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This document outlines the course plan for a chemistry laboratory course. It includes 12 experiments that cover topics like acid-base titrations, qualitative organic analysis, determination of dissociation constants, and chromatography. Evaluation of each experiment will be based on a lab report, written exam, and viva voce exam. Relevant textbooks and websites are also listed to support the course material. Key experiments include determining water hardness using EDTA, identifying elements in a compound, and estimating nickel concentration using dimethyl glyoxime.
This document outlines the course plan for a chemistry laboratory course. It includes 12 experiments that cover topics like acid-base titrations, qualitative organic analysis, determination of dissociation constants, and chromatography. Evaluation of each experiment will be based on a lab report, written exam, and viva voce exam. Relevant textbooks and websites are also listed to support the course material. Key experiments include determining water hardness using EDTA, identifying elements in a compound, and estimating nickel concentration using dimethyl glyoxime.
This document outlines the course plan for a chemistry laboratory course. It includes 12 experiments that cover topics like acid-base titrations, qualitative organic analysis, determination of dissociation constants, and chromatography. Evaluation of each experiment will be based on a lab report, written exam, and viva voce exam. Relevant textbooks and websites are also listed to support the course material. Key experiments include determining water hardness using EDTA, identifying elements in a compound, and estimating nickel concentration using dimethyl glyoxime.
Course No Cours Title Course Planner Lectures Tutorial Practical Credits
CHE102 CHEMISTRY LABORATORY 13608 :: Gurpinder Singh 0 0 2 1 Sr. No. (Web adress) (only if relevant to the courses) Salient Features 6 www.chemguide.co.uk/physical/acidbaseeqia/indicators.html Acid base titrations 7 http://ull.chemistry.uakron.edu/analytical/Titrimetry/ Complete information about Titrimetry 8 http://en.wikipedia.org/wiki/Chromatography Chromatography Sr No Jouranls atricles as compulsary readings (specific articles, Complete reference) 5 Pavia, D. L.; Lampman, G. M.; Kriz, G. S.; Engel, R. G. Introduction to OrganicLaboratory Techniques: A Microscale Approach, 3rd ed.; Saunders College Publishing; New York, 1999, pp 338. J. Mendham, R. C. Denney, J. D. Barnes, and R. C. Denney, Vogel's Quantitative Chemical Analysis, 6th Edition, Prentice Hall, 2000. 1 Text Book: Other Specific Book: J. B. Yadav, Advance Practical chemistry, Krishna Publications, Merrut 12th Revised Edition 2 Basset J Denny. R. C., Jeffery C. H. and Mendham J., Vogel's Textbook of Quantitative Inorganic analysis, ELBS, 1978. (Inorganic) 3 N.K.Vishnoi Advanced Practical Organic Chemistry ,Vikas Publications,New Delhi, 2nd edition 4 Relevant Websites Other Reading *Each experiment of the lab will be evaluated using following relative scheme: Format For Instruction Plan [for Courses with Labs 1 Approved for Autumn Session 2011-12 Component % of Marks J/E 20 WR 50 VIVA 30 List of experiments :- Lecture Number Lecture Topic Pedagogical Tools Or Equipment Planned lab Manual Practical 1 With the help of complexometeric titration how you will determine the hardness of given hard water sample by using EDTA. Provided standard hard water.(1ml of S.H.W.=1mg of CaCO3) Burette, Burette stand, Titration flask, Pipette, Beakers, funnel etc. Not Applicable Practical 2 Identification of elements present in given compound. China dish, water bath, glass rod, glass funnel, filter papers, fusion tube, test tube, beakers etc. Not Applicable Practical 3 Qualitatively analysis of the given organic compound for Carboxylic acids. Water bath, glass rod, glass funnel, filter papers, test tube, beakers etc. Not Applicable Practical 4 Determination of the dissociation constant of acetic acid using pH-meter. pH meter, 100 mL beaker, pH electrode, pipette, burette, funnel etc. Not Applicable Practical 5 Determination of Strength of hydrochloric acid solution (approximately N/10) by titrating it against sodium hydroxide solution conductometrically. Conductivity Bridge, conductivity cell, beaker, funnel, burette and pipette. Not Applicable Practical 6 To test the validity of Beer-Lamberts law using colorimeter and to determine unknown concentration of solution. Colorimeter, test tubes, cuvette, burette, 50 cc measuring flask etc. Not Applicable Mid Term Practical 7 Estimation of nickel in the given sample using dimethyl glyoxime. Beakers, Suction pump, sintered glass crucible, oven, glass rod etc. Not Applicable Practical 8 Determination of the rate constant of hydrolysis in case of ethyl acetate using an alkali. Volumetric flask, 250 mL Beakers, 50 mL Burette, pipette, funnel etc. Not Applicable Practical 9 Determine the strength of given solution of ferrous ammonium sulphate by titrating against potassium dichromate solution. Conical flasks, burette, pipette, Stop watch, water bath etc. Not Applicable Practical 10 Separation of a mixture of organic compounds by thin layer chromatography. Glass plates, beaker, Glass rod etc. Not Applicable Spill Over Practical 11 Not Applicable 2 Approved for Autumn Session 2011-12 Practical 12 Not Applicable 3 Approved for Autumn Session 2011-12