a
19.094 4/24/2013
05965
0.6300
U-10a
19.0941 4/24/2013
0.5985
0.6300 1
U-232
_I
U-10a
19.094 4/24/2013
0.5943
0.6300 I
U-232
U-10a
19.094 4/24/2013
0.5968
0.6300 I
U-232
U-10a
19.094 4/24/2013
0.5949
0.6300
16
17
T
I
I
i
U-232
Version 2.0 08/99
Added
pCi
0.6300
0.51.:3;2 '3
:~
0.6300-1
0.6300
I~
rj
0.5996
0.5962
19
1<11
19.094 4/24/2013
----i---+---t------1
19.0941 4/24/2013
18
0.6300
U-10a
0.5969
U-232
f----
--
19.094 4/24/2013
MSD
Error
Estimate
LCS
0.6300
,-
Tracer
0.6035
U-232
- U--232
Date
Approx
Addition
Volume
Used (g)
0.6088
05
06
19.0941 4/24/2013
I.
Estimate
Known
pCi
Balance Printer Tapes
I Solution~
19.094[ 4/24/2013
U-10a
LCSD
Erro'
s. 15
U-10a
U-232
MS
Added
pCi
Error
Estimate
~--7-.9-4f-l--o.-2-s6-ll---o-.o-o+l--o-.o-o-oll----o-.-oo-ll--o-.o-o-oll---o-.o-of-l--o.-o---lool
U-10a
04
--
Error
Estimate
Tracers
Activity
dpmlg
JBARNARD
4/24/2013 12:01
-0.5969 9
-ci.56E.1 :1
-0.5968 '3
-0.5965 9
-0 = ~59:3~.5 '3
-a.5943 9
-0.5968 g
-0.5949 9
Matrix Spike
Eberline Analytical
Work Orde
13-04105
Lab
Type
LCS
MBL
DUP
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
ClientlD
LCS
BLANK
PZ-204-SS TOT
PZ-204-SS TOT
PZ-204-SS DIS
06
07
08
09
PZ-106-SD TOT
PZ-106-SD DIS
12
13
14
15
S-82 TOT
S-82 DIS
PZ-1 06-SS TOT
PZ-1 06-SS DIS
16
17
18
19
I
l:liU
,._,,
Ia!
r,;~
1-68 TOT
1-68 DIS
D-87 TOT
-
D-87 DIS
10
11
1-9 TOT
1-9 DIS
D-93 TOT
D-93 DIS
Comments
Technician:
Rpt Units
Lab Deadline
Technician
UUISO
liters
5/7/2013
JBARNARD
Muffle Data
Ratio
Post/Pre
Sample
--~-
04
05
Analysis Code
Fraction
01
02
03
Printed: 4/24/2013 11:58 AM

Page 1 of 1
Aliquot Worksheet
Dilution Data
No of Oils
Aliquot Data
Oil Factor
Ratio
Aliquot
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
:
.
.
.
.
.
.
.
.
.-
..
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
:~
'
Date:L~
Net Equiv
Aliquot
NetEquiv
1.0000E+OO
1.0000E+OO
1.0000E+OO
1:0000E+OO
1.0000E+OO
1.0000E+OO
LOOOOE+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
..
H-3 Solids Only

Water Added
H3 Dist
(ml)
Aliq
----
LOOOOE+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
MS Aliquot Data
'
-----~
ex-AiphaTM
Sample Geometry:
SPIKE
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000566
1304105A-UU
01
Shelf 2
Procedure Description:
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Alpha_003
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
System Bkgd 55734
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
1.000E+000 +/- O.OOOE+OOO liter

4/29/2013
7:53:48 AM
4/29/2013
9:59:25 AM
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
170.0 minutes
170.0 minutes
U232 UU-10A
0.609 mL
0.2241 +/- 0.0119
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM
1.2831 +/- 0.0721
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
Control Certificate Name: NatU_U-8A

Chern. Recov. of Control:
U-238
Peak Match Tolerance:
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.276
4.724
4.391
4.146
Net
Pk Area
0.928992 +!-
AREA
REPORT
Pk Area
Error %
440.30
669.47
47.32
641.49
0.067449
9.36
7.59
28.73
7.74
Ambient
Backgnd
1. 70
1. 53
0.68
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
6.8
26.8
6.0
22.7
Tracer Peak used for Effective Efficiency
NUCLIDE ANALYSIS RESULTS
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.990
1. 000
0.990
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.22E+000
7.93E+000
6.92E-001
7.57E+000
+I+I+I+I-
5.42E-001
1.02E+000
2.11E-001
9.81E-001
,A:;
t;/J.rtfr!J
MDA
(pCi/liter
8.70E-002
8.42E-002
8.24E-002
6.19E-002
+I+I+I+I-
9.04E-003
8.75E-003
8.57E-003
6.43E-003
0000056612.CNF
Live Time :10201.000 sec
Rea1 Time :10201.000 sec
Start:
l:l498.4(kev)
Stop : 1024:6549.5(keV)
Acq. Start :Mon Apr 29 09:59:25 2013
60
55
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Channel Data Report
4/29/2013
12:S:h-'J
Page
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************,************************
Sample Title:
01
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Channel Data Report

369:
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2
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lllHl7
Channel Data Report

801:
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0
Sample Title:
12:53:08
0
PM
0
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IH lil8
pex-AiphaTM
BLANK
1304105A-UU
02
Shelf 2
u iso
Detector Name:
Alpha_004
Sample Description:
Spectrum File:
Sample Geometry:

Env. Background:
Reagent Blank:
System Bkgd 55735

<not performed>
1. OOOE+OOO +/- O.OOOE+OOO liter

4/29/2013
7:53:48 AM
9:59:26 AM
4/29/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.604 mL
0.2434 +/- 0.0125
0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM
1.2547 +/- 0.0685
0.150 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.277
4.764
4.410
4.190
AREA
REPORT
Pk Area
Net
Pk Area
Error %
474.15
2.15
4.98
1.83
9.01
161.66
97.79
152.56
Ambient
Backgnd
0.85
0.85
1. 02
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
30.8
2.9
2.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
1. 000
0.996
1.000
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.17E+OOO
2.34E-002
6.70E-002
1. 99E-002
+I+I+I+I-
5.21E-001
3.80E-002
6.59E-002
3.04E-002
It:$
t!/~fl~
MDA
(pCi/liter
6.53E-002
6.53E-002
8.48E-002
4.53E-002
+I+I+I+I-
6.58E-003
6.58E-003
8.54E-003
4.57E-003
0000056613.CNF
Live Time 10200.000 sec
Real Time 10201.000 sec
Start:
13493.l(keV)
stop : 1024 6486.9(kev)
60
Acq. Start Mon Apr 29 09:59:26 2013
55
50
45
40
35
...,
Ul
<::
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5000
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5500
6000
ROI Type: 3
6500
Channel Data Report
4/29/2013
Page
12: 53:'l'l' JIM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
02
Elapsed Live time:

Elapsed Real Time:
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~111
Channel Data Report

369:
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Sample Title:
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0
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.!!1112
Channel Data Report

801:
4/29/2013
0
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12:53:17
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-204-SS TOT-DUP
\\OR-ALPHA1\Canberra\ApexA1pha\Root\Data\00000566
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03
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_010
10
System Bkgd 55736
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:53:48 AM
9:59:21 AM
4/29/2013
170.0 minutes
l70. 0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.604 mL
0.2573 +/- 0.0130
0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM
1.3078 +/- 0.0700
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.274
4.732
4.406
4.142
Net
Pk Area
AREA
REPORT
Ambient
Backgnd
Pk Area
Error %
501.62
283.30
15.32
186.81
8.78
11.69
51.36
14.39
2.38
1. 70
0.68
1.19
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
9.9
17.0
4.4
7.3

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.994
0.994
0.997
0.987
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.18E+000
2.92E+000
1.95E-001
1.92E+000
+I+I+I+I-
5.11E-001
4.47E-001
1. 02E- 001
3.35E-001
fY4
1/in/!J
MDA
(pCi/liter
8.46E-002
7.58E-002
7.18E-002
6.77E-002
+I+I+I+I-
8.35E-003
7.48E-003
7.08E-003
6.68E-003
0000056608.CNF
Start:
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6500
Channel Data Report
4/29/2013
12:53:27 PM
Page
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
03
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Channel Data Report

369:
4/29/2013
1
Sample Title:
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U17
Channel Data Report

801:
4/29/2013
0
Sample Title:
12:~;iti;;j;.
l.'l<!-g-e
0
03
Channell------l-------l-------l-------1-------l-------l-------l-------l
809:
817:
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m11a
ex-AiphaTM
Sample Geometry:
PZ-204-SS TOT
130410SA-UU
04
Shelf 2
U iso
Detector Name:
Alpha_011

Env. Background:
11
System Bkgd 55737
Sample Description:
Spectrum File:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:53:48 AM
4/29/2013
9:59:22 AM
170.0 minutes
170.0 minutes
U232_UU-10A
0.601 mL
0.2227 +/- 0.0119
0.1973 +/- 0.0042 on 12/15/2012 11:28:06 AM
1.1288 +/- 0.0647
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.276
4.725
4.365
4.141
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
431.83
268.66
9.83
207.83
9.43
11.97
63.14
13.60
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.17
0.34
0.17
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
9.7
5.9
2.7
7.1

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.990
0.997
0.987
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.15E+OOO
3.20E+OOO
1.45E-001
2.47E+OOO
+I+I+I+I-
5.39E-001
5.09E-001
9.25E-002
4.23E-001
f'G
lf(Jr1/f.J
MDA
(pCi/liter
4.98E-002
5.70E-002
6.14E-002
4.95E-002
+I+I+I+I-
5.20E-003
5.96E-003
6.42E-003
5.18E-003
0000056609.CNF
Real Time :10201.000 sec
start:
l:l645.8(kev)
Stop : 1024:6374.2(kev)
Acq. start :Mon Apr 29 09:59:22 2013
60
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Channel Data Report
4/29/2013
Page
12:53:)1 -
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
04
Elapsed Live time:

Elapsed Real Time:
10201
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f.J122
Channel Data Report

801:
4/29/2013
0
Sample Title:
Page
12:Sl:U tf;t'
0
04
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1009:
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lil123
pex-AiphaTM
Sample Description:
Spectrum File:
PZ-204-SS DIS
130410SA-UU
OS
Shelf 2
Sample Geometry:
U iso
Detector Name:
Alpha_013

Env. Background:
Reagent Blank:
13
System Bkgd 55738
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:53:48 AM
4/29/2013
9:59:23 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.603 mL
0.2532 +/- 0.0128
0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM
1.3545 +/- 0.0731
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.287
4.743
4.433
4.157
Net
Pk Area
AREA
REPORT
Ambient
Backgnd
Pk Area
Error %
492.47
333.49
9.83
168.49
1.53
0.51
0.17
0.51
8.85
10.74
63.14
15.13
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
32.0
12.8
2.8
19.2
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.998
0.984
0.995
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.17E+OOO
3.50E+OOO
1.27E-001
1.76E+OOO
+I+I+I+I-
5.13E-001
5.12E-001
8.13E-002
3.18E-001
AG
~(~{13
MDA
(pCi/liter
7.46E-002
S.SOE-002
5.40E-002
5.48E-002
+I+I+I+I-
7.41E-003
5.47E-003
5.36E-003
5.44E-003
0000056610.CNF
start:
1:3547. S(kev)
stop : 1024:643B.l(kev)
Acq. Start :Mon Apr 29 09:59:23 2013
60
55
so
45
40
35
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1:11
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5000
Energy(kev)
5500
6000
ROI Type: 3
Channel Data Report
4/29/2013
Page
12:53:45 PM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
05
Elapsed Live time:

Elapsed Real Time:
10201
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369:
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a127
Channel Data Report

801:
4/29/2013
0
Sample Title:
12:53:45
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Page
PM
0
05
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929:
937:
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953:
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969:
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985:
993:
1001:
1009:
1017:
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0
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-m12s
pex-AiphaTM
Spectrum File:
Sample Geometry:
I-68 TOT
1304105A-UU
06
Shelf 2
U iso
Detector Name:
Env. Background:
Alpha_014
Sample Description:
14
System Bkgd 55739
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:53:48 AM
4/9/2013
4/29/2013
9:59:24 AM
170.0 minutes

l70.0 minutes
U232_UU-10A
0.597 mL
0.1471 +/- 0.0094
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
0.7968 +/- 0.0531
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.277
4.723
4.357
4.151
AREA
REPORT
Pk Area
Net
Pk Area
Error %
283.28
151.32
10.66
134.81
11.71
15.98
61.14
16.97
Ambient
Backgnd
2.72
0.68
0.34
1.19
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
14.4
7.2
2.9
6.4
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.990
0.994
0.992
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.12E+OOO
2.73E+000
2.37E-001
2.42E+000
+I+I+I+!-
6.42E-001
S.SSE-001
1.48E-001
5.11E-001
'f(Jq/13
MDA
(pCi/liter
1. SSE-001
1. 02E-001
1. 06E-001
1.18E-001
+I+I+I+I-
1. 94E- 002
1.28E-002
1. 34E-002
1. 49E-002
00000566ll.CNF
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4/29/2013
Page
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s P E C T R A L DATA R E P 0 R T
*****
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06
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'll!132
Channel Data Report

801:
4/29/2013
0
Sample Title:
Page
12;~1~.
06
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Sample Description:
Spectrum File:
Sample Geometry:
I-68 DIS
1304105A-UU
07
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_018
18
System Bkgd 55740
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:53:48 AM
4/29/2013
9:59:59 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.600 mL
0.1693 +/- 0.0102
0.1776 +/- 0.0033 on 12/15/2012
0.9531 +/- 0.0598
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.277
4.730
4.395
4.149
Net
Pk Area
327.64
164.32
9.15
142.79
AREA
1:57:26 PM
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
10.85
15.33
68.23
16.55
1. 36
0.68
0.85
2.21
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
23.5
12.5
3.1
34.4
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.993
0.999
0.991
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.14E+OOO
2.58E+OOO
1.77E-001
2.23E+OOO
+I+I+I+I-
6.04E-001
4.98E-001
1. 23E- 001
4.53E-001
A$
1fiR/13
MDA
(pCi/liter
1.08E-001
8.85E-002
1.16E- 001
1.2SE-001
+I+I+I+I-
1.26E-002
1.04E-002
1.36E-002
1.47E-002
0000056614.CNF
Rea1 Time 10201.000 sec
start:
1 l404.1(kev)
stop : 1024 6604.2(kev)
Acq. start Mon Apr 29 09:59:59 2013
60
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Channel Data Report
4/29/2013
12:54:(!' 11M
Page
*******************************************************
*****
E C T R A L
DATA
R E P 0 R T
*****
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07
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Channel Data Report

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1137
Channel Data Report

801:
4/29/2013
0
Sample Title:
Page
12:54:010 ?M
0
07
ChannelJ------I-------I-------I-------1-------I-------I-------I-------J
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pex-AiphaTM
Sample Geometry:
D-87 TOT
1304105A-UU
08
Shelf 2
U iso
Detector Name:
Alpha_022
Sample Description:
Spectrum File:
Env. Background:
Reagent Blank:
22
System Bkgd 55741
<not performed>

7:53:48 AM
4/9/2013
4/29/2013 10:00:00 AM
170.0 minutes
Sample Size:
Sample Date/Time:
l70.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.600 mL
0.1138 +/- 0.0081
0.1531 +/- 0.0029 on 12/15/2012
0.7432 +/- 0.0549
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.254
4.710
4.429
4.070
T
AREA
REPORT
Net
Pk Area
Pk Area
Error %
220.47
17.15
1.15
4.49
1:57:26 PM
13.25
48.68
249.59
98.45
Ambient
Backgnd
1. 53
0.85
0.85
0.51
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.8
3.1
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.984
0.982
0.986
0. 911
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.15E+000
4.00E-001
3.31E-002
1.04E-001
+!+I+I+I-
7.20E-001
2.03E-001
8.27E-002
1. 04E-001
MDA
(pCi/liter
1. 66E-001
1.40E-001
1.72E-001
1.22E-001
+I+I+I+I-
2.32E-002
1. 96E- 002
2.41E-002
1. 71E- 002
flG
lf/J#(r3
.:m.13S
0000056615.CNF
start:
1:3421.5(kev)
Stop : 1024:6608.8(kev)
Acq. Start :Mon Apr 29 10:00:00 2013
60
55
50
45
40
35
.....
<::
Vl
8 30
25
20
15
10
5
0
! M II I
'
3500
4000
4500
5000
Energy(kev)
5500
6000
.~.
!>J,,
ROI Type: 1
ROI Type: 3
6500
Channel Data Report
4/29/2013
12:5~t>i
Page
*******************************************************
*****
p E C T R A L
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*****
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:UJ142
Channel Data Report

801:
4/29/2013
0
Sample Title:
Page
12:54:15 l!'M
0
08
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ex-AiphaTM
Sample Description:
D-87 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000566
l304l05A-UU
09
Shelf 2
u iso
Detector Name:
Alpha_024
Spectrum File:
Sample Geometry:

Env. Background:
Reagent Blank:
24
System Bkgd 55742
<not performed>
Sample Size:
Sample Date/Time:
l.OOOE+OOO +/- O.OOOE+OOO liter

7:53:48 AM
4/9/20l3
4/29/20l3 lO:OO:Ol AM
l70.0 minutes
170. 0 minutes

U232 UU-lOA
0.597 mL
O.l293 +/- 0.0087
O.l7l0 +/- 0.0032 on l2/l5/20l2
0.7558 +/- 0.0530
O.lSO MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
Nuclide
U-232
U-234
U-235
U-238
(MeV)
T
5.255
4. 7l6
4.495
4.l44
Net
Pk Area
248.98
l2.66
0.66
5.32
AREA
2:02:l5 PM
REPORT
FWHM
(keV)
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
l.02
0.34
0.34
0.68
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
l2.45
55.94
305.45
9l.ll
l2.3
3.l
3.l
3.l
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.984
0.985
0.9l8
0.988
5302.50*
476l. 50*
4385.50*
4l84.40*
Activity
(pCi/liter )
5.l2E+OOO
2.60E-00l
l. 67E-002
l. 09E-00l
+I+I+I+I-
6.78E-00l
l.49E-00l
S.llE-002
l.OOE-OOl
fiG,
J/(.11/13
MDA
(pCi/liter
l. 29E-00l
9.82E-002
l.2lE-00l
l.lSE- OOl
+I+I+I+I-
l. 7lE-002
l. 30E-002
l.60E-002
l. 53E-002
0000056616.CNF
start:
1:3411.6(kev)
stop : 1024:6597.0(kev)
60
55
Acq. Start :Mon Apr 29 10:00:01 2013
I-
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6500
Channel Data Report
4/29/2013
12:54:24 PM
Page
*******************************************************
*****
T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
09
Elapsed Live time:

Elapsed Real Time:
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fil'!.4-6
Channel Data Report

369:
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f\11.47
Channel Data Report

801:
4/29/2013
1
Sample Title:
12:54:24
0
Page
0
09
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
PZ-106-SD TOT
1304105A-UU
10
Shelf 2
u iso
Alpha_025
25
System Bkgd 55743
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:53:48 AM
4/9/2013
4/29/2013 10:00:02 AM
170.0 minutes

170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.596 mL
0.2030 +/- 0.0113
0.1736 +/- 0.0032 on 12/15/2012
1.1698 +/- 0.0686
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.282
4. 715
4.395
4.181
Net
Pk Area
AREA
REPORT
Pk Area
Error %
390.66
24.32
3.83
23.66
1:57:27 PM
9.92
40.39
102.72
40.63
Ambient
Backgnd
0.34
0.68
0.17
0.34
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
7.8
3.1
3.1
4.7

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.985
0.999
1.000
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.11E+000
3.18E-001
6.18E-002
3.08E-001
+I+I+I+1-
5.57E-001
1.33E-001
6.38E-002
1.30E-001
4{'*1( 13
MDA
(pCi/liter
6.26E-002
7.38E-002
6.73E-002
6.23E-002
+I+I+I+I-
6.82E-003
8.04E-003
7.34E-003
6.78E-003
0000056617.CNF
start:
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Stop : 1024:6615.8(kev)
Acq. start :Mon Apr 29 10:00:02 2013
60
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5500
6000
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Channel Data Report
Page
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
10
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Channel Data Report

369:
4/29/20U
1
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8'152
Channel Data Report

801:
4/29/2013
0
Sample Title:
12
:5~hli
I'lag<;~
:3
10
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
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8153
pex-AiphaTM
Sample Geometry:
PZ-106-SD DIS
1304105A-UU
11
Shelf 2
U iso
Detector Name:
Alpha_027
Sample Description:
Spectrum File:

Env. Background:
27
System Bkgd 55744
Reagent Blank:
<not performed>

4/9/2013
7:53:48 AM
4/29/2013 10:00:03 AM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
U232 UU-10A
0.596 mL
0.1921 +/- 0.0109
0.1728 +/- 0.0032 on 12/15/2012
1.1120 +/- 0.0667
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.280
4.726
4.440
4.108
Net
Pk Area
369.81
31.15
1.66
14.32
AREA
2:27:41 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
10.21
35.67
169.38
53.21
1.19
0.85
0.34
0.68
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.0
4.0
3.2
4.8

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.996
0.991
0.979
0. 960
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.11E+OOO
4.31E-001
2.83E-002
1. 97E-001
+I+I+I+I-
5.71E-001
1. 61E- 001
4.80E-002
1.07E-001
ACt
~~(!!>
MDA
(pCi/liter
9.11E-002
8.27E-002
8.15E-002
7.76E-002
+I+I+I+I-
1.02E-002
9.24E-003
9.10E-003
8.67E-003
0000056618.CNF
start:
1:3402 .4(kev)
stop : 1024:6658.l(kev)
Acq. Start :Mon Apr 29 10:00:03 2013
60
55
50
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6500
Channel Data Report
4/29/2013
Page
12:54:43 111M
*******************************************************
s p E C T R A L DATA R E P 0 R T
*****
*****
*******************************************************
Sample Title:
11
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0
815E
Channel Data Report

369:
4/29/2()13
0
Sample Title:
12:i#l~~
Pag.e
0
l1
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~m1s7
Channel Data Report

801:
4/29/2013
0
Sample Title:
12:54:41
0
Page
0
11
Channell------I-------I-------I-------I-------I-------I-------1-------J
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ill158
Sample Description:
Spectrum File:
Sample Geometry:
S-82 TOT
1304105A-UU
12
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_029
29
System Bkgd 55745
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:53:48 AM
4/29/2013 10:00:04 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.597 mL
0.0991 +/- 0.0075
0.1945 +/- 0.0036 on 12/15/2012
0.5092 +/- 0.0399
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.271
4.719
4.367
4.140
T
AREA
REPORT
Pk Area
Error %
Net
Pk Area
190.81
46.98
3.49
40.83
2:30:02 PM
14.24
28.96
113.53
30.75
Ambient
Backgnd
1.19
1. 02
0.51
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
4.9
5.6
3.1
3.9

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.993
0.987
0.997
0.986
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.12E+000
l.26E+000
1.15E-001
1.09E+000
+I+I+I+I-
7.64E-001
4.10E-001
1.32E-001
3.73E-001
MDA
(pCi/liter
1. 77E-001
1. 69E-001
1.74E-001
1.11E-001
+I+I+I+I-
2.64E-002
2.52E-002
2.59E-002
1.66E-002
14
Lj(Jc;(IJ
-!15-9
0000056619.CNF
start:
1:341l.S(kev)
Stop : 1024:659/.S(kev)
Acq. Start :Mon Apr 29 10:00:04 2013
60555045-
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6000
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I I
6500
Channel Data Report
4/29/2013
Page
12:$4;".
*******************************************************
*****
p E
T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
12
Elapsed Live time:

Elapsed Real Time:
10200
10200
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9:
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lll161
Channel Data Report

369:
4/29/2013
0
Sample Title:
Page
12:54:52 PM
0
12
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m1s2
Channel Data Report

801:
4/29/2013
0
Sample Title:
12:l'i.llfiJ
0
:Bage
0
12
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
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pex-AiphaTM
Sample Description:
Spectrum File:
S-82 DIS
l304l05A-UU
l3
Shelf 2
u iso
Detector Name:
Env. Background:
Alpha_033
04026479A
9ll32
System Bkgd 55746
\\OR-ALPHAl\Canbe~~a\ApexAlpha\Root\Data\00000566
Sample
Geomet~y:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
l.OOOE+OOO +/- O.OOOE+OOO

4/9/20l3
7:53:48 AM
4/29/20l3 l0:00:43 AM
l70.0 minutes
l70.0 minutes
lite~
U232 UU-lOA
0.566 mL
O.ll4l +/- 0.0083
O.l825 +/- 0.0032 on l2/l6/20l2
0.6254 +/- 0.0470
Peak Match
O.l50 MeV
Tracer Certificate:
Tracer Quantity:
Tole~ance:
PEAK
Ene~gy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
Net
Pk Area
5.28l
4.74l
4.428
4.l60
AREA
REPORT
Pk Area
Error %
208.49
39.00
0.83
35.00
5:49:l8 PM
l3.59
3l. 78
239.53
33.60
Ambient
Backgnd
O.Sl
0.00
O.l7
0.00
Reagent
FWHM
Backgnd
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
l8.6
3.5
3.0
4.9

Id
Conf.
Ene~gy
Nuclide
U-232
U-234
U-235
U-238
0.997
0.997
0.987
0.996
5302.50*
476l. 50*
4385.50*
4l84.40*
(keV)
Activity
(pCi/liter )
4.85E+OOO
9.07E-00l
2.38E-002
8.llE-OOl
+/+/+/+/-
6.95E-00l
3.l6E-00l
5.72E-002
2.96E-00l
MDA
(pCi/liter
l.22E-00l
l.40E-00l
l.20E-00l
l.39E-00l
+/+/+/+/-
l.75E-002
2.00E-002
l.72E-002
l.99E-002
0000056623.CNF
60
start:
1:3465 .6(kev)
stop : 1024:650l.l(kev)
Acq. Start :Mon Apr 29 10:00:43 2013
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Channel Data Report
4/29/2013
Page
12:55:02 PM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
13
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Channel Data Report

369:
4/29/2013
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12:5S:~~
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m'1G7
Channel Data Report

801:
4/29/2013
0
Sample Title:
12:55
0
=~!
Page
13
809:
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-106-SS TOT
1304105A-UU
14
Shelf 2
u iso
Alpha_034
04026479B
91136
System Bkgd 55747
<not performed>
O.OOOE+OOO liter
l . OOOE+OOO +/7:53:48 AM
4/9/2013
4/29/2013 10:00:45 AM
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes
U232 UU-10A
0.597 mL
0.2413 +/- 0.0125
0.1856 +/- 0.0032 on 12/16/2012
1.3005 +/- 0. 0711
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.282
4.737
4.405
4.162
Net
Pk Area
464.83
53.83
3.66
34.66
AREA
5:49:43 PM
REPORT
FWHM
(keV)
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
0.17
0.17
0.34
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
9.09
26.76
107.87
33.48
54.8
3.0
3.0
5.2

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.996
0.997
0.996
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.12E+OOO
5.92E-001
4.97E-002
3.80E-001
+I+I+I+I-
5.19E-001
l . 70E-001
5.38E-002
l . 33E-001
MDA
(pCi/liter
4.59E-002
4.59E-002
6.49E-002
5.24E-002
+I+I+I+I-
4.66E-003
4.66E-003
6.59E-003
5.32E-003
44
1/JP~j!J
!169
0000056624.CNF
start:
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Channel Data Report
4/29/2013
12:55:28 PM
Page
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
14
Elapsed Live time:

Elapsed Real Time:
10200
10200
Channell------l-------l-------1-------l-------l-------l-------l-------l
1:
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!171
Channel Data Report

369:
4/29/2013
0
Sample Title:
12:SSI~.f
Page
1
14
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4/9/2013
4/29/2013 10:00:46 AM
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0.596 mL
0.2486 +/- 0.0127
0.1826 +/- 0.0032 on 12/16/2012
1.3618 +/- 0.0737
0.150 MeV
PEAK
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(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.299
4.744
4.395
4.168
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8.83
31.83
5:49:42 PM
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66.70
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O.OOE+OOO
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U-238
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0.998
0.999
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4385.50*
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1.16E-001
3.38E-001
+I+I+!+I-
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1.69E-001
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801:
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16
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4/9/2013
7:53:48 AM
4/29/2013 10:00:48 AM
170.0 minutes
170.0 minutes
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U232 UU-10A
0.599 mL
0.1107 +/- 0.0080
0.1783 +/- 0.0033 on 1/26/2013
0.6209 +!- 0.0463
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.286
4.731
4.398
4.171
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Pk Area
AREA
REPORT
Ambient
Backgnd
Pk Area
Error %
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5.66
0.00
1. 83
3:28:25 PM
13.41
85.23
1960.0
152.56
0.17
0.34
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4/29/2013
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Channel Data Report

801:
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8183
Sample Description:
Spectrum File:
Sample Geometry:
I-9 DIS
1304105A-UU
17
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_040
06027396B
91135
System Bkgd 55752
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:53:48 AM
4/29/2013 10:00:50 AM
170. 0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.594 mL
0.1537 +/- 0.0096
0.1900 +/- 0.0033 on 12/16/2012
0.8090 +!- 0.0526
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.274
4.706
4.387
4.179
Net
Pk Area
294.83
11.83
4.83
10.83
AREA
5:49:33 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
11.42
57.46
91.00
60.10
0.17
0.17
0.17
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
16.1
3.0
3.0
5.9

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.994
0.978
1.000
1.000
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.10E+000
2.04E-001
1.03E-001
1.86E-001
+I+I+I+I-
6.26E-001
l.20E-001
9.45E-002
l.14E-001
fJ4
'fl~/(3
MDA
(pCi/liter
7.21E-002
7.21E-002
8.89E-002
7.18E-002
+I+I+I+I-
8.85E-003
8.85E-003
l. 09E-002
8.81E-003
0000056626.CNF
60~

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6000
5500
ROI Type: 3
6500
Channel Data Report
4/29/2013
12:55:51 PM
Page
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t;188
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
D-93 TOT
1304105A-UU
18
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_041
05026930A
91087
System Bkgd 55753
<not performed>
Sample Size:
Sample Date/Time:
1. OOOE+OOO +/-

O.OOOE+OOO liter
4/9/2013
7:53:48 AM
4/29/2013 10:00:51 AM
170.0 minutes
170. 0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.597 mL
0.1713 +/- 0.0102
0.1978 +/- 0.0034 on 12/16/2012
0.8660 +/- 0.0539
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.284
4.725
4.378
4.141
AREA
REPORT
Net
Pk Area
Pk Area
Error %
330.00
25.15
1.49
10.09
5:49:31 PM
10.81
39.85
190.02
74.39
Ambient
Backgnd
0.00
0.85
0.51
3.91
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
33.3
4.5
3.0
4.5

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.991
1. 000
0.987
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.12E+OOO
3.90E-001
2.85E-002
1.56E-001
+/+/+/+/-
5.99E-001
1.62E-001
5.42E-002
1.17E-001
MDA
(pCi/liter
9. 30E-002
9.28E-002
l.OOE-001
1.50E-001
+I+I+I+I-
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993:
1001:
1009:
1017:
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Page 1 of 2
4/29/2013 5:51:06 AM
QA SUMMARY REPORT
Review Of QA Results - Pulser Check
Date
Time
: 4/29/2013
: 5:51 :06 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha Oil
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
21f
21f
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst! OODC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst IOODC
Alpha AnalystlOODO
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
NotDone
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
DATE
4/29/2013 5:29:44 AM
4/29/2013 5:29:45 AM
4/29/2013 5:29:45 AM
4/29/2013 5:29:46 AM
4/29/2013 5:29:47 AM
4/29/2013 5:29:48 AM
4/29/2013 5:29:49 AM
4/29/2013 5:29:50 AM
4/29/2013 5:29:51 AM
4/29/2013 5:29:52 AM
4/29/2013 5:29:53AM
4/29/2013 5:29:53 AM
4/29/2013
4/29/2013
4/29/2013
4/29/2013
4/29/2013
5:29:55 AM
5:29:56 AM
5:29:58 AM
5:29:59 AM
5:30:01 AM
4/29/2013
4/29/2013
4/29/2013
4/29/2013
5:30:03 AM
5:30:04 AM
5:30:06 AM
5:30:07 AM
U199
Page 2 of 2
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
ReviewofQA~- ~~
DEVICE
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
APPROVED BY:
APPROVAL DATE:
4~l!I201S
..
~LA\>
Passed
Passed
Not Done
Passed
Passed
Passed
55106 AM
DATE
4/29/2013 5:30:09 AM
4/29/2013 5:30:11 AM
4/29/2013 5:30:13 AM
4/29/2013 5:30:15 AM
4/29/2013 5:30:17 AM
Library Listing Report
6/12/12
Page
12:17:04 PM
*************************************************************************
L I B R A R Y
*****
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:
Uranium
U-232,-234,-235,-238
Nuclide Library Description:
Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2o174E+009
7o731E+012
2o221E+016
1o410E+017
Energy
(keV )
Energy
uncerto {keV
OoOOO
OoOOO
OoOOO
OoOOO
53020500*
4761o500*
4385o500*
41840400*
key line
TOTALS:
Nuclides
Energy Lines
Yield
{%)
99o8000
99o8000
80o9000
100o2300
Yield
Uncert. (Abs 0+-)
0 00000
OoOOOO
0 0 0000
0.0000
SECTION IX
ANALYTICAL DATA (ISOTOPIC THORIUM)
Eberline Services
Analysis Sheet
13-04105
Printed: 4/30/2013 5:39AM

Page 1 of 3
ThiSO
Run 1
Internal ] Sample
Fraction 1 Desc
Work Order
Run
Date Received
4/16/2013
Lab Deadline
5/7/2013
-~_!14
05
Client I Engineering Management Support, Inc.
Project
West Lake OU-1
Report Level
06
10
WA
NAS NS-3004 Modified
Th-18a
22.467
Carrier
1-
Carrier Cone (mg/ml)
I mGF'1~68
TRG
-----1 I
12
' TRG '
15
TRG__l
16lTRG
17
i TRG
Sample
Aliquot
04/16/13 00:00
1.0000E+OO
_[__ o4fWl13 00:00
1.0000E+OO
39-_.~
1.0000E+OO
~9~ 1.0000~+~~
04/09/13
04/09/13 09:30
1.0000E+OO
45
: 04/o9/1? 10:44
1.0000E+OO
D-87 TOT
42
04/09/13 11:05
1.0000E+OO
D-87 DIS
42
__ I
37
04/09/13_12:00
1.0000E+OO
TOT
PZ-106-SD DIS
S-82 TOT
~~ TR_G_J___
46
04/1J9/131n7
1.0000EOO
41-- _o4/o9,13 12:_56 -:
1.0000E+O~
I-9TOT
43
' 04/09/1313:35
1.0000E+OO
1-9 DIS
43
04/09/1313:35
1.0000E+OO
D-93 TOT
40
_ PZ-106-SS DIS
I1
;;-t~~~
.~
Sample
Date
- -
! TRG :
..
Login
CPM
1-68 DIS
_,_
--~"-1
Alpha Spectroscopy
Th-229
Tracer Act (dpm/g) I
:'04""S TOT
PZ-204-SS DIS
pCi
Radiometric Tracer I
Radiometric Sol#
BLANK
oopz.
[_ TRG
Method I
Instrument Type
LCS
.
' TRG '
Aliquot Units
Matrix
LCS
Client
ID
~2~
01
Analysis Code
Activity Units
D-93 DIS
___
-~+-----
04/09/1314:28l~OOE+OOI
4~__r04/09/1314:2~-l-~OO~
1:<1
r~,l
t~~
t-.1
"'"*Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 4/30/2013 5:39AM

Page 2 of 3
II
Internal
Fraction
Sample
Desc
01
LCS
02
MBL
5.3
DUP I
5.3
Tracer
Aliquot(g)
0.4757
Grav Filter
Final (g)
Tracer Total
ACT(dpm)
---
04
DO
05
TRG
06
TRG
07
08
1--
5.2
0.2316
0.2318
5.2
-I
TRG
0.2321
--+---TRG I
10
TRG
11
TRG
12
TRG
13
TRG
14
TRG I
15
TRG I
16
TRG
5.2
18
TRG
SAF
1.
--- I
0.00
I
0.00
0.2318'
5.2
0.2309
5.2
1---o.oor=-r-_~----o:oor
~:::~: :- --::E
'
'
0.00
:::10.00
_I
I
TRG
19
0.2290 !
11---t-----+,
5.1
n.oo
-----+- --
--+----+ --+---
---
L
1
'
--
__
- --
----1----
--=t=l-----+----r-_
---r_L-J__
--+ I
--+ --~
I
'
-~-:---4
----+---I
t--t
I
---+----+-
lq~)
~I
2.
II
1--
-- --i---
tf:~
SAF
o.oo
o~- _-~
--
TRG
----~!
o.ool
--
17
Mean
%Rec
0.00
'
TRG
1-----
Grav
%ReC
0.00
09
1-----
10.7
-----j------1
03
Grav Filter
Net (g)
* SAF1 is used for Gross Alpha and all other radio nuclides. SAF2 is used for Gross Beta only.
Eberline Services
Analysis Sheet
Printed: 4/30/2013 5:39AM

Page 3 of 3
13-04105
ThiSO
Run 1
Internal
Fraction
Sample
Desc
01
I LCS
02
MBL
03
DUP
Rough Prep
Date
I
I
Rough Prep
By
--l
F --
Prep
Date
Prep
Sep tO
Date/Time
By
04/24/13 11:57 I JBARNARD
! 04/24/13 11 :57
JBARNARD
~ ~n4113 1;:;,_- JBARNARD r
---=
Sep tO
Sep t1
Date/Time
By
+-
Sep t1
By
04/24/
'
tlil
f'i~:ll
IJ"i
Eberline Services
0:
{!
8
.~
~
0
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~
'
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-~
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Work Order: 13-04105-ThiS0-1
Sample
Client
Activity
Oesc
Identification
Units
TH-228
LCS
LCS
pCi/1
4.46E+OO
6.85E-01
5.75E-02
TH-228
MBL
BLANK
pCi/1
5.03E-02
5.23E-02
5.48E-02
Lab
Fraction
Nuclide
01
02
Results
Error Estimate
MDA
4.80E+OO
LCS
%R
LCS
Flag
92.72
OK
RPD
Flag
MDA
Flag
OK
PZ-204-5S TOT
pCi/1
3.15E-01
1.32E-01
5.87E-02
TH-228
DO
PZ-204-5S TOT
pCi/1
2.21E-01
1.07E-01
5.67E-02
OK
04
05
TH-228
TRG
PZ-204-5S DIS
pCi/1
3.81E-02
6.75E-02
1.21 E-01
OK
.c
06
TH-228
TRG
1-68 TOT
pCI/1
2.66E+OO
6.55E-01
7.78E-02
OK
07
TH-228
TRG
1-68 DIS
pCI/1
O.OOE+OO
4.26E-02
9.23E-02
OK
08
TH-228
TRG
D-87TOT
pCI/1
2.17E-01
1.26E-01
9.18E-02
OK
09
TH-228
TRG
D-87 DIS
pCi/1
7.21E-02
6.91E-02
8.39E-02
OK
10
TH-228
TRG
PZ-106-5D TOT
pCi/1
2.11E-01
1.13E-01
1.01E-01
OK
11
TH-228
TRG
PZ-1 06-5D DIS
pCi/1
-9.20E-04
5.64E-02
1.37E-01
OK
12
TH-228
TRG
S-82TOT
pCi/1
1.24E-01
1.01 E-01
1.22E-01
OK
.;
.5
13
TH-228
TRG
S-82 DIS
pCill
-4.23E-03
2.56E-02
8.06E-02
OK
14
TH-228
TRG
PZ-106-5S TOT
pCi/1
3.55E-02
5.81E-02
1.02E-01
"
15
TH-228
TRG
PZ-106-SS DIS
pCi/1
9.24E-03
5.39E-02
1.22E-01
OK
16
TH-228
TRG
1-9TOT
pCi/1
1.47E-01
1.09E-01
1.32E-01
OK
17
TH-228
TRG
1-9 DIS
pCi/1
-7.05E-03
1.13E-01
2.78E-01
OK
18
TH-228
TRG
D-93 TOT
pCi/1
1.60E-01
1.10E-01
1.33E-01
OK
"
19
TH-228
TRG
D-93 DIS
pCi/1
5.45E-02
5.89E-02
8.56E-02
OK
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en
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OK
TH-228
ill
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LCS
Known
03
11!!1
Nl
11!!1
Printed: 5/1/2013 10:07 AM

