A - Basis and B - Basis

Advanced General
Aviation Transport
Experiments
A Basis and B Basis

Design Allowables
for
Epoxy Based Prepreg
TORAY T700SC-12K-50C/#2510
Plain Weave Fabric
[SI Units]
AGATE-WP3.3-033051-134
October 2002
J. Tomblin, J. Sherraden, W. Seneviratne, K. S. Raju

National Institute for Aviation Research
Wichita State University
Wichita, KS 67260-0093
ii
TABLE OF CONTENTS
1.
INTRODUCTION.........................................................................................1
1.1.
Scope ..............................................................................................2
1.2.
Symbols Used ..................................................................................3
1.3.
Acronyms and Definitions ..................................................................4
1.4.
References.......................................................................................5
1.5.
Methodology.....................................................................................9
1.5.1.
Test Matrix..................................................................................9
1.5.2.
Environmental Conditioning .......................................................11
1.5.3.
Fluid Sensitivity Screening .........................................................11
1.5.4.
Normalization Procedures..........................................................13
1.5.5.
Statistical Analysis ....................................................................14
1.5.6.
Material Performance Envelope and Interpolation........................14
1.5.6.1.
Interpolation Example.............................................................16
2.
TORAY T700SC-12K-50C/#2510 PROCEDURES AND PREPREG
PROPERTIES ...................................................................................................18
2.1.
3.
GENERAL......................................................................................19
2.1.1.
Materials...................................................................................19
2.1.2.
Lay-up/Bagging .........................................................................19
2.1.3.
Cure.........................................................................................20
2.1.4.
Non-Destructive Inspection (NDI) ...............................................20
2.1.5.
Tabbing ....................................................................................23
2.1.6.
FAA Test Coupon Conformity and Test Witness ..........................23
2.1.6.1.
Test Coupon Conformity.........................................................23
2.1.6.2.
Test Witness .........................................................................24
2.2.
Prepreg Documentation by Prepreg Lot............................................25
2.3.
Data Documentation .......................................................................28
TORAY T700SC-12K-50C/#2510 LAMINA PROPERTIES...........................31

3.1.
Test Results ...................................................................................32
iii
3.1.1.
Summary..................................................................................32
3.1.2.
Individual Test Summaries.........................................................33
3.1.2.1.
Tension, 1-axis ......................................................................34
3.1.2.2.
Tension, 2-axis ......................................................................35
3.1.2.3.
Compression, 1-axis ..............................................................36
3.1.2.4.
3.1.2.5.
Shear, 12 axis .......................................................................38
3.1.2.6.
Shear, 13 axis .......................................................................39
3.1.3.
Individual Test Charts................................................................40
3.1.3.1.
Tension, 1-axis ......................................................................41
3.1.3.2.
Tension, 2-axis ......................................................................42
3.1.3.3.
3.1.3.4.
3.1.3.5.
Shear, 12 axis .......................................................................45
3.1.3.6.
Shear, 13 axis .......................................................................46
3.2.
Raw Data .......................................................................................47
3.2.1.
Raw Data Spreadsheets and Scatter Charts ...............................48
3.2.2.
Fluid Sensitivity Raw Data Spreadsheets and Scatter Charts .......95
3.2.3.
Representative Shear Stress-Strain Curve ................................ 100
3.3. Statistical Results ............................................................................. 102

APPENDIX A. PHYSICAL AND MECHANICAL TEST PROCEDURES ............. 113
A.1. Physical Properties .......................................................................... 114
A.1.1. Uncured Resin Content ............................................................... 114
A.1.2. Uncured Volatile Content ............................................................ 114
A.1.3. Resin Gel Time .......................................................................... 114
A.1.4. Resin Flow ................................................................................. 114
A.1.5. Uncured Fiber Areal Weight ........................................................ 114
A.1.6. Infrared Spectroscopy................................................................. 114
A.1.7. High Performance Liquid Chromatography (HPLC) ....................... 115
A.1.8. Differential Scanning Calorimetry (DSC) ...................................... 115
A.1.9. Cured Neat Resin Density........................................................... 115
iv
A.1.10. Fiber Volume ............................................................................ 115

A.1.11. Resin Volume ........................................................................... 115
A.1.12. Void Content ............................................................................ 116
A.1.13. Cured Laminate Tg by DMA ...................................................... 116
A.2. TENSILE PROPERTIES................................................................... 116
A.2.1. 0 (Warp) and 90 (Fill) Tensile Properties ................................... 116
A.2.1.1. Tensile Calculations .............................................................. 117
A.2.1.1.1. Tensile Strength (Un-normalized) ..................................... 117
A.2.1.1.2. Tensile Strength (Normalized) .......................................... 118
A.2.1.1.3. Tensile Modulus of Elasticity (Un-normalized) ................... 118
A.2.1.1.4. Tensile Modulus of Elasticity (Normalized) ........................ 118
A.2.1.1.5. 0 (Warp) Tensile Poissons Ratio .................................... 118
A.3. COMPRESSIVE STRENGTH ........................................................... 119
A.3.1. 0 (Warp) and 90 (Fill) Compressive Strength Properties ............. 119
A.3.1.1. Compressive Strength Calculations ........................................ 120
A.3.1.1.1. Compressive Strength Calculation (Un-normalized) ........... 120
A.3.1.1.2. Compressive Strength Calculation (Normalized) ................ 120
A.4. COMPRESSIVE MODULUS ............................................................. 120
A.4.1. 0 (Warp) and 90 (Fill) Compression Modulus Properties ............. 120
A.4.1.1. Compression Modulus Calculations ........................................ 121
A.4.1.1.1. Compressive Modulus Calculation (Un-normalized) ........... 121
A.4.1.1.2. Compressive Modulus Calculation (Normalized) ................ 122
A.5. IN-PLANE (IOSIPESCU) SHEAR ...................................................... 122
A.5.1. In-plane (Iosipescu) Shear Strength Calculations .......................... 123
A.5.1.1. In-plane (Iosipescu) Shear, Ultimate Strength Calculation........ 123
A.5.1.2. In-plane (Iosipescu) Shear, Modulus Calculation..................... 123
A.6. SHORT BEAM SHEAR..................................................................... 123
A.6.1. Short Beam Shear Strength Calculations ..................................... 124
A.6.1.1. Short Beam Shear Strength Calculation.................................. 124
APPENDIX B. MOISTURE CONDITIONING HISTORY CHARTS...................... 125
APPENDIX C. PHYSICAL TEST RESULTS..................................................... 135
APPENDIX D. STATISTICAL ANALYSIS SUMMARY ...................................... 161
APPENDIX E. METHOD FOR TRANSFORMING VARIANCES OF TEST

SAMPLES (SUPPLEMENT TO DOT/FAA/AR-47/00) ........................................ 172
APPENDIX F. RAW TESTING SUMMARIES ................................................... 178
APPENDIX G. DATES OF PANEL MANUFACTURE AND COPY OF FAA
FORM 8130-3 ................................................................................................. 205
vi
1. INTRODUCTION
This material characterization program was performed to characterize the lamina
properties of Toray Composites (America), T700SC-12K-50C/#2510, 190 g/m2,
plain weave fabric, herein designated F6273C-07M. The F6273C-07M prepreg
material system designation shall be used to refer the material in this report. The
material qualification was conducted under FAA project number TC1616SE-A
through Lancair Company that wanted to use the aforementioned material
prepreg system on their LC40 aircraft.
This report contains the test results obtained from the tests conducted for the
material qualification of F6273C-07M in accordance with FAA Document
DOT/FAA/AR-00/47: Material Qualification and Equivalency for Polymer Matrix
Composite Material Systems and Toray Composites (America), Inc. (TCA)
Material Process Specification, TCSPF-T-FC05, Revision 1 dated February 4,
2000. Toray Composites (America), Inc. (TCA), Integrated Technologies (Intec),
National Institute for Aviation Research (NIAR) and Rose Consulting performed
the testing on the unexposed and exposed prepreg materials for lamina baseline
test properties in accordance with ASTM test methods, SACMA test methods,
and TCA test work instructions.
Three batches of F6273C-07M and the corresponding mixed resins were tested
for baseline test properties. The data reported herein will be used to set material
acceptance criteria for future material production and material receipt. The Raw
Test Data, Inspection Records, Fabrication Records, Processing Records and all
other relevant documents of this report, TCQAL-T-1013, are archived at Toray
Composites (America), Inc., and it is available only upon request.
The physical and chemical tests were performed on the mixed resins, the
uncured prepreg materials and cured prepreg laminates. The mixed resins were
evaluated for cured neat resin density. The uncured prepreg samples were
evaluated for resin content, fiber areal weight, volatile content, gel time, flow, IR
(Infrared Spectroscopy), HPLC (High Performance Liquid Chromatography) and
DSC (Differential Scanning Calorimetry). The cured prepreg laminates were
tested for fiber volume, resin volume, void content, cured ply thickness and Tg
(glass transition temperature) by DMA (Dynamic Mechanical Analyzer).
TCA Test Laboratories performed all the physical and chemical tests on the
mixed resins, the uncured prepreg materials and cured prepreg laminates,
except for fiber volume, resin volume and void content that Intec performed and
cured laminate glass transition temperature, dry and wet conditions, that Rose
Consulting performed.
TCA Test Laboratories performed the fabrication of all the test panels and test
specimens, ultrasonic inspection, chemical and humidity conditioning, except for
0 and 90 Compressive Strength specimens that NIAR tabbed and machined.
Also, the TCA Test Laboratories performed the attachment of strain gauges and
mechanical testing, except for specimens tested at 65 F (Dry) that Intec
performed. Moreover, TCA Test Laboratories performed the fluid sensitivity on
one qualification batch by testing in-plane (iosipescu) shear strength only.
All TCA and Intec test equipments were calibrated with standards traceable to
the NIST.
1.1.
Scope
The test methods and results described in this document are intended to provide
basic composite properties essential to most methods of analysis. These
properties are considered to provide the initial base of the building block
approach. Additional coupon level tests and sub-element tests may be required
to fully substantiate the full-scale design.
The test methods and results contained in this document are consistent with MILHDBK-17-1E,2D,3E - Military Handbook for Polymer Matrix Composites. All
material, specimens, fixtures and test results contained within this document
were traceable and conformed by the Federal Aviation Administration (FAA). It
should be noted that before application of the basis values presented in this
document to design, demonstration of the ability to consistently produce
equivalent material properties as that evaluated during this program should be
substantiated through an acceptable test program.
1.2.
Symbols Used
12tu
E1c
E1t
E2c
E2t
F12su
F13su
F1cu
F1tu
F2cu
F2tu
G12s
major Poissons ratio, tension

micro-strain
compressive modulus, longitudinal
tensile modulus, longitudinal
compressive modulus, transverse
tensile modulus, transverse
in plane shear strength
apparent interlaminar shear strength
compressive strength, longitudinal
tensile strength, longitudinal
compressive strength, transverse
tensile strength, transverse
in plane shear modulus
Superscripts
c
cu
s
su
t
tu
compression
compression ultimate
shear
shear ultimate
tension
tension ultimate
Subscripts
1
2
12
13
1 axis; longitudinal
(parallel to warp direction of reinforcement)
2 axis; transverse
(parallel to fill direction of reinforcement)
in plane shear
interlaminar shear (apparent)
1.3.
Acronyms and Definitions

A Basis
AGATE
ASTM
B Basis
C. V.
CTD
CPT
DMA
Dry
content
ETD
ETW
FAR
FAW
Gr/Ep
NASA
RTD
SACMA
Association
SRM
Tg
tply
wet
95% lower confidence limit on the first population

percentile
Advanced General Aviation Transport Experiments
American Society for Testing and Materials
95% lower confidence limit on the tenth population
percentile
coefficient of variation
cold temperature dry
cured ply thickness
dynamic mechanical analysis
specimen tested with an as fabricated moisture
elevated temperature dry
elevated temperature wet
Federal Aviation Regulations
fiber areal weight
graphite/epoxy
National Aeronautics and Space Administration
room temperature dry
Suppliers of Advanced Composite Materials
SACMA Recommended Method
glass transition temperature
cured ply thickness
specimen tested with an equilibrium moisture content
per section 1.5.2
1.4.
References
ASTM Standards
D 792-91
Standard Test Method for Density and Specific Gravity of

Plastics by Displacement, American Society for Testing and
Materials, Philadelphia, PA 1991.
D2344
Standard Test Method for Apparent Interlaminar Shear

Strength of Parallel Fiber Composites by Short-Beam
Method, American Society for Testing and Materials,
Philadelphia, PA.
D2734
Standard Test Method for Void Content of Reinforced

Plastics, American Society for Testing and Materials,
Philadelphia, PA 1994
D3039
Standard Test Method for Tensile Properties of Polymeric

Matrix Composite Materials," American Society for Testing
and Materials, Philadelphia, PA 1995.
D3171-90
Standard Test Method for Fiber Content of Resin-Matrix

Composites by Matrix Digestion, American Society for
Testing and Materials, Philadelphia, PA 1990
D3530-90
Standard Test Method for Volatiles Content of Epoxy Matrix

Prepreg American Society for Testing and Materials,
Philadelphia, PA 1990
D3531-76
Standard Test Method for Resin Flow of Carbon FiberEpoxy Prepreg, American Society for Testing and
Materials, Philadelphia, PA.
D3532
Standard Test Method for Gel Time of Carbon Fiber-Epoxy

Prepreg, American Society for Testing and Materials,
Philadelphia, PA.
D4065-93
Standard Practice for Determining and Reporting Dynamic

Mechanical Properties of Plastics, American Society for
Testing and Materials, Philadelphia, PA 1993.
D4473
Standard Practice for Determining Cure Behavior of

Thermosetting Resins Using dynamic Mechanical
Procedures, American Society for Testing and Materials,
Philadelphia, PA.
D5379-98
Shear Properties of Composite Materials by the V-Notched

Beam Method, American Society for Testing and Materials,
Philadelphia, PA 1998.
E168
General Techniques of Infrared Quantitative Analysis,

American Society for Testing and Materials, Philadelphia, PA
1992.
E1252
Standard Practice for General Techniques for Qualitative

Infrared Analysis, American Society for Testing and
Materials, Philadelphia, PA 1995.
E1356
Glass Transition Termperature by Differential Scanning

Calorimetry or Differential Thermal Analysis, American
Society for Testing and Materials, Philadelphia, PA 1995.
SACMA Standards
SRM-1R-94 Compressive Properties of Oriented Fiber-Resin
Composites," Suppliers of Advanced Composite Materials
Association, 1994.
SRM-18R-94 Glass Transition Temperature (Tg) Determination by DMA
of Oriented Fiber-Resin Composites," Suppliers of Advanced
Composite Materials Association, 1994.
SRM-19R-94 Viscosity characteristics of Matrix Resins," Suppliers of
Advanced Composite Materials Association, 1994.
SRM-20R-94 High Performance Liquid Chromatography of Thermoset
Resins," Suppliers of Advanced Composite Materials
Association, 1994.
SRM-22R-94 Determining the Resin Flow of Preimpregnated B Staged
Material," Suppliers of Advanced Composite Materials
Association, 1994.
SRM-23R-94 Determination of Resin Content and Fiber Areal Weight of
Thermoset Prepreg with Destructive Technique," Suppliers

of Advanced Composite Materials Association, 1994.
SRM-25R-94 Onset Temperature and Peak Temperature for Composite
System Resins Using Differential Scanning Calorimetry
(DSC)," Suppliers of Advanced Composite Materials
Association, 1994.
Toray Documents
TCSPF-T-FC05
Material Process Specification for Torayca Plain

