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  • RAW Materials: Jean Louis HEITZ, CRITT Matériaux Alsace

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    Hardik
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    This document discusses various types of glass defects that can occur during production, including: 1) Contamination from cullet or raw materials such as metals, porcelain, lead oxide, and redox contaminants. 2) Batching errors or poor homogeneity that can lead to unmelted silica or cords. 3) Contamination during melting from refractory wear, volatilization, or devitrification. 4) Contamination during forming, handling, annealing or from the atmosphere. The document outlines analyzing samples using microscopy techniques to identify defects and their causes to improve glass production quality.

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    Defauts_matiere

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    This document discusses various types of glass defects that can occur during production, including: 1) Contamination from cullet or raw materials such as metals, porcelain, lead oxide, and redox contaminants. 2) Batching errors or poor homogeneity that can lead to unmelted silica or cords. 3) Contamination during melting from refractory wear, volatilization, or devitrification. 4) Contamination during forming, handling, annealing or from the atmosphere. The document outlines analyzing samples using microscopy techniques to identify defects and their causes to improve glass production quality.

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    15 просмотров1 страница

    RAW Materials: Jean Louis HEITZ, CRITT Matériaux Alsace

    Загружено:

    Hardik
    This document discusses various types of glass defects that can occur during production, including: 1) Contamination from cullet or raw materials such as metals, porcelain, lead oxide, and redox contaminants. 2) Batching errors or poor homogeneity that can lead to unmelted silica or cords. 3) Contamination during melting from refractory wear, volatilization, or devitrification. 4) Contamination during forming, handling, annealing or from the atmosphere. The document outlines analyzing samples using microscopy techniques to identify defects and their causes to improve glass production quality.

    Авторское право:

    © All Rights Reserved
    Скачайте в формате PDF, TXT или читайте онлайн в Scribd
    Отметить как неприемлемый контент
    из 1

    Glass Defects

    Jean Louis HEITZ, CRITT Matriaux Alsace

    PRIMARY CONTAMINATION
    Cullet : metals, porcelain, vitroceramics

    CONTAMINATION FROM raw material produ tio!


    Lead oxide : corundum, sillimanite, metal lead

    Andalousite

    RAW MATERIALS

    Silicon ball from metallic aluminum

    orcelain

    !itroceramic

    Sand, dolomite : heavy minerals

    Miscellaneous : redox contaminants Ni -> NiS

    deli"er# media corundum, sillimanite, $%oat&' ar&(


    chromite

    "&romite

    "orundum (rub#)

    $ickel sulfide

    %educed lead balls (lead cr#stal glass)

    raw material& &tora)e i! t*e )la&& pla!t

    corundum, SiC, iron oxides


    "orundum (sap&ir)

    BATCHING ERROR
    Unmelted silica, Cords

    POOR BATCH HOMOGENEITY


    Cords

    CONTAMINATION FROM BATCHING


    Metals, Conveyor belt

    BATCHING
    REFRACTORY WEAR Fu&ed a&t' &i!tered' &ili a' ele trode&' re/ra tor# metal&
    Cat scratches !itreous #nots

    F,RNACE MANAGEMENT Temperature' pull.out


    Silica batch stones !olatili"ation

    Top +iew ( ,M) Section (SEM) t&e core of t&e Al / -r enric&ed cords is 23 4m under t&e surface

    A-S superstructure wit& secondar# )irconia (sodalime glass)

    A-S glass contact in a dead water )one wit& secondar# wadeite (lead cr#stal glass)

    (nmelted silica

    MELTING

    Devitri ication stones

    !olatili)ation cords (lead cr#stal glass)

    rimar# A-S stones (lead cr#stal glass, sodalime glass, SEM)

    rimar# silica from superstructure (sodalime glass, ,M, SEM)

    rimar# tin oxide 1 secondar# potassium tin silicates (lead cr#stal glass - ,M, SEM)

    "eramic fibres (sodalime glass, ,M, SEM)

    'iopside b - wollastonite (sodalime glass)

    Silica * air surface de+itrification (borosilicate glass)

    CONTAMINATION FROM CONTACT WITH TOOLS

    CON+ENSATE +RIPPING

    PROCE+,RE
    $% Collection o data and samples in collaboration &ith 'lass&or# production sta (% Sample in-situ examination usin' )LM *polari"in' li'ht microscope+

    FORMING

    Black speck (press-blow sodalime glass, SEM )

    Tin oxide condensates .ron oxide flake stuck (float glass) on t&e inner side of +essel /0 re+ealed b# acid polis&ing (lead cr#stal glass)

    'efect sorting b# categories %epresentati+e defects selection for SEM anal#sis

    ,% S-M.-D/*.0D/+ analysis o selected samples

    ATMOSPHERE CONTAMINATION
    Annealing bloom 7ricti+e damage on top of knurl * smeared metal and crecsent crack

    HAN+LING

    5ptional anal#ses * 6%', 6%7, T57-S.MS, ." , etc8

    2% Synthesis

    "omparison wit& proprietar# database 'efect reference samples 'ismantled furnace reference samples

    ANNEALING

    1% Discussion o results &ith 'lass&or# production sta

    www0 ritt0/r

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