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[ChemSep] Version=6.93 Compiled=2012-9-15 12:36 c6354e7df245 Name=C:\Users\luis\Desktop\CoCo\flash_exemplo1.

sep Title= User=luis Date=2012-12-10 Time=18:56:41 [Paths] Device drivers path=c:\program files\chemsepl6v93\bin\ Help and Info path=c:\program files\chemsepl6v93\help\ Component data path=c:\program files\chemsepl6v93\pcd\ Property data path=c:\program files\chemsepl6v93\ipd\ Section data path=c:\program files\chemsepl6v93\ild\ Executables path=c:\program files\chemsepl6v93\bin\ Temporary path=C:\Users\luis\AppData\Local\Temp\ Scripts path=c:\program files\chemsepl6v93\bin\ [Units] Temperature=K Flow=kmol/s Mass flow=kg/s Pressure=MPa Heat=J/s Enthalpy=J/kmol Entropy=J/kmol/K Fraction=_ Length=m 1/Length=1/m Area=m2 Volume=m3 Mass=kg Angle=rad Velocity=m/s Surface tension=N/m Density=kg/m3 Molar density=kmol/m3 Viscosity=N/m2.s Molecular weight=kg/kmol Heat capacity=J/kmol/K Thermal conductivity=J/s/m/K Diffusivity=m2/s Interaction parameter=J/mol Time=s [Components] 2 21 905 Library Offset, Index DT=2012-09-10,22:16:54 CHK=4132 CAS=7727-37-9 CID=N itrogen Name=Nitrogen Lib=c:\program files\chemsepl6v93\pcd\chemsep1.pcd 31 1 Library Offset, Index DT=2012-09-10,22:16:54 CHK=41697 CAS=74-82-8 CID=Meth ane Name=Methane Lib=c:\program files\chemsepl6v93\pcd\chemsep1.pcd [Operation] 1 Operation Flash * Operation kind *

* Condenser * * Reboiler * 1 Stages 1 Feed stages 0 Sidestream stages F=1 S= 0 Pumparound stages P= [Properties] 350 BIP estimation temperature [Thermodynamics] 2 K model EOS * * Activity coefficient * * Wilson model * * UNIQUAC model * 3 Equation of State Cubic 8 Cubic EOS Peng-Robinson 78 * Virial EOS * * Vapour pressure * 0 Henry's law * Henry's default * [Enthalpy] 9 Enthalpy Peng-Robinson 78 1 Enthalpy reference state Vapour 298.15 Enthalpy reference temperature 1 Formation enthalpies Excluded 298.15 Exergy surroundings temperature [Physical property models] 0 No Check T range * Cubic EOS * * Virial EOS * * Vapour model * * Liquid mixture density * * Liquid component density * * Vapour mixture viscosity * * Vapour mixture viscosity pressure correction * * Vapour component viscosity * * Liquid mixture viscosity * * Liquid component viscosity * Vapour mixture Cp * Vapour component Cp * Liquid mixture Cp * Liquid component Cp * Vapour mixture conductivity * * Vapour component conductivity * * Liquid mixture conductivity * * Liquid component conductivity * Mixture surface tension * * Component surface tension * * Vignes MS D-model * * D mixture model * * Vapour Diffusion Coefficients * 12 Default Liquid Diffusion Coefficients * [Property Data]

[Peng-Robinson 78 Data] i j kij Component Component [Reaction data] 0 Number of reactions [Specifications] Top Bottom [Feeds] 1 Number 1 Feed state T & p 1 Stage Feed1{split-below} 100 Temperature 411900 Pressure * Vapour fraction 2 componentflows 0.5 Component 1 flow 0.5 Component 2 flow [Flash] 5 Flash type Temperature & vapour flow * Pressure 100 Temperature 0 Vapour flow * Liquid flow * Heat duty Q flash [Solve options] 1 Initialization Automatic 1 Method Newton's method 0.5 Flow Step limit 10 Temperature Step limit 1 Composition Step limit 1 Flux Step limit 0.000001 Accuracy 30 Maximum iterations 1 Iteration count & function vector 0 T/V/L profiles 0 X/Y profiles 0 Variable and function vectors 0 Jacobian 1 History Screen History file= 1 Feeds type Stage below 1 Interactive 0 Log thermodynamics 0 Log enthalpy/entropy 0 Log physical properties 0 Log timing 0 CO numeric differencing 0 Log from iteration 0 CS K-value 0 CS enthalpy 0 CS entropy 0 CS flash 0 CS activity coefficient 0 CS vapor pressuure