Weave Carbon Fiber Fabric Preimpregnated with
Epoxy Resin (EP-resin) Prepreg Fabric 250F
Curing System, Revision 1, Toray Composites
(America), Inc., Puyallup, WA, February 4, 2000.
TCWIN-U-C002
Fourier Transform Infrared Analysis," Toray

Composites (America), Inc., Puyallup, WA, 1998.
TCWIN-U-C003
Differential Scanning Calorimetry," Toray Composites

(America), Inc., Puyallup, WA, 1998.
TCWIN-U-C004
High Performance Liquid Chromatography," Toray

TCWIN-U-M003
Lay-up/Vacuum Debulking, Toray Composites

TCWIN-U-M006
Autoclave Curing, Toray Composites

Inc., Puyallup, WA, 1998.
TCWIN-U-M008
Panel Tabbing, Toray Composites (America), Inc.,

Puyallup, WA, 1998.
TCWIN-U-M101
Tensile Specimen Machining," Toray Composites

TCWIN-U-M102
Compression Specimen Machining," Toray

TCWIN-U-M103
Compression Modulus Specimen Machining," Toray

(America),
TCWIN-U-M111
90 Degree Tensile Specimen Machining," Toray

TCWIN-U-M201
Tensile Testing, Toray

Composites (America),
Inc., Puyallup, WA, 1998.
TCWIN-U-M204
Compressive Strength Testing," Toray Composites

TCWIN-U-M206
Compressive Modulus Testing, Toray Composites

TCWIN-U-M214
Strain Gauge Attachment," Toray Composites

TCWIN-U-M215
Laminate Density/Fiber Volume Testing," Toray

TCWIN-U-M216
Strain Gauge Calibration," Toray Composites

TCWIN-U-P001
Volatile Content," Toray Composites (America), Inc.,

Puyallup, WA, 1998.
TCWIN-U-P004
Resin Content/Fiber Areal Weight," Toray

TCWIN-U-P007
Gel Time," Toray Composites America), Inc.,

Puyallup, WA, 1998.
TCWIN-U-P008
Flow," Toray Composites (America), Inc., Puyallup,

WA, 1998
Other Documents
FAA Document DOT/FAA/AR-00/47: Material Qualification and
Equivalency for Polymer Matrix Composite Material Systems, J.S.
Tomblin, Y.C. Ng and K.S. Raju, 2001.
MIL-HDBK-17 1E, 2D, 3E Military Handbook for Polymer Matrix
Composites
1.5.
Methodology
1.5.1. Test Matrix

Testing was performed according to the test methods delineated in the test
matrix, with modifications as referenced in FAA Document DOT/FAA/AR-00/47:
Material Qualification and Equivalency for Polymer Matrix Composite Material
Systems. The test matrix for properties included in this document is listed on the
next page, with the following notation cited in each column:
#x#
where the first # represents the required number of prepreg batches, defined as:
Prepreg containing T700 12K graphite fibers from one mill roll, impregnated with
one batch of resin in one continuous manufacturing operation with traceability to
all components. The second # represents the required number of replicates per
prepreg batch. For example, 3 x 6 refers to three prepreg batches of material
and six specimens per prepreg batch for a total requirement of 18 test
specimens.
Table 1.5.1: Minimum Recommended Test Matrix and Standards Used for
Testing
TEST
0o (warp) Tension Strength
0o (warp) Tension Modulus,
Strength and Poissons Ratio
90o (fill) Tension Strength
90o (fill) Tension Modulus and
Strength
0o (warp) Compression
Strength
0o (warp) Compression
Modulus
90o (fill) Compression Strength
90o (fill) Compression Modulus
In-Plane Shear Strength
In-Plane Shear Modulus and
Strength
Short Beam Shear
Fiber Volume
Resin Volume
Void Content
Cured Neat Resin Density
Glass Transition Temperature
METHOD
ASTM D3039-95
ASTM D3039-95
ASTM D3039-95
ASTM D3039-95
SACMA SRM 1-94
SACMA SRM 1-94
SACMA SRM 1-94
SACMA SRM 1-94
ASTM D5379-93
ASTM D5379-93
ASTM D2344-89
ASTM D3171-90
ASTM D3171-90
ASTM D2734-94
--SACMA SRM 18-94
NO. OF REPLICATES PER

TEST CONDITION
CTD1
1x4
RTD2
3x4
ETW3
3x4
ETD4
3x4
1x2
3x2
3x2
3x2
1x4
3x4
3x4
3x4
1x2
3x2
3x2
3x2
1x6
3x6
3x6
3x6
1x2
3x2
3x2
3x2
1x6
1x2
1x4
3x6
3x2
3x4
3x6
3x2
3x4
3x6
3x2
3x4
1x2
3x2
3x2
3x2
1x6
3x6
3x6
3x6
One sample per panel
Supplied by manufacturer for
material
3 dry, 3 wet per prepreg batch
Notes :
1
2
3
CTD: One prepreg batch of material tested (test temperature = -65 5o F,

moisture content = as fabricated, soak time at 65 was 5 min.)
RTD: Three prepreg batches of material tested (test temperature = 70
10o F, moisture content = as fabricated)
ETW: Three prepreg batches of material tested (test temperature = 180
5o F, moisture content = equilibrium per section 1.5.2, soak time at 180
was 2 min.)
ETD: Three prepreg batches of material tested (test temperature = 180
5o F, moisture content = as fabricated, soak time at 180 was 2 min.)
10
1.5.2. Environmental Conditioning

All wet conditioned samples were exposed to elevated temperature and
humidity conditions to establish moisture saturation of the material. Specimens
were exposed to 85 5 % relative humidity and 145 5 F until an equilibrium
moisture weight gain of traveler, or witness coupons (1 x 1 x specimen
thickness) was achieved. ASTM D5229 and SACMA SRM 11 were used as
guidelines for environmental conditioning and moisture absorption.
Effective moisture equilibrium was achieved when the average moisture content
of the traveler specimen changed by less than 0.05% for two consecutive
readings within a span of 7 0.5 days and was expressed by:
W i - W i - 1 < 0.0005
Wb
where
Wi = weight at current time

Wi-1 = weight at previous time
Wb = baseline weight prior to conditioning
It is common to see small fluctuations in an unfitted plot of the weight gain vs.
time curve. There were no fluctuations that made significant errors in results or
caused rejection in the moisture equilibrium criteria. Once the traveler coupons
passed the criteria for two consecutive readings, the samples were removed from
the environmental chamber and placed in a sealed bag with a moist paper or
cotton towel for a maximum of 14 days until mechanical testing. Strain gauged
specimens were removed from the controlled environment for a maximum of 2
hours for application of gages in ambient laboratory conditions.
1.5.3. Fluid Sensitivity Screening

Although epoxy-based materials historically have not been shown to be sensitive
to fluids other than water or moisture, the influence of some fluids other than
water or moisture on the mechanical properties were characterized. These fluids
fell into two exposure classifications. The first class was considered to be in
contact with the material for an extended period of time, and the second class
was considered to be wiped on and off (or evaporate) with relatively short
exposure times.
To assess the degree of sensitivity of fluids other than water or moisture, Table
1.5.2 shows the fluids which were used in this qualification plan.
11
Table 1.5.2: Fluid Types Used for Sensitivity Studies
Specification
Exposure
Classification
MIL-T-5624
Extended Period
MIL-H-5606G
Extended Period
Laboratory Grade
Extended Period
Fluid Type
Jet Fuel
(JP-4)
Hydraulic Fluid
(Tri-N-butyl phosphate ester)
Solvent
(Methyl Ethyl Ketone)
To assess the influence of various fluids types, a test method sensitive to matrix
degradation was used as an indicator of fluid sensitivity and compared to the
unexposed results at both room temperature dry and elevated temperature dry
conditions. Table 1.5.3 describes the fluid sensitivity-testing matrix with respect
to the fluids defined in Table 1.5.2. Engineering judgment and statistical tests
were used to assess the degree of material degradation. The results of this
screening are included following the data sheets in section 3.2.2.
Table 1.5.3: Material Qualification Program for Fluid Resistance
Fluid Type
Test
Method
Test
Temp.
(o F)
Exposure1
Number of
Replicates2
Jet Fuel JP-4

Hydraulic Fluid
Solvent (MEK)
ASTM D53793
ASTM D53793
ASTM D53793
180
180
Ambient
See note 4
See note 5
See note 5
5
5
5
Notes :
1
2
3
4
5
Soaking in fluid at ambient temperature (immersion).

Only a single batch of material is required.
Shear strength only.
Immersion duration = 500 hours 50 hours
Immersion duration = 60 to 90 minutes
12
1.5.4. Normalization Procedures

The normalization procedure attempts to reduce variability in fiber-dominated
material properties by adjusting raw test values to a specified fiber volume
content. Only the following properties were normalized:
0 (warp) and 90 (fill) Tensile Strength and Modulus

0 (warp) and 90 (fill) Compression Strength and Modulus
The normalization procedure was adopted from MIL-HDBK-17-1E, section

2.4.3.3. The procedure which was used to normalize the data is based on two
primary assumptions:
The relationship between fiber volume fraction and ultimate

laminate strength is linear over the entire range of fiber/resin ratios.
(It neglects the effects of resin starvation at high fiber contents.)
Fiber volume is not commonly measured for each test sample, so

this method accounts for the fiber volume variation between
individual test specimens by utilizing a relationship between fiber
volume fraction and laminate cured ply thickness. This relationship
is virtually linear in the 0.45 to 0.65 fiber volume fraction range.
Additional information is detailed in FAA Document DOT/FAA/AR-00/47: Material

Qualification and Equivalency for Polymer Matrix Composite Material Systems.
For all normalized data contained in this document, the test values are
normalized by cured ply thickness according to:
Normalized Value = Test Value
CPT specimen
CPT normalizing
where:
CPTspecimen =
Average Sample Thickness

# of plies
13
1.5.5. Statistical Analysis

When compared to metallic materials, fiber reinforced composite materials
exhibit a high degree of material property variability. This variability is due to
many factors, including but not limited to: raw material and prepreg manufacture,
material handling, part fabrication techniques, ply stacking sequence,
environmental conditions, and testing techniques. This inherent variability drives
up the cost of composite testing and tends to render smaller data sets than those
produced for metallic materials. This necessitates the usage of statistical
techniques for determining reasonable design allowables for composites.
The analyses and design allowable generation for both A and B basis values
were performed using the procedure detailed in section 5.3 of FAA Document
DOT/FAA/AR-00/47: Material Qualification and Equivalency for Polymer Matrix
Composite Material Systems.
1.5.6. Material Performance Envelope and Interpolation
Using the B-basis numbers, a material performance envelope may be generated
for the material system by plotting these values as a function of temperature.
Figure 1.5.1 shows an example material performance envelope using B-basis
values.
14
120
Actual Basis Value
Estimated Value
B-Basis Strength Values (ksi)
100
RTD
CTD
80
ETD
RTW
60
Material
Performance
Envelope
ETW
40
20
-100
-50
50
100
150
200
Temperature (o F)
Figure 1.5.1 Material performance envelope.
Since each specific aircraft application of the qualified material may have
different Material Operational Limits (MOL) than those tested in the material
qualification (which is usually the upper limit), some applications may require a
reduced MOL. In this case, simple linear interpolation may be used to obtain the
corresponding basis values at the new application MOL.
This interpolation may be accomplished using the following simple relationships
assuming TRTD < TMOL < TETD :
For the corresponding MOL dry basis value, the interpolated basis value using
the qualification data is
B MOL = BRTD
(B RTD B ETD )(TRTD TMOL )

(TRTD TETD )
15
where
BMOL = new application basis value interpolated to TMOL

BRTD = basis RTD strength value
BETD = basis ETD strength value
TRTD = RTD test temperature
TETD = ETD test temperature
TMOL = new application MOL temperature
For the corresponding MOL wet basis value, an estimated Room Temperature
Wet (RTW) value must be calculated. This may be accomplished by the simple
relation
BRTW = BRTD ( BETD BETW )

The interpolated wet basis value using the qualification data may then be
obtained by
BMOL = B RTW
where:
(BRTW BETW )(TRTW TMOL )

(TRTW TETW )
BMOL = new application basis value interpolated to TMOL

BRTW = estimated basis RTW strength value
BETW = basis ETW strength value
TRTW = RTW (i.e., RTD) test temperature
TETW = ETW test temperature
TMOL = new application MOL temperature
These equations may also be used for interpolated mean strengths as well as Abasis values with the appropriate substitutions. It should be noted that because
unforeseen material property drop-offs with respect to temperature and
environment can occur, extrapolation to a higher MOL should not be attempted
without additional testing and verification. In addition, the interpolation equations
shown above are practical for materials obeying typical mechanical behavior. In
most cases, some minimal amount of testing may also be required to verify the
interpolated values.
1.5.6.1.
Interpolation Example
This section provides an example of linear interpolations to a specific application

environment less than the tested upper material limit used in qualification.
16
Assuming a specific application environment of 150o F, Figure 1.5.2 depicts the

linear interpolation of the B-basis design allowable to this environment. Using
the above equations along with the nominal testing temperatures (see Table
1.5.1), the interpolated basis values at 150o F become
ETD
: BMOL = 75.106 ksi
ETW : BMOL = 59.746 ksi

120
Actual Basis Value
Estimated Value
100
CTD
B-Basis Strength Values (ksi)
RTD
80
ETD
RTW
60
ETW
40
20
-100
-50
50
100
150
200
Temperature (o F)
Figure 1.5.2 Example of 150o F interpolation for B-basis values.
17
2. TORAY T700SC-12K-50C/#2510 PROCEDURES AND PREPREG