Page 1 of 3
NA
OK
OK
Eberline Services
~
~
0:
-!:0
-~
"
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Nuclide
Sample
Deso
Sample
Sample
Radiometric
G~
Mean
Date
Aliquot
%Rec
%Rec
%Rec
01
TH-228
LCS
04/16/13 00:00
1.00E+OO
120.84
0.00
0.00
02
TH228
MBL
04/16/13 00:00
1.00E+OO
113.21
0.00
0.00
03
TH-228
DUP
04/09/13 09:30
1.00E+OO
116.15
o.oo
0.00
04
TH-228
DO
04/09/13 09:30
1.00E+OO
115.33
0.00
0.00
05
TH-228
TRG
04/09/13 09:30
1.00E+OO
76.27
0.00
0.00
......c:
06
TH-228
TRG
04/09/13 10:44
1.00E+OO
76.39
o.oo
0.00
07
TH-228
TRG
04/09/13 10:44
1.00E+OO
98.35
0.00
0.00
08
TH-228
TRG
04/09/1311:05
1.00E+OO
91.35
o.oo
0.00
09
TH-228
TRG
04/09/13 11:05
1.00E+OO
115.06
0.00
0.00
10
TH-228
TRG
04/09/1312:00
1.00E+OD
121.12
0.00
0.00
11
TH-228
TRG
04/09/13 12:00
1.00E+OO
115.36
0.00
0.00
12
TH-228
TRG
04/09/13 12:27
1.00E+OO
101.49
0.00
0.00
13
TH-228
TRG
04/09/1312:27
1.00E+OO
132.78
0.00
0.00
14
TH-228
TRG
04/09/1312:56
1.00E+OO
123.17
0.00
0.00
SAF
en
-
'
.;
E
,:
0
0.
0.
'
TH-228
TRG
04/09/1312:56
1.00E+OO
93.37
0.00
o.oo
16
TH-228
TRG
04/09/13 13:35
1.00E+OO
104.89
0.00
0.00
17
TH-228
TRG
04/09/1313:35
1.00E+00
45.61
0.00
0.00
18
TH-228
TRG
04/09/1314:28
1.00E+OO
102.73
0.00
0.00
19
TH-228
TRG
04/09/13 14:28
1.00E+OO
124.85
0.00
0.00
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Printed: 5/1/2013 10:07 AM

Page 2 of 3
Lb
Fraction
-- -
--
--
- - - - - - '---
Eberline Services
~
~
~
0:
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0
(,)
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..
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~
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Fraction
01
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TH-228
Printed: 5/1/2013 10:07 AM

Page 3 of 3

Sample
Dese
Countlng
DatefTime
LCS
0413011311:48
Halfllfe
(days)
Count
Time
Bkg
Detect
Carrier
A_Spec
Alpha_035
170 3.71 E+02
2.00 E-03
18.3
A_Spec
Alpha_037
170 3.83 E+OO
1.00 E-03
17.8
Counts
CPM
Eff
02
TH-228
MBL
04130/13 11 :48
03
TH-228
DUP
04/30/13 11:49
A_Spec
Alpha_040
170 2.57 E+01
2.00 E-03
19
04
TH-228
DO
04130113 11:48
A_Spec
Alpha_041
170 1.87 E+01
2.00 E-03
19.8
05
TH-228
TRG
04/30113 11:49
A_Spec
Alpha_042
170 1.98 E+OO
6.00 E-03
18.5
06
TH-228
TRG
04/30/13 11:48
A_Spec
Alpha_044
170 1.43 E+02
1.00 E-03
19
07
TH-228
TRG
0413011311:48
A_Spec
Alpha_046
170 1.00 E+OO
0.00 E+OO
17.9
08
TH-228
TRG
0413011311:48
A_Spec
Alpha_047
170 1.33 E+01
4.00 E-03
18.2
09
TH-228
TRG
0413011311:48
A_Spec
Alpha_048
170 5.15 E+OO
5.00 E-03
16.8
10
TH-228
TRG
04/30113 12:43
A_Spec
Alpha_018
170 1.68 E+01
1.30 E-02
17.8
11
TH-228
TRG
04/3011312:43
A_Spec
Alpha_022
170 -6.00 E-02
1.80 E-02
15.3
12
TH-228
TRG
04130113 12:43
A_Spec
Alpha_024
170 7.96 E+OO
1.20 E-02
17.1
13
TH-228
TRG
04/30/13 12:43
A_Spec
Alpha_025
170 -3.60 E-01
8.00 E-03
17.4
14
TH-228
TRG
04/30/1312:43
A_Spec
Alpha_027
170 2.79 E+OO
1.30 E-02
17.3
"("'"
-en
~
1-
1--
Nuclide
ill
.;
.E
'!!
0
a.
a.
:l
"'.c
15
TH-228
TRG
04/30/1312:43
A_Spec
Alpha_029
170.02 6.20 E-01
1.40 E-02
19.5
" ..."'
E
16
TH-228
TRG
04/30/13 14:35
A_Spec
Alpha_003
170.02 9.94 E+OO
1.80 E-02
17.5
17
TH-228
TRG
04130/13 14:35
A_ Spec
Alpha_004
170.02 -2.30 E-01
1.90 E-02
19.4
"'c
18
TH-228
TRG
04/30/13 14:35
A_Spec
Alpha_010
170.02 1.19 E+01
2.40 E-02
19.7
19
TH-228
TRG
04/30/13 14:35
A_Spec
Alpha_011
170.02 4.96 E+OO
1.20 E-02
19.7
(,)
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Lab
Fraction
Nuclide
01
Sample
Client
Activity
Doso
Identification
Units
TH-230
LCS
LCS
pCi/1
4.36E+OO
6.74E-01
5.75E-02
02
TH-230
MBL
BLANK
pCi/1
1.40E-01
8.85E-02
6.29E..02
03
TH-230
DUP
PZ-204-SS TOT
pCi/1
1.64E..()1
9.19E..02
5.75E-02
04
TH-230
DO
PZ-204-SS TOT
pCi/1
2.23E..01
1.08E-01
6.96E..02
OK
Cl)
05
TH-230
TRG
PZ-204-SS DIS
pCi/1
9.71E..02
9.34E..02
1.13E-01
OK
J:
06
TH-230
TRG
1-68 TOT
pCi/1
4.14E+OO
9.31E01
7.63E02
OK
07
TH-230
TRG
1-68 DIS
pCi/1
1.06E-01
8.55E-02
9.04E..02
OK
08
TH-230
TRG
D-87 TOT
pCi/1
4.04E..01
1.74E-01
9.00E..02
OK
09
TH-230
TRG
D-87 DIS
pCi/1
1.10E-01
8.27E..02
8.24E02
OK
10
TH-230
TRG
PZ-106-SD TOT
pCI/1
1.33E-01
8.70E-02
8.13E-02
OK
11
TH-230
TRG
PZ-1 06-SD DIS
pCi/1
3.40E..01
1.56E..01
1.03E..01
OK
12
TH-230
TRG
S-82 TOT
pCifl
2.39E-01
1.27E-01
7.31E..02
OK
13
TH-230
TRG
S-82 DIS
pCi/1
8.43E..02
6.56E-02
6.50E02
OK
14
TH-230
TRG
PZ..1 06-SS TOT
pCi/1
1.62E..01
9.55E-02
7.86E..()2
OK
15
TH-230
TRG
PZ-106-SS DIS
pCi/1
1.48E..01
9.88E-02
8.75E..02
OK
16
TH-230
TRG
1-9 TOT
pCi/1
1.11E..01
8.82E..02
9.94E..02
OK
17
TH-230
TRG
1-9 DIS
pCi/1
1.54E..01
1.50E..01
1.80E-01
OK
18
TH-230
TRG
D-93 TOT
pCi/1
8.72E..02
7.52E-02
9.01E..02
OK
c"
19
TH-230
TRG
D-93 DIS
pCi/1
1.58E-01
8.52E-02
5.15E..02
OK
Results
Error Estimate
MDA
1-
~
0
Q.
Q.
:I
U)
~
- "."e
.
C1
:;;
C1
.:
"
;;,
c
w
~i!!!
M
tali
ttl
LCS
LCS
LCS
RPD
MDA
Known
%R
Flag
Flag
Flag
79.52
OK
5.49E+OO
Blank
Flag
OK
OK
T"'
.s
~
0
Printed: 5/1/2013 10:07 AM

Page 1 of 3
NA
OK
OK
Eberline Services
Nuclide
Sample
Desc
Sample
Sample
Radiometric
Gw
Date
Aliquot
%Rec
%Rec
01
TH-230
LCS
04/16/13 00:00
1.00E+OO
120.84
0.00
0.00
02
TH-230
MBL
04/16/13 00:00
1.00E+OO
113.21
0.00
0.00
03
TH-230
DUP
04/09/13 09:30
1.00E+OO
116.15
0.00
0.00
04
TH-230
DO
04/09/13 09:30
1.00E+OO
115.33
0.00
0.00
(/)
05
TH-230
TRG
04/09/13 09:30
1.00E+OO
76.27
0.00
0.00
J:
06
TH-230
TRG
04/09/1310:44
1.00E+OO
76.39
0.00
0.00
07
TH-230
TRG
04/0911310:44
1.00E+00
98.35
0.00
0.00
08
TH-230
TRG
0410911311:05
1.00E+OO
91.35
0.00
0.00
09
TH-230
TRG
0410911311:05
1.00E+OO
115.06
0.00
0.00
10
TH-230
TRG
0410911312:00
1.00E+OO
121.12
0.00
0.00
11
TH-230
TRG
04109113 12:00
1.00E+OO
115.36
0.00
0.00
12
TH-230
TRG
04/09113 12:27
1.00E+OO
101.49
0.00
0.00
13
TH-230
TRG
04109113 12:27
1.00E+OO
132.78
0.00
0.00
14
TH-230
TRG
04109113 12:56
1.00E+OO
123.17
0.00
0.00
15
TH-230
TRG
04109113 12:56
1.00E+OO
93.37
0.00
0.00
"E
16
TH-230
TRG
04109113 13:35
1.00E+OO
104.89
0.00
0.00
17
TH-230
TRG
0410911313:35
1.00E+OO
45.61
0.00
0.00
"'c
18
TH-230
TRG
0410911314:28
1.00E+OO
102.73
0.00
0.00
"
c.
c
19
TH-230
TRG
04109113 14:28
1.00E+OO
124.85
0.00
0.00
Lob
Fraction
Printed: 5/1/201310:07 AM
Page 2 of3
Mean
%Rec
SAF
Sep tO
Sep t1
DatefTime
Date/Time
0:
.g
0
0
-~
-;;;~
c
"
~t:
~
~
"'
--- I-
'I:'""
-1-
ill
.;
.5
1:!
0
c.
c.
::1
Ul
-~
.""'.
::;;
;:
"c
I
'
Ill
ra
....I''~JI,
t!l
_ _ l__
Eberline Services
,:
a:
~
0
0
-~
~
~
<(
t:
~
-~
.,
Lob
Fraction
Nuclide
01
Printed: 5/1/2013 10:07 AM

Page 3 of 3

Sample
Counting
Oesc
Date/Time
TH-230
LCS
02
TH-230
03
Halflife
(days)
Count
Time
Bkg
CPM
Detect
Carrier
04/30/1311:48
A_Spec
Alpha_035
170 3.63 E+02
2.00 E-03
18.3
MBL
04/30/1311:48
A_Spec
Alpha_037
170 1.07 E+01
2.00 E-03
17.8
TH-230
DUP
04/30/1311:49
A_Spec
Alpha_040
170 1.37 E+01
2.00 E-03
19
04
TH-230
DO
04/30/1311:48
A_Spec
Alpha_041
170 1.91 E+01
5.00 E-03
19.8
05
TH-230
TRG
04/30/1311:49
A_ Spec
Alpha_042
170 5.15 E+OO
5.00 E-03
18.5
06
TH-230
TRG
04/30/1311:48
A_Spec
Alpha_044
170 2.27 E+02
1.00 E-03
19
07
TH-230
TRG
04/30/1311:48
A_Spec
Alpha_046
170 7.00 E+OO
0.00 E+OO
17.9
08
TH-230
TRG
04/30/1311:48
A_Spec
Alpha_047
170 2.53 E+01
4.00 E03
18.2
09
TH-230
TRG
04/30/13 11:48
A_Spec
Alpha_048
170 8.00 E+OO
0.00 E+OO
16.8
10
TH-230
TRG
04/30/1312:43
A_Spec
Alpha_018
170 1.08 E+01
7.00 E-03
17.8
11
TH-230
TRG
04/30/1312:43
A_Spec
Alpha_022
170 2.26 E+01
8.00 E-03
15.3
12
TH-230
TRG
04/30/1312:43
A_Spec
Alpha_024
170 1.57 E+01
2.00 E-03
17.1
13
TH-230
TRG
04/30/13 12:43
A_Spec
Alpha_025
170 7.32 E+OO
4.00 E-03
17.4
14
TH-230
TRG
04/30/1312:43
A_Spec
Alpha_027
170 1.30 E+01
6.00 E03
17.3
15
TH-230
TRG
04/30/1312:43
A_Spec
Alpha_029
170.02 1.01 E+01
5.00 E-03
19.5
"E
16
TH-230
TRG
04/30/13 14:35
A_Spec
Alpha_003
170.02 7.64 E+OO
8.00 E-03
17.5
17
TH-230
TRG
04/30/13 14:35
A_Spec
Alpha_004
170.02 5.15 E+OO
5.00 E-03
19.4
"'c
18
TH230
TRG
04/30/13 14:35
A_Spec
Alpha_010
170.02 6.64 E+OO
8.00 E03
19.7
"
a,
c
w
19
TH-230
TRG
04/30/13 14:35
A_Spec
Alpha_D11
170.02 1.47 E+01
2.00 E-03
19.7
Counts
Eff
"('""
-....c
(/)
'
'i:
ill
.E
0
Q.
Q.
:I
"'c
~
~
-~
iJ
"
.:;;.."'
;::
"
'--'---~lin
Ill
....
......
Eberline Services
~
0:
"0
0
-~
~
1ii
~
'<
'
"E
0
"!:
:!l
~
-~
.,
."1::s
ill
Nuclide
01
TH-232
02
TH-232
MBL
BLANK
pCi/1
O.OOE+OO
3.64E-02
7.87E.02
03
TH-232
DUP
PZ-204-SS TOT
pCi/1
1.16E-01
7.67E.02
5.74E-02
04
TH-232
DO
PZ-204-SS TOT
pCi/1
7.88E.02
7.07E-02
9.29E.02
C/)
05
TH-232
TRG
PZ-204-SS DIS
pCi/1
2.48E-02
5.38E-02
1.06E.01
.r:::::
06
TH-232
TRG
1-68 TOT
pCi/1
7.99E.01
2.79E.01
7.61 E-02
OK
07
TH-232
TRG
1-68 DIS
pCi/1
2.76E.02
4.23E.02
6.28E-02
OK
08
TH-232
TRG
D-87TOT
pCi/1
6.10E-02
6.35E-02
6.64E.02
OK
09
TH-232
TRG
D-87 DIS
pCUI
1.37E.02
3.81E.02
8.22E.02
OK
10
TH-232
TRG
PZ-1 06-SD TOT
pCi/1
1.41E.01
9.06E.02
8.75E.02
OK
11
TH-232
TRG
PZ-1 06-SD DIS
pCi/1
-5.40E.03
3.26E.02
1.03E-01
OK
12
TH-232
TRG
S-82TOT
pCill
1.07E.01
8.74E-02
9.62E.02
OK
.5
13
TH-232
TRG
S-82 DIS
pCi/1
3.68E.03
2.38E.02
6.49E.02
OK
t:
0
14
TH-232
TRG
PZ-106-SS TOT
pCi/1
1.64E.02
3.56E-02
7.02E.02
OK
-..
rJ)
"
15
TH-232
TRG
PZ-106-SS DIS
pCi/1
1.46E.02
4.05E.02
8.75E.02
OK
c
E
16
TH232
TRG
1-9 TOT
pCi/1
-1.72E.02
3.12E-02
9.53E.02
OK
17
TH-232
TRG
1-9 DIS
pCi/1
1.04E.01
1.21 E-01
1.57E-01
OK
18
TH-232
TRG
093 TOT
pCi/1
1.06E.02
3.82E-02
8.64E-02
OK
19
TH-232
TRG
093 DIS
pCI/1
2.68E-02
3.72E.02
5.64E.02
OK
Sample
Client
Activity
Desc
Identification
Units
LCS
LCS
pCi/1
Results
5.17E+OO
Error Estimate
7.71E.01
MDA
5.01E-02.
-1-
'
.."'
."'
;;,
c
IU
.l~.j,
LCS
LCS
Flag
%R
4.80E+OO
107.69
__j
RPO
Flag
OK
MOA
Flag
Blank
Flag
OK
OK
NA
OK
OK
OK
OK
'
::;:
lll!l
LCS
Known
Q.
Q.
l'li
Printed: 5/1/2013 10:08 AM

Page 1 of 3
Lob
Fraction
.;
I
!
Eberline Services
0:
{l
0
(.)
-~
..
~
<::
q;
Nuclide
Sample
Desc
Sample
01
TH-232
LCS
04/16/13 00:00
1.00E+OO
120.84
0.00
0.00
02
TH-232
MBL
04/16/13 00:00
1.00E+OO
113.21
0.00
0.00
03
TH-232
DUP
04/09/13 09:30
1.00E+OO
116.15
o.oo
0.00
04
TH-232
DO
04/09/13 09:30
1.00E+OO
115.33
0.00
0.00
en
-....
05
TH-232
TRG
04/09/13 09:30
1.00E+OO
76.27
o.oo
0.00
J:
06
TH-232
TRG
04/09/1310:44
1.00E+OO
76.39
0.00
0.00
07
TH-232
TRG
04/09/13 10:44
1.00E+OO
98.35
0.00
0.00
08
TH-232
TRG
04/09/13 11 :05
1.00E+OO
91.35
0.00
0.00
09
TH-232
TRG
04/09/1311:05
1.00E+OO
115.06
0.00
0.00
10
TH-232
TRG
04/09/13 12:00
1.00E+OO
121.12
0.00
0.00
11
TH-232
TRG
04/09/13 12:00
1.00E+OO
115.36
0.00
0.00
12
TH-232
TRG
04/09/1312:27
1.00E+OO
101.49
0.00
0.00
..;
.E
13
TH-232
TRG
04/09/13 12:27
1.00E+OO
132.78
0.00
0.00
t:0
14
TH-232
TRG
04/09/13 12:56
1.00E+OO
123.17
0.00
0.00
"
15
TH-232
TRG
04/09/13 12:56
1.00E+OO
93.37
0.00
0.00
"
16
TH-232
TRG
04/09/1313:35
1.00E+OO
104.89
0.00
0.00
17
TH-232
TRG
04/09/13 13:35
1.00E+OO
45.61
0.00
0.00
18
TH-232
TRG
04/09/1314:28
1.00E+OO
102.73
0.00
0.00
19
TH'232
TRG
04/09/13 14:28
1.00E+OO
124.85
0.00
0.00
"!:
~
~
.,~
"'
ill
a.
a.
rn
c
E
~
""'.c
..
Date
Sample
Aliquot
Radiometric
%Rec
Gr.w
Mean
%Rec
%Rec
SAF
"'c
c"
"
;;,
c
w
t!l
~,)
l~~
~~
SeptO
Date/Time
Sept1
OatefTime
:;;
;:
Printed: 5/1/201310:08 AM
Page 2 of 3
Lab
Fraction
f-0
Eberline Services
0:
.g
0
(.)
.!/!
...~
""
~
1!
~
~
.,~
.s
ill"
Lab
~<u..:B.
t!lll
01
TH-232
LCS
02
TH-232
03
Halflife
(days)
Count
Time
Bkg
CPM
04/30/1311:48
A_Spec
Alpha_035
170 4.31 E+02
1.00 E-03
18.3
MBL
04/30/1311:48
A_Spec
Alpha_037
170 1.00 E+OO
0.00 E+OO
17.8
TH-232
DUP
04/30/1311:49
A_Spec
Alpha_040
170 9.66 E+OO
2.00 E-03
19
04
TH-232
DO
04/30/1311:48
A_Spec
Alpha_041
170 6.79 E+OO
1.30 E-02
19.8
05
TH-232
TRG
04/30/1311:49
A_Spec
Alpha_042
170 1.32 E+OO
4.00 E-03
18.5
06
TH-232
TRG
04/30/13 11:48
A_Spec
Alpha_044
170 4.38 E+01
1.00 E-03
19
07
TH-232
TRG
04/30/1311:48
A_Spec
Alpha_046
170 1.83 E+OO
1.00 E-03
17.9
08
TH-232
TRG
04/30/1311:48
A_Spec
Alpha_047
170 3.83 E+OO
1.00 E-03
18.2
09
TH-232
TRG
04/30/13 11:48
A_ Spec
Alpha_048
170 1.00 E+OO
0.00 E+OO
16.8
10
TH-232
TRG
04/30/13 12:43
A_Spec
Alpha_018
170 1.15 E+01
9.00 E-03
17.8
11
TH-232
TRG
04130/1312:43
A,_Spec
Alpha_022
170 -3.60 E-01
8.00 E-03
15.3
12
TH-232
TRG
04/30/1312:43
A_ Spec
Alpha_024
170 6.98 E+OO
6.00 E-03
17.1
.;
.5
13
TH-232
TRG
04/30/13 12:43
A_Spec
Alpha_025
170 3.20 E-01
4.00 E-03
17.4
t:0
14
TH-232
TRG
04/30/1312:43
A_Spec
Alpha_027
170 1.32 E+OO
4.00 E-03
17.3
"'"c
15
TH-232
TRG
04/30/13 12:43
A_Spec
Alpha_029
170.02 1.00 E+OO
0.00 E+OO
19.5
Counts
Eff
"('""
-en
.c
1-
"E
""'
16
TH-232
TRG
04/30/13 14:35
A_Spec
Alpha_003
170.02 -1.19 E+OO
7.00 E-03
17.5
17
TH-232
TRG
04/30/13 14:35
A_Spec
Alpha_004
170.02 3.49 E+OO
3.00 E-03
19.4
"'c
18
TH-232
TRG
04/30/1314:35
A_Spec
Alpha_010
170.02 8.10 E-01
7.00 E-03
19.7
"
19
TH-232
TRG
04/30/13 14:35
A_Spec
Alpha_011
170.02 2.49 E+OO
3.00 E-03
19.7
..::;;.
"c
;;,
c
w
fii~
Counting
DateiTime
Cartier
;::
1;;,'!)
Sample
Desc
Detect
Printed: 5/1/2013 10:08 AM

Page 3 of3
Nuclide
Fraction
Q.
Q.
Count Room Report

Printed: 4/30/2013 5:39AM
13-04105-ThiS0-1 (pCi/1) in WA
Tracer ID: Th-18a
Page 1 of 1
/\.- "~ lv-"'

Internal
Fraction
Sample
Desc
Sample
ID
Date
Sample
Aliquot
LCS
04/16/13 00:00
1.0000
0.4757
MBL
BLANK
04/16/1300:00
1.0000
0.2361
DUP
PZ-204-SS TOT
04/09/13 09:30
1.0000
0.2355
5.2910 I
DO
PZ-204-SS TOT
04/09/13 09:30
1..nnnn
___
n---.
?"<1R
_ ,
5.2034
TRG
PZ-204-SS DIS
04/09/13 09:30
1.0000
0.2318
5.2079
O~I(LCS
02
03
04
Client
Tracer
Aliquot (g)
06
-:;~
07
TRG
___
1-68 TOT
04/09/131o:44 -
1-68 DIS
04/09/13 10:44
TR~--
08
~--:: :~:-
, ::;::;: :-:: .::
1.0000
0.2321
5.2146
--rl --::~: ~
T~G-i ---~2 TOT__
04/09/13 12:27
1.000~
--0.2_318 I
5.2079
TRG
04/09/1312:27
1.0000
0.2312
5.1944
0.2309 .
5.1876
i-
;:;._
16
~ ~
~=---j
TRG
i<"'
1..11
+-__
I
---
5.1719
0.00
-----+--- -+-----1 --~
0.2314
5.1989
0.00
J_
1.0000
04/09/1312:56
1.0000 --~301
1-9 TOT
04/09/1313:35 --
1.0000
I-9DIS
04/09/1313:351
1):93 TOT
--
D-93 DIS
1~301
-~oooo__L__
--=
04/09/1314:28
1.~000.
04/09/13 14:28
1.0000___
--~
-------
0.2302
,-04/09/1312:56-
PZ-106-SS DIS
TRG+---TRG
18
-~I
TRG
TOT
0.00
0.00
04/09/1312:00
PZ-106-~S
I
---
==r-o-.~-o+--i---1
----
PZ-106-SD DIS
SAF
2.
::~::~~-l-----=r-i,-.-. .~.~~f~----1
1.0000
1--~
1.0000:-1'
S-82 DIS
--+
o.oo
04/09/1312:00
~--~~l-."1".~
15
-~---
0.00
:
l
5.2168 .
: :::::
SAF
1*
0.00
--~i---j----j
I
1
PZ-106-SDTOT
+---+-- ---
5.3045
o.232Z-
I Radiometric I
% Rec
0.00
1.oo~~---:
,1tc\~
(0 1~-2.:._
Radiometric
Tracer (pCi)
10.6876
1--+----+---~------+-----t------1----
05
Tracer
ACT (dpm)
-I
-=-i
0.00
0.00
0.00
-:-=
i
'I'
t_ L--1
5.1697
0.00
5.1697 __
0.00 ' ---+---1
o.23071_
5.18~
0.2310
5.1899 I --
0.229~ ~
5.1449 --
__
o.oo__
-
.0.00
:
--
__
--~00
I
-----
Eberline Services
Oak Ridge laboratory
Internal Work Order
Run
Analysis Code
Date
Technician
13-04105
ThiSO
4/24/2013 11:52
JBARNARD
LCS & Matrix Spikes

Isotope
Page 1 of 1
Printed: 4/24/2013 11:57 AM
So/#
Activity
dpmlg
Approx
Addition
Th-228
Th-8b
103.5601
412412013
Th-230
Th-1b
23.525
Th-232
Th-Bb
103.560
'
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used{g)
Volume
Used(g)
LCS
Known
pCi
Error
Estimate
0.00
0.000
0.00
0.000
0.00
0.000
4124/2013
0.500
0.5178
5.49
0.148
oool
0.000
0.00
0.000
0.00
0.000
4/24/2013
0.100
0.1030
4801
0.173
0.00
'
0.000
0.00
0.000
0.00
0.000
Activity
dpmlg

Solution
Date
Volume
Used(g)
Approx
Addition
Tracer
LCS
Th-229
Th~18a
22.467 4/24/2013
0.4757
0.2200
02
Th-229
Th~18a
22.467 4/24/2013
0.2361
0.2200
03
Th-229 I Th1Ba
22.467 4/24/2013
0.2355
0.2200
f:J. 2361 '3
04
Th-229
Th18a
22.467 4/24/2013
0.2316
0.2200
05
Th-229
Th-1Ba
22.467 4/24/2013
0.2318
0.2200
2355 '3
-0.2316 9
06
Th-229
Th~18a
22.467 4/24/2013
0.2322
0.2200
07
Th-229
Th-18a
22.467 4/24/2013
0.2321
0.2200
08
Th-229
Th~ 18a
22.467 4/24/2013
. 0.2326
0.2200
09
Th-229
Th~18a
22.467
4124/2013
0.2312
0.2200
10
Th-229
Th-1Ba
22.467 4/24/2013
0.2302
0.2200
11
Th-229
Th1Ba
22.467 4/24/2013
0.2314
0.2200
12
Th-229
Th-18a
22.467 4/24/2013'
. 0.2318
0.2200
13
Th-229
Th~18a
22.467 4/24/2013
0.2312
0.2200
14
Th-229
Th-18a
22.467 4/24/2013
0.2309
0.2200
15
Th-229
Th-18a
22.467 4/24/2013
0;2301
0.2200
0.2301
0.2200
Added
pCi
0.173
01
16
Th-229
Th-1Ba
22.467 4/24/2013
17
Th-229
Th~18a
22.467 4/2412013
0.2307
0.2200
18
Th-229
Th-18a
22.467
4/24/2013
0.2310
0.2200
19
Th-229
Th-18a
22.467 4/24/2013
0.2290
0.2200
Version 2.0 08/99
I Estimate
Error
Known
pCi
4.80
Sol#
~.d!.
MSD
Error
Estimate
0.1030
Isotope
I'~
Added
pCi
0.100
fraction
Witness Initials
MS
Error
Estimate
Tracers
Technician Initials
0~4757
--!j"
-0.2::::.18 g
-0.2322 ':J
-~:3,2321 '3
-{.1. 2326 9
-0.23i2 9
-0. 2::\[i2 g
-0. 23i4 '3
-~0, 2318 9
--0.2312 '3
-0.2309 '3
-1. 2301 '3
-0.2301 '3
-13.2307 ~l
-~1~ 23:t~~i g
-0. 229(1 9
0 __c-1-.,...,
, r o '=!
~
0. 1031
Matrix Spike
Eberline Analytical
Run
Analysis Code
Rpt Units
Lab Deadline
Technician
ThiSO
liters
5/7/2013
JBARNARD
Sample
Muffle Data
R<itio
postiP:re .
Work Order
13-o41os
Lab
Fraction
Type
ClientiD
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
LCS
BLANK
PZ-204-SS TOT
PZ-204-SS TOT
PZ-204-SS DIS
1-68 TOT
1-68 DIS
D-87 TOT
D-87 DIS
PZ-106-SD TOT
PZ-106-SD DIS
S-82 TOT
S-82 DIS
PZ-106-SS TOT
PZ-106-SS DIS
1-9 TOT
1-9 DIS
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
18
19
D-93 TOT
D-93 DIS
TRG
TRG
Dilution Data
No of Oils
Aliquot Data
Dll Factor
Ratio '
Aliquot
LCS
-
MBL
DUP
..
.
..
.
..
.
_.
. ..
-
. .
:
_._.
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO I
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
----
Comments
1:1!1
1'.:1
i-'.!1
-.ll
Technician:
Printed: 4/24/2013 11:57 AM

Page 1 of 1
Aliquot Worksheet
Date:
.4,:>-/~
Net Equiv
MS Aliquot Data
Aliquot
1.0000E+OO
1.0000E+OO
...
..
Net Equiv
H3 Dist
(mil
Aliq
..
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1 ;QQOOE+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
H-3 Solids Only

Water Added
-'--
I
'
.'
__I
--
---
'
..
..
---
'
--
..,
-
.
-
Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1304105A-TH
01
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_035
04026477A
58771
System Bkgd 55748
<not performed>
Sample Size:
Sample Date/Time:

7:24:51 AM
4/30/2013
4/30/2013 11:48:51 AM
170.0 minutes
170.8 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.476 mL
0.2206 +!- 0.0130
0.1826 +/- 0.0032 on 12/16/2012
1.2084 +/- 0.0741
Control Certificate Name: NatTh Th-8

TH-232
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.713
5.397
4. 892
4.660
3.990
Net
Pk Area
1.076885 +/-
AREA
0.088010
REPORT
Pk Area
Error %
27.32
370.66
400.83
362.66
430.83
5:49:42 PM
38.04
10.19
9.79
10.30
9.45
Ambient
Backgnd
0.68
0.34
0.17
0.34
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
12.5
15.4
4.6
18.0
22.6

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.907
1.000
0.998
0.999
1.000
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
3.37E-001
4.46E+000
4.84E+000
4.36E+000
5.17E+000
+I+I+I+I+I-
1.34E-001
6.85E-001
5.57E-001
6.74E-001
7.71E-001
MDA
(pCi/liter
6.95E-002
5.75E-002
5.04E-002
5.75E-002
5.01E-002
+I+I+I+I+I-
8.01E-003
6.62E-003
5.80E-003
6.63E-003
5.78E-003
ftG
5/1(/J
~218
0000056737.CNF
Start:
1: 3463.4(kev)
stop : 1024:6473.5(kev)
Acq. Start :rue Apr 30 11:48:51 2013
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Channel Data Report
4/30/2013
Page
5:28:45 !'M
*******************************************************
R E P 0 R T
S P E C T R A L
DATA
*****
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
10250
1:
9:
17:
25:
33:
41:
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12
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7
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Channel Data Report

369:
4/30/2013
2
Sample Title:
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0
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3
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7
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a221
Channel Data Report

801:
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Sample Title:
Page
5:28:45 l!'M
0
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921:
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937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
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1
0
0
0
0
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0
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0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
2
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
2
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
-fil222
ex-AiphaTM
BLANK
1304105A-TH
02
Shelf 2
Th iso
Detector Name:
Env. Background:
Alpha_037
04026478A
91133
System Bkgd 55750
Sample Description:
Spectrum File:
Sample Geometry:
Reagent Blank:
<not performed>

7:24:51 AM
4/30/2013
4/30/2013 11:48:53 AM
170.0 minutes
Sample Size:
Sample Date/Time:
170.8 minutes
Th229 TH-18A
0.236 mL
0.2018 +/- 0.0163
0.1783 +/- 0.0033 on 1/26/2013
1.1321 +/- 0.0936
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
Net
Pk Area
5.872
5.308
4.876
4.652
3.948
-0.68
3.83
182.00
10.66
0.00
AREA
3:28:25 PM
REPORT
Pk Area
Error %
FWHM
(keV)
Ambient
Reagent
Backgnd
Backgnd
0.68
0.17
0.00
0.34
0.00
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
304.44
102.72
14.57
61.14
1960. 0
0.0
5.9
8.1
4.4
0.0

Id
Con.
Energy
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
0.997
0.956
1. 000
0.998
0.988
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
(keV)
Activity
(pCi/liter )
-9.16E-003
5.03E-002
2.40E+OOO
1. 40E-001
O.OOE+OOO
+I+I+I+I+I-
2.79E-002
5.23E-002
3. 79E-001
8.85E-002
3.64E-002
AG
5/t/I?J
MDA
(pCi/liter
7.59E-002
5.48E-002
7.91E-002
6.29E-002
7.87E-002
+I+I+I+I+I-
1.20E-002
8.65E-003
1. 25E- 002
9.93E-003
1.24E-002
0000056735.CNF
start:
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Stop : 1024:6468.5(kev)
Acq. Start :rue Apr 30 11:48:53 2013
601
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Channel Data Report
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JJJ227
Sample Description:
Spectrum File:
Sample Geometry:
PZ-204-SS TOT-DUP
1304105A-TH
03
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_040
06027396B
91135
System Bkgd 55752
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:24:51 AM
4/30/2013 11:49:02 AM
170.0 minutes
170.8 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.235 mL
0.2207 +/- 0.0171
0.1900 +/- 0.0033 on 12/16/2012
1.1615 +/- 0.0923
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.825
5.389
4.872
4. 671
3.988
AREA
REPORT
Pk Area
Error %
Net
Pk Area
3.66
25.66
198.49
13.66
9.66
5:49:33 PM
107.87
38.99
13.93
53.80
64.35
Ambient
Backgnd
0.34
0.34
0.51
0.34
0.34
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
5.9
16.3
3.0
4.5

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.997
0.999
1.000
l. 000
1.000
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.52E-002
3.15E-001
2.39E+OOO
1.64E-001
l.16E- 001
+I+I+I+I+I-
4.92E-002
l. 32E-001
3.64E-001
9.19E-002
7.67E-002
MDA
(pCi/liter
5.90E-002
5.87E-002
6.33E-002
5.75E-002
5.74E-002
+I+I+I+I+I-
8.97E-003
8.92E-003
9.62E-003
8.74E-003
8.73E-003
lfG
5/1 t~
1.228
0000056738.CNF
start:
1:3459,0(kev)
stop : 1024:6497 .l(kev)
Acq. start :Tue Apr 30 11:49:02 2013
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Channel Data Report
4/30/2013
5:29:05 PM
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P E C T R A L
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R E P 0 R T
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913:
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921:
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1001:
0
0
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1009:
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0
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0
1017:
0
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0
pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:

Env. Background:
PZ-204-SS TOT
1304105A-TH
04
Shelf 2
Th iso
Alpha_04l
05026930A
91087
System Bkgd 55753
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:24:51 AM
4/9/2013
4/30/2013 11:48:59 AM
170.0 minutes
170.8 minutes
Th229 TH-18A
0.232 mL
0.2282 +/- 0.0176
0.1978 +/- 0.0034 on 12/16/2012
1.1533 +/- 0. 0910
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.820
5.379
4.878
4.645
3.957
Net
Pk Area
AREA
REPORT
Pk Area
Ambient
Backgnd
Error %
0.15
18.66
201.83
19.15
6.79
5:49:31 PM
1397.8
45.85
13.80
45.94
88.39
0.85
0.34
0.17
0.85
2.21
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
10.3
3.0
4.5

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.995
0.998
l . 000
0. 996
0.992
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
l . 79E-003
2.21E-001
2.36E+000
2.23E-001
7.88E-002
+I+I+!+I+I-
2.50E-002
1.07E-001
3.55E-001
1.08E-001
7.07E-002
MDA
(pCi/liter
7.14E-002
5.67E-002
4.87E-002
6.96E-002
9.29E-002
+I+!+I+I+I-
l . 08E-002
8.56E-003
7.34E-003
l . 05E-002
l . 40E-002
A<t
511/13
-tl'233
0000056739.CNF
Live Time
Real Time
Start:
I
stop : 1024
Acq. start
10200.000 sec
10249.900 sec
l452.7(kev)
6S06.6(kev)
rue Apr 30 11:48:59 2013
50
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6500
Channel Data Report
4/30/2013
Page
5:29:15 l!'M
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S P E C T R A L
DATA
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*****
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.tg-236
Channel Data Report

801:
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ex-AiphaTM
PZ-204-SS DIS
1304105A-TH
05
Shelf 2
Th iso
Detector Name:
Env. Background:
Alpha_042
05026930B
84185
System Bkgd 55754
Sample Description:
Spectrum File:
Sample Geometry:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Real Time.:

4/9/2013
7:24:51 AM
4/30/2013 11:49:00 AM
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.232 mL
0.1408 +/- 0.0134
0.1846 +/- 0.0032 on 12/16/2012
0.7627 +/- 0.0736
0.175 MeV
170.8 minutes
PEAK
Energy
Nuclide
(MeV)
TH-227
TH-228
TH-229
TH-230
TH-232
5.728
5.268
4.874
4.590
3.988
Net
Pk Area
AREA
REPORT
Pk Area
Error %
2.32
1.98
124.66
5.15
1. 32
5:49:29 PM
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
0.68
1.02
0.34
0.85
0.68
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
149.12
176.34
17.58
94.34
215.97
3.0
3.0
4.5
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.925
0.913
1. 000
0. 966
1. 000
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.49E-002
3.81E-002
2.36E+000
9.71E-002
2.48E-002
+I+I+I+I+I-
6.74E-002
6.75E-002
4.38E-001
9.34E-002
5.38E-002
f)G
s I(fI~
MDA
(pCi/liter
1.09E-001
1.21E-001
9.04E-002
1.13E-001
1.06E-001
+I+I+I+I+I-
2.03E-002
2.25E-002
1. 68E-002
2.10E-002
1. 97E- 002
0000056740.CNF
start:
1:3450.2(kev)
Stop : 1024:6505.5(kev)
Acq. start :rue Apr 30 11:49:00 2013
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6500
Channel Data Report
4/30/2013
5:29:25 PM
Page
*******************************************************
*****
T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
OS
Elapsed Live time:

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l'il2i!1
Channel Data Report

801:
4/30/2013
0
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Page
5:29:25 PM
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
I-68 TOT
1304105A-TH
06
Shelf 2
Th iso
Alpha_044
04026481B
84168
System Bkgd 55756
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:24:51 AM
4/30/2013 11:48:55 AM
170.0 minutes
170.8 minutes
Th229 TH-18A
0.232 mL
0.1453 +/- 0.0136
0.1902 +/- 0.0033 on 12/16/2012
0.7639 +/- 0.0726
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.878
5.278
4.870
4.578
3.898
Net
Pk Area
14.83
142.83
128.83
226.83
43.83
AREA
5:49:26 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
0.17
0.17
0.17
0.17
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
51.24
16.41
17.28
13.02
29.67
FWHM
(keV)
5.9
4.8
3.2
5.3
4.5
T = Tracer Peak used for Effective Efficiency

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.996
0.925
1. 000
0.955
0.950
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.78E-001
2.66E+OOO
2.36E+OOO
4.14E+OOO
7.99E-001
+I+I+I+I+I-
1. 51E- 001
6.55E-001
4.33E-001
9. 31E-001
2.79E-001
.J'/t(t)
MDA
(pCi/liter
7.82E-002
7.78E-002
7.65E-002
7.63E-002
7.61E-002
+I+I+I+I+I-
1.43E-002
1.42E-002
1.40E-002
1.40E-002
1. 39E-002
0000056736.CNF
start:
13447.9(kev)
Stop : 1014 6485.9(kev)
Acq. Start Tue Apr 30 11:48:55 1013
60
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Channel Data Report
4/30/2013
Page
5:29:35 ?M
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*****
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369:
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sus
Channel Data Report

801:
4/30/2013
0
Sample Title:
Page
5:29:35 li'M
0
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1
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0
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0
0
0
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0
l
0
0
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0
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0
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0
0
0
1
0
0
0
0
0
0
0
0
pex-AiphaTM
I-68 DIS
1304105A-TH
07
Shelf 2
Th iso
Detector Name:
Env. Background:
Alpha_046
040264828
58762
System Bkgd 55757
Sample Description:
Spectrum File:
Sample Geometry:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:24:51 AM
4/9/2013
4/30/2013 11:48:57 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.232 mL
0.1760 +/- 0.0152
0.1789 +/- 0.0031 on 12/16/2012
0.9835 +/- 0.0864
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.794
5.297
4.868
4.676
3.952
Net
Pk Area
AREA
REPORT
Pk Area
Error %
3.00
0.00
156.00
7.00
1.83
5:49:23 PM
130.67
1960.0
15.74
79.20
152.56
Ambient
Backgnd
0.00
0.00
0.00
0.00
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
0.0
6.0
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.984
0.946
l. 000
l. 000
0.989
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.64E-002
O.OOE+OOO
2.36E+OOO
1.06E-001
2.76E-002
+I+I+I+I+I-
6.11E-002
4.26E-002
3.98E-001
8.55E-002
4.23E-002
A(.
:511/1)
MDA
(pCi/liter
9.28E-002
9.23E-002
9.07E-002
9.04E-002
6.28E-002
+I+I+I+I+I-
l.57E-002
l.56E-002
1.53E-002
l. 53E- 002
l.06E-002
0000056732.CNF
Real rime :10200.100 sec
start:
1:34SJ.7(kev)
stop : !024:6515.4(kev)
Acq. Start :rue Apr 30 11:48:57 2013
60 155
so-,_
45
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35
~
1-
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::s
8 30-
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201
15 1-
10
0 ~__]_
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3500
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_I __jl_
i__ _l!_
__!L_ I
_l_
__l_
4000
4500
Ni
~>
(j]
I__' I
ROI Type: 1
,, 1'1 ii'l,IM f\ I ,I
"-~luwntili 1! ____lt\f1_!1Vwd1l;t/,
5000
Energy(kev)
__L_
__!
I_
__j_J_
IIL_l
5500
6000
ROI Type: 3
I ___l_
_l_________j
6500
Channel Data Report
4/30/2013
5:29:4"T
Page
]'M
*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
07
Elapsed Live time:

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ex-AiphaTM
D-87 TOT
1304105A-TH
08
Shelf 2
Th iso
Detector Name:
Env. Background:
Alpha_047
02030596A
91086
System Bkgd 55758
Sample Description:
Spectrum File:
Sample Geometry:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:24:51 AM
4/30/2013 11:48:48 AM
170.0 minutes
170.0 minutes
Th229_TH-18A
0.233 mL
0.1664 +/- 0.0146
0.1822 +/- 0.0032 on 12/16/2012
0.9135 +/- 0.0819
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
Net
Pk Area
5. 967
5.325
4.875
4.633
3.948
0.32
13.32
147.83
25.32
3.83
AREA
5:49:21 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
0.68
0.68
0.17
0.68
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
646.93
55.28
16.13
39.56
102.72
FWHM
(keV)
2.9
2.9
5.7
2.9
2.9

Id
Conf.
Energy
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
0.930
0.971
l. 000
0.992
0.987
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
(keV)
Activity
(pCi/liter )
5.24E-003
2.17E-001
2.37E+000
4.04E-001
6.10E-002
+I+I+I+I+I-
3.39E-002
1.26E-001
4.08E-001
l. 74E-001
6.35E-002
MDA
(pCi/liter
9.23E-002
9.18E-002
6.68E-002
9.00E-002
6.64E-002
+I+!+I+!+I-
1.59E-002
l.58E-002
1.15E-002
1.55E-002
l.15E-002
ltG
S/1 /r3
tl253
0000056733.CNF
Start:
1:3457. 9(kev)
Stop : 1024:6467. 7(kev)
Acq. Start :rue Apr 30 11:48:48 2013
60
55
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45
40
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Channel Data Report
4/30/2013
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t\1257
Sample Description:
Spectrum File:
Sample Geometry:
D-87 DIS
1304105A-TH
09
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_048
02030596B
83111
System Bkgd 55759
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:24:51 AM
4/30/2013 11:48:49 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.231 mL
0.1933 +!- 0.0160
0.1680 +/- 0.0030 on 12/16/2012
1.1506 +/- 0.0973
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.962
5.326
4.878
4.649
4.011
Net
Pk Area
AREA
REPORT
Pk Area
Error %
1. 00
5.15
170.66
8.00
1.00
5:49:20 PM
277.19
94.34
15.02
73.50
277.19
Ambient
Backgnd
0.00
0.85
0.34
0.00
0.00
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
12.4
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.937
0.972
1.000
0.997
0.999
5850.00*
5400.00*
4872. 00*
4672.00*
3997.00*
Activity
(pCi/liter )
1.41E-002
7.21E-002
2.35E+OOO
1.10E-001
1. 37E-002
+I+I+I+I+I-
3.91E-002
6.91E-002
3.81E-001
8.27E-002
3.81E-002
MDA
(pCi/liter
8.45E-002
8.39E-002
6.59E-002
8.24E-002
8.22E-002
+I+I+I+I+I-
1.37E-002
1.36E-002
1. 07E- 002
1.33E-002
1.33E-002
AGS(r((J
:ill.258
0000056734.CNF
60

Start:
1 3453.0(kev)
stop : 1024 6472.1(kev)
Acq. Start Tue Apr 30 11:48:49 2013
55+
1501
45
4035
Vl
-1-'
<=
:=s
8 30+
25
20
1510-
t
t
II
~I
3500
~~
lo,li
(Jj
1.0
"II
4000
I
1-
4500
ROI Type: 1
l ill\
. IN~I
H. LUJ'/.ii
~~~111
i ~~~~" .jJ~.
I'
r1
~
~
1nfi 1
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1111\~1 ~1111.1 1
5000
Energy(kev)
,{
.~~.
;!,
I
,\1 U
.1 /,
I I
I
5500
6000
ROI Type: 3
Channel Data Report
4/30/2013
Page
5:32:43 PM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
09
Elapsed Live time:

Elapsed Real Time:
10200
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Channel Data Report

369:
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Sample Title:
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1261
Channel Data Report

801:
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Sample Title:
Page
5:32:43 PM
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-106-SD TOT
1304105A-TH
10
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_018
18
System Bkgd 55740
<not performed>
Sample Size:
Sample Date/Time:

7:24:51 AM
4/9/2013
4/30/2013 12:43:33 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.230 mL
0.2151 +/- 0.0170
0.1776 +/- 0.0033 on 12/15/2012
1.2112 +/- 0.0986
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5. 77l
5.358
4.873
4.642
3.970
Net
Pk Area
AREA
REPORT
Pk Area
Error %
0.94
16.79
189.15
10.81
11.47
1:57:26 PM
Ambient
Backgnd
443.31
5l. 38
14.29
63.34
62.23
3.06
2.21
0.85
l.19
l.53
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
9.4
4.7
3.1

Nuclide
Id
Con.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.968
0.991
1.000
0.995
0.996
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
l.19E-002
2 .llE-001
2.34E+000
l. 33E-001
l.41E-001
+I+I+!+I+I-
5.28E-002
1.13E-001
3.63E-001
8.70E-002
9.06E-002
AG
5/r (I"!:>
MDA
(pCi/liter
l.13E-001
1.01E-001
7.41E-002
8.13E-002
8.75E-002
+I+I+I+I+I-
1.75E-002
l. 56E- 002
l.15E-002
1.26E-002
l.36E-002
0000056741.CNF
l:l404.1(kev)
start:
Stop : 1024:6604.2(kev)
Acq. start :Tue Apr 30 12:43:33 2013
60+
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8 30
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\I
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IF<ii
M
!Ji
~>
ROI
Type: 1
5000
Energy(kev)
'
6000
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Type: 3
'
6500
Channel Data Report
4/30/2013
Page
5:32:51 l"M
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
10
Elapsed Live time:

Elapsed Real Time:
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Channel Data Report

SOl:
4/30/20l3
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Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-106-SD DIS
1304105A-TH
ll
Shelf 2
Th iso
Alpha_022
22
System Bkgd 55741
<not performed>
Sample Size:
Sample Date/Time:

7:24:51 AM
4/9/2013
4/30/2013 12:43:34 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.231 mL
0.1767 +/- 0.0153
0.1531 +/- 0.0029 on 12/15/2012
1.1536 +/- 0.1020
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.794
5.351
4.850
4.646
4.091
Net
Pk Area
1. 98
-0.06
156.13
22.64
-0.36
AREA
1:57:26 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
176.34
6128.9
15.80
42.62
604.11
1.02
3.06
1. 87
1.36
1.36
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
3.4
4.7
3.1

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.983
0.988
0.998
0.996
0.955
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
3.05E-002
-9.20E-004
2.35E+OOO
3.40E-001
-5.40E-003
+I+I+I+I+I-
5.41E-002
5.64E-002
3.98E-001
1. 56E-001
3.26E-002
AG
;f5/f/l)
MDA
(pCi/liter
9.71E-002
1. 37E-001
1.14E-001
1. 03E-001
1. 03E-001
+I+I+I+I+I-
1.64E-002
2.32E-002
1. 93E-002
1.74E-002
1. 74E-002
0000056742.CNF
Live Time
Real Time
start:
I
stop : 1024
Acq. start
60
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10200.000 sec
342!.5(kev)
6608.8(kev)
Tue Apr 30 12:43:34 2013
55
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35
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11
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6500
Channel Data Report
4/30/2013
5:32:59 PM
Page
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*****
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369:
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1271
Channel Data Report

801:
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'fl272
Sample Description:
Spectrum File:
Sample Geometry:
S-82 TOT
1304105A-TH
12
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_024
24
System Bkgd 55742
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:24:51 AM
4/30/2013 12:43:35 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.232 mL
0.1736 +/- 0.0150
0.1710 +/- 0.0032 on 12/15/2012
1.0149 +/- 0.0898
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.789
5.355
4.855
4.621
3.944
Net
Pk Area
-0.89
7.96
153.66
15.66
6.98
AREA
2:02:15 PM
REPORT
Pk Area
Error %
347.60
79.20
15.83
50.15
80.28
Ambient
Backgnd
2.89
2.04
0.34
0.34
1.02
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
4.4
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.981
0.989
0.998
0.986
0.985
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
-1.40E-002
1.24E-001
2.36E+000
2.39E-001
1. 07E-001
+I+I+!+I+I-
4.86E-002
1.01E-001
4.00E-001
1. 27E- 001
8.74E-002
MDA
(pCi/liter
1. 3 7E- 001
1.22E-001
7.33E-002
7 .31E-002
9.62E-002
+I+I+I+I+I-
2.33E-002
2.06E-002
1. 24E- 002
1. 24E-002
1.63E-002
M
c.S/t/1!;
E273
0000056743.CNF
60

start:
1:3411.6(kev)
stop : 1024:6597 .O(kev)
Acq. start :rue Apr 30 12:43:35 2013
"1-
55+
1-
50
451-
40
.t35-.1V>
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ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
6500
Channel Data Report
4/30/2013
5:33:09 PM
Page
*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
12
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~276
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801:
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'8277
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
S-82 DIS
1304105A-TH
13
Shelf 2
Th iso
Alpha_025
25
System Bkgd 55743
<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:24:51 AM
4/30/2013 12:43:36 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.231 mL
0.2305 +/- 0.0177
0.1736 +/- 0.0032 on 12/15/2012
1.3278 +/- 0.1049
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.883
5.411
4.882
4. 642
4.074
Net
Pk Area
1.98
-0.36
203.49
7.32
0.32
AREA
1:57:27 PM
REPORT
Pk Area
Ambient
Backgnd
Error %
176.34
604.11
13.76
76.28
646.93
1.02
1. 36
0.51
0.68
0.68
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
10.2
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.994
0.999
0.999
0.995
0.969
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.34E-002
-4.23E-003
2.35E+000
8.43E-002
3.68E-003
+I+I+I+I+I-
4.14E-002
2.56E-002
3.54E-001
6.56E-002
2.38E-002
MDA
(pCi/liter
7.44E-002
8.06E-002
6.06E-002
6.50E-002
6.49E-002
+I+I+I+I+!-
1.12E-002
1. 21E-002
9.12E-003
9.77E-003
9.76E-003
1\G
5lljl.)
~-278
0000056744.CNF
start:
1 3405. 9(kev)
stop : 1024 6615.8(kev)
Acq. Start rue Apr 30 12:43:36 2013
60
55
50i
45
It
40 If35
V)
+-'
<::
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8 30
25
20-
1510-
50
II,
3500
4000
4500
ll!il
''~)
">i~J
ROI Type: 1
5000
Energy(kev)
5500
.I
6000
ROI Type: 3
6500
Channel Data Report
4/30/2013
Page
5:33:18 PM
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*****
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lll282
pex-AiphaTM
Sample Geometry:
PZ-106-SS TOT
1304105A-TH
14
Shelf 2
Th iso
Detector Name:
Alpha_027
Sample Description:
Spectrum File:

Env. Background:
Reagent Blank:
27
System Bkgd 55744
<not performed>
1. OOOE+OOO +I- O.OOOE+OOO liter

7:24:51 AM
4/9/2013
4/30/2013 12:43:37 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.231 mL
0.2128 +/- 0.0169
0.1728 +/- 0.0032 on 12/15/2012
1.2317 +/- 0.1007
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.823
5. 371
4.879
4.672
3. 942
Net
Pk Area
3.15
2.79
187.64
12.98
1.32
AREA
2:27:41 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
0.85
2.21
1.36
1. 02
0.68
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
126.67
162.88
14.37
56.85
215.97
FWHM
(keV)
3.2
3.2
13.9
3.2
3.2

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.996
0.996
1. 000
1. 000
0.984
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.03E-002
3.55E-002
2.35E+000
1. 62E-001
1. 64E-002
+I+!+I+I+I-
5.14E-002
5.81E-002
3.66E-001
9.55E-002
3.56E-002
MDA
(pCi/liter
7.66E-002
1.02E-001
8.58E-002
7.86E-002
7.02E-002
+I+I+I+I+I-
1.20E-002
1. 59E-002
1. 34E-002
1.23E-002
1.10E-002
f(;
5/t/~J
.fil2-83
0000056745.CNF
Start:
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Stop : 1024:6658.l(kev)
Acq. start :rue Apr 30 12:43:37 2013
60
55
5045
40
35
V)
.....
<=
8 30 ~
25
20-
15
II-
105+
o~~~~--~~~~~~~~-r~~~~~~~--~~~-+~--~~~~~~~~~-+~~
3500
4000
4500
Iii~
5000
Energy(kev)
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r,;~
()()
11::>.
ROI Type: 1
ROI Type: 3
6500
Channel Data Report
4/30/2013
5:33:27 PM
Page
*******************************************************
*****
p E C T R A L
DATA
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*****
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801:
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f1287
Sample Description:
Spectrum File:
Sample Geometry:
PZ-l06-SS DIS
l304l05A-TH
l5
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_029
29
System Bkgd 55745
<not performed>
Sample Size:
Sample Date/Time:
l.OOOE+OOO +/- O.OOOE+OOO liter

4/9/20l3
7:24:5l AM
4/30/20l3 l2:43:38 PM
l70.0 minutes
l70.0 minutes
Tr~cer Certificate:
Tracer Quantity:
Th229 TH-l8A
0.230 mL
O.l8l6 +/- O.Ol55
O.l945 +/- 0.0036 on l2/l5/20l2
0.9337 +/- 0.08l5
O.l75 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.796
5.335
4.884
4.65l
3.840
AREA
REPORT
Pk Area
Error %
Net
Pk Area
4.64
0.62
l59.64
lO.l5
l. 00
2:30:02 PM
Ambient
Backgnd
l05.45
583.53
l5.59
64.47
277.l9
l.36
2.38
l.36
0.85
0.00
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.l
3.l
lO.l
3.l
3.l

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.985
0.978
0.999
0.998
0.879
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
6.95E-002
9.24E-003
2.34E+000
l.48E-00l
l.46E-002
+I+I+I+I+I-
7.42E-002
5.39E-002
3.9lE-00l
9.88E-002
4.05E-002
MDA
(pCi/liter
l. 03E-00l
l.22E-00l
l.OOE-OOl
8.75E-002
8.75E-002
+I+I+I+I+I-
l. 72E-002
2.04E-002
l.68E-002
l. 46E-002
l.46E-002
A.G
5/1/13>
t11288
0000056746.CNF
Live rime 10201.000 sec
start:
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stop : 1024 6597.S(kev)
Acq. Start rue Apr 30 12:43:38 2013
60!
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11-
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:::>
8 30
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5 II~
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~~
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'"
((.n
(.()
!,
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-\
,\\1:,\
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6500
Channel Data Report
4/30/2013
Page
5:34:08 PM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
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15
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291
Channel Data Report

801:
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Sample Description:
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Sample Geometry:
I-9 TOT
1304105A-TH
16
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_003
3
System Bkgd 55734

<not performed>
Sample Size:
Sample Date/Time:

4/9/2013
7:24:51 AM
4/30/2013
2:35:06 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.230 mL
0.1832 +/- 0.0156
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM
1.0489 +/- 0.0912
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.740
5.342
4.869
4.630
3. 949
Net
Pk Area
1.79
9.94
160.98
7.64
-1.19
AREA
REPORT
Pk Area
Error %
229.07
72.51
15.51
77.95
180.59
Ambient
Backgnd
2.21
3.06
1. 02
1. 36
1.19
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
4.7
3.0
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0. 939
0.983
1. 000
0.991
0.988
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.66E-002
1.47E-001
2.34E+OOO
1.11E-001
-1. 72E-002
+I+I+I+I+I-
6.11E-002
1. 09E-001
3.90E-001
8.82E-002
3.12E-002
M
5/1/fJ
MDA
(pCi/liter
1.19E-001
1. 32E-001
9.16E-002
9.94E-002
9.53E-002
+I+I+I+I+I-
1.98E-002
2.20E-002
1. 52E- 002
1.65E-002
1. 59E-002
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Channel Data Report
4/30/2013
5:34:17 PM
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*******************************************************
*****
E C T R A L
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*****
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129&
Channel Data Report

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8297
pex-Aipha
Sample Geometry:
I-9 DIS
1304105A-TH
17
Shelf 2
Th iso
Detector Name:
Env. Background:
Alpha_004
Sample Description:
Spectrum File:
System Bkgd 55735
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:24:51 AM
4/9/2013
4/30/2013
2:35:07 PM
-170.0 minutes

170.0 minutes
Th229 TH-18A
0.231 mL
0.0885 +/- 0.0105
0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM
0.4561 +/- 0.0546
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
Net
Pk Area
5.760
5.309
4.882
4.577
3. 948
-0.38
-0.23
77.98
5.15
3.49
AREA
REPORT
Pk Area
Error %
799.43
1603.6
22.36
94.34
113.53
Ambient
Backgnd
2.38
3.23
1.02
0.85
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
6.8
5.9
5.9
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.958
0.957
0.999
0.954
0.988
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
-1.17E-002
-7.05E-003
2.35E+000
1.54E-001
1. 04E- 001
+I+I+I+I+I-
9.35E-002
1.13E-001
5.44E-001
1.50E-001
1.21E-001
AG
S/r lfJ
MDA
(pCi/liter
2.52E-001
2.78E-001
1. 90E-001
1.80E-001
1.57E-001
+I+I+I+I+I-
5.84E-002
6.45E-002
4.39E-002
4.16E-002
3.64E-002
0000056748.CNF
start:
l:l49l.l(kev)
stop : 1024:6486.9(kev)
Acq. Start :Tue Apr 30 14:35:07 2013
60+
55
50-
II-
45II-
4035
~
11-
Vl
+-'
<=
=>
8 30
25-
!-
20
15+
105 II0
3500
4000
4500
ill,
M
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ri
ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
6500
Channel Data Report
4/30/2013
Page
5:35:01 PM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
17
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!Ulil1
Channel Data Report

801:
4/30/2013
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ex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
D-93 TOT
1304105A-TH
18
Shelf 2
Th iso
Detector Name:
Alpha_010
Env. Background:
Reagent Blank:
10
System Bkgd 55736
<not performed>

4/9/2013
7:24:51 AM
2:35:03 PM
4/30/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.231 mL
0.2021 +/- 0.0165
0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM
1.0273 +/- 0.0857
0.175 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5. 770
5.375
4.874
4.658
3.905
Net
Pk Area
AREA
REPORT
Pk Area
Error %
2.11
11.92
178.30
6.64
0.81
217.70
67.18
14.76
84.69
359.14
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
2.89
4.08
1. 70
1.36
1.19
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
3.9
2.9
5.9

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.967
0.997
1. 000
0.999
0.957
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.84E-002
1. 60E-001
2.35E+OOO
8. 72E-002
1. 06E-002
+I+I+I+I+I-
6.20E-002
1.10E-001
3.75E-001
7.52E-002
3.82E-002
kG
Str//3;
MDA
(pCi/liter
1.18E-001
1. 33E-001
9.68E-002
9.01E-002
8.64E-002
+I+I+I+I+I-
1.88E-002
2.12E-002
1. 54E-002
1. 44E- 002
1.38E-002
0000056749.CNF
60
55
It:

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Channel Data Report
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!13~6
Channel Data Report

801:
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5:35:2! cJMt
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0
ex-AiphaTM
D-93 DIS
1304105A-TH
19
Shelf 2
Th iso
Detector Name:
Alpha_011
Sample Description:
Spectrum File:
Sample Geometry:

Env. Background:
Reagent Blank:
11
System Bkgd 55737
<not performed>

4/9/2013
7:24:51 AM
2:35:04 PM
4/30/2013
170.0 minutes
170. 0 minutes
Sample Size:
Sample Date/Time:
Th229_TH-18A
0.229 mL
0.2463 +/- 0.0185
0.1973 +/- 0.0042 on 12/15/2012 11:28:06 AM
1.2485 +/- 0.0974
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.865
5.362
4.850
4.629
3.981
Net
Pk Area
AREA
REPORT
Pk Area
Error %
0.13
4.96
215.47
14.66
2.49
Ambient
Backgnd
1.87
2.04
1.53
0.34
0.51
2298.1
107.11
13.41
51.88
138.30
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.7
2.7
3.4
2.7
2.7

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.999
0.992
0.997
0.990
0.999
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1.43E-003
5.45E-002
2.33E+OOO
1.58E-001
2.68E-002
+I+I+I+!+!-
3.30E-002
5.89E-002
3.43E-001
8.52E-002
3.72E-002
f\G
5/1{{)
MDA
(pCi/liter
8.37E-002
8.56E-002
7.68E-002
5.15E-002
5.64E-002
+I+I+I+I+I-
1.23E-002
1.26E-002
1.13E-002
7.58E-003
8.31E-003
0000056750.CNF
start:
l:l645.8(kev)
stop : 1024:6374.2(kev)
Acq. Start :Tile Apr 30 14:35:04 2013
605550+
45-
4035 IV>
~301
25
201
15
lOj
. l'~1
I
.-_-[_iH_
oL
'
II
1 _UI
I I
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4000
4500
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Channel Data Report
4/30/2013
E>q.ge
5:3$!lt.
*******************************************************
*****
E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
19
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1
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0
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2
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3
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4
1
2
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1
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ll!J 11
Channel Data Report

801:
4/30/2013
0
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Page
5:35:34 iN
0
19
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945:
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961:
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977:
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1017:
0
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0
0
0
0
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1
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
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0
~312
Page 1 of 2
4/30/2013 5:44:34 AM
ha
QA SUMMARY REPORT
Date
Time
: 4/30/2013
: 5:44:34 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alj>ha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
AlM730
AlM730
AlM730
AIM730
AIM730
AIM730
AlM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystiOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalvstlOODC
Alpha AnalvstlOODC
Alpha Analyst I OODC
Alpha Analyst!OODC
Alpha AnalystlOODC
Alpha Analystl OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
DATE
4/30/2013 5:21:25 AM
4/30/2013 5:21 :26 AM
4/3012013 5:21:27 AM
4/3012013 5:21 :28 AM
4/30/2013 5:21:29 AM
4/30/2013 5:21:30 AM
4/3012013 5:21:30 AM
4/30/2013 5:21:31 AM
4/30/2013 5:21:32 AM
4/30/2013 5:21:33 AM
4/30/2013 5:21:34 AM
4/30/2013 5:21:35 AM
4/30/2013
4/30/2013
4/30/2013
4/29/2013
4/30/2013
5:21:36 AM
5:21:38 AM
5:21:39 AM
5:29:59 AM
5:21:40 AM
4/29/2013
4/3012013
4/3012013
4/30/2013
5:30:03 AM
5:21:42 AM
5:21:43 AM
5:21:45 AM
li313
Page 2 of 2
Review of QA Results - Pulser Check

4/30/2013 5"4434 AM
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha Analyst! OODC
Alpha Analyst!OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
APPROVED BY:
APPROVAL DATE:
FLAG
Passed
Passed
Not Done
Passed
Passed
Passed
DATE
4/29/2013 5:30:09 AM
4/30/2013 5:21:47 AM
4/30/2013 5:21:48 AM
4/30/2013 5:21:50 AM
4/30/2013 5:21:52 AM
6/12/12
Page
12:16:29 PM
*************************************************************************
*****
L I B R A R Y
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Thorium
Nuclide
Name
Half-Life
(Seconds)
TH-227
TH-228
TH-229
TH-230
TH-232
6.873E+008
6.034E+007
2.487E+011
2.379E+012
4.434E+017
Th-227,-228,-229,-230,-232
Energy
(keV )
Energy
Uncert. (keV
0.000
0.000
0.000
0.000
0.000
5850.000*
5400.000*
4872.000*
4672.000*
3997.000*
Yield
(%)
97.5000
99.9400
99.5200
99.8200
100.0000
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0.0000
0.0000
0.0000
key line
TOTALS:
Nuclides
Energy Lines
fii315
SECTION X
ANALYTICAL DATA (RADIUM-226)
8316
Eberline Services
Analysis Sheet
Printed: 5/1/2013 10:51 AM

Page 1 of3
13-04105
Ra226
Run 1
Work Order
~n
Analysis Code
Ra226
Run
Internal
Fraction
01
02
Sample
Desc
Client
ID
LCS
LCS
MBL
BLANK
Login
CPM
Sample
Date
Sample
Aliquot
04/16/13 00:00
1.0000E+OO
04/16/13 00:00
1.5000E+OO
4/16/2013
03
DUP
PZ-106-SS TOT
41
04/09/13 12:56
1.5000E+OO
5/7/2013
04
TRG
PZ-204-SS TOT
39
04/09/13 09:30
1.5000E+OO
05
TRG
PZ-204-SS DIS
39
04/09/13 09:30
1.5000E+OO
West Lake OU-1
06
TRG
1-68 TOT
45
04/09/13 10:44
1.5000E+OO
Report Level
07
TRG
1-68 DIS
45
04/09/13 10:44
1.5000E+OO
Activity Units
pCi
08
TRG
D-87TOT
42
04/09/13 11:05
1.5000E+OO
Aliquot Units
09
TRG
D-87 DIS
42
04/09/13 11 :05
Matrix
WA
10
TRG
PZ-106-SD TOT
37
04/09/13 12:00
1.5000E+OO
Method
EPA 903.0 Modified
11
TRG
PZ-106-SD DIS
37
04/09/13 12:00
1.5000E+OO
Instrument Type
Alpha Spectroscopy
12
TRG
S-82 TOT
46
04/09/13 12:27
1.5000E+OO
Radiometric Tracer
Ba-133
13
TRG
S-82 DIS
46
04/09/13 12:27
1.5000E+OO
Radiometric Sol#
Ba-6a
14
DO
PZ-106-SS TOT
41
04/09/13 12:56
1.5000E+OO
Tracer Act (dpm/g)
1009.23
15
TRG
PZ-106-SS DIS
41
04/09/13 12:56
1.5000E+OO
16
TRG
1-9 TOT
43
04/09/13 13:35
1.5000E+OO
1-9 DIS
43
' 04/09/13 13:35
1.5000E+OO
Date Received
Lab Deadline
Client
Project
Carrier
Carrier Cone (mglrnl)
1.5000E+OO
'
'
17
TRG
18
TRG
D-93 TOT
40
04/09/13 14:28
1.5000E+OO
19
TRG
D-93 DIS
40
04/09/13 14:28
1.5000E+OO
----
&l~
!:.~
'"'J""
* SAF1 'is used for.,Gross Alpha and all other radionuclides. SAF2 is. uSed for Gross,Beta only.
**Actual mass exceeded the calibr'~tion curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 5/1/201310:51 AM
Page 2 of 3
13-04105
Ra226
Run 1
Internal
Fraction
Sample
Desc
01
LCS
0.9100
918.4
372.6
90.07
0.0226
0.0282
0.0056
02
MBL
0.9078
916.2
397.2
96.25
0.0226
0.0287
03
DUP
0.9020
910.3
397.5
96.94
0.0228
04
TRG
0.9022
910.5
390.2
95.14
05
TRG
0.8999
908.2
353.2
06
TRG
0.8974
905.7
07
TRG
0.9000
08
TRG
09
Tracer Total
ACT(dpm)
Tracer
Aliquot (g)
Radiometric
Tracer (pCi)
Radiometric GravCarrier
%Rec
Added(ml)
Grav Filter
Tare (g)
Grav Filter
Final (g)
Grav Filter
Net(g)
Grav
%Rec
Mean
%Rec
SAF
SAF
2.
90.07
2.00
1.00
0.0061
96.25
2.20
1.00
0.0293
0.0065
96.94
2.34
1.00
0.0224
0.0294
0.0070
95.14
2.50
1.00
86.34
0.0222
0.0292
0.0070
86.34
2.50
1.00
303.2
74.32
0.0224
0.0310
0.0086
74.32
2.91
1.00
908.3
396.1
96.81
0.0228
0.0308
0.0080
96.81
2.77
1.00
0.9039
912.2
435.9
106.08
0.0224
0.0321
0.0097
106.08
3.20
1.00
TRG
0.9018
910.1
461.4
112.55
0.0224
0.0314
0.0090
110.00
3.01
1.00
10
TRG
0.9010
909.3
393.0
95.95
0.0226
0.0293
0.0067
95.95
2.40
1.00
11
TRG
0.8990
907.3
395.2
96.70
0.0227
0.0294
0.0067
96.70
2.40
1.00
12
TRG
0.8983
906.6
409.3
100.23
0.0229
0.0316
0.0087
100.23
2.94
1.00
13
TRG
0.8988
907.1
347.9
85.14
0.0228
0.0302
0.0074
85.14
2.61
1.00
14
DO
0.8986
906.9
398.4
97.52
0.0225
0.0294
0.0069
97.52
2.47
1.00
15
TRG
0.8996
907.9
376.6
92.09
0.0228
0.0298
0.0070
92.09
2.50
1.00
16
TRG
0.9039
912.2
385.6
93.84
0.0229
0.0328
0.0099
93.84
3.25
1.00
17
TRG
0.8980
906.3
364.7
89.34
0.0222
0.0310
0.0088
89.34
2.96
1.00
18
TRG
0.8796
887.7
369.7
92.45
0.0223
0.0337
0.0114
92.45
3.77
1.00
19
TRG
0.8995
907.8
423.1
103.47
0.0226
0.0326
0.01001
103.47
3.28
1.00
I'
fl'ol
.-,;~00
',;,
* SAF.1~is used for Gross Alpha and all other radionuclid'$: tSAF2 is used for Gross Beta only.
**Actual mass
excee~d-11;le calibration curve range.
Results should be qualified asiappropriate.
, ..,_.
Eberline Services
Analysis Sheet
Printed: 5/1/2013 10:51 AM

Page 3 of 3
13-04105
Ra226
Run 1
Internal
Fraction
Sample
Desc
Rough Prep
Date
Rough Prep
By
Prep
Date
Prep
SepiO
SepW
Sep 11
By
Dateffime
By
Dateffime
01
LCS
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
02
MBL
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
03
DUP
04/24/13 11:50
JBARNARD
04/30/13 11:38
TSMITH
04
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
05
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
06
TRG
04/24/13 11:50
JBARNARD
04/30/13 11 :38
TSMITH
07
TRG
04/24/13 11:50
JBARNARD
04/30/13 11:38
TSMITH
08
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11:38
TSMITH
09
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
10
TRG
04/24/13 11:50
JBARNARD
04/30/13 11 :38
TSMITH
11
TRG
04/24/13 11:50 ' JBARNARD
04/30/13 11 :38
TSMITH
12
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
13
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
14
DO
04/24/13 11 :50
JBARNARD
04/30/13 11:38
TSMITH
15
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
16
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
17
TRG
04/24/13 11:50
JBARNARD
04/30/13 11 :38
TSMITH
18
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11:38
TSMITH
19
TRG
04/24/13 11 :50
JBARNARD
04/30/13 11 :38
TSMITH
Sep 11
By
~J
!:\:~.""'
fA~
....
~ ~
Ul
o<t..SAF1 is used for Gross Alpha and all other reidienuclides. sAE2 is used for Gross Beta.only.
**Actual mass:.exc-eeded the. calibration curve range. Results should be qualified as appropriate.
Eberline Services
0:
-!:0
"-~
1i;
<
00:
-::
~
-~
"'
Lob
CD
Activity
Units
LCS
LCS
pCI/1
1.04E+01
1.15E+OO
2.26E-01
pCi/1
5.10E-02
7.05E-02
1.07E-01
pCUI
2.63E+OO
4.91E-01
1.37E-01
PZ-204-SS TOT
pCI/1
1.26E+OO
3.56E-01
1.58E-01
OK
01
02
RA-226
RA-226
MBL
BLANK
03
RA-226
DUP
PZ-106-SS TOT
04
RA-226
Results
Error Estimate
LCS
Known
MOA
1.02E+01
LCS
%R
LCS
Flag
101.12
OK
-- ------ - r----
RPO
Flag
MOA
Flag
OK
OK
OK
TRG
--
-------
---------
8.68E-01
3.22E-01
2.18E-01
OK
06
RA-226
TRG
1-68 TOT
pCi/1
3.34E+OO
7.83E-01
3.52E-01
OK
07
RA-226
TRG
1-68 DIS
pCi/1
6.70E-01
2.79E-01
1.41E-01
OK
08
RA-226
TRG
D-87TOT
pCi/1
1.33E+OO
4.17E-01
2.05E-01
OK
09
RA-226
TRG
D-87 DIS
pCi/1
7.53E-01
3.10E-01
2.19E-01
OK
'
10
RA-226
TRG
PZ-106-SD TOT
pCi/1
1.04E+OO
3.08E-01
1.56E-01
ca
----
'
11
RA-226
12
RA-226
-t:0
14
RA-226
"'c
15
RA-226
16
RA-226
c
:;;
c
c:
17
RA-226
18
RA-226
19
RA-226
...."'
"'
"c
a,
~
r--
OK
TRG
PZ-106-SO DIS
pCI/1
G.OBE-01
2.42E-01
1.36E-01
OK
TRG
S-82 TOT
pCi/1
1.63E+OO
4.25E-01
1.68E-01
OK
TRG
S-82 DIS
pCi/1
6.37E-01
2.74E-01
1.56E-01
..
13
''
------
d
.E
OK
pCi/1
0:::
Blank
Flag
OK
PZ-204-SS DIS
Client
Identification
TRG
c.
c.
Desc
RA-226
ill
"''
..!
Sample
05
N
N
Printed: 5/2/2013 10:07 AM

Page 1 of 3
Work Order: 13-04105-Ra226-1
Nuclide
Fraction
RA-226
'
DO
OK
I
------- ---------- -------- ------- ------
------- -------
PZ-1 06-SS TOT
pCi/1
2.80E+OO
5.31E-01
1.20E-01
PZ-106-SS DIS
pCill
3.12E+OO
5.61E-01
1.32E-01
OK
---TRG
OK
-
1-9 TOT
TRG
pCill
1.48E+OO
4.28E-01
2.04E-01
OK
OK
-1-9 DIS
TRG
...
TRG
D-93 TOT
-
TRG
------
I
I
II
pCI/1
6.65E01
2.93E-01
2.00E-01
pCI/1
3.02E+OO
7.10E-01
3.12E-01
pCill
D-93 DIS
----
1.93E+OO
4.81E-01
OK
..
OK
2.12E-01
-~
------ --------
-~
----
Eberline Services
,,.
~
,
0:
~
01
-1:
-~
~
""'
~
"
~
"!:
~
~
-~
.,
02
T""
Sample
!'
Oesc
Sample
Date
LCS
04/16/13 00:00
Sample
Aliquot
RA-226
MBL
1.00E+OO
04/16/13 00:00
1.50E+OO
04
RA-226
TRG
04/09/13 09:30
05
RA-226
TRG
04/09/13 09:30
06
RA~226
TRG
04/09/13 10:44
1.SOE+OO
07
RA-226
TRG
04/09/13 10:44
1.50E+OO
96.81
08
RA-226
TRG
04/09/13 11 :05
1.50E+OO
100.00
09
RA-226
TRG
04/09/13 11 :05
1.50E+OO
'
10
RA-226
TRG
04/09/1312:00
1.50E+OO
0:::
----
11
RA-226
TRG
---------------..;------- - - -
1'>3
~-~
96.94
4/30/2013 11:38
0.00
95.14
4/30/201311:38
1.50E+OO
86.34
0.00
86.34
4/30/201311:38
74.32
0.00
74.32
4/30/201311:38
0.00
96.81
4/30/201311:38
0.00
106.081
4/30/201311:38
100.00
0.00
110.00
4/30/201311:38
95.95
0.00
95.95
4/30/201311:38
0.00
96.70
04/09/13 12:00
1.50E+OO
-~-~--------
------
-~--
04/09/13 12:27
1.50E+OO
TRG
04/09/13 12:27
1.50E+OO
96.70
~;~~-~r
f---
- -
0.00
4/30/201311:38
-- [---------~----100.23
4/30/2013 11:38
85.14
4/30/2013 11:38
-----------,
I
~-
85.14
0.00
-DO
1.50E+OO
04/09/13 12:56
15
RA-226
TRG
04/09/13 12:56
"
16
RA-226
TRG
04/09/13 13:35
17
RA-226
TRG
04/09/1313:35
"'
18
"
;;,
c::
w
19
97.52
0.00
97.52
92.09
4/30/201311:38
- - -----4/30/2013 11 :38
93.84
4/30/2013 11:38
89.34
4/30/2013 11:38
-- - - - - - -
-~
1.50E+OO
92.09
0.00
- - - - - - - - - - ------1.50E+OO
93.84
0.00
1.50E+OO
89.34
0.00
--
-------
:;;
ltd~
~>l
0.00
-~-
96.94
95.14
TRG
RA-226
c::
-~
c::
4/30/2013 11:38
1.50E+OO
RA-226
14
c::
96.25
t:0
".."'
0.00
RA-226
-----
~-
4/30/201311:38
90.07
---- ------
13
"'"c::
Sep t1
DatefTime
Date/Time
---
.;
.5
c.
c.
1.50E+OO
-~
----------
Sep tO
SAF
---- ------- - - - - - - - -
-----~-
12
0.00
96.25
04/09/13 12:56
co
Mean
%Rec
90.07
DUP
N
N
ctS
Grav
% Rec
~~---
---- r----- - - - - - - -
~-------
03
Radiometric
%Rec
RA-226
RA-226
Printed: 5/2/2013 10:07 AM

Page 2 of 3
Work Order: 13-04105-Ra226-1
- ---
r--- - - 0
(J
Nuclide
Fraction
RA-226
TRG
04/09/13 14:28
1.50E+OO
92.45
--
RA-226
TRG
04/09/13 14:28
1.50E+OO
100.00
0.00
92.45
- _.oor---0.00
4/30/201311:38
1---- f- ---------------
103.47
----------- - - - - - r----
---~-----------
4/30/201311:381
r---~-------r-
Eberline Services
(
0
0:
Work Order: 13-04105-Ra226-1
Lb
Fraction
Nuclide
01
RA-226
Desc
Counting
DatefTime
LCS
05/01/13 16:18
Sample
Halflife
(days)
co
02
RA-226
MBL
03
RA-226
DUP
N
N
0
(J
-~
~
1ii
0
<t
C'IS
04
05
Detect
Count
Time
Carrier
IAlpha
A Spec
-----
TRG
19.7
'
A_Spec
Al~~~7~r9 E+OO
3.00 E-03
19.7
05/01/13 16:18
A_Spec
Alpha_013
5.00 E-03
18.7
6.00 E-03
18.5
05/01/13 16:18
TRG
1.10 E-02
Eff
05/01/13 16:18
17011.15 E+02
Alpha_014
A_Spec
----RA-226
CPM
----------- - - -
------
----
RA-226
Bkg
Counts
17~3.46 E+02
010j
-- - - - - - -
T"'
.g
Printed: 5/2/2013 10:07 AM

Page 3 of 3_
170 5.00 E+01
----
--~--
A_Spec
05/01/13 16:18
- - - - - - --- - - - - -
170 3.01 E+01
Alpha_018
--
---
---~-----
17.8
1.10 E-02
---
06
RA-226
07
RA-226
08
RA-226
09
RA-226
'
10
RA-226
11
RA-226
TRG
05/01/13 16:19
A_Spec
12
RA-226
TRG
05/0111316:19
..;
.5
13
RA-226
TRG
05/01113 16:19
14
RA-226
15
RA-226
E
m
" ...."'
16
RA-226
c
:;:
17
RA-226
TRG
05/01/13 16:20
A_ Spec
Alpha_042
170 2.10 E+01
6.00 E-03
18.5
"'c
18
RA-226
TRG
05/02/13 05:32
A_Spec
Alpha_003
170 7.31 E+01
1.10E-02
17.5
c
c
19
RA-226
TRG
05/02/13 05:32
A_ Spec
Alpha_004
170 6.45 E+01
9.00 E-03
19.4
0::
'
'E
0
'!:
-~
.,
.;
ill"'
Q.
Q.
~
"'c
~
~
(J
;::
m
m
c;,
I
~
I.!
~~~!
TRG
05/01/13 16:18
Alpha_022!
170 7.40 E+01
-- ------
iAipha_024j
170 2.27 E+01
A_Spec
;
TRG
05/01/13 16:18
A_Spec
-- ----
TRG
05/01/13 16:18
05/0111316:18
TRG
05/01113 16:18
A_Spec
'
Alpha_02~0.02 4.10 E+01
6.00
E~3
17.4
Alpha_027
17012.45 E+01
9.00 E-03
A_Spec
Alpha_029
--~~~~E+01
8.00 E-03
Alpha_033
170 2.53 E+01
4.00 E-03
18.2
A_Spec
Alpha_034
17015.82 E+01
5.00 E-03
18.6
A_Spec
Alpha_035
i
170!2.15 E+01
3.00 E-03
18.3
2.00 E-03
17.8
3.00 E-03
19
A_ Spec
17.3
19.5
-- - - - -
05/01/13 16:20
Alpha_037
11011.12 E+02
- - ------ - - - - ----A_Spec
Alpha_040
170 1.23 E+02
- - ------- 1---
TRG
17.1
~--------l---
05/01113 16:19
TRG
2.00 E-03
A_Spec
----
--
15.3
---
---- - - ------------- --------------- ---------- -----------
DO
1.20 E-02
---- ---
TRG
r----
----
05/01/13 16:19
A_Spec
Alpha_041
170 4.78 E+01
7.00 E-03
19.8
- - -----
- - ----
--
c---
w
--------------
--------
Count Room Report