0 0 0 0 0 0 0

CS density CS viscosity CS thermal conductivity CS heat capacity CS surface tension CS diffusivity Trace treshold

[Programs] Temporary file=SCRATCH.TMP User program= 1 Compiler Gfortran 1 Show windows Hidden [FlowSheet] <?xml version="1.0" encoding="UTF-8" standalone="no"?> <!DOCTYPE svg PUBLIC "-//W3C//DTD SVG 1.0//EN" "http://www.w3.org/TR/2001/PR-SVG -20010719/DTD/svg10.dtd"> <svg xmlns:svg="http://www.w3.org/2000/svg" xmlns="http://www.w3.org/2000/svg" version="1.0" x="0.0" y="0.0" width="1.0" height="1.0"> <penwidth>1</penwidth> <move2 x=0 y=0 /> <rect x1=0 y1=0 x2=1 y2=1 /> <move2 x=0.35 y=0.3 /> <line2 x=0.35 y=0.7 /> <penstyle>Dot</penstyle> <move2 x=0.35 y=0.7 /> <line2 x=0.55 y=0.7 /> <penstyle>Solid</penstyle> <move2 x=0.55 y=0.7 /> <line2 x=0.55 y=0.3 /> <penstyle>Dot</penstyle> <move2 x=0.55 y=0.3 /> <line2 x=0.35 y=0.3 /> <penstyle>Solid</penstyle> <string x=0.438679 y=0.724528 s="1" /> <arc x1=0.35 y1=0.75 x2=0.55 y2=0.65 x3=0.55 y3=0.7 x4=0.35 y4=0.7 /> <string x=0.438679 y=0.324528 s="1" /> <arc x1=0.35 y1=0.35 x2=0.55 y2=0.25 x3=0.35 y3=0.3 x4=0.55 y4=0.3 /> <move2 x=0.45 y=0.75 /> <line2 x=0.45 y=0.825 /> <move2 x=0.45 y=0.825 /> <line2 x=0.9 y=0.825 /> <line2 x=0.88 y=0.835 /> <line2 x=0.88 y=0.815 /> <line2 x=0.9 y=0.825 /> <string x=0.828302 y=0.894057 s="Top" /> <move2 x=0.45 y=0.25 /> <line2 x=0.45 y=0.175 /> <move2 x=0.45 y=0.175 /> <line2 x=0.9 y=0.175 /> <line2 x=0.88 y=0.185 /> <line2 x=0.88 y=0.165 /> <line2 x=0.9 y=0.175 />

<string x=0.775472 y=0.244057 s="Bottom" /> <move2 x=0.1 y=0.3 /> <line2 x=0.35 y=0.3 /> <line2 x=0.33 y=0.31 /> <line2 x=0.33 y=0.29 /> <line2 x=0.35 y=0.3 /> <string x=0.37 y=0.349057 s="1" /> <string x=0.1 y=0.349057 s="Feed1" /> </svg> [CoCo] <icon chk="29631"> # Coco flash icon generated by ChemSep # Flash WIDTH 7 HEIGHT 10 XGROW 3 YGROW 5 BODY 0 0 6 10 -1 2 LINE THINLINE 7 6 3 6 LINE THINLINE 3 6 5 7 LINE THINLINE 5 7 3 8 LINE THINLINE 3 8 7 8 CONNECTION 3 0 CONNECTION 3 10 VCONNECTION 0 2 8 VCONNECTION 6 2 5 LINE THINLINE WAVE 0.5 5 5.5 5 0.3 2 FREESPACE 7 2 7 5 CONNECTION 7 6 CONNECTION 7 8 </icon> [Settings] <Graphs> ComboBox=ComboBox14 -1 ComboBox=ComboBox20 -1 ComboBox=ComboBox21 -1 CheckBox=CheckBox3 0 Show settings CheckBox=CheckBox1 1 Auto colors CheckBox=CheckBox2 1 Auto points Edit=Edit9 0.2 StringGrid=StringGrid5 2 8 Title Labels Stages Axis color Commands Box Labels box Import data