PROPERTIES
18
2.1. GENERAL
All of the testing described in the report took place at Toray Composites
(America), Inc. in Tacoma, Washington, except for the following tests:
Test Laboratory
Integrated
Technologies
(Intec), Bothell, WA
Rose Consultant,
Half Moon Bay, CA
NIAR
Test Property
acid digestions (fiber volume, resin volume, laminate
density and void content)
-65F (Dry) mechanical tests (0 & 90 Tension, 0 & 90
Comp. Modulus and In-plane Shear)
cured laminate transition glass temperature, Tg
Short Beam Shear (Additional tests)
2.1.1. Materials
The T700SC-12K-50C/#2510, F6273C-07M, Plain Weave Fabric prepreg
batches were manufactured by the hot melt method of resin impregnation.
Toray, Ehime of Japan and Carbon Fibers America (CFA) in Decatur, Alabama
manufactured the carbon fiber. Sakai Composites of Japan performed the
weaving of the plain weave fabric. The resin mixing and impregnation were done
by Toray Composites (America), Inc. at the Frederickson, WA facilities.
This material qualification program characterized the physical, chemical and
mechanical properties of F6273C-07M prepreg material, namely; batches
AF991009, AF991010 and AF991011. The prepreg batches were manufactured
with two lots of plain weave carbon fabric and three batches of resin matrix. The
F6273C-07M batches were manufactured to nominal uncured resin content of 42
% (by weight) and a fiber areal weight (FAW) of 190 grams per square meter.
2.1.2. Lay-up/Bagging
TCA Test Laboratories manufactured all the mechanical test laminates by laying
up plies of the F6273C-07M prepreg material in the desired orientations, and by
vacuum bag cure. Both the ply orientation and vacuum bag assembly for cure
were in accordance with Advanced General Aviation Transport Experiments
(AGATE) Material Qualification Methodology for Epoxy-Based Prepreg
Composite Material System, dated February 1999, TCA Material Process
Specification, TCSPF-T-FC05, Revision 1 dated February 4, 2000, and TCA
work instructions. Figure 2-1 describes the vacuum bag assembly for cure of
19
the test laminates. The test laminates were vacuum debulked in accordance with
TCA work instructions, TCWIN-U-M003.
2.1.3. Cure
The test panels were cured in accordance with TCWIN-Q-M006 and per Figure
2-2. For the specimen selection methodology and batch traceability of each test
property, batch replicates were sampled from at least two different panels
covering at least two independent cycles per Figure 2-3. Test specimens were
selected from each individual test panel. The test specimens were extracted
from panel areas that were good, visually and based on non-destructive
inspection techniques.
2.1.4. Non-Destructive Inspection (NDI)
Laminates fabricated for mechanical testing were non-destructively inspected
using a Sonix/KrautKramer Branson Ultrasonic equipment at 5MHz pulse.
Metal dam*
Vacuum Sealant (one edge only)
(Tack tape)
Vacuum bag
Surface
breather
Pressure plate
1
Solid FEP (optional)
Edge dam
(3 sides tack
tape)
Edge breather
Glass yarn
Solid FEP (optional)
Laminate
Edge breather
Vacuum Sealant
(Tack tape)
Caul
plate
Figure 2-1. Vacuum Bagging Stack Sequence

1
The solid FEP may not be necessary when the caul plate is treated with a release agent, for example, Frekote
release agent.
20
Temp, F
30
250
25
200
20
150
15
100
10
Temperature
50
Vacuum, in Hg
300
Vacuum
0
0
50
100
150
200
0
250
Time, minutes
Notes:
(1) Apply 22 inches Hg minimum vacuum to the vacuum bag assembly and
check for leak before beginning the cure cycle. The leak rate shall be less
than 2.0 inches Hg over 5 minutes.
(2) Apply the temperature ramp from ambient to 270 10 F at a rate of 3.0 1.0
F per minute.
(3) Maintain the cure temperature at 270 10 F for 120 150 minutes.
(4) Cool down the temperature to 170 F or lower at a rate of 4.5 0.5 F per
minute
before removing the vacuum.
(5) Remove the bagged laminates from the autoclave and de-bag for inspection.
FIGURE 2-2. #2510 CURE CYCLE
21
FIGURE 2-3: SPECIMEN SELECTION METHODOLOGY AND BATCH TRACEABILITY

PER ENVIRONMENTAL CONDITION AND TEST METHOD
BATCH 1
Material Batch
LOAD
A
Autoclave Load
(Independent cure Process)
Panel
Manufacturing
BATCH 3
BATCH 2
LOAD
A
LOAD
B
LOAD
A
LOAD
B
LOAD
B
PANEL
A1
PANEL
A2
PANEL
B1
PANEL
B2
PANEL
A1
PANEL
A2
PANEL
B1
PANEL
B2
PANEL
A1
PANEL
A2
PANEL
B1
PANEL
B2
Typical Number of
Specimens (1)
(1) 6 specimens for Tension, Compression Strength, In-plane Shear and Interlaminar Shear
2 specimens for Compression Modulus
22
2.1.5. Tabbing
Tabs were used to ensure the accuracy of the tensile and compressive strength
specimens. Tabs were applied to the tension and compression strength specimens
in accordance with Section 3.1.4 of the AGATE Material Qualification Methodology
for Epoxy-Based Prepreg Composite Material System, dated February 1999, with
the following exceptions;
1.) AF 163-2 film adhesive used to bond the tabs to the test specimens described
below was further cured by placing the test specimens in a temperature chamber at
180 F for 24 hours. This was because the AF163 was not fully cured, initially, at
180F for 5 hours. The 180F cure temperature was selected because it was the
maximum temperature allowed by the AGATE methodology, described in section
3.1.4, since the cure temperature of the P707AG-15 was 270 10F
a.) 0 (warp) & 90 (fill) tension specimens for testing at -65F (Dry), 75F
(Dry), 180F (Dry) and 180F (Wet).
2.) Hysol EA9628 film adhesive used to bond the tabs to the specimens described
below was cured up to 260 F for up to 120 minutes.
a.) 0 (warp) & 90 (fill) compressive strength tested -65F (Dry), 75F (Dry),
180F (Dry) and 180F (Wet).
The same material or strain compatible material tabs as the test coupon were used
for compressive strength specimens. Fiberglass tabs were used for tension
specimens. To retard the absorption of moisture into the tabs and bond lines of the
tension specimens tested at hot/wet condition, the tab section (including the edges)
were masked with a room-temperature curing Plasti Dip rubber coating prior to
humidity conditioning. The rubber coat was peeled off just before testing. The
National Institute for Aviation Research (NIAR) of Wichita State University bonded
the tabs and machined the 0 (warp) & 90 (fill) compressive strength specimens.
2.1.6. FAA Test Coupon Conformity and Test Witness
The material traceability and test specimen conformity were performed for the cured
laminate mechanical test properties of the program. For the physical properties,
material traceability was verified by TCA inspection section only.
2.1.6.1.
Test Coupon Conformity
A conformity traveler accompanied each group of test specimens for cured lamina
mechanical properties. The conformity traveler recorded the materials and process
definition, completion and verification by inspection of each process, that included
lay-up, cure cycle, tabbing and final coupon dimensions. Mr. Wing C. Chin, FAA
Designated Airworthiness Representative (DAR) performed the test specimen
conformity and reviewed the completeness of traveler conformity records. Finally,
Mr. Wing C. Chin, FAA DAR prepared a statement of conformity, FAA 8130-3 tags
23
for all the test panels and test specimens, prior to environmental conditioning and
testing of the test specimens. The conformity of all the test panels was performed
November 15, 1999. However, additional test panels, specifically for compressive
strength test, were fabricated and conformed on March 24, 2000 due to problems in
the testing process, for example, tabbing and machining of specimens. The
conformed additional test panels, for compressive strength test, were replacements
for previously fabricated test panels. The conformity of all the test specimens was
performed December 13, 1999. However, the additional compressive strength
specimens were conformed April 14, 2000 and April 21, 2000, to replace the test
specimen with out-of-mode failure, for example, tab failure due to adhesive failure
and end broom failure.
2.1.6.2.
Test Witness
Mr. Moto Ashizawa, FAA Designated Engineering Representative (DER) witnessed

all the cured lamina mechanical test property testing of at least one batch of the
prepreg material for the program. TCA personnel that were authorized to witness on
behalf of Mr. Moto Ashizawa, FAA DER witnessed the rest of the tests. The test
dates of the lamina mechanical test properties were described in the tables of test
results.
24
2.2. Prepreg Documentation by Prepreg Lot
Prepreg Batch or Lot #

Batch (Lot) ID as labeled on samples
Prepreg Manufacturer & Product ID: Toray Composites F6273C-07M

Material Identification (weave, form, class, etc.): Carbon/Epoxy Plain Weave Fabric
Impregnation Method: Hot Melt
AF991009
AF991010
AF991011
910-056
910-057
910-058
Date of Manufacture
Expiration Date
Resin Content [%]
Reinforcement Areal Weight
& Test Method
Resin Flow
& Test Conditions
Gel Time
& Test Conditions
Volatile Content
10/20/1999
10/20/2001
41.5%
194 g/m2
SACMA SRM 23R-94
23.5%
@ 250F
8.0 minutes
@ 250F
0.13%
Reinforcement Documentation
Fiber Manufacturer & Product ID: Toray T700S-12K-50C

Fabric Manufacturer & Product ID: Sakai CK6273C
Precursor Type: PAN
Nominal Filament Count: 12K
Finish/Sizing Type and %: 50C (1.0%)
Nominal tow or yarn count/inch: 3.05/inch
Twist: Never twisted
138043
138051
04/1998
05/1998
Warp 1.78 g/cc
Warp 1.78 g/cc
Fill 1.80 g/cc
Fill 1.78 g/cc
TY-030B-02
TY-030B-02
Prepreg Documentation
Fabric Batch or Lot #

Date of Manufacture
Average Fiber Density per Lot
& Test Method
10/20/1999
10/20/2001
41.7%
190 g/m2
SACMA SRM 23R-94
23.5%
@ 250F
7.9 minutes
@ 250F
0.21%
10/20/1999
10/20/2001
41.4%
193 g/m2
SACMA SRM 23R-94
23.5%
@ 250F
9.0 minutes
@ 250F
0.18%
138051
05/1998
Warp 1.78 g/cc
Fill 1.78 g/cc
TY-030B-02
Matrix Documentation
Resin Manufacturer & Product ID: Toray Composites #2510
Matrix Batch or Lot #
3-CCH
3-CCG
2-BFC
Date of Manufacture
Average Neat Resin Density by Lot
& Test Method
10/01/1999
1.267
ASTM D792
10/01/1999
1.267
ASTM D792
10/04/1999
1.266
ASTM D792
25
Prepreg Documentation
Prepreg Batch or Lot #
Batch (Lot) ID as labeled on samples
Prepreg Manufacturer & Product ID: Toray Composites F6273C-07M

Material Identification (weave, form, class, etc.): Carbon/Epoxy Plain Weave Fabric
Impregnation Method: Hot Melt
AF020224
AF020324
AF020422
AF020522
A-49, B-50
A-51, B-52
A-53, B-54
A-55, B-56
Date of Manufacture
Expiration Date
Resin Content [%]
Reinforcement Areal Weight
& Test Method
Resin Flow
& Test Conditions
Gel Time
& Test Conditions
Volatile Content
02/21/2002
02/21/2004
40.8%
193 g/m2
SACMA SRM 23R-94
-
03/18/2002
03/18/2004
41.6%
191 g/m2
SACMA SRM 23R-94
-
04/19/2002
04/19/2002
41.3%
191 g/m2
SACMA SRM 23R-94
-
05/01/2002
05/01/2004
41.0%
193 g/m2
SACMA SRM 23R-94
-
9.6 minutes
@ 250F
0.06%
12 minutes
@ 250F
0.19%
10 minutes
@ 250F
0.16%
13 minutes
@ 250F
0.23%
Reinforcement
Documentation
Fiber Manufacturer & Product ID: Toray T700S-12K-50C

Fabric Manufacturer & Product ID: Sakai CK6273C
Precursor Type: PAN
Nominal Filament Count: 12K
Finish/Sizing Type and %: 50C (1.0%)
Nominal tow or yarn count/inch: 3.05/inch
Twist: Never twisted
131121
132021
121031
12/2001
02/2002
03/2001
Warp 1.80g/cc
Warp 1.80g/cc
Warp 1.80g/cc
Fill 1.80 g/cc
Fill 1.80 g/cc
Fill 1.80 g/cc
TY-030B-02
TY-030B-02
TY-030B-02
Fiber Batch or Lot #

Date of Manufacture
Average Fiber Density per Lot
& Test Method
Matrix Documentation
Matrix Batch or Lot #
Date of Manufacture
Average Neat Resin Density by Lot

& Test Method
Resin Manufacturer & Product ID: Toray Composites #2510

2-CMP, 2-CNK, 22-COQ, 2-CPF
2-CQW, 2-CQX
COP
12/29/2001,
02/20/2002,
04/14/2002,
01/19/2002,
03/05/2002
04/15/2002
02/19/2002
-
26
121041
04/2001
Warp 1.80g/cc
Fill 1.80 g/cc
TY-030B-02
2-CRB, 2-CQY
04/17/2002,
04/15/2002
-
Notes: (1)Test methods to determine resin content, reinforcement areal weight, resin flow, gel time, and volatile
content are defined in TORAY Material Specifications (see reference section). (2) These information and test results
were submitted to NIAR by TORAY Composites (AMERICA), Inc.
27
2.3. Data Documentation

MATERIAL IDENTIFICATION
R material identification
R material class
PREPREG ANALYSIS
R ply manufacturer
R date of manufacture
R material lot number
R
R
R
R
commercial designation
material form
reinforcement areal weight
reinforcement areal weight test method
resin content
REINFORCEMENT ANALYSIS
F
precursor type
R
R
manufacturer
R
date of manufacture (fabric)
R
date of manufacture (fiber)
R
lot number (fabric)
R
lot number (fiber)
R
R
R
R
R
R
R
surface treatment (Y/N)

surface finish (sizing) identification
density (Average per lot)
density test method
nominal filament count
nominal tow or yarn count/inch
twist
fiber areal weight (when applicable)
fiber areal weight test method
MATRIX MATERIAL ANALYSIS

R
R
manufacturer
R
date of manufacture
R
lot number (R not prepregged,
F prepregged)
R
nominal density and test method
PROCESSING INFORMATION
F
part (panel) manufacturer
R
date of manufacture (date completed)
cure cycle (for each state)
R
process stage type
R
process time
R
process temperature
R
process pressure
R
other critical control parameters
T700SC-12K-50C/#2510 Plain Weave Fabric

Carbon/Epoxy
Toray Composites (America), Inc
10/1999, 02/2002, 03/2002, 04/2002, 05/2002
AF991009, AF991010, AF991011, AF020224,
AF020324, AF020422, AF020522
F6273C-07M
Plain Weave Fabric Prepreg
185 201 g/m2
Solvent Extraction
39 45 %
PAN
T700SC-12K-50C
Torayca
05/1998, 07/1998, 03/2001, 04/2001, 12/2001, 02/2002
01/1998, 03/1998, 11/2000, 12/2000, 03/2001, 06/2001
138043, 138051, 131121, 132021, 121031, 121041
818012, 818013, 818014, 818033, 811062, 811032,
810112, 810113, 810124
Y
50C
1.78 g/cm3
JIS R 7601
12000/tow
3.0
No Twist
185 201 g/m2
SRM 23
#2510
10/1999, 12/2001, 01/2002, 02/2002, 03/2002, 04/2002
3-CCH, 3-CCG, 2-BFC, 2-CMP, 2-CNK, 2-COP, 2-COQ,
2-CPF, 2-CQW, 2-CQX, 2-CRB, 2-CQY
1.267 g/cc
ASTM D792
original QT: 10/1999 3/2000
additional QT: 05/2002
Cure Cycle
120 +10/-0 minutes
270 3 F
none
minimum 22 inHg vacuum
28
LAMINA ANALYSIS
R
form (panel, tube, etc.)
R
ply count
R
R
F
R
R
R
Panel
12 warp & fill tensile; 12 warp & fill Comp
strength; 14 warp & fill comp modulus;
16 IPS; 12 ILSS
lay-up code
(warp) 12 warp tensile; (fill) 12 fill tensile;
(warp) 12 warp comp strength; (fill) 12 fill comp
strength; (warp) 14 warp comp modulus; (fill) 14
fill comp modulus; (warp/fill) 4S IPS;
(warp) 12 ILSS
fiber volume
49.6% Average
void content
2.3% Average
density
1.501g/cc Average
glass transition temperature (wet, nominal) 267F
glass transition temperature (dry, nominal) 294F
glass transition temperature test method
DMA E
SPECIMEN PREPARATION
R
specimen orientation
fill, warp, fill/warp
F
tab adhesive curing temperature (nominal) up to 260F
MECHANICAL TESTING
R
number of specimens
R
test procedure
(citing all deviations from standard
procedures including reporting
requirements)
R
date of applicable standard
R
date of testing
R
specimen thickness for each specimen
R
R
R
R
R
specimen conditioning method

conditioning temperature
conditioning humidity
conditioning time
conditioning environment (if not lab air)
R
R
R
F
R
R
R
R
fastener type (if any)

fastener torque-up conditions (if any)
test temperature
moisture content
soak time at test conditions
failure mode identification and location
all non-normalized (raw) data
method of calculating modulus
nominal ply thickness
nominal fiber density
nominal fiber areal weight
See data files