Printed: 5/1/2013 10:51 AM

Page 1 of1
13-04105-Ra226-1 (pCi/1) in WA
Tracer ID: Ba-6a
:;_~
I
,(
..A
Internal
Fraction
Sample
Desc
Client
ID
Sample
Date
Sample
Aliquot
01
LCS
LCS
04/16/13 00:00
1.0000
0.9100
918.3993
372.6000
02
MBL
BLANK
04/16/13 00:00
1.5000
0.9078
916.1790
03
DUP
PZ-106-SS TOT
04/09/13 12:56
1.5000
0.9020
04
TRG
PZ-204-SS TOT
04/09/13 09:30
1.5000
05
TRG
PZ-204-SS DIS
04/09/13 09:30
06
TRG
1-68 TOT
07
TRG
08
Tracer
Tracer
ACT(dpm)
Radiometric
Tracer (pCi)
SAF
SAF
2.
90.07
2.00
1.00
397.2000
96.25
2.20
1.00
910.3255
397.5000
96.94
2.34
1.00
0.9022
910.5273
390.2000
95.14
2.50
1.00
1.5000
0.8999
908.2061
353.2000
86.34
2.50
1.00
04/09/13 10:44
1.5000
0.8974
905.6830
303.2000
74.32
2.91
1.00
1-68 DIS
04/09/13 10:44
1.5000
0.9000
908.3070
396.1000
96.81
2.77
1.00
TRG
D-87 TOT
04/09/13 11 :05
1.5000
0.9039
912.2430
435.9000
106.08
3.20
1.00
09
TRG
D-87 DIS
04/09/13 11:05
1.5000
0.9018
910.1236
461.4000
112.55
3.01
1.00
10
TRG
PZ-106-SD TOT
04/09/13 12:00
1.5000
0.9010
909.3162
393.0000
95.95
2.40
1.00
11
TRG
PZ-106-SD DIS
04/09/13 12:00
1.5000
0.8990
907.2978
395.2000
96.70
2.40
1.00
12
TRG
S-82 TOT
04/09/13 12:27
1.5000
0.8983
906.5913
409.3000
100.23
2.94
1.00
13
TRG
S-82 DIS
04/09/13 12:27
1.5000
0.8988
907.0959
347.9000
85.14
2.61
1.00
14
DO
PZ-1 06-SS TOT
04/09/13 12:56
1.5000
0.8986
906.8941
398.4000
97.52
2.47
1.00
15
TRG
PZ-106-SS DIS
04/09/13 12:56
1.5000
0.8996
907.9033
376.6000
92.09
2.50
1.00
16
TRG
1-9 TOT
04/09/13 13:35
1.5000
0.9039
912.2430
385.6000
93.84
3.25
1.00
17
TRG
1-9 DIS
04/09/13 13:35
1.5000
0.8980
906.2885
364.7000
89.34
2.96
1.00
18 I"
TRG
D-93 TOT
04/09/13 14:28
1.5000
0.8796
887.7187
369.7000
92.45
3.77
1.00
19
TRG
D-93 DIS
04/09/13 14:28
1.5000
0.8995
907.8024
423.1000
103.47
3.28
1.00
Aliquot(g)
II
Radiometric
%Rec
t.ll
!'.)
t.~
/~--::~:
'.';-~;~;.
<'"
Eberline Services
Ra-226
Run
Analysis Code
Date
Technician
13-04105
Ra226
4/24/2013 11:48
JBARNARD
Sol#
Printed: 4/24/2013 11:50 AM
Internal Work Order
LCS & Matrix Spikes