Parametric Study On Vertical Black On Off StringGrid=StringGrid4 5 9 Title Start End Tic interval Small tics Grid Logarithmic Scientific notation x1 Flash pressure (MPa) 2.242078E-44 2.522337E-44 5.0E-46 0 Off Off Off y1 Feed1 temperature (K) 95 105 2 0 Off Off Off x2

0 Off Off Off y2

0 Off Off Off StringGrid=StringGrid3 2 14

Label Plot X Plot Y X axis Y axis Units X Units Y Color Points Thickness Style 1st stage Last stage 1 Feed1 temperature (K) PS1 PS2 x1 y1 MPa K Red + Normal Solid 1 10 </Graphs> <Parametrix> Edit=Edit1 10 CheckBox=CheckBox2 0 Use old results CheckBox=CheckBox3 1 Automatic CheckBox=CheckBox1 0 Keep sep-files CheckBox=CheckBox4 1 Restore original StringGrid=StringGrid1 2 6 Name Variable Units Value Start/Valuelist End Feed1 temperature (K) F1T K 100 100 200 StringGrid=StringGrid2 4 3 Name Flash pressure (MPa) Feed1 temperature (K)

Variable FP F1T Units MPa K Current Value 2.369428E-44 100 StringGrid=StringGrid3 12 3 Step Flash pressure (MPa) Feed1 temperature (K) Units MPa K 1 2.369428E-44 100 2 2.369428E-44 111.1111 3 2.369428E-44 122.2222 4 2.369428E-44 133.3333 5 2.369428E-44 144.4444 6 2.369428E-44 155.5556 7 2.369428E-44 166.6667 8 2.369428E-44 177.7778 9 2.369428E-44 188.8889 10 2.369428E-44 200 </Parametrix> <BinaryPhaseDiagram> ComboBox=ComboBox1 -1 ComboBox=ComboBox2 -1 ComboBox=ComboBox3 -1 Edit=Edit1 Edit=Edit2 21

Edit=Edit3 Title ComboBox=ComboBox4 0 ComboBox=ComboBox15 0 Edit=Edit17 Plot font CheckBox=CheckBox2 1 Color=Edit18 1628830 SpinEdit=SpinEdit1 1 CheckBox=CheckBox2 1 Color=Edit19 1628830 Edit=Edit5 StringGrid=StringGrid2 7 2

StringGrid=StringGrid3 7 2

StringGrid=StringGrid4 7 2

Color=BVLEbplineColor 1628830 SpinEdit=SpinEdit2 1 ComboBox=ComboBox13 0 Color=BVLEdplineColor 1628830 SpinEdit=SpinEdit3 1 ComboBox=ComboBox14 0 RadioButton=RadioButton3 TRUE DrawSetColors=BVLEcolors 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 ComboBox=ComboBox7 -1 ComboBox=ComboBox11 -1 ComboBox=ComboBox6 -1 Memo=Memo1 Memo1, </BinaryPhaseDiagram> <TernaryPhaseDiagram> ComboBox=ComboBox1 -1 ComboBox=ComboBox2 -1

ComboBox=ComboBox2 -1 ComboBox=ComboBox4 0 Edit=Edit1 Edit=Edit2 21 Edit=Edit3 Ternary Phase Diagram Edit=Edit5 </TernaryPhaseDiagram> <BinaryPropertyDiagram> 0 0 ComboBox=ComboBox1 -1 ComboBox=ComboBox2 -1 ComboBox=ComboBox3 -1 Edit=Edit1 Edit=Edit2 Edit=Edit3 21 Edit=Edit4 Binary Property Diagram Memo=Memo1 StringGrid=StringGrid1 13 4 Axis Left Right X/Y Property -click to select-click to selectx Title x Units Minimum 0 Maximum 1 Interval