ASTM D 3039 (Tensile),
SACMA SRM 1 (Comp),
ASTM D 5379 (IPS),
ASTM D 2344 (ILSS)
1995(Ten), 1994(Comp), 1993(IPS), 1989(ILSS)
original QT: 12/1999 7/2000
additional QT: 05/2002 06/2002
nominal: 0.1032(warp & fill tensile),
0.1032(warp & fill comp strength),
0.1204 (warp & fill comp modulus),
0.1376 (IPS), 0.1032 (ILSS)
DOT/FAA/AR-00/47 Section 3.2, Sept. 2000
145 5F
85 5%
until saturation (10 to 16 weeks)
for fluid sensitivity: Jet Fuel, Hydraulic Fluid &
MEK (IPS only)
N/A
N/A
-65 5F, 75 5F, 180 5F
Dry : 0.2 - 0.5 % Wet : 1.4 - 2.0%
-65F: 5 6 minutes 180F: 2 3 minutes
Per specimen
Per specimen
1000 3000 microstrain (Tens)
1000 3000 microstrain (Comp)
2500 6500 microstrain (IPS)
0.0086 in.
1.78 g/cm3
193 g/m2
29
R Required for all data

F Required for fully-approved data
These requirements are current for MIL-HDBK-17-1E, which supercedes for any discrepancies.
30
3. TORAY T700SC-12K-50C/#2510 LAMINA PROPERTIES
31
3.1.
Test Results
3.1.1. Summary
MATERIAL:
T700SC-12K-50C/#2510 Plain Weave Fabric
PREPREG:
Toray Composites F6273C-07M
FIBER:
Toray T700S-12K-50C
Tg (dry): 146 C
PROCESSING:
T700 PW/#2510
Summary
T g (wet): 131 C
RESIN:
Toray Composites #2510
Tg METHOD:
DMA (SRM 18-94)
Vacuum bag cure (minimum 560 mmHg): 132 2 C for 120 +10/-0 minutes
Date of fiber manufacture
01/1998 02/2002
Date of testing
12/1999 06/2002
Date of resin manufacture
10/1999 - 04/2002
Date of data submittal
04/2002 07/2002
Date of prepreg manufacture
10/1999 - 05/2002
Date of analysis
07/2002 09/2002
Date of composite manufacture
10/1999 05/2002
LAMINA MECHANICAL PROPERTY SUMMARY

Data Reported as: Measured
(Normalized by CPT= 0.2184 mm)
CTD
RTD
ETD
ETW
B-Basis
Mean
B-Basis
Mean
B-Basis
Mean
B-Basis
Mean
F1tu
(MPa)
738.480
(737.897)
802.874
(803.236)
853.790
(847.726)
917.599
(912.052)
901.601
(896.912)
968.984
(964.970)
978.797
(975.143)
1051.949
(1049.137)
E1 t
(GPa)
---
0.057
(0.057)
---
0.056
(0.056)
---
0.056
(0.056)
---
0.058
(0.058)
---
0.085
---
0.042
---
0.037
---
0.029
12tu
F2tu
(MPa)
614.325
(616.820)
718.773
(722.602)
677.690
(673.994)
775.382
(771.977)
733.095
(727.913)
838.774
(833.734)
780.537
(779.024)
893.055
(892.276)
E2 t
(GPa)
---
0.056
(0.056)
---
0.055
(0.055)
---
0.054
(0.055)
---
0.054
(0.054)
F1cu
(MPa)
621.925
(621.623)
747.203
(749.955)
605.822
(603.589)
708.869
(708.742)
571.291
(565.607)
668.465
(664.143)
404.168
(404.402)
472.915
(474.854)
E1 c
(GPa)
---
0.055
(0.055)
---
0.055
(0.056)
---
0.056
(0.056)
---
0.055
(0.055)
F2cu
(MPa)
654.992
(653.537)
744.535
(741.866)
629.671
(626.087)
702.974
(698.158)
581.719
(579.039)
649.439
(645.694)
529.870
(429.285)
479.913
(478.702)
E2 c
(GPa)
---
0.049
(0.048)
---
0.053
(0.054)
---
0.053
(0.053)
---
0.055
(0.055)
144.345
154.888
124.746
132.570
99.938
106.206
70.168
74.569
---
0.004
---
0.004
---
0.004
---
0.003
---
---
55.317
59.935
---
---
---
---
F12su
G12s
F13su**
(MPa)
(GPa)
(MPa)
** Apparent interlaminar shear strength
32
3.1.2. Individual Test Summaries
33
3.1.2.1.
Tension, 1-axis
Tension, 1-axis
Material:
Toray - TCA T700S-12K-50C/#2510 Plain Weave Fabric
Gr/Ep
Resin content:
39 - 45 wt%
Comp. density:
1.48 - 1.52 g/cc
Fiber volume:
47 - 55 %
Void content:
1.0 - 3.0 %
Ply thickness:
0.2113 - 0.2229 mm
Ply range:
12 plies
Test method:
D3039-95
Normalized by:
0.2184 mm ply thickness
Weave Fabric
[0] 12
linear fit from 1000 - 3000
Modulus calculation:
Test Temperature [C]
CTD
RTD
ETD
ETW
-53.89
23.89
82.22
82.22
Moisture Conditioning
Equilibrium at T, RH
TCA T700S-12K-50C/#2510 Plain
dry
dry
dry
equilibrium
as fabricated
as fabricated
as fabricated
62.78 C, 85%
Source code
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
Mean
803.236
802.874
912.052
917.599
964.970
968.984
1049.137
1051.949
Minimum
756.865
752.490
846.883
842.606
864.643
880.860
1003.433
1002.461
Maximum
848.175
843.194
994.092
998.737
1014.012
1015.816
1109.689
1106.526
4.672
4.720
4.394
4.596
4.567
4.241
3.046
2.938
C.V.(%)
tu
F1
B-value
737.897
738.480
847.726
853.790
896.912
901.601
975.143
978.797
(MPa)
A-value
701.302
702.415
805.025
811.431
851.733
856.870
926.023
930.236
E1
No. Specimens
18
18
No. Prepreg Lots
18
3
Mean
0.057
0.057
0.056
0.056
0.056
0.056
0.058
0.058
Minimum
0.055
0.055
0.054
0.054
0.053
0.053
0.053
0.054
Maximum
0.059
0.060
0.061
0.062
0.063
0.063
0.063
0.063
C.V.(%)
3.298
3.514
3.265
3.553
4.481
4.463
4.606
4.288
(GPa)
No. Specimens
12
12
No. Prepreg Lots
Mean
12
0.085
0.042
12
3
0.037
0.029
No. Specimens
12
12
12
No. Prepreg Lots
34
3.1.2.2.
Tension, 2-axis
Tension, 2-axis
Material:
Gr/Ep
Resin content:
39 - 45 wt%
Comp. density:
1.49 - 1.52 g/cc
Fiber volume:
47 - 54 %
Void content:
1.3 - 3.7 %
Ply thickness:
0.2131 - 0.2210 mm
Ply range:
12 plies
Test method:
D3039-95
Normalized by:
Weave Fabric
[0] 12
CTD
RTD
ETD
ETW
-53.89
23.89
82.22
82.22
dry
dry
dry
equilibrium
as fabricated
as fabricated
as fabricated
62.78 C, 85%
Source code
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
Mean
722.602
718.773
771.977
775.382
833.734
838.774
892.276
893.055
Minimum
696.157
688.155
688.601
687.602
722.975
728.125
752.772
759.543
Maximum
746.775
742.458
852.207
858.027
943.274
942.857
1008.063
1004.365
C.V.(%)
2.788
2.725
7.359
7.512
7.895
7.792
7.883
7.677
F2
B-value
616.820
614.325
673.994
677.690
727.913
733.095
779.024
780.537
(MPa)
A-value
557.575
555.826
608.950
612.839
657.665
662.941
703.844
705.844
tu
E2
No. Specimens
18
18
No. Prepreg Lots
18
3
Mean
0.056
0.056
0.055
0.055
0.054
0.055
0.054
0.054
Minimum
0.056
0.055
0.054
0.053
0.052
0.052
0.051
0.052
Maximum
0.057
0.057
0.056
0.056
0.056
0.057
0.058
0.057
C.V.(%)
1.471
1.536
1.419
1.581
2.207
2.256
2.941
2.502
(GPa)
No. Specimens
12
12
12
No. Prepreg Lots
35
3.1.2.3.
Compression, 1-axis
Compression, 1-axis
Material:
Gr/Ep
Resin content:
39 - 45 wt%
Comp. density:
1.49 - 1.51 g/cc
Fiber volume:
46 - 54 %
Void content:
1.1 - 3.1 %
Ply thickness:
0.2132 - 0.2216 mm
Ply range:
12 - 14 plies
Test method:
SRM 1-94
Normalized by:
Weave Fabric
[0]12, [0] 14
CTD
RTD
ETD
ETW
-53.89
23.89
82.22
82.22
dry
dry
dry
equilibrium
as fabricated
as fabricated
as fabricated
62.78 C, 85%
Source code
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
Mean
749.955
747.203
708.742
708.869
664.143
668.465
474.854
472.915
Minimum
704.469
701.885
589.686
593.713
573.899
580.651
396.111
394.658
Maximum
848.082
844.971
780.970
782.660
765.078
774.079
539.716
531.983
C.V.(%)
6.862
6.862
8.151
7.966
8.753
8.759
9.502
9.126
F 1cu
B-value
621.623
621.925
603.589
605.822
565.607
571.291
404.402
404.168
(MPa)
A-value
549.748
551.760
533.785
537.415
500.195
506.784
357.633
358.531
No. Specimens
No. Prepreg Lots
E1c
(GPa)
6
1
18
3
18
3
18
3
Mean
0.055
0.055
0.055
0.056
0.056
0.056
0.055
0.055
Minimum
0.054
0.054
0.051
0.052
0.054
0.054
0.051
0.051
Maximum
0.055
0.055
0.057
0.058
0.061
0.062
0.062
0.063
C.V.(%)
1.527
1.527
3.391
3.932
4.715
5.436
7.418
7.863
No. Specimens
No. Prepreg Lots
2
1
6
3
6
3
36
6
3
3.1.2.4.
Compression, 2-axis
Compression, 2-axis
Material:
Gr/Ep
Resin content:
39 - 45 wt%
Comp. density:
1.48 - 1.51 g/cc
Fiber volume:
47 - 51 %
Void content:
1.3 - 3.1 %
Ply thickness:
0.2159 - 0.2251 mm
Ply range:
12 - 14 plies
Test method:
SRM 1-94
Normalized by:
Weave Fabric
[0]12, [0] 14
CTD
RTD
ETD
ETW
-53.89
23.89
82.22
82.22
dry
dry
dry
equilibrium
as fabricated
as fabricated
as fabricated
62.78 C, 85%
Source code
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
Mean
741.866
744.535
698.158
702.974
645.694
649.439
478.702
479.913
Minimum
634.596
636.880
640.837
638.979
555.232
556.310
433.678
435.238
Maximum
828.187
831.167
765.583
774.590
703.056
707.857
519.773
523.323
C.V.(%)
9.888
9.888
5.168
5.261
6.108
6.175
5.185
5.249
F2
B-value
653.537
654.992
626.087
629.671
579.039
581.719
429.285
429.870
(MPa)
A-value
604.067
604.841
578.243
581.010
534.790
536.764
396.481
396.650
cu
E2c
No. Specimens
18
18
No. Prepreg Lots
18
3
Mean
0.049
0.048
0.053
0.054
0.053
0.053
0.055
0.055
Minimum
0.048
0.048
0.051
0.051
0.051
0.052
0.049
0.049
Maximum
0.049
0.049
0.056
0.057
0.056
0.056
0.058
0.059
C.V.(%)
1.260
2.192
3.831
3.915
2.845
2.984
5.588
5.798
(MPa)
No. Specimens
No. Prepreg Lots
37
3.1.2.5.
Shear, 12 axis
Shear, 12-axis
Material:
Gr/Ep
Resin content:
39 - 45 wt%
Comp. density:
1.48 - 1.51 g/cc
Fiber volume:
47 - 51 %
Void content:
1.7 - 2.9 %
Ply thickness:
0.2142 - .2214 mm
Ply range:
16 plies
Test method:
D5379-93
Normalized by:
N/A
Weave Fabric
[0/90]4s
CTD
RTD
ETD
ETW
-53.89
23.89
82.22
82.22
dry
dry
dry
equilibrium
as fabricated
as fabricated
as fabricated
62.78 C, 85%
Source code
Normalized
F12
su
(MPa)
G12s
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
Mean
154.888
132.570
106.206
74.569
Minimum
140.140
119.133
99.529
68.150
Maximum
164.811
139.524
110.741
77.954
C.V.(%)
5.806
3.676
2.735
2.865
B-value
144.345
124.746
99.938
70.168
A-value
138.440
119.552
95.777
67.247
No. Specimens
18
18
No. Prepreg Lots
18
3
Mean
0.004
0.004
0.004
0.003
Minimum
0.004
0.004
0.003
0.003
Maximum
0.005
0.005
0.004
0.004
C.V.(%)
10.252
5.266
4.995
7.029
(GPa)
No. Specimens
12
12
12
No. Prepreg Lots
38
3.1.2.6.
Shear, 13 axis
Shear, 13-axis
Material:
Gr/Ep
Resin content:
39 - 45 wt%
Comp. density:
1.45 - 1.55 g/cc
Fiber volume:
47 - 54%
Void content:
0.4 - 3.0 %
Ply thickness:
0.1976 - .2210 mm
Ply range:
12 plies
Test method:
D2344-89
Normalized by:
N/A
Weave Fabric
[0] 12
CTD
RTD
ETD
ETW
-53.89
23.89
82.22
82.22
dry
dry
dry
equilibrium
as fabricated
as fabricated
as fabricated
62.78 C, 85%
Source code
Normalized
F13
su
(MPa)
Measured
Normalized
Measured
Mean
59.935
Minimum
52.403
Maximum
68.707
C.V.(%)
5.213
B-value
55.317
A-value
51.771
No. Specimens
No. Prepreg Lots
Normalized
Measured
Normalized
Measured
149
7
NOTES: These values represent the apparent interlaminar shear properties and are to be used for quality control
purposes only. Do not use these values for interlaminar shear strength design values.
39
3.1.3. Individual Test Charts
40
3.1.3.1.
Tension, 1-axis
0 Tension -- Normalized Strength