Isotope
Page 1 of 1
Ra-5b
Activity
dpmlg
44.071
Solution
Date
4/24/2013
Approx
Addition
0.500
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
0.5157
Witness Initials
LCS
Known
pCi
MS
Error
Estimate
0.471
10.24
Added
pCi
0.00
LCSD
Error
Estimate
0.000
Known
pCi
MSD
Error
Estimate
0.00
Added
pCi
0.000
Tracers
Activity
dpmlg
Solution
Date
Volume
Used(g)
Approx
Addition
LCS
Tracer
fraction
Isotope
Sot#
01
Ba-133
Ba-6a
1009.230 4/24/2013
0.9100
1.0000
02
Ba-133
Ba-6a
1009.230 4/24/2013
0.9078
1.0000
03
Ba-133
Ba-6a
1009.230 4/24/2013
0.9020
1.0000
0. 910;;l .,,
[1. 907:":: '3
04
Ba-133
Ba-6a
1009.230 4/24/2013
0.9022
1.0000
-0. :.102~3 '3
05
Ba-133
Ba-6a
1009.230 4/24/2013
0.8999
1.0000
06
Ba-133
Ba-6a
1009.230 4/24/2013
0.8974
1.0000
-0~9022 g
-[1. 899'3 g
07
Ba-133
Ba-6a
1009.230 4/24/2013
0.9000 i
1.0000
08
Ba-133
Ba-6a
1009.230 4/24/2013
0.9039
1.0000
09
i Ba-133
Ba-6a
1009.230 4/24/2013
0.9018
1.0000
10
Ba-133
Ba-6a
1009.230 4/24/2013
0.9010
1.0000
11
Ba-133
Ba-6a
1009.230 4/24/2013
0.8990
1.0000
12
Ba-133
Ba-6a
1009.230 4/24/2013
0.8983
1.0000
13
Ba-133
Ba-6a
1009.230 4/24/2013
0.8988
1.0000
14
Ba-133
Ba-6a
1009.230 4/24/2013
0.8986
1.0000
15
Ba-133
Ba-6a
1009.230 4/24/2013
0.8996
1.0000
16
Ba-133
Ba-6a
1009.230 4/24/2013
0.9039
1.0000
17
Ba-133
Ba-6a
1009.230 4/24/2013
0.8980
1.0000
18
Ba-133
Ba-6a
1009.230 4/24/2013
0.8796
1.0000
19 __ ~3
Ba-6a
1009.230 4/24/2013
0.8995
1.0000
--
~~~
r.;;
~'>
Version 2.0 08/99
(1.
5104
-0. :::974 ~1
-0w 9H3(1 g
-0. '3039 9
-0. 9lHE1 g
-0,'30W 3
-0.8990 '3
-0. :39f::.J 9
-0# 8988 '3
8986 s
-0.8996 '3
-[i.
-[i.
~~
0.5157 9
9039 '3
-0,8980 :.1
-[1. 8"t36 '3
-0.8995 '3
Matrix Spike
0.00
Error
Estimate
0.000
Eberline Analytical
Work Ord
13-o41os
Lab
Fraction
Analysis Code
Rpt Units
Lab Deadline
Technician
Ra226
liters
5/7/2013
JBARNARD
Sample
Muffle Data
Type
01
02
LCS
BLANK
03
04
05
06
07
08
09
10
11
12
13
14
15
16
PZ-1 06-SS TOT

PZ-204-5S TOT
PZ-204-SS DIS
1-68 TOT
1-68 DIS
D-87 TOT
D-87 DIS
PZ-106-SD TOT
PZ-106-SD DIS
S-82 TOT
S-82 DIS
PZ-106-SS TOT
PZ-106-SS DIS
1-9 TOT
1-9 DIS
D-93 TOT
D-93 DIS
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
18
19
Dilution Data
Post/Pre
No of Oils
Comments
i:\ill
!.~
N
Ul
Technician:
Oil Fcictor'--
Ratio
, .
.
.
: ...
..
.
.
.
.
..
.
Aliquot Data
.
.
--
~ ~
MS Aliquot Data
:
Ratio
Client ID
17
Printed: 4/24/201311:51 AM
Page 1 of 1
Aliquot Worksheet
Aliquot
1.0000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO I ..
1.5000E+OO
1.5000E+OO
1.5000E+OO
Net Equiv
Aliquot
1.0000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1:5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1:5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
H-3 Solids Only
H3 Oist
Aliq
Water Added
(ml)
NetEquiv
...
-----
--
i
i
Date
_tL_2j_g--'
Eberline Services- Oak Ridge

Version 1.0 9/1999
Printed: 4/30/2013 1:32 PM

Page 1 of 1
Gravimetric Worksheet
Gravimetric
Carrier
Analysis
Code
Work Order
Carrier Cone
(mg/ml)
Technician
Ra226
TRetec Engineering Management Support, Inc.
Sample
Type
01
LCS
LCS
02
BLANK
MBL
03
DUP
DUP
04
PZ-204-SS TOT
TRG
05
PZ-204-SS DIS
TRG
--06
1-68 TOT
TRG
07
1-68 DIS
TRG
D-87 TOT
TRG
D-87 DIS
09
TRG
PZ-1 06-SD TOT
10
TRG
TRG
PZ-106-SD DIS
___1_1__
12
S-82 TOT
TRG
--13
S-82 DIS
TRG
14 r--"Pz-1o6=ss TOT~ DO
---PZ-1 06-SS DIS
TRG
15
1-9 TOT
TRG
16
17
1-9 DIS
TRG
--D-93
TOT
TRG
18
..
19
D-93
DIS
TRG
...
..
Fraction
Client ID
Carrier Added
(ml)
llt~
(,~
O"J
Technician:
--
Filter Tare
(g)
0.0226
0.0226
0.0228
0.0224
0.0222
0.0224
0.0228
0.0224
0.0224
0.0226
..
...
...
0.0294 '
0.0292 '
...
I
- - - 0.0229 .
0.0222
.
0.0223
0.0226
- -~--------j-
'
Date:
V{ /""$0 1(}
------
Filter Net
(g)
0.0282
0.0287
0.0293
0.0_2251
0.0228
--
~~
0.0229
,....---0.0228 i
Gravimetric
Filter Final
(g)
o:o2~-
Filter Data
Carrier Data
---as
TSMITH
...
0.0310
0.0308
0.0321
0.0314
0.0293
0.0294
0.0316
0.0302
0.0294
0.0298
0.0328
0.0310
0.0337 '
0.0326
0.0056
0.0061
0.0065
0.0070
0.0070
0.0086
0.0080
0.0097
0.0090
0.0067
0.0067
0.0087
0.0074
0.0069
0.0070
0.0099
0.0088
0.0114
0.0100
%
Recovery
----
----
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
SPIKE
1304105A-RA
01
Shelf 2
Ra
Alpha_010
10
System Bkgd 55736
Reagent Blank:
<not performed>
Sample Size:

2.000E+000
Generic Div. Factor:
5/1/2013
11:38:01 AM
4:18:07 PM
5/1/2013
170.0 minutes
170.0 minutes
Generic Mult. Factor:
Sample Date/Time:
0.9007 +!0.1967 +/0.1772 +/-

0.0000
0.0036 on 12/15/2012 11:26:40 AM
0.0032
Control Certificate Name: Ra226 Ra-5b

RA-226
0.505592 +/Peak Match Tolerance:
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5.531
4.682
Net
Pk Area
AREA
0.032530
REPORT
Pk Area
448.26
346.13
1.000E+000
FWHM
(keV)
Ambient
Backgnd
Reagent
Error %
9.30
10.57
3.74
1.87
O.OOE+OOO
O.OOE+OOO
Backgnd
16.3
6.4

Nuclide
RA-224
RA-226
Id
Conf.
Energy
(keV)
0. 969
5685.50*
4785.00*
0.986
Activity
(pCi/liter )
1.46E+001 +/- 7.38E+002
1.04E+001 +/- 1.15E+000
MDA
(pCi/liter
3.13E-001 +/- 1.58E+001
2.26E-001 +/- 8.09E-003
:&327
0000056902.CNF
start:
1 3505. 7(kevl
stop : 1024 649B.O(kev
Acq. start wed May 0116:18:07 2013
60
55
so
45
40
35
V)
+-'
8"' 30
=>
25
20
15
10
I~ ,,1,.1.1'II[ I
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1'
'
4000
~~
())
I'"
ul!\1..1,,/1'
. II
0
s
'1
ROI
Type: 1
4500
5000
Energy(keV)
5500
6000
6500
Channel Data Report
5/2/2013
Page
8:29:55 AM
*******************************************************
s p E C T R A L DATA R E P 0 R T
*****
*****
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7
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2
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1
3
4
4
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5
3
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5
4
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4
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2
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6
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3
1
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9
3
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0
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3
1
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5
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S331ll
Channel Data Report

801:
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3
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1
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2
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5
4
2
3
4
3
6
5
4
2
5
1
3
3
2
4
1
4
2
0
2
1
3
2
1
4
2
2
1
2
5
2
6
4
4
5
5
2
1
2
3
1
4
3
1
1
1
4
1
0
6
2
2
2
4
4
3
7
7
0
5
4
3
9
3
4
4
4
1
2
1
2
2
5
2
1
4
2
2
3
0
3
3
6
4
6
0
3
6
5
2
2
3
3
0
4
5
1
2
1
5
4
0
1
1
0
4
4
5
0
2
2
5
1
1
3
0
5
4
2
1
4
1
2
5
3
2
0
4
2
1
1
0
0
2
4
1
3
6
6
3
5
1
1
2
3
4
3
5
4
1
4
3
3
1
0
2
1
2
4
0
fil331
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1304105A-RA
02
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_011
11
System Bkgd 55737

<not performed>
Sample Size:
Sample Date/Time:

2.200E+000
11:38:01 AM
5/1/2013
5/1/2013
4:18:08 PM
170.0 minutes
170.0 minutes
0.9625 +/0.1973 +/0.1899 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
OOOE+OOO
0.0000
0.0042 on 12/15/2012 11:28:06 AM
0.0040
0.350 MeV
Nuclide
1.
Net
Pk Area
5.507
4.651
-0.40
2.49
AREA
Pk Area
Error %'
926.99
138.29
REPORT
Ambient
Backgnd
3.40
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
2.7
2.7
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.959
0.977
5685.50*
4785.00*
Activity
(pCi/liter )
-8.93E-003 +/- 4.58E-001
5.10E-002 +/- 7.05E-002
MDA
(pCi/liter
2.07E-001 +/- 1.04E+001
1.07E-001 +/- 4.43E-003
1332
0000056843.CNF
Start:
1:3645. 8(kev)
Stop : 1024:6374.2(kev)
Acq. start :wed May 0116:18:08 2013
60
~
55
50 ~
45
401
3sl
V)
::::1
8 30 ~
25
20 ~
15
~
10
It-
s~
Q
I. '
4000
li'~
w
w
t,...,~
ROI Type: 1
4500
5000
Energy(kev)
5500
6000
Channel Data Report
5/2/2013
8:30 :.8&
Page
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
02
Elapsed Live time:

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5/1/2013
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170.0 minutes

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Energy
(MeV)
RA-224
RA-226
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REPORT
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Net
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0.85
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Backgnd
FWHM
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RA-226
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5685.50*
4785.00*
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2.63E+OOO +/- 4.91E-001
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1.37E-001 +/- 4.95E-003
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,,;,'/d-1<-Ull
Channel Data Report

801:
Page
5/2/2013
1
Sample Title:
03
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Spectrum File:
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Alpha_014
14
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4:18:10 PM
5/1/2013
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0.350 MeV
PEAK
Energy
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RA-224
RA-226
1. OOOE+OOO
170.0 minutes
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c.__
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Error %"
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49.98
61.24
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Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
2.9
2.9
Nuclide
Id
Conf.
Energy
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RA-224
RA-226
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0.949
5685.50*
4785.00*
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St'14t?
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8:30 :!t
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p E C T R A L
DATA
R E P 0 R T
*****
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04
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Channel Data Report

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11l345
Channel Data Report

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0
1
0
0
0
ex-Alpha
PZ-204-SS DIS
1304105A-RA
05
Shelf 2
Ra
Sample Description:
Spectrum File:
Sample Geometry:
Alpha_018
Detector Name:
Env. Background:
Reagent Blank:
18
System Bkgd 55740
<not performed>
Sample Size:

2.500E+000
4/30/2013 11:38:01 AM
4:18:41 PM
5/1/2013
170.0 minutes
Sample Date/Time:
170.0 minutes
0.8634 +/0.1776 +/0.1534 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
1.000E+000
Net
Pk Area
5.498
4.618
11.30
30.13
0.0000
0.0033 on 12/15/2012
0.0029
AREA
1:57:26 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
1. 70
1. 87
O.OOE+OOO
O.OOE+OOO
63.23
36.98
FWHM
(keV)
3.1
3.1

Id
Conf.
Energy
Nuclide
RA-224
RA-226
0.955
0.964
5685.50*
4785.00*
(keV)
Activity
(pCi/liter )
4.29E-001 +/- 1.33E+002
8.68E-001 +/- 3.22E-001
MDA
(pCi/liter
2.79E-001 +/- 8.64E+001
2.18E-001 +/- 7.94E-003
1!1347
0000056846.CNF
Start:
1:3404.1(kev)
stop : 1024:6604.2(kev)
60
55
50
45
40
35
...,"'s::::
8 30
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15
10
5
0
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3500
~
0:.1
.t'Jit.
0)
ROI Type: 1
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Energy(kev)
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6000
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Channel Data Report
5/2/2013
8:30: ~
.w
Page
*******************************************************
*****
p E C T R A L
DATA
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Sample Title:
05
Elapsed Live time:

Elapsed Real Time:
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:m-Jss
Channel Data Report

801:
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0
Sample Title:
8:la"
0
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P<!-ge
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05
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~351
ex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
I-68 TOT
1304105A-RA
06
Shelf 2
Ra
Alpha_022
22
System Bkgd 55741
Reagent Blank:
<not performed>

2.910E+000
4/30/2013 11:38:01 AM
4:18:42 PM
5/1/2013
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.7432 +/0.1531 +/0.1138 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
5.533
4.626
1:57:26 PM
0.350 MeV
Nuclide
0.0000
0.0029 on 12/15/2012
0.0022
1.000E+000
AREA
REPORT
Net
Pk Area
Pk Area
Error %
46.45
73.96
29.67
23.16
Ambient
Backgnd
2.55
2.04
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
5.5
4.7
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0. 969
0. 967
5685.50*
4785.00*
Activity
(pCi/liter )
2.77E+OOO +/- 8.57E+002
3.34E+OOO +/- 7.83E-001
MDA
(pCi/liter
S.OOE-001 +/- 1.55E+002
3.52E-001 +/- 1.31E-002
1352
0000056847.CNF
60+
1:3421.5(kev)
start:
Stop : 1024:6608.8(kev)
55
so
45
40
35
v>
.....
c:
8 30
25
20
15
10
5
0
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3500
~
t.IJI
til
tl
ROI Type: 1
4000
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/2/2013
Page
8:30:37 AM
*******************************************************
*****
E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
06
Elapsed Live time:

Elapsed Real Time:
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1:
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Channel Data Report

801:
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Sample Title:
a: J,O.l ~lit
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<not performed>
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5/1/2013
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0.9681 +/0.1710 +/0.1656 +/-
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RA-224
RA-226
5.549
4.582
1. OOOE+OOO
Net
Pk Area
0.0000
0.0032 on 12/15/2012
0.0031
AREA
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Error %
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2:02:15 PM
Ambient
Backgnd
99.27
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3.57
0.34
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(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.1
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Id
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Nuclide
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RA-226
0.975
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5685.50*
4785.00*
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6.70E-001 +/- 2.79E-001
MDA
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Channel Data Report
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Channel Data Report

801:
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Sample Title:
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8:30:410 ~
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07
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3.200E+000
4/30/2013 11:38:01 AM
4:18:44 PM
5/1/2013
170.0 minutes
170.0 minutes
1.0000 +/0.1736 +/0.1736 +/-

Energy
(MeV)
RA-224
RA-226
1:57:27 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/15/2012
0.0032
1.000E+000
Net
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19.13
40.98
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Error %
Ambient
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Reagent
Backgnd
FWHM
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31.06
1. 87
1. 02
O.OOE+OOO
O.OOE+OOO
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.975
0.936
5685.50*
4785.00*
Activity
(pCi/liter )
8.21E-001 +/- 2.55E+002
1.33E+000 +/- 4.17E-001
MDA
(pCi/liter
3.25E-001 +/- 1.01E+002
2.05E-001 +/- 7.50E-003
!Y38.2
0000056849.CNF
start:
1:3405.9(kev)
Stop : 1024:6615.8(kev)
60+
55
II
50
45
40
35
...,<=
V>
8 30
25
20
15
10
5
0
'
3500
&!!
U.l
Crl
l-1
ROI
Type: 1
4000
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/2/2013
8:30:SB ~
Page
*******************************************************
*****
p E
T R A L
DATA
R E P 0 R T
*****
*******************************************************
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-fSJ365
Channel Data Report

801:
5/2/2013
0
Sample Title:
Page
8:30:5$ ~
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1ll366
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
D-87 DIS
1304105A-RA
09
Shelf 2
Ra
Alpha_027
27
System Bkgd 55744
Reagent Blank:
<not performed>
Sample Size:

3.010E+000
4/30/2013 11:38:01 AM
5/1/2013
4:18:45 PM
170.0 minutes
Sample Date/Time:
170.0 minutes
1.0000 +!0.1728 +/0.1728 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
0.0000
0.0032 on 12/15/2012
0.0032
2:27:41 PM
0.350 MeV
Nuclide
1.000E+000
Net
Pk Area
5.507
4.573
8.30
24.47
AREA
REPORT
Pk Area
Ambient
Error %
Backgnd
75.75
41.05
1. 70
1.53
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
3.2
3.2

Nuclide
Id
Con.
Energy
(keV)
RA-224
RA-226
0.959
0.943
5685.50*
4785.00*
Activity
(pCi/liter )
3.37E-001 +/- 1.04E+002

7.53E-001 +/- 3.10E-001
MDA
(pCi/liter
2.98E-001 +/- 9.24E+001
2.19E-001 +/- 8.04E-003
0000056850.CNF
Start:
1 3402.4(kev)
Stop : 1024 6658.1(keV)
Acq. Start Wed May 0116:18:45 2013
60+
II_
55
50
45
40
...
35
V>
<=
8 30
25
20
15
10
5
'
3500
riel
l..l
ll'l
00
ROI Type: 1
'
4000
'
4500
'
5000
Energy(keV)
'
5500
6000
6500
Channel Data Report
5/2/2013
Page
8:31:03 AM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
09
Elapsed Live time:

Elapsed Real Time:
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Channel[------l-------l-------l-------l-------l-------l-------l-------[
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:m37m
Channel Data Report

801:
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Page
8:31:03 AM
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m371
pex-Aipha
PZ-106-SD TOT
1304105A-RA
10
Shelf 2
Ra
Detector Name:
Alpha_029
Sample Description:
Spectrum File:
Sample Geometry:

Env. Background:
Reagent Blank:
29
System Bkgd 55745
<not performed>
Sample Size:

2.400E+000
4/30/2013 11:38:01 AM
4:18:46 PM
5/1/2013
170.0 minutes
Sample Date/Time:
170.0 minutes
0.9595 +/0.1945 +/0.1867 +/-
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
1.000E+000
Net
Pk Area
5.545
4.567
21.13
45.64
0.0000
0.0036 on 12/15/2012
0.0034
AREA
2:30:02 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
44.79
29.51
1.87
1. 36
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
3.1
3.1
NDCLIDE ANALYSIS RESULTS

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.974
0. 940
5685.50*
4785.00*
Activity
(pCi/liter )
6.33E-001 +/- 1.96E+002
1.04E+000 +/- 3.08E-001
MDA
(pCi/liter
2.27E-001 +/- 7.03E+001
1.56E-001 +/- 5.61E-003
000005685l.CNF
60
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5/2/2013
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:fYJ75
Channel Data Report

801:
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Sample Title:
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1ll37E
PZ-106-SD DIS
1304105A-RA
Sample Description:
Spectrum File:
Sample Geometry:
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_033
04026479A
91132
System Bkgd 55746
<not performed>
11

2.400E+000
4/30/2013 11:38:01 AM
5/1/2013
4:19:52 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.9670 +/0.1825 +/0.1765 +/-
PEAK
Energy
(MeV)
RA-224
RA-226
5:49:18 PM
0.350 MeV
Nuclide
0.0000
0.0032 on 12/16/2012
0.0031
1. OOOE+OOO
Net
Pk Area
5.513
4.596
6.66
25.32
AREA
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
78.18
39.56
0.34
0.68
O.OOE+OOO
O.OOE+OOO
3.0
3.0
NDCLIDE ANALYSIS RESULTS
Nuclide
Id
Con.
Energy
(keV)
RA-224
RA-226
0.961
0.954
5685.50*
4785.00*
Activity
(pCi/liter )
2.11E-001 +/- 6.54E+001
6.08E-001 +/- 2.42E-001
MDA
(pCi/liter
1.51E-001 +/- 4.70E+001
1.36E-001 +/- 4.67E-003
-W377
0000056853.CNF
start:
1: 3465 .6(kev)
Stop : 1024:6503.3(kev)
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E C T R A L
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Channel Data Report

801:
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4:19:48 PM
5/1/2013
170.0 minutes
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0.8514 +/0.1826 +/0.1554 +/-

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RA-226
5:49:42 PM
0.350 MeV
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Channel Data Report
5/2/2013
Page
8:31:31'..,.
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
13
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Channel Data Report

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Sample Title:
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f:l39lll
Channel Data Report

801:
5/2/2013
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0
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0
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-106-SS TOT
1304105A-RA
14
Shelf 2
Ra
Detector Name:
Env. Background:
Alpha_037
04026478A
91133
System Bkgd 55750
Reagent Blank:
<not performed>
Sample Size:

2.470E+000
4/30/2013 11:38:01 AM
5/1/2013
4:19:50 PM
170.0 minutes
Sample Date/Time:
170.0 minutes
0.9752 +/0.1783 +/0.1739 +/-
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5.485
4.614
1.000E+000
0.0000
0.0033 on 1/26/2013
0.0032
AREA
REPORT
Pk Area
Error %
Net
Pk Area
26.83
111.66
37.98
18.58
3:28:25 PM
Ambient
Backgnd
0.17
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
4.4
3.9

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.948
0.963
5685.50*
4785.00*
Activity
(pCi/liter )
8.88E-001 +/- 2.75E+002
2.80E+OOO +/- 5.31E-001
MDA
(pCi/liter
1.38E-001 +/- 4.28E+001
1.20E-001 +/- 4.37E-003
0000056856.CNF
start:
1:3463. S(kev)
stop : 1024:6468.S(kev)
60
55
50
45
40
35
V>
+-'
<=
::s
s 30
25
20
15
10
5
0
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to
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4000
4500
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Energy(kev)
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5/2/2013
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*******************************************************
*****
T R A L
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1D395
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801:
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pex-AiphaTM
Sample Description:
PZ-106-SS DIS
1304105A-RA
15
Shelf 2
Ra
Detector Name:
Env. Background:
Alpha_040
06027396B
91135
System Bkgd 55752
Spectrum File:
Sample Geometry:
Reagent Blank:
<not performed>
Sample Size:

2.500E+000
4/30/2013 11:38:01 AM
5/1/2013
4:20:04 PM
170.0 minutes
170.0 minutes
Sample Date/Time:
0.9209 +!0.1900 +/0.1750 +/-
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5.500
4.599
0.0000
0.0033 on 12/16/2012
0.0030
AREA
28.32
123.49
37.34
17.68
5:49:33 PM
REPORT
Pk Area
Error %
Net
Pk Area
l . OOOE+OOO
Ambient
Backgnd
0.68
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
3.0
4.9
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.956
0.956
5685.50*
4785.00*
Activity
(pCi/liter )
9.43E-001 +/- 2.92E+002
3.12E+000 +/- 5.61E-001
MDA
(pCi/liter
1.88E-001 +/- 5.82E+001
1.32E-001 +/- 4.50E-003
m397
0000056857.CNF
Start:
1:3459.0(keV)
Stop : 1024:6497.3(keV)
60+
55
50
45
40
35
V>
.....
c
8 30
25
20
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5
0
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3500
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f.j~l
(.!)
():)
ROI
Type: 1
'
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Energy(kev)
'
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Channel Data Report
5/2/2013
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l!li! lll!l
Channel Data Report

801:
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5/2/2013
0
Sample Title:
8:5!,:8
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Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:

Env. Background:
Reagent Blank:
I-9 TOT
1304105A-RA
16
Shelf 2
Ra
Alpha_041
05026930A
91087
System Bkgd 55753
<not performed>

3.250E+000
4/30/2013 11:38:01 AM
5/1/2013
4:19:58 PM
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes

0.9384 +/0.1978 +/0.1857 +/-
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
1. OOOE+OOO
Net
Pk Area
16.66
47.81
5.511
4.574
0.0000
0.0034 on 12/16/2012
0.0032
AREA
5:49:31 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
48.59
28.76
0.34
1.19
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
4.5
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.961
0.943
5685.50*
4785.00*
Activity
(pCi/liter )
6.79E-001 +/- 2.11E+002
1.48E+OOO +/- 4.28E-001
MDA
(pCi/liter
1.95E-001 +/- 6.05E+001
2.04E-001 +/- 6.90E-003
0000056858.CNF
start:
1:3452. 7(kev)
stop : 1024:6506.6(kev)
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Channel Data Report
5/2/2013
S;l,~;.t~
Jtl'
Page
*******************************************************
*****
p E C T R A L
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*****
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Channel Data Report

801:
5/2/2013
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Sample Title:
8:32:~;\
Page
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0
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Sample Description:
Spectrum File:
Sample Geometry:
I-9 DIS
1304105A-RA
17
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_042
05026930B
84185
System Bkgd 55754
<not performed>
Sample Size:
Sample Date/Time:

2.960E+000
4/30/2013 11:38:01 AM
4:20:01 PM
5/1/2013
170.0 minutes
170. 0 minutes
0.8934 +/0.1846 +/0.1649 +/-

PEAK
Energy
(MeV)
Net
Pk Area
5.528
4.604
RA-224
RA-226
5:49:29 PM
0.350 MeV
Nuclide
0.0000
0.0032 on 12/16/2012
0.0029
1.000E+000
11.15
20.98
AREA
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
61.26
43.99
0.85
1.02
O.OOE+OOO
O.OOE+OOO
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.968
0.958
5685.50*
4785.00*
Activity
(pCi/liter )
4.66E-001 +/- 1.45E+002
6.65E-001 +/- 2.93E-001
MDA
(pCi/liter
2.50E-001 +/- 7.76E+001

2.00E-001 +/- 6.81E-003
0000056859.CNF
Live Time
Real Time
Start:
I
stop : 1024
Acq. Start
60
10200.000 sec
10200.200 sec
l450.2(kev)
6505.5(kev)
wed May 0116:20:01 2013
55
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!:..
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Channel Data Report
5/2/201_3
Page
8:32:2! AM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
17
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Channel Data Report

369:
5/2/2013
0
Sample Title:
8:l~~jj
Page
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Channel Data Report

801:
5/2/2013
0
Sample Title:
Page
8:32:23 M4'
0
17
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Ei411
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
D-93 TOT
1304105A-RA
18
Shelf 2
Ra
Detector Name:
Alpha_003
Env. Background:
System Bkgd 55734
Reagent Blank:
<not performed>
Sample Size:

3.770E+000
4/30/2013 11:38:01 AM
5/2/2013
5:32:48 AM
170.0 minutes
170.0 minutes
Sample Date/Time:
0.9245 +/0.1746 +/0.1614 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
Net
28.62
73.13
5. 530
4.561
0.0000
0.0033 on 12/15/2012 11:26:47 AM
0.0030
AREA
REPORT
Pk Area
Error %
Pk Area
1. OOOE+OOO
38.38
23.26
Ambient
Backgnd
Reagent
Backgnd
2.38
O.OOE+OOO
O.OOE+OOO
1. 87
FWHM
(keV)
6.0
4.5

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.968
0.937
5685.50*
4785.00*
Activity
(pCi/liter )
1.73E+000 +/- 7.82E+002
3.02E+000 +/- 7.10E-001
MDA
(pCi/liter
4.95E-001 +/- 2.24E+002
3.12E-001 +/- 1.14E-002
0000056890.CNF
Live rime 10200.000 sec
start:
1 3498.4(kev)
stop : 1024 6549.S(kev)
Acq. Start Thu May 02 05:32:48 2013
60+
55
IL
50
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40
35
...,<=
V>
8 30
25
20
15
10
5
0
3500
4000
(1!;
...
t~i!:i.
~~
ROI
Type: 1
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/2/2013
8:32:3!1
Page
"""
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
18
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Bi!1.4
Channel Data Report

369:
5/2/2013
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Sample Title:
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6~15
Channel Data Report

801:
5/2/'2013
0
Sample Title:
S:l~:.;t~
Jt1
1
Page
0
18
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U16
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
D-93 DIS
1304105A-RA
19
Shelf 2
Ra
Alpha_004
4
System Bkgd 55735

<not performed>
Reagent Blank:

3.280E+000
4/30/2013 11:38:01 AM
5/2/2013
5:32:49 AM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
1.0000 +!0.1940 +/0.1940 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5.551
4.612
0.0000
0.0036 on 12/15/2012 11:26:46 AM
0.0036
AREA
REPORT
Pk Area
Error %
Net
Pk Area
16.11
64.47
1. OOOE+OOO
53.71
24.75
FWHM
(keV)
Backgnd
Reagent
Backgnd
2.89
1. 53
O.OOE+OOO
O.OOE+OOO
Ambient
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.976
0.962
5685.50*
4785.00*
Activity
(pCi/liter )
7.04E-001 +/- 3.19E+002
1.93E+000 +/- 4.81E-001
MDA
(pCi/liter
3.83E-001 +/- 1.73E+002
2.12E-001 +/- 7.64E-003
iil417
0000056891.CNF
Start:
1 3493.1(kev)
stop : 1024 6486. 9(kev)
Acq. Start Thu May 02 05:32:49 2013
60+
II_
55
50
45
40
35
.._,
V>
s:::
8 30
25
20
15
10
5
0
3500
""
i..i.
!))
ROI Type: 1
4000
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
5/2/2013
8:32:4''
Page
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
19
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
9:
17:
25:
33:
41:
49:
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65:
73:
81:
89:
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105:
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273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10200
0
1
1
0
0
0
0
0
0
0
0
2
0
1
0
0
2
0
0
0
0
0
0
1
0
0
0
0
1
1
0
0
1
1
1
0
1
0
1
1
0
1
0
2
0
10200
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
1
0
1
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
1
1
0
1
0
0
0
0
0
0
0
0
0
0
2
1
0
1
0
3
0
0
1
0
0
0
0
1
0
1
0
1
0
0
0
0
1
1
0
1
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
1
1
1
0
1
1
0
0
1
1
0
0
0
1
0
1
1
0
1
0
1
1
0
2
0
0
0
1
1
0
0
0
0
0
0
1
1
0
0
1
0
0
0
0
0
1
1
0
1
0
0
1
0
0
0
1
0
0
1
1
1
1
0
1
0
1
0
0
1
0
2
0
0
1
0
0
0
0
0
1
0
0
0
0
1
2
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
3
0
1
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
2
1
0
1
1
0
0
2
0
2
1
0
0
1
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
2
0
1
0
2
0
0
0
0
0
2
0
0
0
0
2
0
0
0
0
0
0
0
1
0
0
0
0
1
f.QJ119
Channel Data Report

369:
5/2/2013
0
Sample Title:
8:32:4li'
1
w
0
Page
0
19
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1
0
0
1
0
2
0
0
0
1
0
0
1
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
1
1
2
0
1
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
1
0
1
0
0
0
0
0
0
0
0
1
0
0
0
1
0
1
0
0
1
1
2
0
0
0
1
0
0
1
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
1
0
1
0
0
0
0
0
0
0
1
0
0
2
0
0
2
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
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0
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0
0
1
0
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0
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0
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1
0
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0
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0
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0
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0
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0
0
0
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0
0
0
0
0
0
0
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0
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0
0
0
0
0
0
1
0
0
0
0
1
0
1
0
0
1
0
0
0
1
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
2
0
1
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
1
1
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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1
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
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0
0
1
0
0
0
1
2
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
1
0
2
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
1
U21D
Channel Data Report

801:
5/2/2013
0
Sample Title:
Page
8:32:47 AM
0
19
809:
817:
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905;
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
1
0
0
1
1
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
8421
Page 1 of 2
5/1/2013
5:42:12 AM
QA SUMMARY REPORT
Date
Time
: 5/1/2013
5:42:12 AM
CHAMBER
Alpha 001
Aljlha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
AljJ_ha 010
Al]Jha Oil
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alp_ha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AJM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AJM730
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
A Jpha Analyst 1OODC
A Jpha Analyst 1OODC
Alpha Analyst] OODC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
DATE
Not Done
Not Done
Passed
Passed
511/2013 5:26:43 AM
5/112013 5:26:44 AM
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
5/1/2013 5:26:45 AM
5/112013 5:26:45 AM
Not Done
Passed
Passed
5/112013 5:26:46 AM
511/2013 5:26:47 AM
Not Done
Not Done
Not Done
Passed
5/1/2013 5:26:48 AM
Not Done
Not Done
Not Done
Passed
511/2013 5:26:49 AM
Not Done
Passed
Passed
Not Done
Passed
5/1/2013 5:26:50 AM
5/112013 5:26:51 AM
5/1/2013 5:26:51 AM
Not Done
Passed
Not Done
Not Done
5/1/2013 5:26:52 AM
Not Done
Passed
Passed
Passed
Passed
Passed
5/112013 5:26:53 AM
5/1/2013 5:26:55 AM
5/1/2013 5:26:56 AM
4/29/2013 5:29:59 AM
511/2013 5:26:58 AM
Not Done
Passed
Passed
Passed
Passed
4/29/2013 5:30:03 AM
5/1/2013 5:26:59 AM
5/1/2013 5:27:01 AM
5/1/2013 5:27:02 AM
~422
Page 2 of 2
Review of QA Results - Pulser Cheek

5/1/2013
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha AnalystiOODC
AI]Jha AnalystlOODC
Alpha Analyst! OODC
Alpha Analyst!OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Passed
Passed
Not Done
Passed
Passed
Passed
APPROVED BY:
APPROVAL DATE:
l (/II?
5"4212AM
DATE
4/29/2013 5:30:09 AM
5/I/2013 5:27:04 AM
5/1/2013 5:27:06 AM
5/1/2013 5:27:08 AM
5/I/2013 5:27:09 AM
Page 1 of 2
5/2/2013
5:59:41 AM
ex-AI ha
QA SUMMARY REPORT
Date
Time
: 5/2/2013
: 5:59:41 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha Oil
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 03 I
Aljlha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2If
2If
2If
2If
2If
2If
2If
2If
2If
2If
2lf
2lf
2If
2If
2lf
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst!OODC
Alpha AnalystlOODC
Alpha AnalystiOODC
Alpha Analyst! OODC
Alpha Analyst!OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
DATE
5/2/2013 5:15:45 AM
5/2/2013 5:15:46 AM
5/2/2013 5:15:47 AM
51212013 5:15:48 AM
5/2/2013 5:15:49 AM
5/2/2013 5:15:49 AM
5/2/2013 5:15:50 AM
5/2/2013 5:15:51 AM
5/2/2013 5:15:52 AM
5/2/2013 5:15:53 AM
5/2/2013 5:15:54 AM
5/2/2013 5:15:54 AM
5/2/2013 5:15:56 AM
5/2/2013 5:15:57 AM
5/2/2013 5:15:59 AM
4/29/2013 5:29:59 AM
5/2/2013 5:16:01 AM
4/29/2013 5:30:03 AM
5/2/2013 5:16:03 AM
5/2/2013 5:16:04 AM
5/2/2013 5:16:06 AM
Page 2 of 2
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
Review of QA Rm;yll$- ~ ~
DEVICE
Alpha Analvst!OODC
Al]lha Analyst!OODC
Alpha Analyst!OODC
Alpha Analyst 1OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
..
5/2/2013
".FLAG
Passed
Passed
Not Done
Passed
Passed
Passed
APPROVED BY: - - - - - ~
APPROVAL DATE: ----'J-'-{t,_U.c,l
55941 AM
DATE
4/29/2013 5:30:09 AM
5/2/2013 5:16:09 AM
5/2/2013 5:16:12 AM
5/2/2013 5:16:15 AM
5/2/2013 5:16:18 AM
6/12/12
Page
12:16:17 PM
*************************************************************************
LIBRARY
*****
LISTING
REPORT
*****
*************************************************************************
Radium

Nuclide
Name
Half-Life
(Seconds)
Energy
(kev )
P0-218
RN-222
RA-226
5.049E+010
5.049E+010
5.049E+010
6003.000*
5490.000*
4785.000*
Ra-226, Po-218, Rn-222

Energy
Uncert. (keV
0.000
0.000
0.000
Yield
( %)
99.9800
99.9200
100.0000
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0.0000
* ; key line
TOTALS:
Nuclides
Energy Lines
Blt1.26
SECTION XI
ANALYTICAL DATA (RADIUM-228)
Eberline Services
Analysis Sheet
Printed: 51912013 8:55AM

Page 1 of 3
13-04105
Ra228
Run 1
I ,
Work Order
Internal
Fraction
______()_~--~
Ra228
Analysis Code
Sample
Desc
Run
02
Client
ID
1
1
Date Received
4/16/2013
03
5/7/2013
04
-----------
MBL .
'
DUP
Lab Deadline
--------Client
41
PZ-204-SS TOT
05
. .
Project
West Lake OU-1
..
i TRG
Activity Units
07
pCi
08
TRG
09
TRG
TRG
1-68 DIS
..
'
04/09/13 12:56
1.5000E+OO
04/09/13 09:30
1.5000E+OO
04/09/13 09:30
1.5000E+OO
45
04/09/13 10:44
1.5000E+OO
45
04/09/13 10:44
1.5000E+OO
D-87TOT
D-87 DIS
..
42
I 04roem11 oos
1.5000E+OO
42
04/09/13 11 :05
1.5000E+OO
-~
WA
10
TRG
PZ-106-SD TOT
37
! . 04/09/13 12:00
EPA 904.0 Modified
11
: TRG
PZ-106-SD DIS
37
'
Matrix
1.5000E+OO
..
Aliquot Units
1.0000E+OO
------
-----
Report Level
39
1-68 TOT
TRG i
'
'
..
---
---~--
Sample
Aliquot
-----
PZ-204-SS DIS
06
39
------
04/16/13 00:00
------- ------
PZ-106-SS TOT
TRG
04/16/13 00:00
--
---~------
Sample
Date
-----
BLANK
..
LCS
LCS
Login
CPM
1.5000E+OO
Method
..
Instrument Type
..
04/09/13 12:00
1.5000E+OO
--
Alpha/Beta GPC
12
TRG
S-82 TOT
46
Ba-133
13
TRG
S-82 DIS
46
04/09/13 12:27
1.5000E+OO
..
Radiometric Tracer
-
Radiometric Sol#
Ba-6a
14
1009.23
15
'
DO
PZ-106-SS TOT
TRG
PZ-106-SS DIS
Carrier
TRG
17
04/09/13 12:27
1.5000E+OO
...
41
04/09/13 12:56
41
04/09/13 12:56
1.5000E+OO
1-9 TOT
43
04/09/13 13:35
1.5000E+OO
TRG
1-9 DIS
43
04/09/13 13:35
1.5000E+OO
18
TRG
D-93 TOT
40
04/09/13 14:28
1.5000E+OO
19
! TRG
D-93 DIS
40
04/09/13 14:28
1.5000E+OO
Tracer Act (dpm/g)
'
1.5000E+OO
Yttirum
16
I
Carrier Cone (mg/ml)
34
G~
~
(:!)
Eberline Services
Analysis Sheet
13-04105
Printed: 5/9/2013 8:55 AM

Page 2 of 3
Ra228
Run 1
Internal
Fraction
01
f---~2
I Sample
Desc
[
!
Tracer
Aliquot (g)
Tracer Total
1 ACT (dpm)
MBL
Radiometric
Tracer {pCi)
'
--0~907~
03
DUP
0.9020
___ _
04
TRG
05
r--
06
TRG
,_
TRG
Radiometric Grav Carrier

% Rec
Added (ml)
'
i'
90.07
91-6.2_t __ 397.2-L~-~6.25
I
---
'
918.~6
0.9100
LCS
910.3 !
__
0.902~~10.5t
0.8999
908.2
0.8974 i
905.7
---
397.5
Grav Filter
Final (g)
2.000
0.0929,
2.000!
_0.0923
Grav Filter
Net (g)
0.1474
0.1ii~~--
96.94
2.000
0.0921
0.0545
80.15
72.19
0.0534
78.53
75.58
0.0511
95.14
2.000
0.0918
0.1483
0.0565
86.34
2.000
0.0914;
.
0.0914
0.1477
0.14821
0.0563
74.32
82.79
. 0.0568
83.53
;=08.3 396.1
96.81
2.000
0.0902
0.1440'
f--08
TRG
0.9039
_912.2-- 435.9 ' 106.08
2.000
0.0908
0.1434
0~~526
77.35
_09
TRG
~9018
'
TRG '
0.8988
DO
1.00
_
0.0538
79.05r-1:_~~-
=1:00
71.48' 1.00
1.00 I
-1.00 .
62.08
1.00
76.59
1.00 I 1.00
I --
79.12
1.00
_ __
1.00-~l
- 82.06_ 1.00
I
'
----~
0.0926
0.1455
0.0529'
77.79
85.57
1.00_ -~~0-
909.3
393.0
95.95
2.000
0.0905
0.1436
0.0531
78.09
74.92
1.00
1.00
395.2 .
96.70
2.000
0.0908
0.1432 I
0.0524
77.06
74.51
1.00
. 1.00
. 907.1
409.3
347.9
100.23
I
2.000
0.0925'
0.1432
0.0507
74.56
74.73
1.00
1.00
85.14
2.000 -
0.0902
0.14421
0.0540
79.41
67.61
1.00
1{)0"
97.52
2.000
0.0909
0.1429
0.0520
76.49
74.59
1.00
1.00
92.09
2.000
0.0928
0.1458
0.0530
77.94
71.77
1.00
1.00
0.0904
0.1410
0.0506
74.41
69.83
1~00 ~
0.0905
0.1467
0.0562
82.65
73.83
1.00
-~
0.0928
0.1468
0.0540
79.41
73.42
1.00
0.0560
82.35
85.21
1.00
..
906.9 !
398.4
0.8996
907.9
376.6
16
TRG
0.9039
912.2
385.6
93.84
2.000
17
TRG
0.8980
906.3
364.7
89.34
2.000
18
TRG
0.8796
887.7
369.7
92.45
2.000
--
907.8
423.1
0.8986
0.8995
-1~00.
1.00
2.000
TRG '
TRG
1.00
112.55
15
19
1.00
461.~
14
SAF
2*
910.1 !
11
TRG i 0.8990 '
. 907.3
- - - + - - - t - - - - - 1 - - - - '
12
TRG
0.8983
906.6 .
13
SAF
1*
---
0.9000
TRG .
72.85
83.09 1
TRG
10
390.2 !
' ...
2.000'
75.15
---
07
'
Mean
% Rec
---- . - - - -
0.1432!
303.2
-Grav
% Rec
--------
353.2
1
1
Grav Filter
Tare (g)
103.47
2.000
0.0906
0.1466
'
1.00 .
I
1.00
I
ll!!l
t<:~.
r.:~
tl)
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
13-04105
Printed: 5/9/2013 8:55AM

Page 3 of 3
Ra228
Run 1
.
Internal
Fraction
01
Sample
Desc
Rough Prep
Date
Rough Prep
By
1 LCS
04/24/13 11 :51
I
..
o4t24t1311:51
04/24/13 11 :51
08
09
TSMITH
TSMITH
TRG
11
TRG
.
12
I JBARNARD
TSMITH
04/30/13 11 :38
05/09/13 05:32
TSMITH
04/24/1311:51
JBARNARD
04/24/13 11 :51
JBARNARD I 04/30/13 11:38
04/30/13 11 :38
I
04/24/13 11:51
04/24/13 11 :51
-
05/09/13 05:32
TSMITH
i
TSMITH
05/09/13 05:32
o5to9t13 o5:32
04/24/13 11:51 1 JBARNARD
TSMITH
TSMITH
---
TSMITH
05/09/13 05:32
TSMITH
TSMITH
05/09/13 05:32
TSMITH
05/09/13 05:32
TSMITH
--
04/30/13 11:38
TSMITH
I
JBARNARD
04/30/13 11 :38
TSMITH
05/09/13 05:32
TSMITH
JBARNARD
04/30/13 11:38
TSMITH
05/09/13 05:32
TSMITH
JBARNARD
04/30/13 11 :38
TSMITH
i 05/09/13 05:32
TSMITH
JBARNARD
04/30/13 11 :38
TSMITH
05/09/13 05:32
JBARNARD
04/30/13 11:38
TSMITH
TRG
::____
13
TSMITH
----
10
05/09/13 05:32
..
TRG
TSMITH
--- ------.-
TSMITH
04/30/13 11 :38
---
--
05/09/13 05:32
04/30/13 11 :38
JBARNARD
I 04/24/13 11:51
TRG
TRG
Sep t1
By
----
JBARNARD 1 04/30/1311:38
I -
TRG
o4t3ot13 11 :38
TSMITH
Sep 11
Date/Time
-----
07
04/30/13 11 :38 I
JBARNARD
04/24/1311:51
TRG
06
SepW
By
..
f--
SepW
Date/Time
-----
TRG
05
i JBARNARD
! 04/24/13 11:51
DUP
04
JBARNARD
~---~
03
Prep
By
.-
MBL
02
Prep
Date
~4124/13 11 '"
4/24/1311:51
TRG
TSMITH
...
14
DO
4/24/13 11 :51
05/09/13 05:32
15
TRG
04/24/1311:51
JBARNARD
04/30/13 11 :38
TSMITH
! 05/09/13 05:32
16
TRG
04/24/13 11 :51
JBARNARD
04/30/13 11 :38
TSMITH
05/09/13 05:32
17
TRG
04/24/13 11 :51
JBARNARD
04/30/13 11:38
TSMITH
05/09/13 05:32
04/24/1311:51
JBARNARD
04/30/13 11 :38
TSMITH
, 05/09/13 05:32
TSMITH
TSMITH
f
TSMITH
TSMITH
..
18
TRG
19
TRG
TSMITH
-
..
f----
04/24/13 11:51
-
JBARNARD
04/30/13 11:38
TSMITH
05/09/13 05:32
TSMITH
---
e~
til!!
Eberline Services
,:
~
~
0:
.g
u0
-~
..
~
-!:
-~
.,
Lab
Fraction
Printed: 5/9/2013 2:27PM

Page 1 of 3
Work Order: 13-04105-Ra228-1
Sample
Nuclide
Desc
I LCS
Client
Identification
01
RA-228
02
RA-228
MBL
BLANK
03 '
RA-228
DUP
04
RA-228
05
Activity
Results
Units
I
'
Error Estimate
MDA
LCS
Known
LCS
%R
'
LCS
RPD
MDA
Blank
Flag
Flag
Flag
Flag
OK
OK
9.90E+OO
1.03E+OO
1.26E+OO
pCi/1
5.71E-01
4.17E-01
8.25E-01
PZ-106-SS TOT
pCi/1
8.91E-01
4.58E-01
8.77E-01
TRG
PZ-204-SS TOT
pCill
1.16E+OO
4.26E-01
7.75E-01
OK
RA-228
TRG
PZ-204-SS DIS
pCi/1
7.44E-01
4.65E-01
9.10E-01
OK
06
RA-228
TRG
1-68 TOT
pCi/1
1.97E+OO
6.36E-01
1.16E+OO
OK
07
RA-228
TRG
1-68 DIS
pCill
1.37E+OO
5.28E-01
9.71E-01
OK
08
RA-228
TRG
D-87TOT
pCi/1
2.99E+OO
5.88E-01
9.41E-01
OK
09
RA-228
TRG
D-87 DIS
pCi/1
9.45E-01
4.83E-01
9.29E-01
OK
10
RA-228
TRG
PZ-106-SD TOT
pCi/1
3.36E-01
5.49E-01
1.14E+OO
OK
11
RA-228
TRG
PZ-106-SD DIS
pCi/1
8.93E-01
5.27E-01
1.02E+OO
OK
12
RA-228
TRG
S-82TOT
pCi/1
2.04E+OO
5.82E-01
1.01E+OO
OK
13
RA-228
TRG
S-82 DIS
pCi/1
1.17E+OO
5.63E-01
1.06E+OO
OK
14
RA-228
DO
PZ-106-SS TOT
pCi/1
7.14E-01
5.39E-01
1.07E+OO
OK
"
rn
c
15
RA-228
TRG
PZ-106-SS DIS
pCi/1
5.07E-01
5.69E-01
1.16E+OO
OK
16
RA-228
TRG
1-9 TOT
pCi/1
3.81E+OO
7.75E-01
1.30E+OO
OK
"'c.
17
RA-228
TRG
1-9 DIS
pCi/1
1.49E+OO
6.01E-01
1.12E+OO
OK
"'c
18
RA-228
TRG
D-93 TOT
pCi/1
4.79E+OO
7.41E-01
1.12E+OO
OK
"c
19
RA-228
TRG
D-93 DIS
pCi/1
2.89E+OO
5.95E-01
9.66E-01
OK
co
N
N
ca
'
ill
<.i
.E
t!
0
ll.
ll.
-~ ...
~
LCS
pCUI
8.96E+OO
110.59
OK
NA
::;;
;::
"
c.
c
OK
--
~<!
"""
OM
!.l
OK
--
[_
Eberline Services
I
Lab
Fraction
0::
.g
0
<J
-~
...~
~
..:
'
"E
0
-!:
"'
~
Nuclide
01
Printed: 5/9/2013 2:27 PM

Page 2 of3
Work Order: 13-04105-Ra228-1

I Oesc
Sample
Sample
Date
Sample
Aliquot
Radiometric
%Rec
Grev
%Rec
Mean
%Rec
'
SAF
SeptO
DatefTime
Sep 11
DatefTime
RA-228
LCS
04116113 00:00
1.00E+OO
90.07
80.15
72.19
1.00
413012013 11 :38
51912013 5:32
RA-228
MBL
04116113 00:00
1.50E+OO
96.25
78.53
75.58
1.00
413012013 11 :38
51912013 5:32
03
RA-228
DUP
04109113 12:56
1.50E+OO
96.94
75.15
72.85
1.00
41301201311:38
51912013 5:32
04
RA-228
TRG
04109113 09:30
1.50E+OO
95.14
83.09
79.05
1.00
4/301201311:38
51912013 5:32
05
RA-228
TRG
04109113 09:30
1.50E+OO
86.34
82.79
71.48
1.00
4/30/2013 11 :38
519/2013 5:32
06
RA-228
TRG
04/09113 10:44
1.50E+OO
74.32
83.53
62.081
1.00
4/301201311:38
519/2013 5:32
07
RA-228
TRG
04/09/13 10:44
1.50E+OO
96.81
79.12
76.59
1.00
4/30/2013 11 :38
519/2013 5:32
08
RA-228
TRG
04/0911311:05
1.50E+OO
106.08
77.35
82.06
1.00
41301201311:38
51912013 5:32
09
RA-228
TRG
04/09/1311:05
1.50E+OO
112.55
77.79
85.57
1.00
413012013 11 :38
51912013 5:32
10
RA-228
TRG
04/0911312:00
1.50E+OO
95.95
78.09
74.92
1.00
4130/201311:38
51912013 5:32
11
RA-228
TRG
04/09/13 12:00
1.50E+OO
96.70
77.06
74.51
1.00
413012013 11 :38
51912013 5:32
12
RA-228
TRG
04/0911312:27
1.50E+OO
100.23
74.56
74.73
1.00
4130/2013 11:38
5/912013 5:32
13
RA-228
TRG
04/09113 12:27
1.50E+OO
85.14
79.41
67.61
1.00
4/301201311:38
519/2013 5:32
14
RA-228
DO
04109113 12:56
1.50E+OO
97.52
76.49
74.59
1.00
4/30/201311:38
5/912013 5:32
15
RA-228
TRG
04/09/1312:56
1.50E+OO
92.09
77.94
71.77
1.00
4/30/2013 11 :38
519/2013 5:32
16
RA-228
TRG
04109113 13:35
1.50E+OO
93.84
74.41
69.83
1.00
4/301201311:38
51912013 5:32
17
RA-228
TRG
04/09/1313:35
1.50E+OO
89.34
82.65
73.83
1.00
4130/2013 11 :38
51912013 5:32
"'c
18
RA-228
TRG
04109113 14:28
1.50E+OO
92.45
79.41
73.42
1.00
413012013 11:38
519/2013 5:32
c
c
19
RA-228
TRG
04/09/1314:28
1.50E+OO
103.47
82.35
85.21
1.00
41301201311:38
51912013 5:32
co
N
N
ns
0::
ill
.;
.s
~
0
c.
c.
:J
Cf)
.
."'...
::;:
~
02
t:
;;,
w
L _ _ L.
~"'
w
l"i;.l
--
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~
~
~
0:
~
0
"
-~
~
~
"'
Lab
"!:
~
~
"'.s
) Sample
Counting
Halflife
Datemme
(days)
Oesc
T""
co
N
N
C'G
~
Count
Bkg
Detect
Carrier
L84110A
L84110A
C1
C2
120
170 1.033333333.
L84110A
C3
120
209
1.15
'
L84110A
C4
120
226
1.05
L84110A
02
120
200 1.183333333
L84110A
04
120
315
1.5
L84110R
A1
120
229
1.1
0.4776
L84110R
A2
120
360
1.15
0.4699
Time
Counts
Eff
CPM
01
02
Printed: 5/9/2013 2:27 PM

Page 3 of3
Work Order: 13-04105-Ra228-1
RA-228
LCS
'
05/09/13 09:17
~-
RA228
03
RA-228
04
RA228
'
M8L
05/09/13 09:17
DUP
05/09/13 09:17
TRG
05/09/13 09:17
120
640 1.016666667
0.4667
I
...
----
0.4578
--0.4699
__
0.4692
. ...
05
RA-228
TRG
05/09/13 09:17
06
RA-228
TRG
05/09/13 09:17
07
RA-228
TRG
05/09/13 10:57
08
RA-228
TRG
05/09/1310:57
09
RA-228
TRG
05/09/13 10:57
L84110R
A3
120
229 1.283333333
0.4809
10
RA-228
TRG
05/09/1310:57
L84110R
A4
120
195 1.433333333
o.4732
11
RA-228
TRG
05/09/13 10:57
L84110R
81
120
199
1.15
0.4754
12
RA-228
TRG
05/09/13 10:57
L84110R
82
120
267 1.083333333
0.4658
..;
.5
13
RA-228
TRG
05/09/1310:57
L84110R
83
120
192
0.4713
t:
14
RA-228
DO
05/09/1310:57
L84110R
84
120
203 1.283333333
0.4773
15
RA-228
TRG
05/09/13 10:57
L84110R
C1
120
195
1.35
0.4705
16
RA-228
TRG
05/09/1310:57
L84110R
C2
120
430 1.583333333
0.4676
r:
17
RA-228
TRG
05/09/13 10:57
L84110R
C3
120
252 1.283333333
0.4614
r:
18
RA-228
TRG
05/09/13 10:57
L84110R
C4
120
478 1.316666667
0.4714
r:
19
RA-228
TRG
05/09/13 11:22
L84110A
02
120
354 1.183333333
0.4682
'
Nuclide
Fraction
'
ill"
c.
c.
:I
Ul
..
...."'
:;;
"'
...
~
'
0.4682
i
'
r:
""
~
"i:
a,
r:
w
Ia
""t.-J
!,.)
Count Room Report

Internal
Fraction
Sample
Desc
Client
~-~m=
: DUP
TRG I
04
i
I
Sample
Date
/0
-~LCS!
03
13-04105-Ra228-1 (pCi/1) in WA
Tracer ID: Ba-Ga
LCS
BLANK
--
. ;iJ
1 04/16/13 oo:oo
-----
1 oooo
PZ-106-SS TOT
PZ-204-SS TOT
o.romn "'"' .
04/09/13 09:30
--
05
TRG
Tracer
Aliquot (g)
Tracer
ACT(dpm)
IRadiometric
Radiometric
Tracer (pCi)
,.
SAF
1.00
1.00
SAF
%Rec
2'
o.91oo
?9o78J--
'~::
15
'"'"
0.9022
918.3993
916:~_790 I
'""'"'
910.5273
372.6000
90.07
--
--
397.2000
96.25
-- --
397.5000
390.2000
1.00
1.00
'"i
96.94
1.00
95.14
1.00
1.00
86.34
1.00
1.00
-~
04/09/13 09:30
PZ-204-SS DIS
1.~ooo ~-
04f16t13 oo.oo-
--"
Sample
Aliquot
Printed: 5/9/2013 8:55AM

Page 1 of 1
0.8999--l
908.2061
353.2000
1.00
~-~-
06
TRG
1-68 TOT
--
07
TRG
f------
'~' "'s ::
08
TRG j__
D-87 TOT
09
TRG
D-87 DIS
10
TRG
PZ-106-SD TOT
r-----
04/09/13 10:44
I~'"""""'"
1.5000
1.5000
04/09/13 11:05
1.5000
04/09/13 11 :05
1.5000
04/09/13 12:00
1.5000
0.8974
303.2000
74.32
1.00
1.00
908.3070
396.1000
96.81
1.00
1.00
912.2430
435.9000
106.08
1.00
1.00
0.9018
910.1236
461.4000
112.55
1.00
1.00
0.9010
909.3162
393.0000
95.95
1.00
1.00
395.2000
96.70
1.00
1.00
906.5913
409.3000
100.23
1.00
907.0959
347.9000
85.14
1.00
1.00
905.6830
--
-----
0.9000
I
o.9o39
I
1
1--
11
TRG
PZ-106-SD DIS
12
TRG
13
TRG .
~-
~I-f""
S-82 TOT
04/09/13 12:27
1.5000
S-82 DIS
04/09/13 12:27
1.5000
DO
PZ-106-SS TOT
04/09/13 12:56
1.5000
0.8986
906.8941
398.4000
97.52
1.00
1.00
15
TRG
PZ-106-SS DIS
04/09/13 12:56
1.5000
0.8996
907.9033
376.6000 '
92.09
1.00
1.00
16
TRG
1-9 TOT
04/09/13 13:35
1.5000
0.9039 I
912.2430
385.6000
93.84
1.00
1.00
17
TRG
1-9 DIS
04/09/13 13:35
1.5000
0.8980
906.2885
364.7000
89.34
1.00
1.00
18
TRG
D-93 TOT
04/09/13 14:28
0.8796
887.7187
369.7000
92.45
1.00
1.00
0.8995
907.8024
423.1000
103.47
1.00
19
~.~lt.
1.5000
r------
(""'JI
---
04/09/13 12:00 I
14
Ill
I TRG
1.5000
0.8983
0.8988
1.00
D-93 DIS
04/09/13 14:28
1.5000
1.00
Eberline Services
Internal Work Order
Run
Analysis Code
Date
Technician
13-04105
Ra228
4/24/2013 11 :50
JBARNARD
LCS & Matrix Spikes

Isotope
Sol#
Ra-228
Ra-11
Activity
dpmlg
Solution
Date
Approx
Addition
4/24/2013
38.955
0.510
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
0.5104
8.96
Solution
Date
Volume
Used(g)
Approx
Addition
fraction
Isotope
Sol#
01
Ba-133
Ba-6a
1009.230 4/24/2013
0.9100
1.0000
02
Ba-133
Ba-6a
1009.230 4/24/2013
0.9078
1.0000
03
Ba-133
Ba-6a
0.9020
1.0000
04
Ba-133
Ba-6a
1009.230 4/24/2013
1009.230 4/24/2013
0.9022
1.0000
05
Ba-133
Ba-6a
1009.230 4/24/2013
0.8999
1.0000
06
Ba-133
Ba-6a~30
4/24/2013
0.8974
1.0000
07
Ba-133
Ba-6a
1009.230 4/24/2013
0.90_00
1.0000
1009.230 4/24/2013
0.9039
1.0000
t".!M!.
1-Jt
Ul
08
Ba-133
Ba-6a
09
Ba-133
Ba-6a
1009.230 4/24/2013
0.9018.
1.0000
0.9010.
1.0000
'
10
Ba-133
Ba-6a
1009.230 4/24/2013
11
Ba-133
Ba-6a
1009.230 4/24/2013
0.8990
1.0000
12
Ba-133
Ba-6a
1009.230 4/24/2013
0.8983
1.0000
13
Ba-133
Ba-6a
1009.230' 4/24/2013
0.8988
1.0000
14
Ba-133
Ba-6a
1009.230 4/24/2013
0.8986
1.0000
15
Ba-133
Ba-6a
1009.230 4/24/2013
0.899_6.
1.0000
16
Ba-133
Ba-6a
1009.230 4/24/2013
0.9039
1.0000
17
Ba-133
Ba-6a
1009.230 4/24/2013
0.8980
1.0000
18
Ba-133
Ba-6a
1009.230, 4/24/2013
0.8796
1.0000
19
Ba-133
Ba-6a
1009.230 4/24/2013
0.8995
1.0000
Version 2.0 08/99
MS
Error
Estimate
0.457
Added
pCi
0.00
LCSD
Erro'
Estimate
0.000
Known
pCi
MSD
Erro'
Estimate
0.00
0.000
Activity
dpm!g
Witness Initials
LCS
Known
pCi
Tracers
i<ll
Page 1 of 1
Printed: 4/241201311:51 AM
-----
Tracer
LCS
Matrix Spike
Added
pCi
0.00
Error
Estimate
0.00(
Eberline Analytical
Work Order
13-041os
Lab
Analysis Code
Rpt Units
Lab Deadline
Technician
Ra228
liters
5/7/2013
JBARNARD
Sample
Muffle Data
Type
-Ratio
Post/Pre.
R
1
Fraction
Client 10
01
02
03
04
05
06
07
~09
10
11
12
13
14
15
-16
17
18
19
LCS
BLANK
PZ-106-SS TOT
PZ-204-SS TOT
PZ-204-SS DIS
1-68 TOT
1-68 DIS
D-87 TOT
D-87 DIS
PZ-106-SD TOT
DIS
- - - -PZ-106-SD
-S-82 TOT
S-82 DIS
PZ-106-SS TOT
PZ-106-SS DIS
1-9 TOT
1-9 DIS
D-93 TOT
D-93 DIS
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
.~~.
Aliquot Data
. -- 1-- NoofDils
Oil Factor
Ratio
.
.
..
..
MS Aliquot Data
H-3 Solids Only
._
..
.
..
. .
Net Equiv
Aliquot
1.0000E+OO
1.0000E+OO
1.5000E+OO
1o5000E+OO
1.5000E+OO 1:5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO :, 1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO .1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1:5000E+OO
1.5000E+OO
J:5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
15000E+OO
Aliquot
I :-.,
Water Added
(ml)
Net Eqliiv
H3 Dist
Aliq
1'
-----
~~--
--
Comments
I!~
W
Ill
Dilution Data
.
.
-
Printed: 41241201311:51 AM
Page 1 of 1
Aliquot Worksheet
Technician:
.--.
~k
Date
Lj :2:.
-~
Eberline Services - Oak Ridge

Version 1.0 911999
Work Order
TRetec
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
Client ID
LCS
BLANK
DUP
PZ-204-SS TOT
PZ-204-SS DIS
1-68 TOT
1-68 DIS
D-87 TOT
D-87 DIS
PZ-106-SD TOT
PZ-1 06-SD DIS
S-82 TOT
S-82 DIS
PZ-106-SS TOT
PZ-106-SS DIS
1-9 TOT
1-9 DIS
D-93 TOT
D-93 DIS
Printed: 51912013 8:55AM

Page 1 of 1
Gravimetric Worksheet
Sample
Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
-DO
TRG
TRG
TRG
TRG
TRG
Analysis
Code
Gravimetric
Carrier
Carrier Cone
(mg/ml)
Technician
Ra228
Yttirum
34.0000
TSMITH
Filter Data
Carrier Data
Carrier Added
(ml)
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
Filter Tare
(g)
o.o9_29 I
0.0923
0.0921
0.0918
0.0914 ! -
0.0914
0.0902
0.0908 !
0.0926
0.0905
0.0908
0.0925
0.0902
0.0909
0.0928
0.0904
0.0905
0.0928
0.0906
Gravimetric
Filter Net
Filter Final
(g)
0.1474
0.1457
0.1432
0.1483
0.1477
0.1482
0.1440
0.1434
0.1455
0.1436
0.1432
0.1432
0.1442
0.1429
0.1458
0.1410
0.1467
0.1468
0.1466
~~~
.J
Technician:
~~
Date:
~ -19 -1-\ )-
(g)
0.0545
'. 0.0534
0.0511
0.0565
.
0.0563
0.0.568
0.0538
0.0526
.
.
0.0529
..
0.0531
0.0524
,_ . 0.0507 .
..
0.0540
0.0520
.. ::.
0.0530 .
0.0506
0.0562
0.0540
.C ~
0.0560
%
Recovery
..
I"'t,,j
. .
80.15.
78.53
75.15
83.09
82.79
83.53
79.12
. _77.35
77.79
78.09
77.06
74.56
79.41
76.49
_,_77.94
. 74.41
82.65
79.41
.82.35
Sheet1
~\.\)
\:--1'7
Detector ID Sample ID Alpha Beta Count Time Voltage

TOD
02
1304105-19 22
354
120
1400 5/9/13 13:22
13
~
C.l
(!)
:,JS
Page 1
CSheet1
)!71!)
(!)
TOD
Detector ID Sample ID Alpha Beta Count Time Voltage
1400 5/9/1311:17
1304105-01 23
640
120
C1
1400 5/9/13 11:17
C2
1304105-02 21
170
120
1400 5/9/13 11:17
1304105-03 12
209
120
C3
226
120
1400 5/9/13 11:17
C4
1304105-04 13
1400 5/9/1311:17
200
120
D2
1304105-05 14
315
1400 5/9/13 11:17
1304105-06 21
120
D4
Iilli
""'t.>ltO
Page 1
c._
Sheet1
)/?/!?~
rJ)
TOO
Detector ID Sample ID Alpha Bela Count Time Voltage
120
1400 5/9/13 12:57
195
1304105-15
6
C1
120
1400 5/9/13 12:57
430
1304105-16 23
C2
120
1400 5/9/13 12:57
1304105-17
7
252
C3
120
1400 5/9/13 12:57
1304105-18 20
478
C4
1400 5/9/13 12:57
229
120
1304105-07 27
A1
1400 5/9/13 12:57
120
1304105-08 18
360
A2
1400 5/9/13 12:57
120
229
1304105-09 16
A3
1400 5/9/13 12:57
195
120
1304105-10 19
A4
5/9/13 12:57
1400
120
1304105-11
16
199
81
5/9/13 12:57
1400
267
120
1304105-12
9
82
120
1400 5/9/13 12:57
192
1304105-13 16
83
1400 5/9/13 12:57
120
1304105-14 16
203
84
,Pt..
S'!D
ll:.-lJ
Page 1
Eberllne Analytical
GPC Detector Report
Printed: 5/9/2013 7:04AM

Pagelofl
(ALL Backgrounds)
c._
1<!1
'"'
,j;:;a,
1-1
Detector
Alpha/Beta
Calibration Date
Count Date
Bkg CPM
PFW
LCL
Mean
UCL
LB4110A- A1
Alpha
11/18/2007
5/9/2013
3.33E-02
-2.18E+01
2.93E-01
2.24E+01
LB4110A - A2
Alpha
11/18/2007
5/9/2013
5.00E-02
-1.85E+01
2.62E-01
1.90E+01
LB4110A - A3
Alpha
11/18/2007
5/9/2013
3.33E-02
LB4110A- A4
Alpha
11/18/2007
5/9/2013
---- ------
p
3.33E-02
LB4110A- B1
Alpha
11/18/2007
LB4110A - B2
Alpha
11/18/2007
5/9/2013
5/9/2013
6.67E-02
6.67E-02
LB4110A- B3
Alpha
5/9/2013
1.67E-02
LB4110A- B4
Alpha
11/18/2007
11/18/2007 -
5/9/2013
LB4110A- C1
Alpha
11/18/2007
5/9/2013
LB4110A- C2
Alpha
11/18/2007
LB4110A - C3
Alpha
LB4110A- C4
f{y/I:J
-1.80E+01
2.24E-01
1.85E+01
-1.91E+01
2.45E-01
1.96E+01
7.51E-02
7.27E-02
2.49E-01
-9.88E-02
-7.93E-02
-6.39E-02
----:-:--- ----- - - - -
p
1.33E-01
-1.44E-01
5.32E-02
1. 70E-01
7.92E-02
3.02E-01 '
1.33E-01
-1.53E-01
8.92E-02
3.31E-01
5/9/2013
3.33E-02
-1.80E-01
8.82E-02
11/18/2007
5/9/2013
8.33E-02
-1.76E-01
1.01E-01
3.56E-01
3.78E-01
Alpha
11/18/2007
5/9/2013
3.33E:oz
-6.28E-02
6.88E-02
2.00E-01
LB4110A- D1
Alpha
11/18/2007
5/9/2013
3.33E-02
-5.36E-02
8.41E-02
2.22E-01
LB4110A - D2
Alpha
11/18/2007
5/9/2013
3.33E-02
-7.03E-02
6.04E-02
LB4110A- D3
Alpha
5/9/2013
11/18/2007
- - - - - - - -------LB4110A- D4
Alpha ---11/18/2007 -- -- 5/9/2013
5.00E-02
1.00E-01
-4.75E-02
1.91E-01 I
1.91E-01 !
-- p
2.25E-01
-5. 74E-02
7.19E-02
7.09E-02
LB4110R- A1
Alpha
11/24/2006
5/9/2013
8.33E-02
-1.01E-01
1.01E-01
3.03E-01
LB4110R- A2
Alpha
11/24/2006
5/9/2013
8.33E-02
-9.01E-02
7.74E-02
2.45E-01
LB4110R - A3
LB4110R- A4
LB4110R- 81
Alpha
Alpha
Alpha
11/24/2006
5/9/2013
11/24/2006
11/24/2006
5/9/2013
5/9/2013
6.67E-02
1.17E-01
5.00E-02
-7.36E-02
-5.30E-02
-9.58E-02
7.68E-02
7.17E-02
6.20E-02
2.27E-01
1.96E-01
2.20E-01
LB4110R- B2
Alpha
11/24/2006
5/9/2013
1.67E-02
-6.94E-02
6.44E-02
1.98E-01
----
1.99E-01
LB4110R- B3
Alpha
11/24/2006
5/9/2013
5.00E-02
-6.53E-02
7.01E-02
2.05E-01
LB4110R- B4
Alpha
11/24/2006
5/9/2013
5.00E-02
-6.48E-02
7.08E-02
2.06E-01
LB4110R- C1
Alpha
11/24/2006
5/9/2013
6.67E-02
-7. 79E-02
7.44E-02
2.27E-01
LB4110R- C2
Alpha
11/24/2006
5/9/2013
1.67E-02
-7.54E-02
7.22E-02
2.20E-01
LB4110R - C3
Alpha
11/24/2006
5/9/2013
8.33E-02
-8.90E-02
8.48E-02
2.59E-01
-6.23E-02
8.20E-02
2.26E-01
LB4110R- C4
Alpha
11/24/2006
5/9/2013
1.67E-02
LB4110R- D1
Alpha
11/24/2006
5/9/2013
O.OOE+OO
-9.93E-02
7.30E-02
2.45E-01
LB4110R- D2
LB4110R - D3
Alpha
11/24/2006
5/9/2013
5/9/2013
O.OOE+OO
2.18E-01
O.OOE+OO
-7.34E-02
___-7.87E-02
..
7.24E-02
-7.01E-02
7. 71E-02
2.23E-01
--2~24E-01
-1.56E-02
9.58E-02
2.07E-01
Alpha
11/24/2006
-------- - - -
LB4lliJR - D4
Alpha
11/24/2006
5/9/2013
O.OOE+OO
LB5100 - 1
Alpha
7/10/2006
10/26/2007
5.00E-02
________ r--------7.22E-02
-!
I
'
i
i
Eberline Analytical
GPC Detector Report