0.2 Grid Off Off Off Log Off Off Off Color Blue Red Black Line Normal Normal Style Solid Solid Point None None Edit=Edit5 ComboBox=ComboBox7 -1 ComboBox=ComboBox6 -1 </BinaryPropertyDiagram> [End Settings] [End of Input] [Results] 1 Converged 4 Iterations [Feed stream 1] 0 Stage Number 1.0000000000000E+00 Flow rate 1.0000000000000E+02 Temperature [K] 4.1190000000000E+05 Pressure [Pa] -1.2709496176595E+07 Enthalpy [J/kmol] -1.4358970891185E+05 Entropy [J/kmol/K] 4.8377992507193E-02 Vapour fraction [-] 1.0000000000000E+00 Liquid phase split ratio [-] 5.0000000000000E-01 Mole fraction of component 5.0000000000000E-01 Mole fraction of component 4.8377992507193E-02 Flow rate 9.4273049777191E-01 Mole fraction of component 5.7269502228094E-02 Mole fraction of component 9.5162200749281E-01 Flow rate 4.7749273079513E-01 Mole fraction of component 5.2250726920487E-01 Mole fraction of component

1 2 1 2 1 2

2.7328426689342E+01 1.4966898742291E+01 6.7027656538179E-06 1.0401976184134E-02 2.9457270022040E+04 2.1759065068509E+01 5.8540342879813E+02 9.6610549031942E-05 1.5585107706915E-01 6.2194522682804E+04 1.0029647325163E-02 [Top product]

Molar mass Density Viscosity Thermal conductivity Heat capacity Molar mass Density Viscosity Thermal conductivity Heat capacity Surface tension

0 Stage Number 0.0000000000000E+00 Flow rate 1.0000000000000E+02 Temperature [K] 4.2695816634371E+05 Pressure [Pa] -6.0294788808100E+06 Enthalpy [J/kmol] -4.3616045547718E+04 Entropy [J/kmol/K] 1.0000000000000E+00 Vapour fraction [-] 1.0000000000000E+00 Liquid phase split ratio [-] 9.4623100301252E-01 Mole fraction of component 5.3768996987484E-02 Mole fraction of component 0.0000000000000E+00 Flow rate 9.4623100301252E-01 Mole fraction of component 5.3768996987484E-02 Mole fraction of component 2.7370331239928E+01 Molar mass 1.5597507324301E+01 Density 6.7130386312977E-06 Viscosity 1.0421510874457E-02 Thermal conductivity 2.9443136522247E+04 Heat capacity * Surface tension [Bottom product] 0 Stage Number 1.0000000000000E+00 Flow rate 1.0000000000000E+02 Temperature [K] 4.2695816634371E+05 Pressure [Pa] -1.2949565140433E+07 Enthalpy [J/kmol] -1.0003350697117E+05 Entropy [J/kmol/K] 0.0000000000000E+00 Vapour fraction [-] 1.0000000000000E+00 Liquid phase split ratio [-] 5.0000000000000E-01 Mole fraction of component 5.0000000000000E-01 Mole fraction of component 1.0000000000000E+00 Flow rate 5.0000000000000E-01 Mole fraction of component 5.0000000000000E-01 Mole fraction of component 2.2028499603271E+01 Molar mass 5.9155523365345E+02 Density 9.5033872811385E-05 Viscosity 1.5333391113994E-01 Thermal conductivity 6.2243335332735E+04 Heat capacity 9.7723054707443E-03 Surface tension [Flash Heat Duty] -2.400689638E+05 [K-values]

1 2 1 2

1 2 1 2

Component

K-values:

1 1.892462006E+00 2 1.075379940E-01 [End of Results] [ChemSep Output] ChemSep (TM) - COL2 6.93 Copyright (c) 1988-2012 Harry Kooijman and Ross Taylor License: 2100- 6 LITE free license Build: de6d96a18fa1 Checking data file C:\Users\luis\Desktop\CoCo\FLASH_~1.SEP Reading configuration Reading component property libraries Reading thermodynamic property options Reading physical property options Reading thermodynamic property data Reading specifications Checking Component Data 7727-37-9 Nitrogen 74-82-8 Methane Determining feed conditions Solving TP flash Reading flash specifications Solving TV flash Iteration P 1 4.1180E+05 2 4.2641E+05 3 4.2696E+05 4 4.2696E+05 Convergence obtained Time 16 milliseconds FixMem driver done [End ChemSep Output] Error 4.5122 3.0532 0.1646 -5.5004

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