TCA T700S-12K-50C/#2510 Plain Weave Fabric
1200
Strength (MPa)
1000
800
600
400
Conditioning
X Dry
O Wet
200
0
-100
-50
50
100
Temperature (C)
NOTE: The symbols represent the pooled average of all tests, and the bars represent the upper and lower limit of
the data. The 180 dry and wet data has been staggered for clarity
41
3.1.3.2.
Tension, 2-axis
90 Tension -- Normalized Strength

1200
Strength (MPa)
1000
800
600
400
Conditioning
X Dry
O Wet
200
0
-100
-50
50
100
Temperature (C)
the data. The 180 dry and wet data has been staggered for clarity.
42
3.1.3.3.
Compression, 1-axis
0 Compression -- Normalized Strength

1000
Strength (MPa)
800
600
400
Conditioning
200
0
-100
X Dry
O Wet
-50
50
100
Temperature (C)
43
3.1.3.4.
Compression, 2-axis
90 Compression -- Normalized Strength

1000
Strength (MPa)
800
600
400
Conditioning
200
0
-100
X Dry
O Wet
-50
50
100
Temperature (C)
44
3.1.3.5.
Shear, 12 axis
In-Plane Shear -- Measured Strength

175
150
Strength (MPa)
125
100
75
50
Conditioning
X Dry
O Wet
25
0
-100
-50
50
100
Temperature (C)
the data. The 180 dry and wet data has been staggered for clarity
45
3.1.3.6.
Shear, 13 axis
Apparent Interlaminar Shear -- Measured Strength

80
Strength (MPa)
60
40
20
Conditioning
X Dry
0
-100
-50
50
100
Temperature (C)
46
3.2.
Raw Data
Specimen Naming Convention

Test coupons were identified using a ten-digit specimen code, with the significance of each digit delineated
below. A representative sample ID is shown for reference purposes.
A1 910-041 1-3
0 Tension
1st Character: Independent Cure Cycle
A designates a cure cycle that was
independently cured from B cure cycle
2nd Character: Panel Number
Numeric order of the panel fabricated for each cure
cycle
3rd ~ 8th Character: Master Roll Number
Prepreg Master Roll number used to
fabricate the panel
9th ~ 10th Character: Sample Number
The samples cut from each panel,
increasing numerically.
Panel Type ID
Panels/specimens were also identified with
the test type
47
3.2.1. Raw Data Spreadsheets and Scatter Charts
48
0 Tension -- (RTD)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-1
A2-910-056-1-1
A1-910-056-1-6
B1-910-056-1-1
B2-910-056-1-1
B1-910-056-1-6
A1-910-057-1-1
A2-910-057-1-1
A1-910-057-1-6
B1-910-057-1-1
B2-910-057-1-1
B1-910-057-1-6
A1-910-058-1-7
A2-910-058-1-7
A1-910-058-1-6
B1-910-058-1-7
B2-910-058-1-7
B1-910-058-1-6
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Strength
[MPa]
931.083
854.083
998.737
901.475
931.011
842.606
925.146
949.049
906.782
943.333
892.232
881.665
950.632
939.799
943.037
977.498
869.287
879.324
Modulus
[GPa]
0.055
0.055
Poisson's
Ratio
0.025
0.015
0.054
0.057
0.020
0.040
0.057
0.056
0.025
0.040
0.057
0.056
0.045
0.025
0.054
0.057
0.050
0.135
0.056
0.062
0.045
0.035
Average
917.599
0.056
0.042
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
42.177
4.596
842.606
998.737
18
0.002
3.553
0.054
0.062
12
0.031
75.433
0.015
0.135
12
49
Avg. Specimen
Thickn. [mm]
2.608
2.599
2.609
2.623
2.536
2.670
2.604
2.604
2.614
2.607
2.623
2.604
2.608
2.602
2.618
2.584
2.579
2.612
# Plies in
Laminate
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
Averagenorm
Avg. t ply
[mm]
0.21734
0.21660
0.21742
0.21861
0.21135
0.22253
0.21700
0.21700
0.21785
0.21721
0.21855
0.21696
0.21734
0.21681
0.21816
0.21531
0.21495
0.21770
Strengthnorm
[MPa]
926.392
846.883
994.092
902.174
900.790
858.364
919.050
942.795
904.322
938.031
892.664
875.685
945.842
932.787
941.849
963.479
855.388
876.342
Modulusnorm
[GPa]
0.054
0.055
0.21715
912.052
0.056
40.079
4.394
846.883
994.092
18
0.002
3.265
0.054
0.061
12
Standard Dev. norm

Coeff. of Var. [%]norm
Min.
Max.
Number of Spec.
0.2113
0.2225
0.054
0.055
0.056
0.056
0.057
0.056
0.054
0.057
0.055
0.061
Pooled Average = 912.052 [MPa]

Pooled Standard Deviation = 40.079 [MPa]
Pooled Coeff. of Variation = 4.394 [%]
0 Tension -- (RTD)
Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400
1600
1800
0 Tensile Strength [MPa]
Pooled Average = 0.056 [GPa]

Pooled Standard Deviation = 0.002 [GPa]
0 Tension -- (RTD)
Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.020
0.040
0.060
0 Tensile Modulus [GPa]
50
0.080
0.100
0.120
Prepreg Lot #
ASAP Batch #
0 Tension -- (CTD)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-7
A2-910-056-1-7
A2-910-056-1-8
B1-910-056-1-7
B2-910-056-1-7
B2-910-056-1-8
Cure
Cycle
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
ASAP
Batch #
1
1
1
2
2
2
Strength
[MPa]
843.194
765.594
802.934
810.573
842.461
752.490
Modulus
[GPa]
0.060
0.055
Average
802.874
0.057
0.085
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
37.896
4.720
752.490
843.194
6
0.002
3.514
0.055
0.060
4
0.019
22.528
0.070
0.110
4
0.056
0.057
Poisson's Avg. Specimen # Plies in

Ratio
Thickn. [mm] Laminate
0.110
2.606
12
0.070
2.616
12
2.609
12
0.090
2.629
12
0.070
2.639
12
2.637
12
51
Avg. tply
[mm]
0.21717
0.21802
0.21738
0.21908
0.21992
0.21971
Averagenorm 0.21855
Standard Dev. norm
Coeff. of Var. [%] norm
Min.
Max.
Number of Spec.
0.2172
0.2199
Strengthnorm
[MPa]
838.291
764.111
799.044
812.929
848.175
756.865
Modulusnorm
[GPa]
0.059
0.055
803.236
0.057
37.526
4.672
756.865
848.175
6
0.002
3.298
0.055
0.059
4
0.056
0.058
Pooled Average = 803.236 [Mpa]

0 Tension -- (CTD)
Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400
0
1800
1600

0 Tension -- (CTD)
Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.020
0.040
0.060
52
0.080
0.100
0.120
Prepreg Lot #
ASAP Batch #
0 Tension -- (ETW)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-3
A2-910-056-1-3
A1-910-056-1-4
B1-910-056-1-3
B2-910-056-1-3
B1-910-056-1-4
A1-910-057-1-3
A2-910-047-1-3
A1-910-057-1-4
B1-910-057-1-5
B2-910-057-1-3
B1-910-057-1-4
A1-910-058-1-3
A2-910-058-1-3
A1-910-058-1-4
B1-910-058-1-3
B2-910-058-1-3
B1-910-058-1-4
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Strength
[MPa]
1029.085
1106.526
1105.084
1074.110
1031.145
1056.629
1074.747
1063.688
1063.892
1003.072
1051.592
1007.153
1046.771
1055.648
1027.570
1077.413
1058.495
1002.461
Average 1051.949
Standard Dev.
30.909
Coeff. of Var. [%]
2.938
Min. 1002.461
Max. 1106.526
Number of Spec.
18
Modulus
[GPa]
0.054
0.061
0.063
0.055
0.057
0.056
0.059
0.058
0.057
0.059
0.059
0.059
0.058
0.002
4.288
0.054
0.063
12

Ratio
0.029
2.628
12
0.026
2.603
12
2.632
12
0.035
2.640
12
0.033
2.557
12
2.660
12
0.036
2.603
12
0.029
2.626
12
2.586
12
0.038
2.623
12
0.017
2.624
12
2.622
12
0.028
2.618
12
0.032
2.598
12
2.622
12
0.041
2.604
12
0.011
2.585
12
2.624
12
0.029
0.009
29.313
0.011
0.041
12
53
Averagenorm
Standard Dev. norm
Min.
Max.
Number of Spec.
Avg. tply
[mm]
0.21903
0.21692
0.21935
0.22003
0.21308
0.22166
0.21689
0.21886
0.21554
0.21861
0.21869
0.21850
0.21819
0.21654
0.21848
0.21700
0.21541
0.21865
Strengthnorm
[MPa]
1031.877
1098.806
1109.689
1081.916
1005.866
1072.192
1067.145
1065.749
1049.768
1003.849
1052.814
1007.446
1045.554
1046.442
1027.769
1070.314
1043.828
1003.433
Modulusnorm
[GPa]
0.054
0.060
0.21786
1049.137
31.952
3.046
1003.433
1109.689
18
0.058
0.003
4.606
0.053
0.063
12
0.2131
0.2217
0.063
0.053
0.057
0.057
0.059
0.058
0.057
0.059
0.059
0.058

0 Tension -- (ETW)
Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400
0
1800
1600

0 Tension -- (ETW)
Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.020
0.040
0.060
54
0.080
0.100
0.120
Prepreg Lot #
ASAP Batch #
0 Tension -- (ETD)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-2
A2-910-056-1-2
A2-910-056-1-6
B1-910-056-1-2
B2-910-056-1-2
B2-910-056-1-6
A1-910-057-1-2
A2-910-057-1-2
A2-910-057-1-6
B1-910-057-1-2
B2-910-057-1-2
B2-910-057-1-6
A1-910-058-1-8
A2-910-058-1-8
A2-910-058-1-6
B1-910-058-1-8
B2-910-058-1-8
B2-910-058-1-6
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Strength
[MPa]
969.265
989.999
984.976
936.392
910.994
1005.439
909.322
931.598
997.251
1002.260
990.633
939.436
1009.674
1006.581
1015.816
1000.107
880.860
961.103
Average 968.984
Standard Dev.
41.099
Coeff. of Var. [%]
4.241
Min. 880.860
Max. 1015.816
Number of Spec.
18
Modulus
[GPa]
0.054
0.055
0.054
0.057
0.063
0.056
0.058
0.056
0.057
0.053
0.056
0.058
0.056
0.003
4.463
0.053
0.063
12

Ratio
0.035
2.615
12
0.065
2.609
12
2.675
12
0.035
2.642
12
0.020
2.566
12
2.644
12
0.070
2.614
12
0.025
2.625
12
2.628
12
0.015
2.623
12
0.025
2.623
12
2.622
12
0.045
2.589
12
0.050
2.598
12
2.598
12
0.050
2.558
12
0.005
2.573
12
2.583
12
0.037
0.020
54.338
0.005
0.070
12
55
Avg. tply
[mm]
0.21795
0.21738
0.22293
0.22013
0.21383
0.22030
0.21785
0.21872
0.21903
0.21855
0.21859
0.21848
0.21575
0.21649
0.21649
0.21315
0.21442
0.21527
Average norm 0.21752

Standard Dev. norm
Min.
0.2131
Max.
0.2229
Number of Spec.
Strengthnorm
[MPa]
967.105
985.203
1005.210
943.651
891.750
1014.012
906.855
932.772
999.957
1002.746
991.305
939.619
997.249
997.608
1006.761
975.879
864.643
947.133
Modulusnorm
[GPa]
0.054
0.055
964.970
44.067
4.567
864.643
1014.012
18
0.056
0.003
4.481
0.053
0.063
12
0.054
0.055
0.063
0.056
0.058
0.056
0.056
0.053
0.055
0.056

0 Tension -- (ETD)
Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400
0
1800
1600

0 Tension -- (ETD)
Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.020
0.040
0.060
56
0.080
0.100
0.120
Prepreg Lot #
ASAP Batch #
90 Tension -- (RTD)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-6
A2-910-056-1-1
A1-910-056-1-9
B1-910-056-1-1
B2-910-056-1-1
B1-910-056-1-9
A1-910-057-1-1
A2-910-057-1-1
A1-910-057-1-6
B1-910-057-1-1
B2-910-057-1-1
B1-910-057-1-6
A1-910-058-1-7
A2-910-058-1-7
A1-910-058-1-6
B1-910-058-1-7
B2-910-058-1-7
B1-910-058-1-6
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
746.858
850.979
807.172
844.361
852.066
858.027
845.191
721.069
687.602
762.646
736.201
733.458
705.490
786.398
707.472
749.836
740.118
821.938
Modulus
[GPa]
0.053
0.056
775.382
58.245
7.512
687.602
858.027
18
0.055
0.001
1.581
0.053
0.056
12
0.055
0.056
0.054
0.055
0.055
0.054
0.056
0.055
0.055
0.054
Avg. Specimen # Plies in

2.644
12
2.557
12
2.600
12
2.632
12
2.617
12
2.604
12
2.603
12
2.599
12
2.625
12
2.620
12
2.590
12
2.606
12
2.600
12
2.583
12
2.638
12
2.612
12
2.623
12
2.631
12
Avg. tply
[mm]
0.22030
0.21311
0.21664
0.21935
0.21812
0.21696
0.21692
0.21658
0.21876
0.21829
0.21586
0.21713
0.21668
0.21527
0.21982
0.21766
0.21855
0.21922

Standard Dev. norm
Min.
0.2131
Max.
0.2203
Number of Spec.
57
Strength norm
[MPa]
753.227
830.199
800.524
847.879
850.827
852.207
839.294
714.921
688.601
762.128
727.498
729.051
699.816
774.967
711.928
747.148
740.477
824.885
Modulusnorm
[GPa]
0.054
0.055
771.977
56.806
7.359
688.601
852.207
18
0.055
0.001
1.419
0.054
0.056
12
0.056
0.056
0.054
0.054
0.055
0.054
0.055
0.054
0.055
0.054

90 Tension -- (RTD)
Normalized Strength
6
ASAP Batch #
4
2
3
Prepeg Lot #
ASAP Batch #
Prepreg Lot #
0
0
200
400
600
800
1000
1200
1400
1600

90 Tension -- (RTD)
Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.010
0.020
0.030
0.040
0.050
0.060
58
0.070
0.080
0.090
0.100
Prepreg Lot #
ASAP Batch #
90 Tension -- (CTD)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-7
A2-910-056-1-7
A1-910-056-1-8
B1-910-056-1-7
B2-910-056-1-7
B1-910-056-1-8
Cure
Cycle
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
ASAP
Batch #
1
1
1
2
2
2
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
742.458
736.290
718.240
688.155
719.311
708.183
718.773
19.586
2.725
688.155
742.458
6
Modulus Avg. Specimen # Plies in