(ALL Backgrounds)
Detector
Alpha/Beta
Calibration Date
Count Date
.t'-l~
LCL
Mean
UCL
Beta
11/18/2007
5/9/2013
7.62E+00
-2.96E+02
7.63E+OO
3.11E+02
Beta
11/18/2007
5/9/2013
3.63E+OO
-3.11E+01
2.55E+OO
3.62E+01
LB4110A - A3
Beta
11/18/2007
5/9/2013
1.17E+OO
__:-:c-
-5.13E+01
2.67E+OO
_,-:-
LB4110A- A4
Beta
11/18/2007
5/9/2013
7.12E+OO
-3.33E+01
3.03E+OO
3.94E+01
LB4110A - B1
Beta
11/18/2007
5/9/2013
1.65E+00
-1.04E+01
3.26E+00
1.70E+01
-7.55E+OO
1.99E+OO
1.15E+01
~------
.... -
LB4110A - B2
Beta
11/18/2007
5/9/2013
1.38E+00
LB4110A- B3
Beta
11/18/2007
5/9/2013
2.25E+00
1.06E-01
LB4110A- B4
Beta
11/18/2007
5/9/2013
1.92E+OO
-7.61E+OO
-5.50E+OO
c_
'J(l((")
5.66E+01
------
1.36E+OO ,__~:62E+OO
1.15E+01
1.97E+OO
2.15E+OO
9.81E+OO
LB4110A- C1
Beta
11/18/2007
5/9/2013
1.02E+OO
LB4110A- C2
Beta
11/18/2007
5/9/2013
1.03E+OO -
3.80E-01
1.27E+OO
2.16E+OO
LB4110A - C3
LB4110A- C4
LB4110A- D1
Beta
11/18/2007
5/9/2013
1.15E+OO .
4.69E-01
1.47E+00
2.47E+00
Beta
5/9/2013
5/9/2013
1.05E+00.
6.05E+OO
2.13E+OO
-1.77E+OO
-2.38E+OO
2.14E+00
Beta
11/18/2007
11/18/2007
2.59E+OO
7.56E+00
LB4110A- D2
Beta
11/18/2007
5/9/2013
1.18E+OO.
-6.81E-01
L57E+00
3.81E+OO
LB4110A- 03
Beta
11/18/2007
5/9/2013
4.55E+OO
1.22E+OO
4.47E+00
7.73E+OO
LB4110A- D4
Beta
11/18/2007
-4.5H:-01
Beta
11/24/2006
11/24/2006
Beta
Beta
11/24/2006
1.50E+00 .
1.10E+00,
1.15E+OO.
L28E+OO
LB4110R- A1
LB4110R- A2
LB4110R- A3
5/9/2013
5/9/2013
5/9/2013
5/9/2013
-6.20E+01
-4.92E+01
-4.56E+01
L37E+00
3.77E+00
2.05E+OO
2.80E+OO
3.20E+OO
6.95E+01
5.34E+01
5.12E+01
LB4110R- A4
Beta
11/24/2006
5/9/2013
1.43E+00,
-4.55E+01
2.02E+OO
4.95E+01
LB4110R- B1
Beta
11/24/2006
5/9/2013
1.15E+00.
-4.79E+01
2.05E+00
5.20E+01
-4, 78E+01
2.08E+OO
2. 71E+00
5.20E+01 I
--
-::--:-:-
LB4110R- 82
Beta
11/24/2006
5/9/2013
1.08E+OO,
LB4110R- 83
LB4110R- 84
Beta
11/24/2006
l.OOE+OO
1.2BE+00
-4. 76E+01
11/24/2006
5/9/2013
5/9/2013
-4.80E+01
L95E+OO
5.19E+01
1.35E+00.
-4.77E+01
3.03E+OO
5.38E+01
--Beta
5.30E+01
L84110R- C1
Beta
11/24/2006
5/9/2013
LB4110R- C2
Beta
11/24/2006
5/9/2013
1.58E+OO
-4.77E+01
2.75E+00
5.32E+01
LB4110R - C3
LB4110R- C4
Beta
11/24/2006
5/9/2013
1.28E+OO,
1.32E+OO,
2.56E+OO
2.99E+OO
5.33E+01
-4.82E+01
-5.44E+01
-Beta
11/24/2006
5/9/2013
6.04E+01
LB4110R - D1
Beta
11/24/2006
5/9/2013
O.OOE+OO
-4.51E+01
5.78E+OO
5.67E+01
LB4110R- 02
Beta
11/24/2006
5/9/2013
O.OOE+OO
-4.87E+01
1.95E+00
5.26E+01
LB4110R- D3
Beta
11/24/2006
5/9/2013
O.OOE+OO
-5.20E+01
5.75E+OO
6.35E+01
LB4110R - D4
Beta
11/24/2006
5/9/2013
O.OOE+OO
-4.83E+01
2.32E+OO
5.30E+01
Beta
7/10/2006
10/26/2007
4.52E+00
-3.19E-01
1.58E+00
3.48E+OO
LB5100 - 1
""
PFW
LB4110A- A1
--
Bkg CPM
LB4110A- A2
- - - - - - - --
Printed: 5/9/2013 7:04AM

Page 1 of 1
1-----
------ - - - - - -
'
Eberline Analytical
GPC Detector Report

(ALL Efficiencies)
Detector
LCL
Mean
UCL
0.2147
0.4482
0.1725
0.4013
5/9/2013
0.2393
LB4110A- A2
Alpha
11/18/2007
5/9/2013
0.2070
-0.0188
-0.0562
LB4110A- A3
Alpha
11/18/2007
5/9/2013
0.2093
-0.0799
0.1614
0.4027
LB4110A- A4
Alpha
11/18/2007
5/9/2013
0.2196
-0.0583
0.1803
0.4190
LB4110A- B1
Alpha
11/18/2007
5/9/2013
0.2164
0.1943
0.2246
0.2550
LB4110A- B2
Alpha
11/18/2007
5/9/2013
0.2036
0.1929
0.2218
0.2507
LB4110A- B3
Alpha
11/18/2007
5/9/2013
0.2319
0.1293
0.2326
0.3359
0.2248
0.2090
0.2367
0.2644
Alpha
11/18/2007
5/9/2013
LB4110A- C1
Alpha
11/18/2007
5/9/2013
0.2168
0.1973
0.2208
0.2444
LB4110A- C2
Alpha
11/18/2007
5/9/2013
0.2220
0.1966
0.2252
0.2538
0.2514
0.2228
0.2494
0.2759
5/9/2013
0.2144
0.1965
0.2258
0.2550
0.2036
0.2334
0.2632
0.2584
0.2890
Alpha
11/18/2007
5/9/2013
LB4110A- C4
Alpha
LB4110A- D1
Alpha
11/18/2007
5/9/2013
0.2272
LB4110A- D2
Alpha
11/18/2007
5/9/2013
0.2542
0.2278
5/9/2013
0.2680
0.2315
0.2639
0.2963
0.1651
0.1999
0.2347
Alpha
11/18/2007
11/18/2007
LB4110A- D4
Alpha
11/18/2007
5/9/2013
0.1888
LB4110R- A1
Alpha
11/24/2006
5/9/2013
0.2423
0.2031
0.2389
0.2747
0.2051
0.1899
0.2207
0.2514
Alpha
11/24/2006
5/9/2013
LB4110R- A3
Alpha
11/24/2006
5/9/2013
0.2194
0.1963
0.2249
0.2534
LB4110R- A4
Alpha
11/24/2006
5/9/2013
0.2443
0.2159
0.2457
0.2755
0.2226
0.1877
0.2261
0.2645
0.1801
0.2176
0.2550
LB4110R- B1
Alpha
11/24/2006
5/9/2013
LB4110R- B2
Alpha
11/24/2006
5/9/2013
0.2094
LB4110R- B3
Alpha
11/24/2006
5/9/2013
0.2429
0.2067
0.2440
0.2813
0.2205
0.1938
0.2320
0.2702
0.1861
0.2153
0.2445
LB4110R- B4
Alpha
11/24/2006
5/9/2013
LB4110R- C1
Alpha
11/24/2006
5/9/2013
0.2104
LB4110R- C2
Alpha
11/24/2006
5/9/2013
0.2201
0.1963
0.2248
0.2533
LB4110R- C3
Alpha
11/24/2006
5/9/2013
0.2307
0.2064
0.2398
0.2731
0.2066
0.1859
0.2229
0.2600
0.0383
0.2074
0.3764
LB4110R- C4
Alpha
11/24/2006
5/9/2013
LB4110R- D1
Alpha
11/24/2006
5/9/2013
0.0000
LB4110R- D2
Alpha
11/24/2006
5/9/2013
0.0000
0.0443
0.2358
0.4272
LB4110R- D3
Alpha
11/24/2006
5/9/2013
0.0000
0.0436
0.2316
0.4197
LB4110R- D4
Alpha
11/24/2006
5/9/2013
0.0000
0.0334
0.1867
0.3399
7/10/2006
10/26/2007
0.3368
':'____
0.3332
_0.3455
0.3578
LB5100- 1
~~jo
PFW
11/18/2007
LB4110R- A2
(,.,)
Eff
Alpha
LB4110A- D3
Count Date
LB4110A- A1
LB4110A- C3
11:>.
Calibration Date
LB4110A- B4
'
Alpha/Beta
Printed: 5/9/2013 7:04AM

Page 1 of 1
Alpha
c
Jlftt)
Eberline Analytical
GPC Detector Report

(ALL Efficiencies)

Detector
Alpha/Beta
Calibration Date
Count Date
Eff
PFW
LCL
Mean
UCL
LB4110A- A1
Beta
11/18/2007
5/9/2013
0.5612
0.2034
0.5628
0.9222
LB4110A- A2
Beta
11/18/2007
5/9/2013
0.4889
0.1542
0.4633
0.7724
LB4110A- A3
Beta
11/18/2007
5/9/2013
0.4808
0.0815
0.4570
0.8326
LB4110A- A4
Beta
11/18/2007
5/9/2013
0.5300
0.1339
0.4877
0.8416
LB4110A- B1
Beta
11/18/2007
5/9/2013
0.5094
0.4637
0.5306
0.5974
LB4110A- B2
Beta
11/18/2007
5/9/2013
0.5039
0.4639
0.5276
0.5914
0.3190
0.5321
0.7451
0.5546
0.5027
0.6171
0.5552
Beta
11/18/2007
5/9/2013
0.5356
11/18/2007
11/18/2007
5/9/2013
5/9/2013
0.5363
0.4933
LB4110A- C1
Beta
Beta
0.4922
0.4501
LB4110A- C2
Beta
11/18/2007
5/9/2013
0.4844
0.4279
0.5011
0.5744
LB4110A- C3
LB4110A- C4
LB4110A- D1
Beta
Beta
5/9/2013
5/9/2013
5/9/2013
0.5926
0.5054
0.5297
Beta
11/18/2007
11/18/2007
11/18/2007
0.5277
0.4567
0.4798
0.5901
0.5251
0.5543
0.6526
o.5934
0.6287
LB4110A- D2
Beta
11/18/2007
5/9/2013
0.5559
0.4905
0.5888
0.6871
LB4110A- D3
Beta
11/18/2007
5/9/2013
0.6119
0.5368
0.6156
0.6943
LB4110A- B3
LB4110A- B4
tj,
Beta
11/18/2007
11/24/2006
5/9/2013
5/9/2013
0.4462
0.5712
0.3864
0.4813
0.4735
0.5680
0.5605
0.6546
Beta
11/24/2006
5/9/2013
0.4969
0.4209
0.5089
0.5969
0.5238
0.4580
0.5398
0.6216
0.5100
0.5917
0.5428
0.5203
0.6321
0.6093
0.5913
0.6810
Beta
LB4110R- A2
Beta
11/24/2006
5/9/2013
LB4110R- A4
Beta
11/24/2006
5/9/2013
0.6035
LB4110R- B1
Beta
Beta
11/24/2006
11/24/2006
5/9/2013
5/9/2013
Beta
11/24/2006
5/9/2013
0.5280
0.5123
0.6008
0.4535
0.4312
0.5016
LB4110R- B4
Beta
11/24/2006
5/9/2013
0.5220
0.4623
0.5500
0.6377
LB4110R- C1
LB4110R- C2
LB4110R- C3
Beta
Beta
5/9/2013
5/9/2013
5/9/2013
0.4682
0.5117
p
p
0.4242
0.4503
0.5033
0.5292
0.5824
0.6082
Beta
11/24/2006
11/24/2006
11/24/2006
0.5612
0.4813
0.5713
0.6613
LB4110R- C4
Beta
11/24/2006
5/9/2013
0.4873
0.4324
0.5265
0.6206
LB4110R- Dl
Beta
11/24/2006
5/9/2013
0.0000
0.0907
0.4959
0.9010
LB4110R- D2
LB4110R- D3
Beta
11/24/2006
5/9/2013
0.0000
0.1026
0.5572
1.0117
0.0000
0.0996
0.5412
0.9827
LB4110R- D4
Beta
11/24/2006
11/24/2006
5/9/2013
5/9/2013
0.0000
0.0785
0.4455
0.8124
LB5100- 1
Beta
7/10/2006
10/26/2007
0.4428
0.4555
0.4731
0.4906
LB4110R- B2
LB4110R- B3
~~'
LB4110A- D4
LB4110R- A1
LB4110R- A3
!:!!
11:>.
Printed: .5/9/2013 7:04AM

Page 1 of 1
Beta
0.6735
f7Ttr?
SECTION XII
BARIUM-133 ANALYTICAL TRACER DATA
VAX/VMS Peak Search Report Generated

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
rtttl?
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP- 130410501- GE3 BAFIL 191136.CN

PEAK Vl6.9 PEAKEFF V2.2
SPIKE
1-MAY-2013 00:00:00.
1304105-01
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
27.94
30.78
34.85
52.46
56.95
61.58
65.80
80.95
84.54
87.53
92.11
111.75
115.98
192.27
241.12
277.12
282.85
285.53
295.56
302.85
307.61
324.89
333.70
352.38
356.13
377.03
384.07
387.07
414.53
417.87
421.53
436.98
478.29
511.06
583.49
609.36
32
1901
496
99
20
287
161
777
39
20
25
244
58
23
32
36
15
10
24
121
19
19
60
21
497
24
94
169
22
22
16
104
9
17
10
10
116
85
93
69
68
67
78
89
73
72
73
72
65
101
47
45
4
10
14
13
18
25
42
4
12
8
12
13
10
10
12
3
1
10
1
5
3
3
3
9
9
9
9
2
2
2
0
3
3
0
0
0
1
1
0
1
1
0
0
5
5
0
4
4
1
1
1
0
0
0
0
0
C--
1-MAY-2013 07:27:21.57
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.73
1.41
1. 75
2.74
1.99
1. 94
2.33
1.51
1. 55
1. 71
1. 02
1. 89
1.93
6.61
4.80
2.19
1. 71
1.79
3.46
1. 57
1. 81
1. 81
1. 36
2.68
1. 57
1. 56
2.49
1. 37
1. 89
1. 90
1.90
2.01
2.85
2.79
1. 65
1. 21
28.26
31.10
35.17
52.78
57.27
61.90
66.12
81.27
84.86
87.85
92.43
112.07
116.30
192.58
241.43
277.43
283.16
285.84
295.87
303.16
307.92
325.19
334.00
352.69
356.43
377.34
384.37
387.37
414.83
418.17
421.83
437.28
478.59
511.35
583.79
609.66
Left
Pw
26
26
26
50
50
50
50
76
76
76
91
108
108
189
237
272
282
282
292
300
300
321
330
351
351
374
381
381
412
412
412
431
476
506
581
606
15
15
15
22
22
22
22
15
15
15
5
16
16
10
8
11
7
7
9
11
11
9
8
12
12
7
9
9
15
15
15
11
6
10
7
7
1-MAY-2013 07:11:58.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.90 0.4%
4096
10.00000
Cts/Sec %"Err
3.51E-02
2.11E+00
5.51E-01
l.lOE-01
2.25E-02
3.19E-01
1.79E-01
8.64E-Ol
4.29E-02
2.25E-02
2.76E-02
2.72E-01
6.41E-02
2.51E-02
3.55E-02
4.00E-02
1. 68E-02
1.07E-02
2.66E-02
1.34E-01
2.13E-02
2.08E-02
6.62E-02
2.32E-02
5.52E-01
2.69E-02
1.05E-Ol
1. BSE-01
2.48E-02
2.46E-02
1. 82E- 02
1.15E-01
9.78E-03
1.89E-02
l.OSE-02
1.11E-02
70.0
2.4
5.4
16.4
74.7
7.6
12.7
4.0
39.8
74.1
55.2
8.4
29.9
85.6
41.9
39.5
30.3
67.3
35.8
10.1
38.7
54.7
22.9
28.3
4.6
28.4
17.1
9.0
32.5
39.1
44.7
10.3
39.8
42.4
38.6
49.3
Fit
9.68E+00
5.38E+00
3.12E+00
8.67E-01
5.29E+00
4.74E-01
9.17E-Ol
4.41E+00
3.58E+00
Summary of Nuclide Activity

Sample ID : 1304105-01
Acquisition date
Total number of lines in spectrum

Number of unidentified lines
Number of lines tentatively identified by NID
36
30
6
Page :
2
1-MAY-2013 07:11:58
16.67%
Nuclide Type : FISSION

Nuclide
Hlife
CD-109
464.00D
BA-133
10.50Y
NP-237 2.14E+06Y
Decay
1. 00
1. 00
1. 00
Total Activity
Wtd Mean
Uncorrected
pCi/filter
9.565E+01
3.726E+02
2.764E+01
Wtd Mean
Decay Corr
pCi/filter
9.569E+01
3.726E+02
2.764E+01
4.959E+02
4.960E+02
Decay Corr
2-Sigma
2-Sigma Error %Error Flags
14.21E+01
148.48
17.72
0.660E+02
148.47
4.104E+01
Nuclide Type : NATURAL

Nuclide
Hlife
PA-231 3.28E+04Y
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
2.533E+03
1. 00
8.557E+02
Total Activity
Grand Total Activity :
Flags: "K"
"E"
Wtd Mean
Decay Corr
pCi/filter
2.533E+03
8.557E+02
3.388E+03
3.388E+03
3.884E+03
3.884E+03
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
0.685E+03
27.05
1.417E+02
16.56
Manually accepted
Nuclide specific abn. limit
Nuclide Line Activity Report

Sample ID : 1304105-01
Acquisition date
Page :
3
1-MAY-2013 07:11:58
Nuclide Type: FISSION

Nuclide
CD-109
Energy
88.03
%Abn
3.72*
Final Mean for

BA-133
81.00
302.84
356.01
NP-237
86.50
1 Valid Peaks
33.00*
17.80
60.00
Final Mean for
1.899E+01
6.222E+00
5.860E+00
3 Valid Peaks
12.60*
Final Mean for
Uncorrected Decay Corr 2-Sigma

%Eff
pCi/filter pCi/filter %Error
1.712E+01 9.565E+01
9.569E+01 148.48
1.749E+01
9.569E+01+/- 1.421E+02 (148. 48%)
3.726E+02
3.273E+02
4.242E+02
;
3.726E+02
3.273E+02
4.243E+02
17.72
28.87
16.47
OK
OK
OK
3.726E+02+/- 6.602E+01 ( 17.72%)
2.764E+01
1 Valid Peaks;
Status
OK
2.764E+01 148.47
OK
2.764E+01+/- 4.104E+01 (148.47%)
Nuclide Type: NATURAL

Nuclide
PA-231
Energy
9.28
10.11
283.67
302.67
%Abn
42.00*
20.20
1.60
2.30
Final Mean for

TH-234
63.29
Flag:
2 Valid Peaks ;
3.80*
Final Mean for
Uncorrected
%Eff
pCi/filter
1.000E+02 ----- Line
1.000E+02 ----- Line
6.406E+00 4.421E+02
6.224E+00 2.533E+03
2.648E+01
2.533E+03+/- 6.850E+02
8.557E+02
1 Valid Peaks ;
Decay Corr 2-Sigma

pCi/filter %Error
Out Of Range ---Out Of Range ---4.421E+02 63.24
2.533E+03 27.05
8.557E+02
Status
Absent
Absent
OK
OK
( 27.05%)
16.56
OK
8.557E+02+/- 1.417E+02 ( 16.56%)
"*" ; Key line
-Bi!i!-8
Combined Activity-MDA Report

Sample ID : 1304105-01
Acquisition date
4
Page :
1-MAY-2013 07:11:58
---- Identified Nuclides

Nuclide
CD-109
BA-133
PA-231
TH-234
NP-237
Activity
(pCi/filter)
9.569E+01
3.726E+02
2.533E+03
8.557E+02
2.764E+01
Act error
1.421E+02
6.602E+01
6.850E+02
1.417E+02
4.104E+01
MDA
(pCi/ filter)
2.131E+02
2.157E+01
3.138E+00
1.153E+02
6.150E+01
MDA error
Act/MDA
1.757E+01
3.299E+00
4.463E-02
6.195E+00
4.971E+00
0. 449
17.276
807.113
7.419
0.449
MDA error
Act/MDA
1.208E+00
3.883E-02
9.693E-01
-0.009
0.878
2.036
Non-Identified Nuclides
Nuclide
C0-57
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-9.699E-02
2.396E+00
4.013E+01
Act error
6.610E+00
1.518E+00
9.652E+00
MDA
(pCi/filter)
1.058E+01
2.730E+00
1.971E+01

Configuration.
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
c__
'A'ttn
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP 130410502 - GE3 _BAFIL_

BLANK
1-MAY-2013 00:00:00.
1304105-02
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
27.95
30.77
34.82
53.51
58.97
61.81
65.45
69.68
80.94
92.73
111.76
115.83
142.29
160.73
216.19
276.46
295.99
302.93
333.83
338.15
356.05
365.02
383.79
386.87
390.87
414.53
417.87
437.29
468.31
511.66
53
2118
510
73
29
247
116
21
829
21
232
56
18
25
24
67
78
79
127
49
77
72
55
167
119
51
37
102
98
45
26
28
26
16
11
27
18
11
9
7
18
28
13
14
12
2
2
2
0
2
2
2
2
0
0
1
1
0
0
0
0
0
0
3
3
0
0
1
1
1
1
1
0
0
0
1-MAY-2013 07:46:16.71
71
18
141
63
20
534
12
147
251
46
39
29
108
17
15
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.57
1.39
1.59
4.01
1. 65
1.66
1.67
1.38
1.48
1.83
1.59
1. 60
2.61
1. 91
1.16
1. 76
1.41
1.30
1. 86
2.22
1. 80
2.56
1. 87
1.87
1.88
1.89
1. 90
1.97
1.86
2.21
28.27
31.09
35.14
53.83
59.29
62.13
65.77
70.00
81.26
93.05
112.07
116.15
142.60
161.04
216.50
276.77
296.30
303.23
334.14
338.45
356.36
365.33
384.09
387.17
391.17
414.83
418.17
437.60
468.61
511.95
1-MAY-2013 07:30:54.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.99 0. 4%
4096
10.00000
Left
Pw
Cts/Sec %"Err
27
27
27
50
58
58
58
58
76
90
107
107
138
158
213
273
292
300
329
329
351
362
381
381
381
411
411
433
464
508
13
13
13
8
16
16
16
16
10
7
20
20
9
9
7
7
9
6
16
16
5.88E-02 23.7
2.35E+00 2.2
5.66E-01 5.4
8.17E-02 28.9
3.22E-02 33.9
2.75E-01 8.6
1.29E-Ol 16.4
2.33E-02 55.9
9.21E-01 4.5
2.33E-02 88.9
2.58E-Ol 8.3
6.26E-02 24.3
2.01E-02103.0
2.75E-02 75.1
2.66E-02 50.9
7.87E-02 16.9
1.97E-02 60.9
1.56E-01 10.2
7.01E-02 16.1
2.24E-02 44.2
5.93E-Ol 4.7
1.37E-02 56.2
1.63E-01 9.4
2.79E-Ol 7.9
5.16E-02 26.9
4.31E-02 24.0
3.19E-02 36.4
1.20E-Ol 11.9
1.86E-02 45.9
1.65E-02 51.0
11
6
18
18
18
11
11
11
8
11
1138.CN
Fit
1.85E+01
6.22E+00
3.22E+00
2.38E+00
1.38E+Ol
5.18E+00

Sample ID : 1304105-02
Acquisition date

30
25
5
Page :
2
1-MAY-2013 07:30:54
16.67%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3. 972E+02
Total Activity
Nuclide Type
---------
3.972E+02
Wtd Mean
Uncorrected
Decay pCi/filter
7.376E+02
1. 00
1. 00
8.388E+00
--------Total Activity
=
---------
Decay Corr
2-Sigma
0.724E+02
18.23
3.972E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
AM-241
432.20Y
Flags: "K"
"E"
Wtd Mean
Decay Corr
pCi/filter
3.972E+02
---------
7.460E+02
7.460E+02
1.143E+03
1.143E+03
Keyline not found

edited
= Manually
Wtd Mean
Decay Corr
pCi/filter
7.376E+02
8.388E+00
"M"
"A"
Decay Corr
2-Sigma
1.359E+02
18.42
5.714E+00
68.12
= Manually
=
accepted

Sample ID : 1304105-02
Acquisition date
Page :
3
1-MAY-2013 07:30:54

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%-Eff
pCi/filter pCi/filter %-Error
3.972E+02 18.23
1.899E+01 3.972E+02
3.813E+02 29.05
6.222E+00 3.813E+02
4.558E+02 16.60
5.860E+00 4.558E+02
3 Valid Peaks =
3.972E+02+/- 7.240E+01
Status
OK
OK
OK
18. 23%-)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
Flag: "*" = Keyline
1 Valid Peaks =
35.90*
Final Mean for

%-Eff
7.376E+02 18.42
2.648E+01 7.376E+02
2.893E+01
7.376E+02+/- 1.359E+02 ( 18.42%-)
8.388E+00
1 Valid Peaks=
Status
OK
8.388E+OO
68.12
OK
8.388E+OO+/- 5.714E+OO ( 68.12%-)

Sample ID : 1304105-02
Acquisition date
Page :
4
1-MAY-2013 07:30:54

Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filter)
3.972E+02
7.376E+02
8.388E+00
Act error
7.240E+01
1.359E+02
5.714E+00
MDA
(pCi/filter)
2.083E+01
1.298E+02
1.255E+01
MDA error
Act/MDA
3.185E+00
6.970E+00
6.168E-01
19.072
5.684
0.669
MDA error
Act/MDA
1.138E+00
1.681E+01
4.890E-02
4.068E-02
4.848E+00
-0.140
-0.452
0.979
1.169
0.639
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/filter)Ided
-1.391E+00
-9.210E+01
3.365E+00
3.345E+00
3.833E+01
Act error
5.862E+00
1.576E+02
1.698E+00
1.463E+00
3.737E+01
MDA
(pCi/filter)
9. 960E+00
2.038E+02
3.438E+00
2.861E+00
5.998E+01
c._
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
!Ytll'l)
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP 130410503 GE3 BAFIL 191139.CN

PZ-106-SS TOT
1-MAY-2013 00:00:00.
1304105-03
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
27.88
30.74
34.85
53.35
59.35
61.64
65.60
80.93
111.47
160.61
276.78
302.85
306.86
311.53
324.16
333.86
337.81
356.06
383.69
387.05
391.06
412.70
416.56
422.04
437.09
467.29
512.27
535.56
610.02
30
1955
490
45
31
268
126
829
222
28
47
176
27
15
19
85
21
519
124
197
46
8
28
19
88
23
12
7
11
129
86
78
99
99
72
101
136
130
90
27
18
13
11
20
15
11
25
18
10
8
1
3
0
15
5
13
0
5
3
3
3
5
5
5
5
0
0
0
0
1
1
1
0
1
1
0
2
2
2
6
6
6
0
0
0
0
0
1-MAY-2013 08:10:30.41
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 73
1.40
1. 75
2.18
2.20
1.61
2.22
1. 57
1.35
2.16
1.16
1.60
1.81
1. 81
1. 61
1.83
1.83
1.93
2.06
1. 80
2.06
1. 72
3.05
2.53
1.98
1.44
2.02
2.70
1. 35
28.20
31.06
35.17
53.67
59.67
61.96
65.92
81.25
111.78
160.93
277.09
303.16
307.16
311.84
324.46
334.17
338.12
356.37
383.99
387.36
391.36
413.00
416.86
422.34
437.39
467.59
512.57
535.86
610.32
Left
Pw
26
26
26
48
48
48
48
77
109
158
275
293
293
293
320
330
330
351
380
380
380
411
411
411
432
464
508
533
607
14
14
14
22
22
22
22
7
7
8
6
27
27
27
8
13
13
11
18
18
18
15
15
15
10
7
8
6
6
1-MAY-2013 07:54:44.
1. OOOOOE+OO filter
0
BAFIL
0 00:15:03.45 0.4%
4096
10.00000
Cts/Sec %Err
3.31E-02
2.17E+00
5.45E-01
5.04E-02
3.45E-02
2.98E-01
1.40E-01
9.22E-01
2.47E-01
3.14E-02
5.19E-02
1.96E-01
2.96E-02
1.69E-02
2.09E-02
9.48E-02
2.29E-02
5.77E-01
1.38E-01
2.19E-01
5.08E-02
9.21E-03
3.15E-02
2.14E-02
9.77E-02
2.53E-02
1.33E-02
7.78E-03
1.27E-02
77.4
2.4
5.3
41.1
74.9
7.9
16.5
4.2
10.8
60.6
23.4
8.1
39.3
44.5
47.4
12.7
43.4
4.8
10.6
8.0
26.7
35.3
30.4
26.1
13.5
26.8
58.5
37.8
41.7
Fit
9.94E+00
2.63E+00
2.52E+00
8.04E-01
4.01E+00
4.89E+00

Sample ID : 1304105-03
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.975E+02
Total Activity
:
17.24%
FISSION
Hlife
10.50Y
Nuclide Type
29
24
5
Page :
2
1-MAY-2013 07:54:44
---------
3.975E+02
Wtd Mean
Decay Corr
pCi/filter
3.975E+02
---------
Decay Corr
2-Sigma
0.711E+02
17.88
3.975E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
AM-241
432.20Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
8.007E+02
1. 00
8.977E+00
Total Activity
---------
Wtd Mean
Decay Corr
pCi/filter
8.007E+02
8.977E+00
---------
8.097E+02
8.097E+02
1.207E+03
1.207E+03
Flags: "K"
Keyline not found
"E" ; Manually edited
Decay Corr
2-Sigma
1.379E+02
17.22
13.46E+00
149.92
"M" ; Manually accepted

"A" ; Nuclide specific abn. limit

Sample ID : 1304105-03
Acquisition date
Page :
3
1-MAY-2013 07:54:44

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.975E+02
3.975E+02 17.88
6.222E+00 4.779E+02
4.779E+02 26.23
5.860E+00 4.434E+02
4.435E+02 16.64
3 Valid Peaks =
Status
OK
OK
OK
3.975E+02+/- 7.108E+01 ( 17.88%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
Flag: "*" = Keyline
1 Valid Peaks =
35.90*
Final Mean for

%Eff
2.648E+01 8.0Q7E+02
8.007E+02 17.22
2.893E+01
8.007E+02+/- 1.379E+02 ( 17.22%)
8.977E+00
1 Valid Peaks =
Status
OK
8.977E+00 149.92
OK
8.977E+00+/- 1.346E+01 (149.92%)

Sample ID : 1304105-03
Acquisition date
Page :
4
07:54:44
1-MAY-2013
Identified Nuclides
Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filter)
3.975E+02
8.007E+02
8.977E+00
Act error
7.108E+01
1.379E+02
1.346E+01
MDA
(pCi/ filter)
2.286E+01
1.292E+02
1.249E+01
MDA error
Act/MDA
3.496E+00
6.941E+00
6.142E-01
17.389
6.196
0. 719
MDA error
Act/MDA
1.210E+OO
1.690E+01
4.330E-02
3.838E-02
5.099E+00
-0.078
-0.330
0.573
1.069
0.069
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/filter) Ided
-8.215E-01
-6.769E+01
1.746E+00
2.886E+00
4.342E+00
Act error
6.182E+00
1.244E+02
1.562E+00
1.458E+00
3.924E+01
MDA
(pCi/filter)
1.059E+01
2.050E+02
3.044E+00
2.699E+00
6.307E+01

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
C-.
fti//:J
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30410504 GE3 BAFIL 191142. CN

PZ-204-SS TOT
1-MAY-2013 00:00:00.
1304105-04
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30.72
34.92
45.81
52.11
61.57
65.75
80.95
84.52
92.33
111.70
190.90
302.86
307.15
333.83
338.14
356.06
383.62
386.87
391.54
414. 92
418.20
421. 54
437.20
467.88
472.52
511.23
559.41
609.78
1935
499
25
86
244
130
814
25
38
197
21
132
29
93
21
478
145
222
62
57
31
11
92
30
13
19
3
6
87
64
51
98
74
81
69
60
89
130
57
15
21
13
26
30
8
6
4
8
5
4
10
6
1
12
5
3
2
2
2
0
2
2
2
2
0
0
0
3
3
3
3
0
1
1
1
3
3
3
0
1
1
0
0
0
1-MAY-2013 08:28:18.60
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.29
1. 59
1.62
2.24
1. 66
1. 67
1.41
1.70
1.28
1.27
1.24
1. 53
2.19
1.81
2.22
1. 89
1. 87
1. 87
1.88
2.29
2.29
2.30
1.98
1. 93
1. 94
1. 98
1.10
2.04
31.04
35.24
46.13
52.43
61.89
66.07
81.26
84.84
92.65
112.02
191.21
303.17
307.46
334.14
338.45
356.36
383.93
387.17
391.84
415.23
418.51
421. 85
437.50
468.18
472.82
511.52
559.70
610.07
1-MAY-2013 08:12:59.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.54 0.4%
4096
10.00000
Left
Pw
Cts/Sec %Err
27
27
27
49
57
57
77
77
90
108
189
299
299
328
328
351
381
381
381
409
409
409
432
463
463
506
556
606
22
22
22
8
17
17
13
13
7
7
6
12
12
14
14
11
18
18
18
16
16
16
10
14
14
10
6
7
2.15E+00 2.4
5.54E-01 5.2
2.75E-02 56.9
9.60E-02 22.4
2. 71E-Ol 8.6
1.45E-01 13.7
9.05E-Ol 3.8
2.83E-02 84.2
4.22E-02 44.0
2.19E-01 11.9
2.37E-02 59.6
1.46E-Ol 9.5
3.19E-02 38.3
1.03E-Ol 11.9
2.38E-02 50.2
5.32E-Ol 5.1
1. 61E-Ol 8.8
2.47E-Ol 8.4
6.92E-02 15.0
6.29E-02 18.0
3.40E-02 33.5
1.28E-02 67.6
1.02E-01 12.2
3.33E-02 20.2
1.42E-02 39.6
2.08E-02 42.2
3.06E-03139.7
6.67E-03 64.8
Fit
2.94E+00
1.15E+00
1.68E+00
3.67E+00
3.25E+00
2.21E+Ol
1.86E+00
1.22E+00

Sample ID : 1304105-04
Acquisition date

Nuclide Type
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.902E+02
1.00 3.467E+01
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.291E+02
Total Activity
=
=
---------
4.249E+02
Wtd Mean
Decay Corr
pCi/filter
3.902E+02
3.467E+01
---------
Decay Corr
2-Sigma
0.683E+02
17.51
168.57
5.844E+01
4.249E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
17.86%
FISSION
Nuclide
Hlife
BA-133
10.50Y
NP-237 2.14E+06Y
Nuclide Type
28
23
5
Page :
2
1-MAY-2013 08:12:59
---------
Wtd Mean
Decay Corr
pCi/filter
7.291E+02
---------
7.291E+02
7.291E+02
1.154E+03
1.154E+03
Keyline not found

Manually edited
Decay Corr
2-Sigma
1.341E+02
18.39
"M" = Manually accepted

"A" = Nuclide specific abn. limit

Sample ID : 1304105-04
Acquisition date
Page :
3
1-MAY-2013 08:12:59

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

NP-237
86.50
3 Valid Peaks
12.60*
Final Mean for

%Eff
3.902E+02 17.51
1.899E+01 3.902E+02
3.570E+02 28.08
6.222E+00 3.570E+02
5.860E+00 4.086E+02
4.086E+02 17.02
1.749E+01
3.902E+02+/- 6.832E+Ol ( 17.51%)
3.467E+01
1 Valid Peaks=
Status
OK
OK
OK
3.467E+01 168.57
OK
3.467E+Ol+/- 5.844E+01 (168.57%)

Nuclide
TH-234
Energy
63.29
3.80*
Final Mean for

Flag: "*"
Key line

2.648E+01 7.291E+02
7.291E+02 18.39
%Eff
%Abn
1 Valid Peaks
Status
OK
7.291E+02+/- l.341E+02 ( 18.39%)

Sample ID : 1304105-04
Acquisition date
Page :
4
1-MAY-2013 08:12:59

Nuclide
BA-133
TH-234
NP-237
Activity
(pCi/ filter)
3.902E+02
7.291E+02
3.467E+01
Act error
6.832E+01
1.341E+02
5.844E+01
MDA
(pCi/filter)
2.157E+01
1.253E+02
6.150E+01
MDA error
Act/MDA
3.299E+00
6.732E+00
4.971E+00
18.091
5.817
0.564
MDA error
Act/MDA
1.139E+00
1.545E+01
4.330E-02
3.925E-02
9.749E-01
-0.364
0. 422
0.617
1.049
1.890
Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-3.625E+00
7.903E+01
1.878E+00
2.894E+00
3.747E+01
Act error
6.123E+00
1.204E+02
1.551E+00
1.421E+00
1.026E+01
MDA
(pCi/filter)
9.971E+00
1.874E+02
3.044E+00
2.760E+00
1.983E+01

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
fLtit-
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410505_ GE3 BAFIL 191144.CN