[GPa]
0.057
2.637
12
0.055
2.652
12
2.614
12
0.056
2.652
12
0.055
2.637
12
2.621
12
Avg. tply
[mm]
0.21971
0.22098
0.21781
0.22098
0.21971
0.21844

Standard Dev.norm
Min.
0.2178
Max.
0.2210
Number of Spec.
0.056
0.001
1.536
0.055
0.057
4
59
Strength norm
[MPa]
746.775
744.851
716.152
696.157
723.493
708.183
Modulusnorm
[GPa]
0.057
0.056
722.602
20.145
2.788
696.157
746.775
6
0.056
0.001
1.471
0.056
0.057
4
0.057
0.056

90 Tension -- (CTD)
Normalized Strength
6
ASAP Batch #
4
2
3
Prepeg Lot #
ASAP Batch #
Prepreg Lot #
2
1
1
0
0
200
400
600
800
1000
1200
1400
1600

90 Tension -- (CTD)
Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.010
0.020
0.030
0.040
0.050
0.060
60
0.070
0.080
0.090
0.100
Prepreg Lot #
ASAP Batch #
90 Tension -- (ETW)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-3
A2-910-056-1-3
A1-910-056-1-4
B1-910-056-1-3
B2-910-056-1-3
B1-910-056-1-4
A1-910-057-1-3
A2-910-057-1-3
A1-910-057-1-4
B1-910-057-1-3
B2-910-057-1-3
B1-910-057-1-4
A1-910-058-1-3
A2-910-058-1-3
A1-910-058-1-4
B1-910-058-1-3
B2-910-058-1-3
B1-910-058-1-4
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Strength
[MPa]
1004.365
910.374
959.089
892.883
939.668
860.894
922.318
926.701
964.121
940.165
956.127
917.293
759.543
788.752
807.087
866.181
807.541
851.891
Average 893.055
Standard Dev. 68.559
Coeff. of Var. [%]
7.677
Min. 759.543
Max. 1004.365
Number of Spec.
18
Modulus
[GPa]
0.054
0.054
0.057
0.055
0.053
0.056
0.054
0.055
0.054
0.052
0.054
0.054

2.631
12
2.618
12
2.641
12
2.647
12
2.590
12
2.645
12
2.620
12
2.610
12
2.618
12
2.624
12
2.612
12
2.617
12
2.598
12
2.575
12
2.631
12
2.624
12
2.624
12
2.611
12
0.054
0.001
2.502
0.052
0.057
12
Avg. tply
[mm]
0.21924
0.21819
0.22007
0.22056
0.21584
0.22039
0.21829
0.21749
0.21819
0.21865
0.21764
0.21812
0.21649
0.21457
0.21922
0.21869
0.21869
0.21759

Standard Dev. norm
Min.
0.2146
Max.
0.2206
Number of Spec.
61
Strengthnorm
[MPa]
1008.063
909.316
966.245
901.535
928.468
868.569
921.692
922.660
963.000
941.076
952.606
915.960
752.772
774.766
809.980
867.188
808.480
848.589
Modulusnorm
[GPa]
0.054
0.054
892.276
70.336
7.883
752.772
1008.063
18
0.054
0.002
2.941
0.051
0.058
12
0.058
0.055
0.053
0.056
0.054
0.054
0.054
0.051
0.054
0.054

90 Tension -- (ETW)
Normalized Strength
6
ASAP Batch #
4
2
3
Prepeg Lot #
ASAP Batch #
Prepreg Lot #
0
0
200
400
600
800
1000
1200
1400
1600

90 Tension -- (ETW)
Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.010
0.020
0.030
0.040
0.050
0.060
62
0.070
0.080
0.090
0.100
Prepreg Lot #
ASAP Batch #
90 Tension -- (ETD)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-2
A2-910-056-1-2
A1-910-056-1-9
B1-910-056-1-2
B2-910-056-1-2
B1-910-056-1-9
A1-910-057-1-2
A2-910-057-1-2
A2-910-057-1-6
B1-910-057-1-2
B2-910-057-1-2
B2-910-057-1-6
A1-910-058-1-8
A2-910-058-1-8
A2-910-058-1-6
B1-910-058-1-8
B2-910-058-1-8
B2-910-058-1-6
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
942.543
940.611
942.857
850.558
837.930
913.203
747.872
728.125
859.851
838.631
786.527
840.919
760.737
774.174
815.034
823.343
841.968
853.039
Modulus
[GPa]
0.054
0.054
838.774
65.356
7.792
728.125
942.857
18
0.055
0.001
2.256
0.052
0.057
12
0.055
0.056
0.056
0.052
0.054
0.055
0.054
0.056
0.057
0.055

2.623
12
2.576
12
2.598
12
2.601
12
2.590
12
2.633
12
2.618
12
2.603
12
2.615
12
2.622
12
2.602
12
2.621
12
2.582
12
2.609
12
2.584
12
2.584
12
2.610
12
2.625
12
Avg. tply
[mm]
0.21861
0.21463
0.21654
0.21679
0.21584
0.21939
0.21819
0.21689
0.21791
0.21850
0.21681
0.21844
0.21520
0.21742
0.21533
0.21537
0.21749
0.21872

Standard Dev. norm
Min.
0.2146
Max.
0.2194
Number of Spec.
63
Strength norm
[MPa]
943.274
924.205
934.635
844.130
827.943
917.185
747.003
722.975
857.768
838.875
780.658
840.919
749.459
770.573
803.424
811.775
838.296
854.113
Modulusnorm
[GPa]
0.054
0.053
833.734
65.826
7.895
722.975
943.274
18
0.054
0.001
2.207
0.052
0.056
12
0.055
0.055
0.056
0.052
0.054
0.054
0.054
0.056
0.056
0.055

90 Tension -- (ETW)
Normalized Strength
6
ASAP Batch #
4
2
3
Prepeg Lot #
ASAP Batch #
Prepreg Lot #
0
0
200
400
600
800
1000
1200
1400
1600

90 Tension -- (ETW)
Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.010
0.020
0.030
0.040
0.050
0.060
64
0.070
0.080
0.090
0.100
Prepreg Lot #
ASAP Batch #
0 Compression -- (RTD)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-8
A2-910-056-1-5
A1-910-056-1-10
A2-910-056-1-1
B1-910-056-1-5
B2-910-056-1-7
B2-910-056-1-8
B2-910-056-1-1
A1-910-057-1-5
A2-910-057-1-7
A2-910-057-1-8
A2-910-057-1-1
B1-910-057-1-5
B2-910-057-1-7
B2-910-057-1-8
B2-910-057-1-1
A1-910-058-1-4
A1-910-058-1-5
A2-910-058-1-4
A2-910-058-1-1
B1-910-058-1-4
B1-910-058-1-5
B2-910-058-1-4
B2-910-058-1-1
Cure
Cycle
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
5
6
6
6
6
Strength
[MPa]
677.158
662.500
640.284
Modulus
[GPa]
0.056
773.197
724.194
707.896
0.056
659.142
761.160
759.365
0.056
782.660
616.231
593.713
0.057
774.963
724.387
714.168
0.052
717.585
715.597
755.441
0.058
Average
Standard Dev.
708.869
56.467
0.056
0.002
Coeff. of Var. [%]

Min.
Max.
Number of Spec.
7.966
593.713
782.660
18
3.932
0.052
0.058
6

2.616
12
2.616
12
2.616
12
3.009
14
2.616
12
2.616
12
2.616
12
3.011
14
2.604
12
2.604
12
2.604
12
3.019
14
2.604
12
2.604
12
2.604
12
2.985
14
2.642
12
2.642
12
2.642
12
3.051
14
2.642
12
2.642
12
2.642
12
3.013
14
Avg. tply
[mm]
0.21802
0.21802
0.21802
0.21490
0.21802
0.21802
0.21802
0.21508
0.21696
0.21696
0.21696
0.21566
0.21696
0.21696
0.21696
0.21323
0.22013
0.22013
0.22013
0.21793
0.22013
0.22013
0.22013
0.21521

Standard Dev. norm
Min.
Max.
Number of Spec.
65
0.2132
0.2201
Strengthnorm
[MPa]
675.845
661.216
639.043
Modulusnorm
[GPa]
0.055
771.698
722.791
706.524
0.055
654.671
755.997
754.215
0.055
777.351
612.051
589.686
0.056
780.970
730.003
719.705
0.051
723.147
721.145
761.297
0.057
708.742
57.768
0.055
0.002
8.151
589.686
780.970
18
3.391
0.051
0.057
6

Normalized Strength
6
ASAP Batch #
Prepeg Lot #
ASAP Batch #
Prepreg Lot #
200
400
600
800
1000
0
1400
1200
0 Compression Strength [MPa]

Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0.020
0.040
0.060
0.080
0 Compression Modulus [GPa]
66
0.100
0
0.120
Prepreg Lot #
ASAP Batch #
0 Compression -- (CTD)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-4
A1-910-056-1-5
A2-910-056-1-4
A2-910-056-1-6
B1-910-056-1-4
B2-910-056-1-4
B2-910-056-1-5
B2-910-056-1-6
Cure
Cycle
A
A
A
A
B
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
1
1
ASAP
Batch #
1
1
1
1
2
2
2
2
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
723.024
701.885
731.741
Modulus
[GPa]
0.054
844.971
758.523
723.076
0.055
747.203
51.276
6.862
701.885
844.971
6

2.631
12
2.631
12
2.631
12
3.071
14
2.631
12
2.631
12
2.631
12
3.071
14
0.055
0.001
1.527
0.054
0.055
2
Avg. tply
[mm]
0.21924
0.21924
0.21924
0.21935
0.21924
0.21924
0.21924
0.21935

Standard Dev. norm
Min.
0.2192
Max.
0.2193
Number of Spec.
67
Strengthnorm
[MPa]
725.687
704.469
734.435
Modulusnorm
[GPa]
0.054
848.082
761.316
725.739
0.055
749.955
51.465
6.862
704.469
848.082
6
0.055
0.001
1.527
0.054
0.055
2
Normalized Strength


6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400
Normalized Modulus


6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0.020
0.040
0.060
0.080
68
0.100
0
0.120
Prepreg Lot #
ASAP Batch #
0 Compression -- (ETW)
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-1
A1-910-056-1-2
A2-910-056-1-1
A2-910-056-1-3
B1-910-056-1-2
B1-910-056-1-1
B2-910-056-1-1
B2-910-056-1-3
A1-910-057-1-1
A1-910-057-1-2
A2-910-057-1-1
A2-910-057-1-3
B1-910-057-1-1
B1-910-057-1-2
B2-910-057-1-1
B2-910-057-1-3
A1-910-058-1-1
A2-910-058-1-1
A2-910-058-1-2
A2-910-058-1-3
B1-910-058-1-1
B2-910-058-1-1
B2-910-058-1-2
B2-910-058-1-3
Cure
Cycle
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
5
6
6
6
6
Strength
[MPa]
456.991
473.407
394.658
Modulus
[GPa]
0.057
419.416
400.440
531.552
0.052
482.242
463.025
439.285
0.051
527.114
446.287
446.260
0.063
524.241
504.937
488.704
0.055
531.983
488.411
493.512
0.053
Average
Standard Dev.
472.915
43.159
0.055
0.004
Coeff. of Var. [%]

Min.
Max.
Number of Spec.
9.126
394.658
531.983
18
7.863
0.051
0.063
6

2.631
12
2.631
12
2.631
12
3.037
14
2.631
12
2.631
12
2.631
12
3.043
14
2.604
12
2.604
12
2.604
12
3.050
14
2.604
12
2.604
12
2.604
12
3.012
14
2.659
12
2.659
12
2.659
12
3.042
14
2.659
12
2.659
12
2.659
12
3.041
14
Avg. tply
[mm]
0.21924
0.21924
0.21924
0.21690
0.21924
0.21924
0.21924
0.21739
0.21696
0.21696
0.21696
0.21784
0.21696
0.21696
0.21696
0.21512
0.22162
0.22162
0.22162
0.21732
0.22162
0.22162
0.22162
0.21722

Standard Dev. norm
Min.
Max.
Number of Spec.
69
0.2151
0.2216
Strengthnorm
[MPa]
458.673
475.150
396.111
Modulusnorm
[GPa]
0.057
420.960
401.914
533.509
0.052
478.971
459.884
436.305
0.051
523.539
443.260
443.233
0.062
531.861
512.276
495.807
0.055
539.716
495.510
500.685
0.052
474.854
45.123
0.055
0.004
9.502
396.111
539.716
18
7.418
0.051
0.062
6

Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400

Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
1
0
0.000
0
0.020
0.040
0.060
0.080
70
0.100
0.120
Prepreg Lot #
ASAP Batch #
0 Compression -- (ETD)
Strength & Modulus
normalizing t ply
[mm]
0.2184

Specimen
Number
A1-910-056-1-9
A2-910-056-1-8
A2-910-056-1-9
A2-910-056-1-2
B1-910-056-1-8
B1-910-056-1-9
B2-910-056-1-9
B2-910-056-1-2
A1-910-057-1-8
A1-910-057-1-9
A2-910-057-1-9
A2-910-057-1-2
B1-910-057-1-8
B1-910-057-1-9
B2-910-057-1-9
B2-910-057-1-2
A1-910-058-1-9
A2-910-058-1-5
A2-910-058-1-9
A2-910-058-1-2
B1-910-058-1-9
B2-910-058-1-5
B2-910-058-1-9
B2-910-058-1-6
Cure
Cycle
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
5
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
591.862
592.073
586.996
Modulus
[GPa]
0.055
660.847
661.520
670.195
0.054
678.870
774.079
658.037
0.057
722.308
738.506
580.651
0.062
659.631
680.408
611.657
0.055
701.614
716.942
746.174
0.054
668.465
58.548
8.759
580.651
774.079
18
# Plies in
Laminate
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
Avg. t ply
[mm]
0.21696
0.21696
0.21696
0.21550
0.21696
0.21696
0.21696
0.21630
0.21590
0.21590
0.21590
0.21717
0.21590
0.21590
0.21590
0.21367
0.21823
0.21823
0.21823
0.21726
0.21823
0.21823
0.21823
0.22022
Strengthnorm
[MPa]
587.847
588.057
583.014
Averagenorm
Standard Dev.norm
0.21694
664.143
58.129
8.753
573.899
765.078
18
Avg. Specimen
Thickn. [mm]
2.604
2.604
2.604
3.017
2.604
2.604
2.604
3.028
2.591
2.591
2.591
3.040
2.591
2.591
2.591
2.991
2.619
2.619
2.619
3.042
2.619
2.619
2.619
3.083
0.056
0.003
5.436
0.054
0.062
6

Min.
Max.
Number of Spec.
71
0.2137
0.2202
Modulusnorm
[GPa]
0.054
656.365
657.033
665.649
0.054
670.976
765.078
650.386
0.056
713.909
729.919
573.899
0.061
658.992
679.749
611.064
0.055
700.934
716.248
745.451
0.054
0.056
0.003
4.715
0.054
0.061
6

Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400
Normalized Modulus


6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
1
0
0.000
0
0.020
0.040
0.060
0.080
72
0.100
0.120
Prepreg Lot #
ASAP Batch #
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-5
A2-910-056-1-8
A2-910-056-1-9
A2-910-056-1-1
B1-910-056-1-5
B1-910-056-1-8
B2-910-056-1-4
B2-910-056-1-1
A1-910-057-1-8
A2-910-057-1-4
A2-910-057-1-5
A2-910-057-1-1
B1-910-057-1-7
B2-910-057-1-4
B2-910-057-1-5
B2-910-057-1-1
A1-910-058-1-4
A1-910-058-1-5
A2-910-058-1-4
A2-910-058-1-1
B1-910-058-1-4
B1-910-058-1-5
B2-910-058-1-4
B2-910-058-1-1
Cure
Cycle
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
5
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
672.954
659.447
649.514
Modulus
[GPa]
0.051
666.617
723.408
774.590
0.052
715.706
724.567
704.268
0.054
729.546
745.664
728.080
0.053
734.190
638.979
675.819
0.055
696.084
684.123
729.969
0.057
702.974
36.981
5.261
638.979
774.590
18
Avg. Specimen
Thickn. [mm]
2.591
2.591
2.591
3.033
2.591
2.591
2.591
3.071
2.591
2.591
2.591
3.064
2.591
2.591
2.591
3.029
2.629
2.629
2.629
3.062
2.629
2.629
2.629
3.028
# Plies in
Laminate
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
Avg. tply
[mm]
0.21590
0.21590
0.21590
0.21666
0.21590
0.21590
0.21590
0.21938
0.21590
0.21590
0.21590
0.21884
0.21590
0.21590
0.21590
0.21639
0.21908
0.21908
0.21908
0.21871
0.21908
0.21908
0.21908
0.21626
Averagenorm 0.21715
0.054
0.002
3.915
0.051
0.057
6
Standard Dev. norm

Min.
Max.
Number of Spec.
73
0.2159
0.2194
Strengthnorm
[MPa]
665.129
651.779
641.962
Modulusnorm
[GPa]
0.051
658.866
714.997
765.583
0.052
707.384
716.142
696.079
0.054
721.063
736.993
719.614
0.052
736.325
640.837
677.783
0.055
698.107
686.112
732.091
0.056
698.158
36.083
5.168
640.837
765.583
18
0.053
0.002
3.831
0.051
0.056
6

Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400

Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
1
0
0.000
0
0.010
0.020
0.030
0.040
0.050
0.060
74
0.070
0.080
0.090
0.100
Prepreg Lot #
ASAP Batch #
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-4
A2-910-056-1-4
A2-910-056-1-5
A2-910-056-1-6
B1-910-056-1-3
B1-910-056-1-4
B2-910-056-1-3
B2-910-056-1-6
Cure
Cycle
A
A
A
A
B
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
1
1
ASAP
Batch #
1
1
1
1
2
2
2
2
Strength
[MPa]
756.768
636.880
695.550
Modulus
[GPa]
Average
744.535
0.048
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
73.620
9.888
636.880
831.167
6
0.001
2.192
0.048
0.049
2
0.049
729.911
831.167
816.935
0.048
Avg. Specimen
Thickn. [mm]
2.612
2.612
2.612
3.063
2.612
2.612
2.612
3.104
# Plies in
Laminate
12
12
12
14
12
12
12
14
Avg. tply
[mm]
0.21766
0.21766
0.21766
0.21880
0.21766
0.21766
0.21766
0.22171
Averagenorm 0.21831
Standard Dev. norm
Min.
Max.
Number of Spec.
75
0.2177
0.2217
Strengthnorm
[MPa]
754.055
634.596
693.056
Modulus norm
[GPa]
0.049
727.294
828.187
814.006
0.048
741.866
0.049
73.356
9.888
634.596
828.187
6
0.001
1.260
0.048
0.049
2

Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400

Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
0
0.000
0.010
0.020
0.030
0.040
0.050
0.060
76
0.070
0.080
0.090
0
0.100
Prepreg Lot #
ASAP Batch #
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-1
A2-910-056-1-1
A2-910-056-1-2
A2-910-056-1-3
B1-910-056-1-1
B2-910-056-1-1
B2-910-056-1-2
B2-910-056-1-3
A1-910-057-1-1
A1-910-057-1-2
A2-910-057-1-1
A2-910-057-1-3
B1-910-057-1-1
B2-910-057-1-1
B2-910-057-1-2
B2-910-057-1-3
A1-910-058-1-1
A2-910-058-1-1
A2-910-058-1-2
A2-910-058-1-3
B1-910-058-1-1
B2-910-058-1-1
B2-910-058-1-2
B2-910-058-1-3
Cure
Cycle
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
5
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
443.124
481.103
453.010
Modulus
[GPa]
0.049
435.238
492.096
479.735
0.055
495.807
518.135
466.330
0.054
471.276
501.172
523.323
0.059
513.293
481.238
495.435
0.056
465.136
461.665
461.324
0.055
479.913
25.188
5.249
435.238
523.323
18
Avg. Specimen
Thickn. [mm]
2.612
2.612
2.612
3.046
2.612
2.612
2.612
3.081
2.604
2.604
2.604
3.152
2.604
2.604
2.604
3.026
2.629
2.629
2.629
3.061
2.629
2.629
2.629
3.036
# Plies in
Laminate
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
Avg. tply
[mm]
0.21766
0.21766
0.21766
0.21759
0.21766
0.21766
0.21766
0.22004
0.21696
0.21696
0.21696
0.22512
0.21696
0.21696
0.21696
0.21617
0.21908
0.21908
0.21908
0.21868
0.21908
0.21908
0.21908
0.21684
Averagenorm 0.21819
0.055
0.003
5.798
0.049
0.059
6
Standard Dev. norm

Min.
Max.
Number of Spec.
77
0.2162
0.2251
Strengthnorm
[MPa]
441.536
479.378
451.386
Modulusnorm
[GPa]
0.049
433.678
490.332
478.015
0.055
492.444
514.621
463.167
0.055
468.080
497.772
519.773
0.058
514.785
482.637
496.875
0.056
466.489
463.007
462.665
0.055
478.702
24.823
5.185
433.678
519.773
18
0.055
0.003
5.588
0.049
0.058
6

Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
0
0
200
400
600
800
1000
1200
1400

90 Compression -- (HTW)
Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.010
0.020
0.030
0.040
0.050
0.060
78
0.070
0.080
0.090
0.100
Prepreg Lot #
ASAP Batch #
Strength & Modulus
normalizing tply
[mm]
0.2184

Specimen
Number
A1-910-056-1-7
A1-910-056-1-8
A2-910-056-1-10
A2-910-056-1-2
B1-910-056-1-9
B2-910-056-1-5
B2-910-056-1-9
B2-910-056-1-2
A1-910-057-1-10
A2-910-057-1-8
A2-910-057-1-9
A2-910-057-1-2
B1-910-057-1-8
B2-910-057-1-10
B2-910-057-1-11
B2-910-057-1-2
A1-910-058-1-9
A2-910-058-1-8
A2-910-058-1-9
A2-910-058-1-6
B1-910-058-1-9
B2-910-058-1-8
B2-910-058-1-9
B2-910-058-1-2
Cure
Cycle
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
A
A
A
A
B
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
5
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
653.659
556.310
589.406
Modulus
[GPa]
0.052
600.151
683.364
703.935
0.053
632.877
701.496
707.857
0.052
646.723
648.515
638.429
0.056
673.102
651.037
620.254
0.053
651.003
664.063
667.730
0.052
649.439
40.100
6.175
556.310
707.857
18
Avg. Specimen
Thickn. [mm]
2.616
2.616
2.616
3.040
2.616
2.616
2.616
3.075
2.604
2.604
2.604
3.061
2.604
2.604
2.604
3.030
2.599
2.599
2.599
3.052
2.599
2.599
2.599
3.033
# Plies in
Laminate
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
12
12
12
14
Avg. tply
[mm]
0.21802
0.21802
0.21802
0.21712
0.21802
0.21802
0.21802
0.21962
0.21696
0.21696
0.21696
0.21866
0.21696
0.21696
0.21696
0.21641
0.21660
0.21660
0.21660
0.21799
0.21660
0.21660
0.21660
0.21663
Averagenorm 0.21733
0.053
0.002
2.984
0.052
0.056
6
Standard Dev. norm

Min.
Max.
Number of Spec.
79
0.2164
0.2196
Strengthnorm
[MPa]
652.392
555.232
588.264
Modulusnorm
[GPa]
0.052
598.988
682.040
702.571
0.053
628.584
696.737
703.056
0.052
642.336
644.116
634.098
0.056
667.428
645.549
615.025
0.053
645.515
658.465
662.101
0.051
645.694
39.442
6.108
555.232
703.056
18
0.053
0.002
2.845
0.051
0.056
6

Normalized Strength
6
ASAP Batch #
Prepreg Lot #
4
2
3
Prepeg Lot #
ASAP Batch #
1
1
0
0
200
400
600
800
1000
1200
1400

Normalized Modulus
6
ASAP Batch #
Prepreg Lot #
4
2
3
2
1
0
0.000
0
0.010
0.020
0.030
0.040
0.050
0.060
80
0.070
0.080
0.090
0.100
Prepreg Lot #
ASAP Batch #
In-Plane Shear -- (RTD)

Strength & Modulus
Specimen
Number
A1-910-056-1-5
A1-910-056-1-6
A1-910-056-1-27
B1-910-056-1-5
B1-910-056-1-6
B1-910-056-1-27
A1-910-057-1-1
A1-910-057-1-2
A1-910-057-1-11
B1-910-057-1-1
B1-910-057-1-2
B1-910-057-1-11
A1-910-058-1-1
A1-910-058-1-2
A1-910-058-1-11
B1-910-058-1-1
B1-910-058-1-2
B1-910-058-1-11
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
132.930
131.264
119.133
135.001
139.524
127.040
131.403
136.107
129.827
132.209
132.249
131.599
139.408
138.150
129.980
131.098
131.647
137.698
Modulus
[GPa]
0.004
0.005
132.570
4.873
3.676
119.133
139.524
18
0.004
0.000
5.266
0.004
0.005
12
81
0.004
0.004
0.004
0.004
0.004
0.004
0.004
0.004
0.005
0.004
Avg. Specimen
Thickn. [mm]
3.529
3.538
3.524
3.529
3.522
3.498
3.505
3.498
3.483
3.4628
3.4943
3.4595
3.438
3.452
3.447
3.443
3.458
3.445
# Plies in
Laminate
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
Avg. t ply
[mm]
0.22058
0.22111
0.22023
0.22058
0.22011
0.21863
0.21908
0.21863
0.21768
0.21642
0.21839
0.21622
0.21487
0.21574
0.21542
0.21522
0.21611
0.21531
Average
0.2178
Min.
Max.
0.2149
0.2211


Measured Strength
6
3
ASAP Batch #
Prepreg Lot #
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0
0
50
100
150
200
250
In-Plane Shear Strength [MPa]


Measured Modulus
6
3
ASAP Batch #
Prepreg Lot #
2
3
2
1
0
0.000
0
0.001
0.002
0.003
0.004
0.005
In-Plane Shear Modulus [GPa]
82
0.006
0.007
0.008
Prepreg Lot #
ASAP Batch #
In-Plane Shear -- (CTD)

Strength & Modulus
Specimen
Number
A1-910-056-1-1
A2-910-056-1-2
A1-910-056-1-3
B1-910-056-1-1
B2-910-056-1-2
B1-910-056-1-3
Cure
Cycle
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
ASAP
Batch #
1
1
1
2
2
2
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
164.811
158.190
140.140
159.376
158.554
148.258
Modulus
[GPa]
0.005
0.005
154.888
8.994
5.806
140.140
164.811
6
0.004
0.000
10.252
0.004
0.005
4
83
0.004
0.004
Avg. Specimen
Thickn. [mm]
3.526
3.518
3.523
3.526
3.528
3.533
# Plies in
Laminate
16
16
16
16
16
16
Avg. tply
[mm]
0.22035
0.21987
0.22019
0.22035
0.22050
0.22082
Average
0.2203
Min.
Max.
0.2199
0.2208


Measured Strength
6
3
ASAP Batch #
Prepreg Lot #
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0
0
50
100
150
200
250


Measured Modulus
6
3
ASAP Batch #
Prepreg Lot #
2
3
2
1
0
0.000
0
0.001
0.002
0.003
0.004
0.005
84
0.006
0.007
0.008
Prepreg Lot #
ASAP Batch #
In-Plane Shear -- (ETW)

Strength & Modulus
Specimen
Number
A1-910-056-1-10
A1-910-056-1-13
A1-910-056-1-9
B1-910-056-1-9
B1-910-056-1-10
B1-910-056-1-11
A1-910-057-1-5
A1-910-057-1-6
A1-910-057-1-7
B1-910-057-1-5
B1-910-057-1-6
B1-910-057-1-7
A1-910-058-1-5
A1-910-058-1-6
A1-910-058-1-7
B1-910-058-1-5
B1-910-058-1-6
B1-910-058-1-7
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
74.777
77.954
73.069
75.230
76.201
73.632
76.311
68.150
73.249
74.530
74.540
74.732
76.030
76.421
76.375
73.480
72.642
74.919
Modulus
[GPa]
0.003
0.003
74.569
2.136
2.865
68.150
77.954
18
0.003
0.000
7.029
0.003
0.004
12
85
0.003
0.003
0.003
0.003
0.003
0.003
0.004
0.003
0.003
0.003
Avg. Specimen
Thickn. [mm]
3.533
3.462
3.539
3.482
3.462
3.436
3.511
3.510
3.513
3.480
3.490
3.483
3.473
3.471
3.469
3.478
3.489
3.487
# Plies in
Laminate
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
Avg. t ply
[mm]
0.22082
0.21638
0.22117
0.21760
0.21634
0.21474
0.21942
0.21936
0.21958
0.21752
0.21812
0.21769
0.21709
0.21693
0.21682
0.21736
0.21809
0.21796
Average
0.2179
Min.
Max.
0.2147
0.2212


Measured Strength
6
3
ASAP Batch #
Prepreg Lot #
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0
0
50
100
150
200
250


Measured Modulus
6
3
ASAP Batch #
Prepreg Lot #
2
3
2
1
0
0.000
0
0.001
0.002
0.003
0.004
0.005
86
0.006
0.007
0.008
Prepreg Lot #
ASAP Batch #
In-Plane Shear -- (ETD)