PEAK V16.9 PEAKEFF V2.2
PZ-204-SS DIS
1-MAY-2013 00:00:00.
1304105-05
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
27.95
30.73
34.89
51.95
61.79
65.54
80.93
111.74
115.83
205.26
224.01
295.30
302.87
308.51
333.95
338.26
356.10
373.87
376.87
383.68
386.98
391.58
414.72
418.06
437.31
468.28
511.35
523.48
56
1970
465
54
276
103
737
238
37
26
36
23
114
21
86
33
516
9
22
107
224
50
36
23
93
19
13
9
129
84
72
142
105
86
166
74
62
76
68
14
24
28
17
14
33
0
2
4
7
9
11
13
27
7
2
0
2
2
2
0
1
1
0
1
1
0
0
0
0
0
4
4
0
1
1
9
9
9
2
2
0
0
0
0
<:...--
1-MAY-2013 08:46:30.43
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.57
1.37
1. 59
2.34
1.51
1.52
1. 50
1. 59
1.60
1.27
5.28
2.10
1.44
1. 21
1. 91
2.44
1. 87
1. 86
1.86
1.97
1. 80
1.79
2.08
2.09
1. 89
1.42
1.40
1. 33
28.27
31.05
35.21
52.26
62.11
65.86
81.25
112.06
116.15
205.57
224.32
295.61
303.18
308.82
334.25
338.56
356.40
374.17
377.17
383.99
387.29
391.88
415.02
418.36
437.61
468.58
511.65
523.78
Left
Pw
26
26
26
49
58
58
77
107
107
202
220
292
300
307
328
328
351
373
373
381
381
381
410
410
433
464
509
520
15
15
15
8
11
11
7
14
14
8
10
7
7
6
17
17
11
8
8
17
17
17
17
17
11
7
7
8
1-MAY-2013 08:31:09.
1.00000E+00 filter
0
BAFIL
0 00:15:03.67 0. 4%
4096
10.00000
Cts/Sec %Err
6.18E-02
2.19E+00
5.17E-01
6.00E-02
3.07E-01
1.14E-01
8.19E-01
2.64E-01
4.16E-02
2.85E-02
4.03E-02
2.56E-02
1.27E-01
2.33E-02
9.56E-02
3.65E-02
5.73E-01
9. 71E-03
2.50E-02
1.19E-01
2.48E-01
5.58E-02
4.00E-02
2.56E-02
1.03E-01
2.08E-02
1.44E-02
l.OOE-02
41.8
2.4
5.8
40.4
8.2
17.7
4.7
8.6
38.7
62.6
45.6
34.1
11.7
45.6
13.4
31.7
4.9
26.2
26.0
11.8
7.4
17.1
23.7
41.0
14.8
33.0
32.9
33.3
Fit
7.46E+00
6.14E+00
1.94E+00
1.64E+00
1.55E+00
4.82E+00
1.11E+00

Sample IP : 1304105-05
Acquisition date

Number of lines tentatively identified by NIP
Nuclide Type
Nuclide
BA-133
28
24
4
Page :
2
1-MAY-2013 08:31:09
14.29%
FISSION
Hlife
10.50Y
Wtd Mean
Uncorrected
Pecay pCi/filter
1. 00
3.532E+02
---------
Total Activity
3.532E+02
Wtd Mean
Pecay Corr
pCi/filter
3.532E+02
---------
2-Sigma
Pecay Corr
0.649E+02
18.37
3.532E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Pecay pCi/filter
1.00 8.249E+02
---------
Total Activity
Grand Total Activity
Flags:
uKu
"E"
=
=
Wtd Mean
Pecay Corr
pCi/filter
8.249E+02
---------
8.249E+02
8.249E+02
1.178E+03
1.178E+03
Keyline not found

Manually edited
Pecay Corr
2-Sigma
1.458E+02
17.68
"Mn = Manually accepted

HAll

Sample ID : 1304105-05
Acquisition date
Page :
3
1-MAY-2013 08:31:09

Nuclide
BA-133
Energy
81.00
302.84
356.01
33.00*
17.80
60.00
Final Mean for

1.899E+01 3.532E+02
3.532E+02 18.37
3.089E+02 31.18
6.222E+00 3.088E+02
4.409E+02 16.80
5.860E+00 4.408E+02
%Eff
%Abn
3 Valid Peaks
Status
OK
OK
OK
3.532E+02+/- 6.490E+01 ( 18.37%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" ; Keyline

2.648E+01 8.249E+02
8.249E+02 17.68
%Eff
1 Valid Peaks ;
Status
OK
8.249E+02+/- 1.458E+02 ( 17.68%)

Sample ID : 1304105-05
Acquisition date
Page :
4
1-MAY-2013 08:31:09

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.532E+02
8.249E+02
Act error
6.490E+01
1.458E+02
MDA
(pCi/filter)
2.346E+01
1.470E+02
MDA error
Act/MDA
3.588E+00
7.897E+00
15.058
5.610
MDA error
Act/MDA
1.197E+00
1.761E+01
4.620E-02
4.130E-02
5.203E+00
9.793E-01
0.125
-0.349
0.308
1.188
0.179
1.492
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
1.309E+00
-7.455E+01
1.002E+00
3.451E+00
1.150E+01
2.972E+01
Act error
6.355E+00
1.301E+02
1.750E+00
1.569E+00
3.943E+01
1.081E+01
MDA
(pCi/ filter)
1.047E+01
2.136E+02
3.248E+00
2.904E+00
6.436E+01
1.992E+01
lll465
C-VAX/VMS Peak Search Report Generated

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
f/1111?
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410506 GE3 BAFIL 191146. CN

I-68 TOT
1-MAY-2013 00:00:00.
1304105-06
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
30.72
34.94
52.14
61.81
65.75
80.82
83.68
111.67
115.54
142.57
146.83
159.82
276.92
299.69
302.86
306.69
311.96
324.08
333.97
337.71
356.27
369.71
377.20
383.71
386.98
414.53
417.87
421.61
437.04
458.38
468.09
472.32
511.02
1662
441
41
206
84
633
18
171
49
23
22
29
53
10
128
21
16
19
63
24
402
26
24
99
180
59
26
12
99
9
26
15
22
63
51
170
83
78
78
48
56
51
39
36
42
26
16
25
21
13
12
4
5
26
4
5
19
47
1
2
3
5
1
6
2
0
2
2
0
2
2
1
1
1
1
1
1
0
0
1
1
1
0
0
2
2
0
0
0
2
2
1
1
1
0
0
0
0
0
1-MAY-2013 09:02:30.64
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.41
1.59
3.21
1. 66
1.67
1.54
1.41
1. 59
1.60
1.63
1.64
1.62
1.25
1.64
1. 80
1.64
1.78
2.83
2.01
2.02
1.84
3.60
1. 54
2.06
1. 85
1.89
1.90
1.90
1. 74
1.67
1.41
2.63
3.08
31.04
35.26
52.46
62.13
66.06
81.14
84.00
111.99
115.85
142.88
147.15
160.13
277.23
300.00
303.16
307.00
312.27
324.38
334.28
338.02
356.57
370.01
377.50
384.02
387.29
414.83
418.17
421.91
437.35
458.68
468.38
472.62
511.32
Left
Pw
26
26
48
58
58
77
77
107
107
140
140
157
273
299
299
299
310
320
328
328
353
367
374
381
381
410
410
410
433
456
465
471
507
13
13
10
15
15
10
10
13
13
16
16
6
8
12
12
12
6
8
21
21
10
7
7
10
10
15
15
15
9
5
6
5
10
ri
1-MAY-2013 08:47:08.
1.00000E+00 filter
0
BAFIL
0 00:15:03.47 0.4%
4096
10.00000
Cts/Sec %Err
1.85E+00
4.90E-01
4.50E-02
2.29E-01
9.36E-02
7.03E-01
2.03E-02
1.90E-01
5.44E-02
2.50E-02
2.40E-02
3.27E-02
5.91E-02
l.OSE-02
1.42E-01
2.29E-02
1.77E-02
2.06E-02
6.96E-02
2.66E-02
4.47E-01
2.87E-02
2.62E-02
1.10E-01
2.00E-01
6.57E-02
2.94E-02
1.31E-02
1.09E-01
9.78E-03
2.89E-02
1.72E-02
2.44E-02
2.5
5.5
62.2
9.7
20.5
4.6
99.6
10.5
30.6
46.2
47.4
39.6
21.5
57.8
10.5
40.8
44.1
41.4
14.8
34.1
5.6
24.2
26.2
13.6
9.4
12.6
31.2
45.7
10.8
38.6
24.6
29.0
21.3
Fit
5.63E+00
2.11E+00
5.77E+00
3.59E+00
1.31E+00
1.48E+01
1.59E+00
9.38E+00
9.29E+00

Sample ID : 1304105-06
Acquisition date

33
29
4
Page :
2
1-MAY-2013 08:47:08
12.12%

Nuclide
BA-133
Hlife
l0.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.032E+02
Total Activity
3.032E+02
Wtd Mean
Decay Corr
pCi/filter
3.032E+02
Decay Corr
2-Sigma
18.24
0.553E+02
3.032E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 6.155E+02
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
6.155E+02
6.155E+02
6.155E+02
9.187E+02
9.187E+02
Keyline not found

Manually edited
Decay Corr
2-Sigma
20.49
1.261E+02

U67

Sample ID : 1304105-06
Acquisition date
Page :
3
1-MAY-2013 08:47:08

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.032E+02 18.24
1.899E+01 3.032E+02
3.467E+02 29.35
6.222E+00 3.467E+02
3.435E+02 17.71
5.860E+00 3.435E+02
3 Valid Peaks
Status
OK
OK
OK
3.032E+02+/- 5.532E+01 ( 18.24%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
2.648E+01 6.155E+02
6.155E+02 20.49
1 Valid
Peaks~
Status
OK
6.155E+02+/- 1.261E+02 ( 20.49%)

Sample ID : 1304105-06
Acquisition date
Page :
4
1-MAY-2013 08:47:08

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
3.032E+02
6.155E+02
5.532E+01
1.261E+02
1.973E+01
1.196E+02
3.017E+00
6.422E+00
15.372
5.148
Act error
MDA
(pCi/ filter)
MDA error
Act/MDA
1.116E+OO
1.521E+01
3.835E-02
3.812E-02
4.128E+00
8.644E-01
0.320
0.120
0.200
1.417
0.061
1.511
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
3.123E+00
2.218E+01
5.401E-01
3.799E+00
3.114E+00
2.656E+01
5.602E+00
1.121E+02
1.446E+00
1.371E+00
3.126E+01
9.187E+00
9.768E+00
1.844E+02
2.696E+00
2.680E+00
5.106E+01
1.758E+01
(._.

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Yttrn
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP- 130410507 GE3 BAFIL 191150. CN

I-68 DIS
1-MAY-2013 00:00:00.
1304105-07
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
27.95
30.74
34.92
52.66
61.75
65.65
80.84
111.55
277.56
282.28
302.82
307.13
333.83
337.25
356.04
364.35
383.69
386.89
415.01
418.87
433.63
436.87
467.35
510.82
609.98
40
1971
438
88
227
135
827
201
40
10
135
15
74
19
534
15
141
194
36
25
7
98
36
21
11
138
88
71
134
99
94
187
133
56
11
21
28
23
12
29
12
37
32
7
8
8
9
4
4
0
2
2
2
0
1
1
0
0
0
0
3
3
3
3
0
0
3
3
2
2
1
1
0
0
0
1-MAY-2013 09:21:24.39
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.57
1.41
1. 59
2.68
1.51
1.52
1. 55
1. 49
1. 48
1.12
1. 51
2.19
2.21
2.02
1. 77
1. 62
2.26
1.55
2.08
1. 90
1.91
1. 91
1. 64
1.50
2.88
28.27
31.06
35.24
52.98
62.06
65.97
81.16
111.86
277.87
282.59
303.13
307.44
334.14
337.55
356.35
364.65
384.00
387.19
415.31
419.17
433.93
437.17
467.65
511.12
610.27
Left
Pw
26
26
26
50
58
58
76
107
273
281
297
297
330
330
352
362
381
381
412
412
432
432
463
507
606
15
15
15
8
12
12
10
8
9
5
14
14
11
11
9
5
9
9
13
13
12
12
8
8
9
1-MAY-2013 09:06:04.
1.00000E+00 filter
0
BAFIL
0 00:15:03.71 0. 4%
4096
10.00000
Cts/Sec %Err
4.49E-02
2.19E+00
4.87E-01
9.77E-02
2.52E-01
1.50E-01
9.18E-01
2.23E-01
4.48E-02
1. 16E- 02
1.50E-01
1.68E-02
8.17E-02
2.10E-02
5.93E-01
1.70E-02
1.56E-01
2.16E-Ol
4.04E-02
2.74E-02
8.20E-03
l.Q8E-01
4.00E-02
2.33E-02
1.22E-02
57.9
2.3
6.1
25.0
9.6
14.4
4.7
12.2
37.0
54.1
9.8
74.9
16.0
51.0
4.7
42.7
13.3
8.8
20.8
33.0
54.2
11.8
19.2
27.4
30.2
Fit
7.72E+00
4.11E+00
2.25E+00
8.08E+00
4.99E+Ol
1.93E+00
8.80E+00

Sample ID : 1304105-07
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.961E+02
---------
Total Activity
:
3. 961E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
2.838E+03
1. 00
6.780E+02
---------
Total Activity
=
Wtd Mean
Decay Corr
pCi/filter
3.961E+02
---------
2-Sigma
Decay Corr
0.727E+02
18.35
3. 961E+02
NATURAL
Nuclide
Hlife
PA-231 3.28E+04Y
TH-234 4.47E+09Y
Flags: IlK II
20.00%
FISSION
Hlife
10.50Y
Nuclide Type
25
20
5
Page :
2
1-MAY-2013 09:06:04
Wtd Mean
Decay Corr
pCi/filter
2.838E+03
6.780E+02
---------
3.516E+03
3.516E+03
3.913E+03
3.913E+03
Key line not found
"E" = Manually edited
uM" =
"An =
Decay Corr
2-Sigma
0.754E+03
26.56
20.26
1. 374E+02
Manually accepted
6471

Sample ID : 1304105-07
Acquisition date
Page :
3
1-MAY-2013 09:06:04

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+Ol 3.961E+02
3.961E+02 18.35
3.669E+02 28.42
6.222E+00 3.669E+02
5.860E+00 4.562E+02
4.562E+02 16.56
3 Valid Peaks =
Status
OK
OK
OK
3.961E+02+/- 7.269E+Ol ( 18.35%)

Nuclide
PA-231
Energy
9.28
10.11
283.67
302.67
%Abn
42.00*
20.20
1.60
2.30
Final Mean for

TH-234
63.29
Flag:
"*" = Keyline
2 Valid Peaks =
3.80*
Final Mean for
Uncorrected
%Eff
pCi/filter
l.OOOE+02 ----- Line
l.OOOE+02 ----- Line
6.406E+00 3.060E+02
6.224E+00 2.838E+03
2.648E+01
Status
Absent
Absent
OK
OK
2.838E+03+/- 7.540E+02 ( 26.56%)
6.780E+02
1 Valid Peaks =
Decay Corr 2-Sigma

pCi/filter %Error
Out Of Range ---Out Of Range ---3.060E+02 109.69
2.838E+03 26.56
6.780E+02
20.26
OK
6.780E+02+/- 1.374E+02 ( 20.26%)

Sample ID : 1304105-07
Acquisition date
Page :
4
1-MAY-2013 09:06:04

Nuclide
BA-133
PA-231
TH-234
Activity
(pCi/filter)
3.961E+02
2.838E+03
6.780E+02
Act error
7.269E+01
7.540E+02
1.374E+02
MDA
(pCi/filter)
1.944E+01
3.354E+00
1.402E+02
MDA error
Act/MDA
2.973E+00
4.771E-02
7.530E+00
20.378
846.211
4.836
MDA error
Act/MDA
1.229E+00
1.609E+01
3.930E-02
4.599E+00
9.498E-01
0.181
0.202
1.273
0.067
1. 494
Nuclide
C0-57
CD-109
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
1.951E+00
3.935E+01
3.518E+00
3.811E+00
2.887E+01
Act error
5.996E+00
1.175E+02
1.458E+OO
3.513E+01
1.040E+01
MDA
(pCi/filter)
1.075E+01
1.951E+02
2.763E+00
5.690E+01
1.932E+01
<:......-

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
(ill)
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410508 - GE5 BAFIL 191140.CN

D-87 TOT
1-MAY-2013 00:00:00.
1304105-08
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
19.08
20.03
21.12
28.57
29.56
31.08
35.19
36.07
53.52
54.23
61.94
66.33
79.73
81.19
84.62
88.17
111.31
112.09
112.51
160.72
276.23
276.91
303.09
307.38
333.83
356.15
383.98
386.91
391.27
15
21
84
29
31
1914
384
102
48
12
230
118
40
863
10
12
23
163
58
25
43
21
13
17
10
31
23
20
44
23
20
5
33
36
6
14
27
11
22
32
21
12
9
3
12
0
12
6
4
14
9
3
3
3
3
3
3
1
1
2
2
0
0
1
1
0
0
5
5
5
0
4
4
0
0
0
0
0
0
0
1-MAY-2013 08:10:41.66
96
33
39
351
84
151
32
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
1-MAY-2013 07:55:22.
1.00000E+00 filter
0
BAFIL
0 00:15:01.16 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
188.48
197.59
208.00
279.57
289.00
303.58
343.09
351.46
518.94
525.79
599.77
641.91
770.45
784.49
817.36
851.41
1073.49
1081.00
1085.00
1547.59
2656.00
2662.57
2913.76
2954.94
3208.77
3422.94
3689.96
3718.02
3759.86
182
182
182
268
268
268
333
333
511
511
588
629
761
761
799
843
1069
1069
1069
1536
2647
2647
2897
2941
3193
3406
3675
3703
3745
34
34
34
52
52
52
26
26
18
18
21
28
38
38
23
13
29
29
29
19
22
22
28
24
23
31
25
29
26
1.64E-02 49.3
2.38E-02 53.8
9.33E-02 14.7
3.26E-02 49.5
3.40E-02 44.8
2.13E+00 2.4
4.27E-01 6.6
1.13E-01 21.9
5.34E-02 24.5
1.34E-02 47.1
2.56E-01 8.4
1.31E-01 15.4
4.41E-02 27.9
9.59E-01 3.5
1.15E-02114.2
1.38E-02 55.0
2.51E-02 34.3
1.81E-01 11.4
6.41E-02 31.7
2.82E-02 31.8
4.79E-02 18.0
2.31E-02 35.0
1. 07E-01 12.3
3.67E-02 17.4
4.33E-02 22.6
3.90E-01 5.5
9.33E-02 11.9
1. 67E-01 9.6
3.56E-02 25.8
0.66
0.67
0.51
0.72
0.54
0.73
0.61
0.62
0.76
0.51
0.95
1. 35
0.76
0.69
0.27
0.45
0.50
0.77
0.77
0.78
1. 03
0.78
0.72
0.21
0.98
0.96
1. 03
1.00
1.18
Fit
1.24E+00
1.71E+00
6.95E-01
3.68E+00
1.20E+00
4.08E+00
1.88E+00

Sample ID : 1304105-08
Acquisition date

29
22
7
Page :
2
1-MAY-2013 07:55:22
24.14%

Nuclide
Hlife
CD-109
464.00D
BA-133
10.50Y
NP-237 2.14E+06Y
Decay
1. 00
1.00
1.00
Total Activity
Wtd Mean
Uncorrected
pCi/filter
8.685E+01
4.359E+02
2.343E+01
Wtd Mean
Decay Corr
pCi/filter
8.690E+01
4.359E+02
2.343E+01
5.462E+02
5.463E+02
Decay Corr
2-Sigma
9.593E+01
110.39
0.733E+02
16.82
2.585E+01
110.33

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.081E+02
Total Activity
Flags: "K"
"E"
= Keyline
=
Wtd Mean
Decay Corr
pCi/filter
2.081E+02
2.081E+02
2.081E+02
7.543E+02
7.543E+02
not found
Manually edited
"M"
"A"
Decay Corr
2-Sigma
0.360E+02
17.29
= Manually accepted
=
tlit175

Sample ID : 1304105-08
Acquisition date
Page :
3
1-MAY-2013 07:55:22

Nuclide
CD-109
Energy
88.03
%Abn
3.72*
Final Mean for

BA-133
81.00
302.84
356.01
NP-237
86.50
1 Valid Peaks =
33.00*
17.80
60.00
Final Mean for
1.802E+Ol
2.575E+00
4.312E+00
1.262E+Ol
4.359E+02
6.291E+02
4.079E+02
16.82
36.08
18.19
OK
OK
OK
4.359E+02+/- 7.331E+Ol ( 16.82%")
2.343E+01
1 Valid Peaks =
Status
OK
8.690E+01+/- 9.593E+01 (110.39%")
4.359E+02
6.290E+02
4.079E+02
3 Valid Peaks =
12.60*
Final Mean for

%"Eff
1.153E+Ol 8.685E+Ol
8.690E+Ol ll0.39
2.343E+Ol llO. 33
OK
2.343E+01+/- 2.585E+01 (110.33%")

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11

8.750E+01 2.081E+02
2.081E+02 17.29
%Eff
1 Valid Peaks =
Status
OK
2.081E+02+/- 3.598E+01 ( 17.29%")
* 11 = Key line
8.d7S

Sample ID : 1304105-08
Acquisition date
Page :
4
1-MAY-2013 07:55:22

Nuclide
CD-109
BA-133
TH-234
NP-237
Activity
(pCi/filter)
Act error
8.690E+01
4.359E+02
2.081E+02
2.343E+01
MDA
(pCi/filter)
MDA error
Act/MDA
9.593E+01
7.331E+01
3.598E+01
2.585E+01
1.590E+02
1.365E+01
2.626E+01
4.950E+01
1.530E+01
2.009E+00
3.379E-01
4.366E+00
0.547
31.945
7.923
0.473
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
8.405E+00
1.816E-02
2.424E-02
3.133E-02
-0.295
0.016
1.805
0.689
Nuclide
C0-57
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
-7.309E+00
2.541E-02
3.887E+00
1.917E+00
1. 4 74E+01
8.707E-01
1.153E+00
1.505E+00
2.479E+01
1.613E+00
2.154E+00
2.783E+00
fiL177

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
c..JV//J
DKAlOO: [GAMMA.SCOSR.ARCHIVE]SMP_130410509_GE5 BAFIL 191143.CN

D-87 DIS
1-MAY-2013 00:00:00.
1304105-09
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
4.09
21.17
31.05
35.18
36.14
45.68
53.59
61.88
66.18
79.72
81.21
87.64
112.07
116.25
159.03
160.92
276.58
303.05
307.34
333.91
356.18
384.08
387.16
11
97
2030
431
88
9
39
277
101
56
914
46
187
46
6
25
43
106
30
51
364
62
142
29
16
100
29
41
8
31
27
45
21
10
18
68
30
15
13
5
5
0
5
16
10
12
0
0
0
4
4
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
1-MAY-2013 08:28:51.89
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
Left
Pw
0.27
0.64
0. 71
0.70
0.76
0.13
0.51
0.98
0.28
0.76
0. 72
2.27
0.46
0.99
0.19
0.29
0.38
0.66
0.64
0.39
0.74
0.83
0.97
41
201
290
334
334
433
509
585
628
759
759
829
1069
1108
1519
1539
2645
2898
2940
3194
3407
3675
3705
7
18
27
27
27
15
19
33
29
36
36
37
20
20
19
18
25
27
25
26
30
27
29
44.65
208.54
303.35
342.95
352.20
443.71
519.58
599.20
640.46
770.34
784.66
846.31
1080.77
1120.86
1531.41
1549.51
2659.40
2913.38
2954.50
3209.50
3423.18
3690.88
3720.46
1-MAY-2013 08:13:33.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:01.17 0.1%
4096
10.00000
Cts/Sec %Err
Fit
1.27E-02 85.4
1.07E-01 14.4
2.26E+00 2.6
4.79E-01 5.8 2.29E+00
9.74E-02 25.6
9.44E-03 78.1
4.36E-02 33.3
3.08E-Ol 7.7
1.12E-Ol 18.7
6.24E-02 24.2 1.20E+00
1.02E+00 3.4
5.07E-02 29.2
2.08E-01 11.7
5.16E-02 28.6
6.89E-03119.4
2.76E-02 33.3
4.73E-02 19.3
1.18E-01 10.5
3.33E-02 18.3
5.64E-02 16.4
4.04E-01 5.7
6.87E-02 16.3
1.58E-01 9.6

Sample ID : 1304105-09
Acquisition date

Nuclide Type
Decay
1. 00
1.00
1.00
Total Activity
:
---------
8.670E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
2.504E+02
---------
Total Activity
=
Wtd Mean
Uncorrected
pCi/filter
3.194E+02
4.614E+02
8.617E+01
Wtd Mean
Decay Corr
pCi/filter
3.196E+02
4.614E+02
8.617E+01
---------
Decay Corr
2-Sigma
1.899E+02
59.42
0.771E+02
16.71
5.109E+01
59.29
8.672E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
30.43%
FISSION
Nuclide
Hlife
CD-109
464.00D
BA-133
10.50Y
NP-237 2.14E+06Y
Nuclide Type
23
16
7
Page :
2
1-MAY-2013 08:13:33
Wtd Mean
Decay Corr
pCi/filter
2.504E+02
---------
2.504E+02
2.504E+02
1.117E+03
1.118E+03
Key line not found
"Eu = Manually edited
2-Sigma
Decay Corr
0.400E+02
15.95
"Mu = Manually accepted
"A"
mt.f79

Sample ID : 1304105-09
Acquisition date
Page :
3
1-MAY-2013 08:13:33

Nuclide
CD-109
Energy
88.03
%-Abn
3.72*
Final Mean for

BA-133
81. 00
302.84
356.01
NP-237
86.50
1 Valid Peaks =
33.00*
17.80
60.00
Final Mean for
1. 802E+01
2.575E+00
4.312E+00
1.262E+Ol
4.614E+02
6. 968E+02
4.221E+02
16.71
33.78
18.45
OK
OK
OK
4.614E+02+/- 7.708E+01 ( 16. 71%-)
8.617E+01
1 Valid Peaks =
Status
OK
3.196E+02+/- 1.899E+02 ( 59. 42%-)
4.614E+02
6. 968E+02
4.220E+02
3 Valid Peaks =
12.60*
Final Mean for

%-Eff
3.196E+02 59.42
1.153E+01 3.194E+02
8.617E+Ol
59.29
OK
8.617E+01+/- 5.109E+Ol ( 59.29%-)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
"*" = Keyline

%-Eff
8.750E+01 2.504E+02
2.504E+02 15.95
1 Valid Peaks =
Status
OK
2.504E+02+/- 3.995E+Ol ( 15.95%-)

Sample ID : 1304105-09
Acquisition date
Page :
4
1-MAY-2013 08:13:33

Nuclide
CD-109
BA-133
TH-234
NP-237
Activity
(pCi/filter)
Act error
3.196E+02
4.614E+02
2.504E+02
8.617E+01
1.899E+02
7.708E+01
3.995E+01
5.109E+01
MDA
(pCi/ filter)
1.551E+02
1.077E+01
2.707E+01
4.827E+01
MDA error
Act/MDA
1.492E+01
1.586E+00
3.483E-01
4.258E+00
2.061
42.834
9.250
1.785
MDA error
Act/MDA
8.667E+00
1.923E-02
2.265E-02
2.668E-02
-0.140
-0.012
2.223
0.486
Nuclide
C0-57
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-3.570E+00
-2.024E-02
4.474E+00
1.151E+00
Act error
1.441E+01
9.368E-01
1.302E+00
1.308E+00
MDA
(pCi/filter)
2.557E+01
1.708E+00
2.012E+00
2.370E+00
nl481

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
C-
)11/?
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410510 GE5 BAFIL 191145.CN

PZ-106-SD TOT
1-MAY-2013 00:00:00.
1304105-10
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
10.97
13.87
18.79
20.20
21.18
31.06
35.21
36.12
47.30
53.36
58.54
61.98
65.92
67.01
79.77
81.20
112.10
276.57
303.06
307.32
333.83
356.17
356.65
383.78
384.54
387.01
387.65
15
14
12
13
66
2020
425
95
10
50
9
222
81
20
54
778
183
37
112
40
46
335
14
79
29
90
31
12
3
11
14
19
117
21
9
6
17
14
57
30
12
15
13
43
11
13
2
8
12
9
6
6
16
8
0
0
0
0
0
0
2
2
0
0
0
0
4
4
2
2
0
0
0
0
0
4
4
3
3
3
3
1-MAY-2013 08:47:01.83
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
1-MAY-2013 08:31:44.
1.00000E+OO filter
0
BAFIL
0.1%
0 00:15:01.14
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
0.89
1. 09
0.12
0.37
0.57
0.80
0.68
0.57
0.18
0.65
0.46
0.75
0.96
0.60
0.75
0.70
0.47
0.72
0.51
0.80
0.14
0.90
1.24
1.16
0.84
1.16
0.85
104
131
175
193
202
292
330
330
453
508
559
587
625
625
759
759
1070
2645
2898
2940
3197
3409
3409
3674
3674
3704
3704
13
14
16
9
13
25
29
29
11
17
14
26
28
28
37
37
23
24
27
24
21
26
26
28
28
26
26
1.69E-02 54.9
1.52E-02 39.6
1.38E-02 67.8
1.39E-02 60.1
7.28E-02 18.6
2.24E+00 2.7
4.72E-01 5.9
1.Q5E-01 18.3
1.06E-02 57.8
5.56E-02 21.5
1.04E-02 79.8
2.46E-01 10.5
9.00E-02 19.8
2.23E-02 32.5
6.021;:-02 28.1
8.65E-01 3.7
2.03!!:-01 11.0
4.08E-02 24.9
1.24E-01 11.4
4.45E-02 17.2
5.07E-02 18.6
3.72E-01 6.0
1.54E-02127.1
8.75E-02 13.2
3.26E-02 29.7
9.96E-02 15.4
3.43E-02 30.4
110.62
138.45
185.70
199.20
208.66
303.40
343.24
352.00
459.26
517.38
567.10
600.17
637.93
648.42
770.81
784.54
1081.07
2659.26
2913.46
2954.38
3208.72
3423.13
3427.72
3688.00
3695.28
3719.00
3725.15
Fit
1.16E+00
8.18E-01
7.57E-01
6.92E-01
1.73E+00
1.82E+00
8-482

Sample ID : 1304105-10
Acquisition date

27
19
8
Page :
2
1-MAY-2013 08:31:44
29.63%"

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.930E+02
Total Activity
Wtd Mean
Decay Corr
pCi/filter
3.930E+02
3.930E+02
3.930E+02
Wtd Mean
Uncorrected
pCi/filter
1.084E+00
3.034E+00
2.001E+02
7.819E-01
Wtd Mean
Decay Corr
pCi/filter
1.084E+00
3.034E+00
2.001E+02
7.819E-01
2.050E+02
2.050E+02
5.980E+02
5.980E+02
Decay Corr
2-Sigma
2-Sigma Error %"Error Flags
0.668E+02
16.98

Nuclide
Hlife
PA-231 3.28E+04Y
PA-234 4.47E+09Y
TH-234 4.47E+09Y
AM-241
432.20Y
Decay
1. 00
1. 00
1.00
1.00
Total Activity
Flags: "K"
"E"
=
=
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
2-Sigma Error %"Error Flags
1.191E+00
109.81
37.39
1.134E+00
0.429E+02
21.43
12.49E-01
159.68
Manually accepted
!L483

Sample ID : 1304105-10
Acquisition date
Page :
3
1-MAY-2013 08:31:44

Nuclide
BA-133
Energy
8l. 00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.930E+02 16.98
1.802E+Ol 3.930E+02
7.327E+02 34.83
2.575E+00 7.326E+02
4.312E+00 3.886E+02
3.886E+02 18.80
3 Valid Peaks =
Status
OK
OK
OK
3.930E+02+/- 6.675E+01 ( 16. 98%)

Nuclide
PA-231
Energy
9.28
10.11
283.67
302.67
%Abn
42.00*
20.20
l. 60
2.30
Final Mean for

PA-234
9.89
21.72
37.93
131.42
TH-234
63.29
59.54
Flag:
"*"
Key line
8.750E+01
1.000E+02
5.117E-01 109.81
3.034E+DO 37.39
1.197E+01 36.83
Not Found -----
OK
OK
OK
Absent
3.034E+00+/- 1.134E+00 ( 37.39%)
2.001E+02
2.001E+02
21.43
OK
2.001E+02+/- 4.288E+01 ( 21.43%)
7.819E-01
1 Valid Peaks=
Status
OK
OK
Absent
OK
1.084E+00+/- 1.191E+00 (109.81%)
5 .117E-01
3.034E+00
1.197E+01
----- Line
1 Valid Peaks =
35.90*
Final Mean for
1.000E+02
1.000E+02
1.000E+02
2.473E+00
3 Valid Peaks =
3.80*
Final Mean for

AM-241
3 Valid Peaks =
89.00
64.90*
23.75
20.40
Final Mean for

%Eff
1.000E+02 1.084E+00
1.084E+00 109.81
1.000E+02 2.255E+00
2.255E+00 109.81
2.191E+00 ----- Line Not Found ----2.572E+00 5.678E+03
5.678E+03 33.37
7.819E-01 159.68
OK
7.819E-01+/- 1.249E+00 (159.68%)

Sample ID : 1304105-10
Acquisition date
Page :
4
1-MAY-2013 08:31:44

Nuclide
BA-133
PA-231
PA-234
TH-234
AM-241
Activity
(pCi/filter)
3.930E+02
1.084E+00
3.034E+00
2.001E+02
7.819E-01
Act error
6.675E+01
1.191E+00
1.134E+00
4.288E+01
1.249E+00
MDA
(pCi/filter)
1.240E+01
1.514E+00
1.134E+00
2.593E+01
2.590E+00
MDA error
Act/MDA
1.825E+00
1.705E-02
1.276E-02
3.336E-01
2.915E-02
31.707
MDA error
Act/MDA
8.338E+00
2.046E+01
3.977E+00
-0.166
0.522
-0.845
0. 716
2.676
7.717
0.302
Nuclide
C0-57
CD-109
NP-237
Key-Line
Activity K.L.
(pCi/filter) Ided
-4.092E+00
1.109E+02
-3.808E+01
Act error
1.395E+01
1.049E+02
3.010E+01
MDA
(pCi/filter)
2.460E+01
2.126E+02
4.509E+01

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
(_....
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410511_GE5 BAFIL 1

PZ-106-SD DIS
1-MAY-2013 00:00:00.
1304105-11
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
20.93
28.63
31.05
35.20
36.02
45.35
46.45
53.35
61.65
62.24
66.23
79.70
80.14
81.23
112.14
115.57
116.22
160.69
276.41
302.98
303.96
307.45
334.02
356.15
383.99
384.51
387.12
387.63
141
26
1982
410
7
24
140
48
19
10
5
6
33
20
68
16
22
12
45
9
35
14
0
7
2
5
7
9
2
2
10
6
0
0
0
3
3
0
0
0
2
2
0
5
5
5
0
7
7
0
0
5
5
0
0
0
1
1
1
1
1-MAY-2013 09:03:22.52
71
8
4
48
135
126
104
47
15
783
182
8
35
26
61
128
17
26
63
409
115
12
117
12
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
l-MAY-2013 08:47:48.
1. OOOOOE+OO filter
0
BAFIL
0 00:15:01.09 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
1.41
0.69
0.68
0.70
0.61
0.20
0.11
0.56
0.75
0.62
0.73
0.90
0.84
0.65
0.71
0.37
0.77
0.91
0.60
1.27
0.70
0.42
0.63
0.83
1.16
1.16
1. 28
1.16
188
273
286
329
329
429
444
511
587
587
628
762
762
762
1069
1112
1112
1536
2645
2897
2897
2942
3196
3404
3674
3674
3706
3706
33
12
28
32
32
16
9
15
22
22
28
32
32
32
22
16
16
18
25
28
28
23
25
34
28
28
24
24
1.56E-01 10.4
2.94E-02 41.7
2.20E+00 2.8
4.55E-01 6.5
7.89E-02 33.4
8. 89E-03101. 6
3. 89E-03121. 6
5.34E-02 18.9
1.50E-01 14.2
1.40E-01 11.9
1.16E-01 21.5
5.20E-02 20.8
1.62E;-02170.9
8.70E-01 3.7
2.02E-01 10.8
9.39E-03 54.3
3.85E-02 35.6
2.89E-02 33.4
6.78E-02 12.8
1.42E-01 9.8
1.85E-02 24.1
2.93E-02 24.4
6.98E-02 15.0
4.54E-01 5.2
1.28E-01 8.4
1.31E-02 74.6
1.30E-01 10.0
1.31E-02 77.2
206.22
280.07
303.35
343.16
351.05
440.52
451.14
517.31
596. 94
602.62
640.89
770.18
774.40
784.80
1081.46
1114.33
1120.57
1547.32
2657.74
2912.73
2922.10
2955.55
3210.58
3422.88
3690.00
3695.00
3720.11
3725.00
{Jttn
147.CN
Fit
2.14E+00
1.65E+00
1.53E+00
3.17E+00
1.30E+00
6.20E+00
1.22E+00
u<~ss

Sample ID : 1304105-11
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 3.952E+02
---------
Total Activity
:
---------
3.952E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 1.13 7E+02
---------
Total Activity
=
Wtd Mean
Decay Corr
pCi/filter
3.952E+02
Decay Corr
2-Sigma
0.671E+02
16.98
3.952E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
21.43%
FISSION
Hlife
10.50Y
Nuclide Type
28
22
6
Page :
2
1-MAY-2013 08:47:48
Wtd Mean
Decay Corr
pCi/filter
1.137E+02
---------
1.137E+02
1.137E+02
5.089E+02
5.089E+02
Key line not found
Decay Corr
2-Sigma
0.275E+02
24.19
"Mn = Manually accepted

II
All
U87

Sample ID : 1304105-11
Acquisition date
Page :
3
1-MAY-2013 08:47:48

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.802E+01 3.952E+02
3.952E+02 16.98
2.575E+00 8.379E+02
8.380E+02 32.87
4.748E+02 17.82
4.312E+00 4.747E+02
3 Valid Peaks =
Status
OK
OK
OK
3.952E+02+/- 6.709E+Ol ( 16.98%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: ''*" = Keyline

%Eff
8.750E+01 1.137E+02
1.137E+02 24.19
1 Valid Peaks =
Status
OK
1.137E+02+/- 2.751E+Ol ( 24.19%)

Sample ID : 1304105-11
Acquisition date
4
Page :
1-MAY-2013 08:47:48

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.952E+02
1.137E+02
6.709E+01
2.751E+01
MDA
(pCi/filter)
1.403E+01
3.121E+01
MDA error
Act/MDA
2.066E+00
4.015E-01
28.169
3.644
MDA error
Act/MDA
9.807E+00
1.605E+01
1.575E-02
2.420E-02
3.243E+00
3.003E-02
0.101
0.046
-0.027
3.028
-0.803
0. 772
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
2.930E+00
7.598E+00
-3.816E-02
6.510E+00
-2.951E+01
2.060E+00
Act error
1.540E+01
8.934E+01
7.505E-01
1.387E+00
2.472E+01
1.369E+00
MDA
(pCi/filter)
2.893E+01
1.668E+02
1.399E+00
2.150E+00
3.677E+01
2.668E+00

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
(__
flt((?

S-82 TOT
1-MAY-2013 00:00:00.
1304105-12
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
21.27
25.29
26.02
28.56
29.66
31.05
35.19
36.07
53.34
61.41
61.97
62.45
65.72
66.66
79.65
81.21
110.93
112.06
116.29
170.35
276.66
302.99
303.43
333.88
355.43
356.26
384.04
386.49
387.04
414.52
415.07
70
9
12
21
22
1950
356
74
34
52
125
33
35
52
44
811
30
222
57
16
38
80
47
54
11
295
71
12
141
12
54
15
15
6
39
48
69
19
7
20
18
19
17
31
24
6
6
5
13
7
11
3
9
5
5
1
3
7
11
14
4
4
0
0
0
4
4
4
1
1
0
1
1
1
1
1
1
1
5
5
0
0
0
5
5
0
2
2
0
1
1
4
4
1-MAY-2013 09:22:07.00
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
1-MAY-2013 09:06:49.
1.00000E+00 filter
0
BAFIL
0 00:15:01.13 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
209.50
248.07
255.05
279.39
290.00
303.37
343.08
351.46
517.20
594.62
600.00
604.59
636.00
645.00
769.67
784.63
1069.81
1080.69
1121.29
1640.03
2660.10
2912.80
2917.00
3209.21
3416.00
3423.94
3690.52
3714.00
3719.35
3983.00
3988.27
203
239
251
273
273
273
332
332
509
585
585
585
626
626
761
761
1063
1063
1110
1626
2646
2897
2897
3193
3406
3406
3677
3704
3704
3969
3969
14
12
8
42
42
42
26
26
15
29
29
29
28
28
35
35
38
38
22
22
24
27
27
26
32
32
25
27
27
29
29
7.80E-02 17.2
9.86E-03 93.6
1.36E-02 44.7
2.33E-02 64.7
2.45E-02 84.0
2.17E+00 2.5
3. 96E-01 6.3
8.27E-02 17.5
3.81E-02 29.8
5.80E-02 30.6
1.39E-01 14.0
3.62E-02 48.0
3.91E-02 40.3
5.83E-02 27.2
4.87E-02 22.1
9.01E-01 3.6
3.38E-02 28.6
2.46E-01 8.0
6.30E-02 16.8
1.79E-02 46.9
4.28E-02 18.4
8.90E-02 13.9
5.19E-02 19.3
5.98E-02 15.8
1.27E-02139.6
3.28E-01 6.6
7.92E-02 13.8
1.31E-02 95.4
1.57E-01 9.4
1.35E-02 58.8
5.98E-02 12.2
0. 71
0.88
0.34
0.79
0.54
0.80
0.62
0.55
0.47
0. 71
0.65
0.58
0.66
0.66
0.76
0.68
0.89
0.92
1. 07
1.00
0.78
1.15
1. 06
0.53
1.12
1.02
1.09
1.16
1.14
1.19
1. 31
Fit
1.29E+00
8.57E-01
1.53E+00
1.17E+00
9.94E-01
8.19E-01
2.88E+00
9.48E-01
1.25E+00
1.30E+00

Sample ID : 1304105-12
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 4.093E+02
---------
Total Activity
:
22.58%
FISSION
Hlife
10.50Y
Nuclide Type
31
24
7
Page :
2
1-MAY-2013 09:06:49
4.093E+02
Wtd Mean
Decay Corr
pCi/filter
4.093E+02
---------
2-Sigma
Decay Corr
0.690E+02
16.85
4.093E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
AM-241
432.20Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.943E+01
1.00 4.368E+00
---------
Total Activity
Wtd Mean
Decay Corr
pCi/fHter
2.943E+01
4.368E+00
---------
3.380E+01
3.380E+01
4.431E+02
4.431E+02
Flags: "Ku = Key line not found

2-Sigma
Decay Corr
96.18
2.831E+01
2.678E+00
61.31

= Nuclide specific abn. limit
nAil

Sample ID : 1304105-12
Acquisition date
Page :
3
1-MAY-2013 09:06:49

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.802E+01 4.093E+02
4.093E+02 16.85
2.575E+00 5.247E+02
5.248E+02 38.35
4.312E+00 3.426E+02
3.426E+02 19.59
3 Valid Peaks =
Status
OK
OK
OK
4.093E+02+/- 6.898E+Ol ( 16. 85%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
1 Valid Peaks =
35.90*
Final Mean for

%Eff
8.750E+01 2.943E+01
2.943E+01 96.18
1.000E+02
2.943E+01+/- 2.831E+01 ( 96.18%)
4.368E+00
1 Valid Peaks =
Status
OK
4.368E+00
61.31
OK
4.368E+00+/- 2.678E+00 ( 61.31%)
Flag: "*" = Keyline
lll492

Sample ID : 1304105-12
Acquisition date
Page :
4
1-MAY-2013 09:06:49

Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filter)
Act error
4.093E+02
2.943E+01
4.368E+00
6.898E+01
2.831E+01
2.678E+00
MDA
(pCi/filter)
1.312E+01
3.121E+01
1.721E+00
MDA error
Act/MDA
1.932E+00
4.015E-01
1.937E-02
31.189
0.943
2.538
MDA error
Act/MDA
8.587E+00
1.470E+01
2.109E-02
2.223E-02
4.097E+00
0.124
0.114
0.211
1. 645
0.070
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/ filter) Ided
3.129E+00
1.741E+01
3.957E-01
3.249E+00
3.246E+00
Act error
1.309E+01
7.884E+01
9.760E-01
1.127E+00
2.479E+01
MDA
(pCi/filter)
2.533E+01
1.527E+02
1.873E+00
1.975E+00
4.645E+01

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMAoSCUSRoARCHIVE]SMP_130410513 GE5 BAFIL

PEAK V16o9 PEAKEFF V2o2
S-82 DIS
1-MAY-2013 OO:OO:OOo
1304105-13
FILTER
GE5
0 00:15:00000
25
3o00000
No
Pk I t
Energy
Area
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
14o56
21.15
25016
31o04
35o34
41075
47o06
53o56
61091
66020
81021
112o05
116o31
276o67
303o05
307o46
333086
334o53
356023
384 011
386o80
387042
391.27
9
101
22
1789
433
6
6
33
230
102
689
138
27
48
93
22
23
22
351
64
127
67
30
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
1
1
0
1-MAY-2013 09:41:25o27
Bkgnd
2
13
12
150
20
7
7
18
14
26
72
31
22
0
0
5
2
1
20
12
15
12
2
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
Left
Pw
:).45 013
208o30
246o80
303025
344o48
405o99
456o92
519028
599o44
640o65
784o69
1080o59
1121o47
2660o23
2913035
2955o66
3209o00
3215o44
3423063
3691019
3717000
3723o00
3759o89
141
199
236
292
334
395
448
510
586
630
772
1069
1111
2646
2897
2939
3191
3191
3406
3674
3705
3705
3747
8
18
17
25
25
15
14
15
28
24
23
20
17
26
27
24
28
28
29
30
28
28
24
Oo33
Oo55
Oo31
Oo76
Oo59
Oo80
Oo93
Oo66
Oo76
Oo65
Oo61
Oo65
Oo32
Oo45
Oo81
Oo56
1010
Oo99
Oo92
Oo76
1.16
1o16
1049
c_
1,an
3 oCN
191~
1-MAY-2013 09:26:050
1. OOOOOE+OO filter
0
BAFIL
0 00:15:01.14 0.1%
4096
10000000
Cts/Sec %Err
Fit
1. OOE-02 43o0
1. 12E- 01 1302
2o41E-02 43o3
1o99E+00 3o0
4o81E-01 5o5
6o15E-03115o8
6o15E-03110o6
3o72E-02 29o1
2o56E-01 7o6
1.13E-01 15 o2
7o66E-01 4o6
1o53E-01 11o 9
2o96E-02 40o0
5o33E-02 1404
1o03E-01 10o4
2o47E-02 2800
2o60E-02 3200 7o26E-01
2o42E-02 1902
3o90E-01 6o0
7 o11E-02 16o5
1.41E-01 10o3 4o89E+00
7o47E-02 19o1
3o30E-02 2007

Sample ID : 1304105-13
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.479E+02
---------
Total Activity
:
3.479E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.079E+02
---------
Total Activity
=
Wtd Mean
Decay Corr
pCi/filter
3.479E+02
---------
Decay Corr
2-Sigma
17.87
0.622E+02
3.479E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
21.74%
FISSION
Hlife
10.50Y
Nuclide Type
23
18
5
Page :
2
1-MAY-2013 09:26:05
Wtd Mean
Decay Corr
pCi/filter
2.079E+02
--- ----....
2.079E+02
2.079E+02
5.558E+02
5.559E+02
Key line not found
"En = Manually edited
Decay Corr
2-Sigma
0.330E+02
15.85
"Mu = Manually accepted

II A"
= Nuclide specific abn.
limit

Sample ID : 1304105-13
Acquisition date
Page :
3
1-MAY-2013 09:26:05

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.802E+01 3.479E+02
3.479E+02 17.87
2.575E+00 6.092E+02
6.093E+02 33.57
4.312E+00 4.071E+02
4. 072E+02 18.83
3 Valid Peaks
3.479E+02+/- 6.215E+01
Status
OK
OK
OK
17.87%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" ; Key line

%Eff
8.750E+01 2.079E+02
2.079E+02 15.85
1 Valid Peaks ;
Status
OK
2.079E+02+/- 3.295E+01 ( 15.85%)

Sample ID : 1304105-13
Acquisition date
4
Page :
1-MAY-2013 09:26:05

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.479E+02
2.079E+02
Act error
MDA
(pCi/ filter)
MDA error
Act/MDA
6.215E+01
3.295E+01
1.624E+01
2.063E+01
2.391E+00
2.655E-01
21.424
10.078
MDA error
Act/MDA
8.992E+00
1.158E+01
1. 859E-02
2.360E-02
4.000E+00
2.531E-02
-0.024
-0.453
0.241
2.219
0.236
0.250
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/ filter) Ided
-6.282E-01
-5.454E+01
3.979E-01
4.651E+00
1.070E+01
5.611E-01
Act error
1.444E+01
7.386E+01
8.296E-01
1.239E+00
2.290E+01
1.344E+00
MDA
(pCi/filter)
2.653E+Ol
1.203E+02
1.652E+00
2. 096E+00
4.535E+01
2.248E+OO
ffh1S7
c.___
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410514 - GE5 - BAFILPEAK V16.9 PEAKEFF V2.2

PZ-106-SS TOT
1-MAY-2013 00:00:00.
1304105-14
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
0
0
4
4
2
2
0
0
0
2
2
5
5
2
2
0
0
0
0
0
0
0
0
21.11
25.69
29.51
31.04
35.19
36.02
48.51
53.11
61.84
65.40
66.17
79.79
81.19
111.09
111.89
116.30
160.95
276.89
303.12
333.92
356.20
384.22
387.01
97
6
33
2075
399
126
13
69
249
43
52
52
789
28
181
31
26
31
117
45
361
52
133
29
24
17
16
11
3
3
28
34
8
27
9
12
18
34
25
9
13
3
5
23
23
17
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
1-MAY-2013 10:01:08.82
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
1-MAY-2013 09:45:33.
1.00000E+00 filter
0
BAFIL
0 00:15:01.12 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
1.02
0.34
0.60
0.77
0.68
0.57
0.76
0.63
0.79
0.65
0.80
0.78
0.69
0.78
0.93
0.52
0.14
0.82
0.93
0.67
0.76
0.78
0.94
197
243
273
273
330
330
465
503
587
627
627
764
764
1067
1067
1111
1539
2645
2898
3193
3407
3680
3706
18
11
45
45
31
31
13
25
23
31
31
30
30
27
27
21
18
25
25)
27
29
25
24
1.08E-01 16.2
6.37E-03172.7
3. 72E-02 39.6
2.31E+OO 2.3
4.44E-01 5.9
1.39E-01 15.5
1.49E-02 38.4
7.69E-02 21.4
2.76E-01 8.2
4.75E-02 24.3
5.78E-02 31.2
5.75E-02 17.8
8.77E-01 3.7
3.16E-02 23.1
2.01E-01 10.3
3.48E-02 38.1
2.89E-02 28.6
3.39E-02 29.7
1.30E-01 9.7
4.96E-02 18.0
4.02E-01 5.9
5.82E-02 21.9
1.48E-01 10.4
207.93
251.90
288.52
303.24
343.07
351.00
470.85
514.99
598.74
632.94
640.33
771.00
784.41
1071.35
1079.07
1121.41
1549.81
2662.34
2914.04
3209.61
3423.33
3692.27
3719.03
)lrtr
191155.~
Fit
1.49E+00
1.20E+00
1.52E+00
4.59E-01
4.49E+00

Sample ID : 1304105-14
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.983E+02
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.245E+02
Total Activity
=
=
---------
3.983E+02
Wtd Mean
Decay Corr
pCi/filter
3.984E+02
---------
Decay Corr
2-Sigma
0.674E+02
16.92
3.984E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
26.09%
FISSION
Hlife
10.50Y
Nuclide Type
23
17
6
Page :
2
1-MAY-2013 09:45:33
---------
Wtd Mean
Decay Corr
pCi/filter
2.245E+02
---------
2.245E+02
2.245E+02
6.228E+02
6.228E+02
Keyline not found

Manually edited
"M"
"A"
=
=
2-Sigma
Decay Corr
16.93
0.380E+02
Manually accepted
!ll499

Sample ID : 1304105-14
Acquisition date
Page :
3
1-MAY-2013 09:45:33

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.984E+02 16.92
1.802E+01 3.983E+02
7.654E+02
7.654E+02 32.76
2.575E+00
4
.196E+02 18.71
4.312E+00 4.195E+02
3 Valid Peaks
Status
OK
OK
OK
3.984E+02+/- 6.742E+01 ( 16. 92%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" ; Keyline

%Eff
2.245E+02 16.93
8.750E+01 2.245E+02
1 Valid Peaks ;
Status
OK
2.245E+02+/- 3.800E+01 ( 16.93%)

Sample ID : 1304105-14
----
Acquisition date
Page :
4
1-MAY-2013 09:45:33
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.984E+02
2.245E+02
6.742E+01
3.800E+01
MDA
(pCi/filter)
1.312E+01
2.063E+01
MDA error
Act/MDA
1.932E+00
2.655E-01
30.354
10.879
MDA error
Act/MDA
8.629E+00
1.475E+01
1. 726E-02
2.359E-02
3.603E+00
2.750E-02
-0.009
0.214
0.120
2.150
-0.558
0.480
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-2.167E-01
3.272E+01
1.834E-01
4.505E+00
-2.278E+01
1.173E+00
Act error
1.372E+01
7.639E+01
7.917E-01
1.468E+00
2.566E+01
1.366E+00
MDA
(pCi/ filter)
2.545E+01
1.532E+02
1.533E+00
2.096E+00
4.084E+01
2.443E+00

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
G
;[t {{/
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30410515 GE3 BAFIL I91152.CN

PZ-106-SS DIS
1-MAY-2013 00:00:00.
1304105-15
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
27.97
30.73
34.81
46.02
52.62
61.65
65.54
80.90
92.73
111.64
116.28
239.23
276.44
295.45
303.04
307.04
333.78
338.35
351.14
356.12
365.00
377.86
383.60
386.87
390.84
414.72
417.34
437.31
468.01
511.29
609.20
36
2032
500
25
60
232
112
786
45
196
51
14
45
13
149
28
61
23
12
485
15
12
128
204
52
43
30
99
20
19
7
139
94
89
98
56
99
119
172
146
129
70
42
32
15
20
21
29
17
3
16
11
14
13
9
7
7
12
14
9
5
1
3
3
3
0
1
1
1
0
0
0
0
0
0
4
4
4
4
4
3
3
0
0
1
1
1
2
2
0
0
0
0
1-MAY-2013 09:40:32.39
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 73
1. 36
1. 75
2.53
1.49
1.51
1.52
1.59
2.29
1.33
1.97
2.56
1.51
2.39
1.87
1.99
1.84
2.44
2.23
1.53
1.20
2.26
1.87
1. 83
1.88
2.08
2.09
1.91
1. 30
1. 80
1. 05
28.29
31.05
35.13
46.34
52.94
61.96
65.86
81.22
93.05
111.95
116.60
239.54
276.75
295.76
303.35
307.34
334.08
338.66
351.45
356.42
365.30
378.17
383.91
387.17
391.14
415.02
417.64
437.61
468.31
511. 59
609.49
Left
Pw
26
26
26
44
50
50
50
76
89
108
115
235
272
293
293
293
329
329
351
351
363
374
380
380
380
410
410
434
464
506
606
14
14
14
7
20
20
20
8
9
7
6
6
8
20
20
20
14
14
13
13
6
7
19
19
19
12
12
7
8
12
6
1-MAY-2013 09:25:15.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.59 0.4%
4096
10.00000
Cts/Sec %Err
4.02E-02
2.26E+00
5.55E-01
2.77E-02
6.65E-02
2.58E-Ol
1. 24E- 01
8.73E-Ol
4.95E-02
2.18E-01
5.70E-02
1.52E-02
5.00E-02
1.49E-02
1.66E-01
3.14E-02
6.83E-02
2.60E-02
1.34E-02
5.39E-Ol
1.66E-02
1. 33E- 02
1.42E-01
2.27E-01
5.74E-02
4.79E-02
3.34E-02
l.lOE-01
2.23E-02
2.12E-02
7.36E-03
65.4
2.3
5.3
68.4
24.5
9.4
16.6
4.6
51.2
12.0
30.6
81.2
26.4
53.2
9.3
40.1
18.4
45.2
18.2
4.7
43.1
59.2
10.2
8.7
24.2
19.6
31.8
11.8
34.9
34.0
48.3
Fit
2.40E+Ol
5.13E+00
1.93E+00
1.80E+00
2.52E+00
5.84E+00
2.81E+00
til5ill2

Sample ID : 1304105-15
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.766E+02
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
l . 00
6.924E+02
Total Activity
=
=
---------
3.766E+02
Wtd Mean
Decay Corr
pCi/filter
3.766E+02
---------
Decay Corr
2-Sigma
18.28
0.688E+02
3.766E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
12.90%
FISSION
Hlife
10.50Y
Nuclide Type
31
27
4
Page :
2
1-MAY-2013 09:25:15
---------
Wtd Mean
Decay Corr
pCi/filter
6.924E+02
---------
6.924E+02
6.924E+02
1.069E+03
1.069E+03
Keyline not found

Manually edited
"M"
"A"
2-Sigma
Decay Corr
1.387E+02
20.03
Manually accepted
specific abn. limit
= Nuclide
1ll5lll3

Sample ID : 1304105-15
Acquisition date
Page :
3
1-MAY-2013 09:25:15

Nuclide
BA-133
Energy
81.00
302.84
356.01
%-Abn
33.00*
17.80
60.00
Final Mean for

%-Eff
3.766E+02 18.28
1.899E+01 3.766E+02
6.222E+00 4.049E+02
4.049E+02 27.73
4.141E+02 16.56
5.860E+00 4.141E+02
3 Valid Peaks
Status
OK
OK
OK
3.766E+02+/- 6.883E+01 ( 18.28%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" ; Key line

%Eff
2.648E+01 6.924E+02
6.924E+02 20.03
1 Valid Peaks ;
Status
OK
6.924E+02+/- 1.387E+02 ( 20.03%)

Sample ID : 1304105-15
----
Acquisition date
4
Page :
1-MAY-2013 09:25:15
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.766E+02
6.924E+02
6.883E+01
1.387E+02
MDA
(pCi/filter)
2.393E+01
1.451E+02
MDA error
Act/MDA
3.659E+00
7.794E+00
15.741
4. 772
MDA error
Act/MDA
1.041E+00
1.581E+01
4.157E-02
3.895E-02
4.640E+00
9.570E-01
-0.088
-0.796
0.198
1.194
-0.655
1.426
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-8.043E-01
-1.527E+02
5.781E-01
3.270E+00
-3.762E+01
2.776E+01
Act error
5.733E+00
1.363E+02
1.582E+00
1.458E+00
4.593E+01
1.058E+01
MDA
(pCi/filter)
9.114E+00
1.917E+02
2.923E+00
2.738E+00
5.740E+01
1.946E+01
c
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

I-9 TOT
1-MAY-2013 00:00:00.
1304105-16
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
30.70
34.98
52.76
61.69
65.92
80.88
92.40
111.52
160.42
274.03
276.55
302.94
334.16
338.46
352.60
356.17
383.89
387.02
391.20
414.83
418.50
421.90
437.19
468.12
471.65
510.86
610.06
1986
467
42
259
135
805
16
203
25
10
64
120
59
20
18
491
88
207
49
29
27
18
107
17
7
26
7
90
94
108
76
92
187
78
153
98
8
15
31
41
16
4
5
16
10
7
13
14
13
7
5
2
0
1
3
3
0
3
3
0
0
0
0
2
2
0
0
0
6
6
5
5
5
4
4
4
0
3
3
0
0
Ji ((1/'7
1-MAY-2013 09:59:49.94
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 34
1. 57
2.34
1. 52
1.83
1. 43
1.97
1.47
1. 08
1.95
1. 96
1.46
1. 31
1. 75
2.51
1.54
2.16
1. 85
2.07
2.47
2.52
2.53
1. 95
2.34
2.34
4.66
1.40
31.02
35.30
53.08
62.01
66.24
81.20
92.72
111.84
160.74
274.34
276.85
303.25
334.47
338.76
352.90
356.48
384.19
387.32
391.51
415.13
418.80
422.20
437.50
468.42
471.95
511.15
610.35
Left
Pw
26
26
50
58
58
76
91
108
158
272
272
299
331
337
351
351
381
381
381
409
409
409
434
464
464
508
608
14
14
6
17
17
10
6
8
7
10
10
7
7
5
10
10
18
18
18
20
20
20
7
12
12
8
5
1-MAY-2013 09:44:28.
1.00000E+00 filter
0
BAFIL
0. 4%
0 00:15:03.68
4096
10.00000
Cts/Sec %Err
2.21E+00
5.19E-01
4.66E-02
2.87E-01
1.50E-01
8.94E-01
1.72E-02
2.26E-01
2.76E-02
1.11E-02
7.12E-02
1.34E-01
6.58E-02
2.24E-02
2.01E-02
5.45E-01
9.83E-02
2.30E-01
5.39E-02
3.17E-02
3.00E-02
2.04E-02
1.19E-01
1.87E-02
7.88E-03
2.89E-02
7. 71E-03
2.3
5.6
42.2
8.0
15.2
4.8
94.1
12.7
69.4
51.1
15.9
12.0
21.8
37.2
28.1
4.6
14.5
7.9
25.7
28.8
37.4
50.4
10.5
36.6
82.5
19.6
44.6
Fit
4.38E+00
1.54E+00
5.19E+00
2.78E+00
5.67E+00
1.47E+00
1.01E+00

Sample ID : 1304105-16
Acquisition date

27
23
4
Page :
2
1-MAY-2013 09:44:28
14.81%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.856E+02
Total Activity
3.856E+02
Wtd Mean
Decay Corr
pCi/filter
3.856E+02
Decay Corr
2-Sigma
0.711E+02
18.44
3.856E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.715E+02
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
7.715E+02
7.715E+02
7.715E+02
1.157E+03
1.157E+03
Keyline not found

Manually edited
Decay Corr
2-Sigma
1.338E+02
17.34
"M" "' Manually accepted


Sample IP : 1304105-16
Acquisition date
Page :
3
1-MAY-2013 09:44:28

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.856E+02 18.44
1.899E+01 3.856E+02
6.222E+00 3.263E+02
3.264B+02 31.65
4.190E+02 16.42
5.860E+00 4.189E+02
3 Valid Peaks =
3.856E+02+/- 7.112E+01
Status
OK
OK
OK
18.44%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
''*" = Keyline

%Bff
2.648E+01 7.715E+02
7.715E+02 17.34
1 Valid Peaks=
Status
OK
7.715E+02+/- 1.338E+02 ( 17.34%)

Sample ID : 1304105-16
Acquisition date
Page :
4
1-MAY-2013 09:44:28

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.856E+02
7.715E+02
Act error
7.112E+01
1.338E+02
MDA
(pCi/filter)
1.958E+01
1.340E+02
MDA error
Act/MDA
2.995E+00
7.200E+00
19.691
5.756
MDA error
Act/MDA
1.099E+00
1.480E+01
4.514E-02
4.110E-02
4.376E+00
9.174E-01
-0.279
0.071
0.432
1. 290
-0.535
1.468
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-2.681E+00
1.266E+01
1.372E+00
3.729E+00
-2.899E+01
2.740E+01
Act error
5.808E+00
1.247E+02
1.675E+OO
1.538E+00
4.253E+01
9.981E+00
MDA
(pCi/filter)
9.620E+00
1.795E+02
3.173E+00
2.890E+00
5.413E+01
1.866E+01
c....__
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
(lift?
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130410517 - GE3_BAFIL_ 191158.CN

I-9 DIS
1-MAY-2013 00:00:00.
1304105-17
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30.73
34.98
53.43
61.68
65.54
80.82
83.68
111.47
161.76
193.05
276.77
302.90
307.47
311.59
333.79
337.62
341.05
356.13
364.50
383.72
386.99
391.38
415.05
418.34
437.05
467.78
509.11
512.15
1994
459
28
247
100
761
23
245
44
25
62
156
37
13
74
32
12
501
11
110
209
52
29
22
109
28
6
11
85
82
153
105
114
78
48
115
88
90
47
21
17
14
8
7
6
17
17
10
13
14
18
12
5
2
5
7
3
3
0
1
1
1
1
0
0
0
0
2
2
2
2
2
2
0
0
2
2
2
2
2
0
0
4
4
1-MAY-2013 10:23:05.20
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 44
1.58
1.66
1.51
1. 52
1. 54
1. 41
1.44
1.70
3.21
1.48
1. 56
1.99
1.99
2.01
2.02
2.02
1.90
1.47
2.06
1.83
2.06
2.08
2.09
1. 91
2.01
2.37
2.61
31.05
35.30
53.75
62.00
65.86
81.14
84.00
111.78
162.07
193.37
277.08
303.21
307.78
311.89
334.10
337.93
341.35
356.44
364.80
384.02
387.29
391.68
415.35
418.64
437.35
468.08
509.41
512.45
Left
Pw
26
26
50
58
58
77
77
108
158
188
273
299
299
299
330
330
330
353
362
381
381
381
411
411
432
463
506
506
13
13
7
12
12
10
10
7
9
9
9
19
19
19
15
15
15
9
6
17
17
17
15
15
10
8
11
11
1-MAY-2013 10:07:45.
1.00000E+00 filter
0
BAFIL
0 00:15:03.64 0.4%
4096
10.00000
Cts/Sec %Err
2.22E+00
5.10E-01
3.14E-02
2.74E-01
1.11E-01
8.45E-01
2.51E-02
2. 72E-01
4.89E-02
2.77E-02
6.84E-02
1.73E-01
4.07E-02
1.48E-02
8.24E-02
3.53E-02
1.34E-02
5.56E-01
1.19E-02
1.22E-01
2.32E-01
5.74E-02
3.22E-02
2.41E-02
1.21E-01
3.07E-02
6. 71E-03
1. 22E- 02
2.3
5.7
74.9
9.2
18.5
4.1
87.9
9.7
41.3
72.1
23.9
8.9
25.5
60.5
13.6
27.3
64.4
4.7
67.6
11.5
7.9
18.7
29.7
40.5
10.3
21.1
81.5
52.3
Fit
7.94E+00
6.94E+00
1.18E+01
1. 96E+00
1.07E+00
4.68E+00
1.98E+00
1.07E+00

Sample ID : 1304105-17
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
3.646E+02
1. 00
Total Activity
:
14.29%
FISSION
Hlife
10.50Y
Nuclide Type
28
24
4
Page :
2
1-MAY-2013 10:07:45
---------
3.646E+02
Wtd Mean
Decay Corr
pCi/filter
3.647E+02
---------
Decay Corr
2-Sigma
0.650E+02
17.82
3.647E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.366E+02
Total Activity
---------
Wtd Mean
Decay Corr
pCi/filter
7.366E+02
---------
7.366E+02
7.366E+02
1.101E+03
1.101E+03
Flags: "K" = Keyline not found

"M"
"A"
=
=
Decay Corr
2-Sigma
1.447E+02
19.65
Manually accepted
iil511

Sample ID : 1304105-17
Acquisition date
Page :
3
1-MAY-2013 10:07:45

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.647E+02 17.82
1.899E+01 3.646E+02
4.222E+02 27.27
6.222E+00 4.221E+02
5.860E+00 4.275E+02
4.275E+02 16.62
3 Valid Peaks =
Status
OK
OK
OK
3.647E+02+/- 6.497E+01 ( 17.82%)

Nuclide
TH-234
Energy
63.29
3.80*
Final Mean for

2.648E+01 7.366E+02
7.366E+02 19.65
%Eff
%Abn
Valid Peaks=
Status
OK
7.366E+02+/- 1.447E+02 ( 19.65%)
Flag: ''*" = Keyline
U1512
Page :

Sample ID : 1304105-17
Acquisition date
1-MAY-2013 10:07:45

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.647E+02
7.366E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.497E+01
1.447E+02
2.298E+01
1.544E+02
3.515E+00
8.295E+00
15.868
4.769
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
1.233E+00
1.570E+01
3.765E-02
4.027E-02
4.579E+00
1.009E+00
-0.168
-0.230
0.220
1.058
0.221
1. 477
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-1.815E+00
-4.389E+01
5.828E-01
2.995E+00
1.250E+01
3.031E+01
6.411E+00
1.236E+02
1.412E+00
1.548E+00
3.400E+01
1.124E+01
1.079E+01
1.905E+02
2.647E+00
2.832E+00
5.664E+01
2.052E+01
1QS13
<LVAX/VMS Peak Search Report Generated

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
J7ft/7

D-93 TOT
1-MAY-2013 00:00:00.
1304105-18
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
21.09
29.66
31.06
35.15
36.11
39.45
53.40
62.03
66.00
66.68
67.41
79.73
81.19
92.75
111.78
112.41
115.95
116.47
143.13
151.21
276.33
276. 96
302.60
303.32
333.74
356.19
383.78
384.19
386.95
3 91. 08
392.02
94
23
1880
356
104
10
43
225
118
21
15
48
732
14
134
88
28
27
5
14
35
37
93
70
49
376
81
12
114
35
12
24
62
49
40
30
8
35
43
11
8
10
23
20
9
34
16
10
12
8
11
11
5
11
3
0
8
2
2
18
5
0
0
4
4
5
5
0
0
0
6
6
6
3
3
0
1
1
1
1
0
0
1
1
1
1
0
0
1
1
0
6
6
1-MAY-2013 10:23:41.24
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
1-MAY-2013 10:08:21.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:01.12 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
207.76
290.00
303.38
342.71
351.86
383.90
517.84
600.56
638.69
645.26
652.22
770.40
784.48
895.38
1078.00
1084.00
1118.00
1123.00
1378.80
1456.34
2657.00
2663.00
2909.00
2916.00
3207.90
3423.31
3688.00
3692.00
3718.44
3758.08
3767.06
197
281
281
333
333
373
502
588
629
629
629
759
759
884
1069
1069
1105
1105
1368
1440
2643
2643
2898
2898
3192
3407
3676
3676
3704
3746
3746
18
38
38
28
28
16
23
34
28
28
28
35
35
18
22
22
32
32
12
22
28
28
25
25
26
29
25
25
27
24
24
1.05E-01 15.7
2.51E-02 74.6
2.09E+00 2.5
3.95E-01 7.1
1.16E-01 21.3
1.11E-02 70.7
4.75E-02 33.9
2.50E-01 9.9
1. 32E-01 11.2
2.33E-02 43.5
1. 67E- 02 39.5
5.33E-02 34.1
8.14E-01 3.9
1.56E-02 50.5
1.49E-01 13.2
9.83E-02 17.9
3.13E-02 36.4
3.00E-02 38.4
5.56E-03107.7
1.53E-02 54.0
3.87E-02 28.4
4.08E-02 22.1
1.04E-01 12.2
7.81E-02 13.3
5.44E-02 14.3
4.18E-01 5.4
9. 04E-02 10.7
1.31E-02 73.9
1.27E-01 11.8
3.93E-02 20.3
1.34E-02 24.5
0.81
0.54
0.77
0.72
0.69
1.33
0.36
0.91
0.95
0.35
0.62
0.92
0.70
1.22
0.77
0.77
0.77
0.77
0.48
0.10
1.03
1.03
1. 06
1. 06
1. 30
0.88
1.16
1.16
0.78
1. 28
0.62
Fit
1.17E+00
1.89E+00
1.45E+00
1.33E+00
4.43E+00
7.86E-01
1.10E+00
6.51E+00
4.16E-01
7. 96E-01

Sample IP : 1304105-18
Acquisition date

Number of lines tentatively identified by NIP
Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.697E+02
---------
Total Activity
:
3.697E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
2.030E+02
---------
Total Activity
HEll
=
=
Wtd Mean
Decay Corr
pCi/filter
3.697E+02
---------
Decay Corr
2-Sigma
17.14
0.634E+02
3.697E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: nK"
19.35%
FISSION
Hlife
10.50Y
Nuclide Type
31
25
6
Page :
2
1-MAY-2013 10:08:21
Wtd Mean
Decay Corr
pCi/filter
2.030E+02
---------
2.030E+02
2.030E+02
5.726E+02
5.727E+02
Key line not found

Manually edited
2-Sigma
Decay Corr
0.410E+02
20.20
liM II = Manually accepted
"A"
lll515

Sample ID : 1304105-18
Acquisition date
Page :
3
1-MAY-2013 10:08:21

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.697E+02 17.14
1.802E+01 3.697E+02
2.575E+00 6.124E+02
6.125E+02 35.89
4.370E+02 18.02
4.312E+00 4.369E+02
3 Valid Peaks
Status
OK
OK
OK
3.697E+02+/- 6.337E+01 ( 17.14%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
8.750E+Ol 2.030E+02
2.030E+02 20.20
1 Valid Peaks
Status
OK
2.030E+02+/- 4.100E+01 ( 20.20%)
Keyline
S51E

Sample ID : 1304105-18
----
Acquisition date
Page :
4
l-MAY-2013 10:08:21
Identified Nuclides
Nuclide
BA-133
TH-234
Act error
Activity
(pCi/filter)
3.697E+02
2.030E+02
6.337E+01
4.100E+01
MDA
(pCi/filter)
1.381E+01
2.626E+01
MDA error
Act/MDA
2.033E+00
3.379E-01
26.771
7.729
MDA error
Act/MDA
9.123E+00
1.424E+01
1.727E-02
2.283E-02
4.037E+00
2.970E-02
0.136
-0.279
-0.027
2.150
0.083
0. 458
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
3.663E+00
-4.130E+01
-4.152E-02
4.361E+00
3.819E+00
1.210E+00
Act error
1.402E+01
8.630E+01
8.336E-01
1.382E+00
2.428E+01
1.523E+00
MDA
(pCi/filter)
2.691E+01
1.479E+02
1.534E+00
2.028E+00
4.577E+01
2.638E+00
~5:1"7

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP 130410519 - GE5 - BAFIL- 19116l.CN

D-93 DIS
1-MAY-2013 00:00:00.
1304105-19
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
21.23
31.04
35.40
49.32
53.38
56.28
61.45
62.28
66.20
79.73
81.20
112.02
194.28
276.02
276.65
302.80
303.43
307.15
333.75
356.19
383.36
383.99
387.08
82
2131
539
10
48
24
115
135
128
42
838
226
6
13
45
123
11
30
60
399
12
102
143
46
78
49
9
11
0
0
0
0
0
0
1
1
0
1
1
0
0
1
1
1
1
0
0
0
1
1
0
1-MAY-2013 10:41:01.45
11
5
6
39
12
12
23
10
5
5
3
0
6
6
3
3
8
26
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
1-MAY-2013 10:25:44.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:01.17 0.1%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
0.74
0.67
0.64
0.79
0.62
0.18
0.65
0.65
0.67
0.76
0.69
0.69
0.19
1.03
1. 03
1.06
1.06
0.56
0.37
0.98
1.16
1.16
0.71
198
292
331
469
509
537
588
588
626
761
761
1071
1857
2645
2645
2898
2898
2938
3191
3406
3673
3673
3703
20
25
30
15
16
16
25
25
29
33
33
24
16
24
24
26
26
25
28
31
30
30
28
9.07E-02 23.8
2.37E+00 2.4
5.99E-Ol 5.8
1.08E-02 80.8
5.29E-02 21.7
2.70E-02 32.7
1. 28E- 01 13.0
1.50E-Ol 12.1
1. 43E- 01 14.7
4.72E-02 24.0
9.31E-01 3.5
2.51E-Ol 8.4
6.42E-03103.8
1.39E-02 58.1
5.02E-02 17.3
1.37E-Ol 9.3
1.20E-02 87.1
3.32E-02 24.8
6. 71E-02 15.0
4.43E-Ol 5.1
1.31E-02 77.1
1.13E-01 10.1
1.59E-Ol 10.8
209.12
303.24
345.03
478.60
517.57
545.41
595.00
603.00
640.64
770.42
784.59
1080.31
1869.67
2654.00
2660.00
2911.00
2917.00
2952.74
3207.92
3423.32
3684.00
3690.00
3719.67
Fit
3.31E+00
7.66E-Ol
6.47E-Ol
2.38E+00
2.65E+00

Sample ID : 1304105-19
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.230E+02
--------Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 1.222E+02
1.00 9.606E+00
Total Activity
= Keyline
=
4.230E+02
Wtd Mean
Decay Corr
pCi/filter
4.231E+02
---------
Decay Corr
2-Sigma
0.712E+02
16.83
4.231E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
AM-241
432.20Y
Flags: "K"
"E"
26.09%
FISSION
Hlife
10.50Y
Nuclide Type
23
17
6
Page :
2
1-MAY-2013 10:25:44
---------
Wtd Mean
J;Jecay Corr
pCi/filter
1.222E+02
9.606E+00
---------
1.318E+02
1.318E+02
5.548E+02
5.548E+02
not found
Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
0.299E+02
24.48
2.522E+00
26.25
Manually accepted

Sample ID : 1304105-19
Acquisition date
Page :
3
1-MAY-2013 10:25:44

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.802E+01 4.230E+02
4.231E+02 16.83
2.575E+00 8.076E+02
8.076E+02 32.33
4.312E+00 4.626E+02
4.627E+02 17.69
3 Valid Peaks
Status
OK
OK
OK
4.231E+02+/- 7.118E+01 ( 16. 83%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
Flag: "*"
Key line
1 Valid Peaks
35.90*
Final Mean for

8.750E+01 1.222E+02
1.222E+02 24.48
%Eff
1.000E+02
1 Valid Peaks
1.222E+02+/- 2.991E+01 ( 24.48%)
9.606E+00
=
Status
OK
9.606E+00
26.25
OK
9.606E+00+/- 2.522E+OO ( 26.25%)

Sample ID : 1304105-19
Acquisition date
Page :
4
1-MAY-2013 10:25:44

Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filter)
Act error
4.231E+02
1.222E+02
9.606E+00
7.118E+01
2.991E+01
2.522E+00
MDA
(pCi/filter)
1.016E+01
2.651E+01
1.812E+OO
MDA error
Act/MDA
1.497E+00
3.410E-01
2.039E-02
41.622
4.608
5.302
MDA error
Act/MDA
8.985E+00
1.699E+01
1.964E-02
2.288E-02
4.549E+00
0.064
0.236
0.375
1.859
0.202
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/filter)Ided
1.702E+00
4.169E+01
6.541E-01
3.778E+00
1.041E+01
Act error
1.405E+01
9.022E+01
8.472E-01
1.806E+00
2.699E+01
MDA
(pCi/filter)
2.650E+01
1.766E+02
1.745E+00
2.032E+00
5.157E+01

Engineering Management Support, Inc.: West Lake OU-1

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ENGINEERING MANAGEMENT SUPPORT, INC.

West Lake OU-1

EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

Chain of Custody & pH Check Sheet

Analytical Results Summary

Quality Control Sample Results Summary

Laboratory Technician's Notes

Analytical Data (Isotopic Uranium)

Analytical Data (Isotopic Thorium)

Analytical Data (Radium-226)

Analytical Data (Radium-228)

Barium-133 Analytical Tracer Data

Last Page Number

STANDARD OPERATING PROCEDURE

Eberline Services- Oak Ridge Laboratory

Eberline Services Work Order # _ _

Client in Possession of Data

Technical/Clerical Corrections, Signatures Needed, Problems, Etc

Date package approved by:

Chain of Custody Record

Send Report To:~J

Sampler (Print Name):"]~ \:) ~,'1\J

P3-- ~cG- '55

Rec8ivad by: (Signature)

Total # Containers Received?

Sample Custodian Remarks (Completed By Laboratory):

'f.o 'fJ i\) Xl

(lo be comp~..d!;; lab)

X, f!( )() :() )<l

Ook Aklgo, TN 37830

Sampler (Print Name):

CCC Seals Present?

COC Seals Intact?

Received Containers Intact?

Oak Ridge Laboratory

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Prilied: 4/16/2013 11:22AM

Oak Ridge Laboratory

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Oak Ridge Laboratory

Location (circle one)

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Printed: 4/16/2013 11:22AM

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Printed: 4/16!2013 11:22AM

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