Strength & Modulus
Specimen
Number
A1-910-056-1-7
A1-910-056-1-8
A1-910-056-1-28
B1-910-056-1-7
B1-910-056-1-8
B1-910-056-1-28
A1-910-057-1-3
A1-910-057-1-4
A1-910-057-1-12
B1-910-057-1-3
B1-910-057-1-4
B1-910-057-1-12
A1-910-058-1-3
A1-910-058-1-4
A1-910-058-1-12
B1-910-058-1-3
B1-910-058-1-4
B1-910-058-1-12
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
107.616
106.355
101.556
109.170
110.242
99.529
106.805
108.718
104.875
105.847
104.682
105.336
110.741
106.868
103.851
104.875
105.366
109.275
Modulus
[MPa]
0.004
0.003
106.206
2.904
2.735
99.529
110.741
18
0.004
0.000
4.995
0.003
0.004
12
87
0.003
0.003
0.004
0.004
0.003
0.004
0.004
0.003
0.004
0.004
Avg. Specimen
Thickn. [mm]
3.536
3.542
3.524
3.512
3.501
3.505
3.501
3.506
3.466
3.495
3.485
3.459
3.457
3.466
3.448
3.466
3.470
3.428
# Plies in
Laminate
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
16
Avg. t ply
[mm]
0.22103
0.22138
0.22023
0.21947
0.21879
0.21908
0.21881
0.21915
0.21665
0.21844
0.21781
0.21622
0.21606
0.21665
0.21550
0.21661
0.21690
0.21423
Average
0.2179
Min.
Max.
0.2142
0.2214


Measured Strength
6
3
ASAP Batch #
Prepreg Lot #
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0
0
50
100
150
200
250


Measured Modulus
6
3
ASAP Batch #
Prepreg Lot #
2
3
2
1
0
0.000
0
0.001
0.002
0.003
0.004
0.005
88
0.006
0.007
0.008
Prepreg Lot #
ASAP Batch #
Apparent Interlaminar Shear -- (RTD)

Strength
Specimen
Number
A1-910-056-1-1
A1-910-056-1-2
A1-910-056-1-3
B1-910-056-1-1
B1-910-056-1-2
B1-910-056-1-3
A1-910-057-1-1
A1-910-057-1-2
A1-910-057-1-3
B1-910-057-1-1
B1-910-057-1-2
B1-910-057-1-3
A1-910-058-1-1
A1-910-058-1-2
A1-910-058-1-3
B1-910-058-1-1
B1-910-058-1-2
B1-910-058-1-3
A-49-1-1
A-49-1-3
A-49-1-5
A-49-4-7
A-49-4-9
A-49-4-11
A-49-8-19
A-49-8-15
A-49-1-2
A-49-1-4
A-49-1-6
A-49-4-8
A-49-4-10
A-49-4-12
A-19-8-14
A-19-8-16
A-19-8-18
Cure
Cycle
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
B
B
B
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
NOTE: This table is continued in next four pages.
89
Strength
[MPa]
57.920
58.551
57.803
60.352
60.745
58.369
60.601
59.346
61.704
60.376
54.675
57.335
59.497
59.855
59.073
57.103
59.581
55.447
61.863
62.396
63.195
55.749
56.031
61.862
55.962
54.073
57.560
58.535
59.580
55.659
54.701
62.263
57.602
54.034
56.668
Avg. Specimen
Thickn. [mm]
2.642
2.640
2.652
2.457
2.413
2.371
2.619
2.631
2.637
2.648
2.650
2.648
2.610
2.597
2.652
2.634
2.629
2.630
2.558
2.549
2.554
2.588
2.596
2.586
2.637
2.634
2.554
2.551
2.582
2.584
2.581
2.592
2.629
2.637
2.643
# Plies in
Laminate
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
Avg. tply
[mm]
0.22013
0.22003
0.22098
0.20479
0.20108
0.19759
0.21823
0.21929
0.21971
0.22066
0.22087
0.22066
0.21749
0.21643
0.22098
0.21950
0.21908
0.21918
0.21315
0.21241
0.21283
0.21569
0.21632
0.21548
0.21971
0.21950
0.21283
0.21262
0.21516
0.21537
0.21505
0.21601
0.21908
0.21971
0.22024

Strength
Specimen
Number
B-50-1-1
B-50-1-3
B-50-1-5
B-50-4-7
B-50-4-9
B-50-4-11
B-50-8-13
B-50-8-15
B-50-1-2
B-50-1-4
B-50-1-6
B-50-4-8
B-50-4-10
B-50-4-12
B-50-8-14
B-50-8-16
B-50-8-18
A-51-2-1
A-51-2-3
A-51-2-5
A-51-5-7
A-51-5-9
A-51-5-11
A-51-8-13
A-51-8-15
A-51-2-2
A-51-2-4
A-51-2-6
A-51-5-8
A-51-5-10
A-51-5-12
A-51-8-14
A-51-8-16
Cure
Cycle
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
Prepreg
Lot #
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
ASAP
Batch #
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
90
Strength
[MPa]
60.383
59.713
59.096
62.109
66.875
63.098
62.651
62.481
60.359
59.635
62.105
60.448
61.147
62.881
57.243
59.439
61.484
58.579
56.016
53.355
59.925
58.768
56.709
59.538
57.405
56.428
55.804
59.361
59.384
56.773
59.957
61.007
57.059
Avg. Specimen
Thickn. [mm]
2.570
2.573
2.582
2.541
2.554
2.548
2.546
2.549
2.573
2.576
2.564
2.545
2.548
2.548
2.549
2.546
2.551
2.609
2.600
2.592
2.582
2.574
2.574
2.563
2.549
2.606
2.593
2.596
2.577
2.568
2.565
2.554
2.553
# Plies in
Laminate
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
Avg. tply
[mm]
0.21421
0.21442
0.21516
0.21177
0.21283
0.21230
0.21220
0.21241
0.21442
0.21463
0.21368
0.21209
0.21230
0.21230
0.21241
0.21220
0.21262
0.21738
0.21664
0.21601
0.21516
0.21452
0.21452
0.21357
0.21241
0.21717
0.21611
0.21632
0.21474
0.21400
0.21378
0.21283
0.21273

Strength
Specimen
Number
B-52-2-1
B-52-2-3
B-52-2-5
B-52-5-7
B-52-5-9
B-52-5-11
B-52-8-13
B-52-8-15
B-52-2-2
B-52-2-4
B-52-2-6
B-52-5-8
B-52-5-10
B-52-5-12
B-52-8-14
B-52-8-16
A-53-1-1
A-53-1-3
A-53-1-5
A-53-6-7
A-53-6-9
A-53-6-11
A-53-7-13
A-53-7-15
A-53-1-2
A-53-1-4
A-53-1-6
A-53-6-8
A-53-6-10
A-53-6-12
A-53-7-14
A-53-7-16
Cure
Cycle
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
Prepreg
Lot #
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
ASAP
Batch #
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
11
11
11
11
11
11
11
11
11
11
11
11
11
11
11
11
91
Strength
[MPa]
58.841
62.585
58.986
58.822
63.797
62.302
60.569
57.056
55.612
56.155
56.251
58.946
58.941
57.519
60.910
59.357
54.943
63.995
59.350
62.989
66.662
61.593
60.238
59.058
60.611
58.794
62.150
64.657
61.962
63.132
57.863
57.380
Avg. Specimen
Thickn. [mm]
2.629
2.631
2.638
2.573
2.572
2.579
2.496
2.496
2.630
2.642
2.634
2.577
2.573
2.581
2.496
2.498
2.567
2.563
2.574
2.630
2.628
2.635
2.635
2.634
2.562
2.567
2.572
2.630
2.631
2.640
2.638
2.639
# Plies in
Laminate
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
Avg. tply
[mm]
0.21908
0.21929
0.21982
0.21442
0.21431
0.21495
0.20796
0.20796
0.21918
0.22013
0.21950
0.21474
0.21442
0.21505
0.20796
0.20817
0.21389
0.21357
0.21452
0.21918
0.21897
0.21960
0.21960
0.21950
0.21347
0.21389
0.21431
0.21918
0.21929
0.22003
0.21982
0.21992

Strength
Specimen
Number
B-54-1-1
B-54-1-3
B-54-1-5
B-54-6-7
B-54-6-9
B-54-6-11
B-54-7-13
B-54-7-15
B-54-1-2
B-54-1-4
B-54-B-6
B-54-6-8
B-54-6-10
B-54-6-12
B-54-7-14
B-54-7-16
A-55-1-1
A-55-1-3
A-55-1-5
A-55-3-7
A-55-3-9
A-55-3-11
A-55-8-13
A-55-8-15
A-55-1-2
A-55-1-4
A-55-1-6
A-55-3-8
A-55-1-3-10
A-55-3-12
A-55-8-14
A-55-8-16
A-55-8-18
Cure
Cycle
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
Prepreg
Lot #
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
ASAP
Batch #
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
13
13
13
13
13
13
13
13
13
13
13
13
13
13
13
13
13
92
Strength
[MPa]
58.083
60.695
64.497
65.876
61.291
63.554
61.054
56.860
57.750
58.821
63.336
64.157
61.997
61.184
57.644
57.504
59.698
58.242
57.977
67.924
68.707
65.772
60.305
59.223
56.621
56.811
55.460
65.113
59.485
63.402
52.403
57.681
56.039
Avg. Specimen
Thickn. [mm]
2.560
2.568
2.573
2.590
2.591
2.586
2.592
2.595
2.564
2.570
2.570
2.590
2.593
2.591
2.590
2.593
2.569
2.545
2.577
2.564
2.529
2.559
2.507
2.507
2.551
2.559
2.581
2.540
2.545
2.572
2.502
2.513
2.535
# Plies in
Laminate
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
Avg. tply
[mm]
0.21336
0.21400
0.21442
0.21579
0.21590
0.21548
0.21601
0.21622
0.21368
0.21421
0.21421
0.21579
0.21611
0.21590
0.21579
0.21611
0.21410
0.21209
0.21474
0.21368
0.21071
0.21325
0.20892
0.20892
0.21262
0.21325
0.21505
0.21167
0.21209
0.21431
0.20849
0.20944
0.21124

Strength
Specimen
Number
B-56-1-1
B-56-1-3
B-56-1-5
B-56-3-7
B-56-3-9
B-56-3-11
B-56-8-13
B-56-8-15
B-56-1-2
B-56-1-4
B-56-1-6
B-56-3-8
B-59-3-10
B-56-3-12
B-56-8-14
B-56-8-16
Cure
Cycle
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
Prepreg
Lot #
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
ASAP
Batch #
14
14
14
14
14
14
14
14
14
14
14
14
14
14
14
14
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
93
Strength
[MPa]
60.252
64.434
61.858
66.401
65.081
64.469
61.837
62.762
61.919
62.915
60.770
66.881
60.064
58.835
60.979
60.349
59.935
3.124
5.213
52.403
68.707
149
Avg. Specimen
Thickn. [mm]
2.558
2.564
2.559
2.574
2.582
2.572
2.634
2.642
2.560
2.564
2.546
2.577
2.578
2.559
2.635
2.643
# Plies in
Laminate
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
12
Avg. t ply
[mm]
0.21315
0.21368
0.21325
0.21452
0.21516
0.21431
0.21950
0.22013
0.21336
0.21368
0.21220
0.21474
0.21484
0.21325
0.21960
0.22024
Average
0.2150
Min.
Max.
0.1976
0.2210


Measured Strength
14
ASAP Batch #
Prepreg Lot #
10
6
5
0
0
20
40
60
80
Apparent Interlaminar Shear Strength [MPa]
94
100
120
Prepreg Lot #
ASAP Batch #
12
3.2.2. Fluid Sensitivity Raw Data Spreadsheets and Scatter Charts
95
In-Plane Shear -- (MEK - RTD)

Strength
Specimen
Number
A1-910-056-1-23
A1-910-056-1-24
B1-910-056-1-23
B1-910-056-1-24
B1-910-056-1-25
Batch
Number
1
1
2
2
2
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[MPa]
131.221
131.218
128.020
126.021
127.089
Avg. Specimen
Thickn. [mm]
3.491
3.463
3.506
3.494
3.468
128.714
2.394
1.860
126.021
131.221
5
# Plies in
Laminate
16
16
16
16
16
Avg. tply
[mm]
0.21817
0.21646
0.21912
0.21839
0.21677
0.2178
Min.
Max.
0.2165
0.2191

In-Plane Shear -- (MEK - RTD)

Measured Strength
Batch #
0
0
20
40
60
80
96
100
120
140
In-Plane Shear -- (JP-4 JET FUEL - ETD)

Strength
Specimen
Number
A1-910-056-1-15
A1-910-056-1-16
B1-910-056-1-16
B1-910-056-1-17
B1-910-056-1-18
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Batch
Number
1
1
2
2
2
Strength
[MPa]
98.341
97.558
98.739
101.630
99.987
Avg. Specimen
Thickn. [mm]
3.492
3.494
3.515
3.520
3.528
99.251
1.594
1.606
97.558
101.630
5
# Plies in
Laminate
16
16
16
16
16
Avg. tply
[mm]
0.21825
0.21839
0.21968
0.22003
0.22047
0.2194
Min.
Max.
0.2182
0.2205

Pooled Standard Deviation = 1.594 [Mpa]
Pooled Coeff. of Variation = 1.606[%]
In-Plane Shear -- (JP-4 JET FUEL - ETD)

Measured Strength
Batch #
0
0
20
40
60
80
97
100
120
140
In-Plane Shear -- (Hydraulic Fluid - ETD)

Strength
Specimen
Number
A1-910-056-1-19
A1-910-056-1-20
A1-910-056-1-21
B1-910-056-1-19
B1-910-056-1-20
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Batch
Number
1
1
1
2
2
Strength
[MPa]
106.900
106.192
106.000
104.771
107.037
Avg. Specimen
Thickn. [mm]
3.510
3.514
3.515
3.531
3.530
106.180
0.904
0.851
104.771
107.037
5
# Plies in
Laminate
16
16
16
16
16
Avg. tply
[mm]
0.21934
0.21963
0.21971
0.22071
0.22063
0.2200
Min.
Max.
0.2193
0.2207

Pooled Standard Deviation = 0.904 [Mpa]
In-Plane Shear -- (Hydraulic Fluid - ETD)

Measured Strength
Batch #
0
0
20
40
60
80
In-Plane Shear Strength [Mpa]
98
100
120
140
Fluid Sensitivity Comparison:

Average In-Plane Shear Strength
with Fluid (MPa)
Same Environment In-Plane Shear

Strength without Fluid (MPa)
Worst Case Environment In-Plane

Shear Strength (MPa)
MEK (RTD)
(RTD)
(ETW)
128.714
132.570
74.569
The RTD average in-plane shear strength was reduced by 3% after exposure to MEK. However, it remained 73%
higher than water exposure in ETW condition.
with Fluid (MPa)


JP-4 JET FUEL (ETD)
(ETD)
(ETW)
99.251
106.206
74.569
The ETD average in-plane shear strength was reduced by 6.5% after exposure to JP-4 Jet Fuel. However it
remained 33% higher than water exposure in ETW condition.
with Fluid (MPa)


HYDRAULIC FLUID (ETD)
(ETD)
(ETW)
106.180
106.206
74.569
The ETD average in-plane shear strength was not reduced after exposure to Hydraulic Fluid.
99
3.2.3. Representative Shear Stress-Strain Curve

The following stress-strain curve is representative of the TORAY T700SC-12K50C/#2510 Plain Weave Fabric prepreg system. The tension and compression
stress-strain curves are not presented in graphical form. If strain design allowables
from these tests are required, simple one-dimensional linear stress-strain
relationships may be used to obtain corresponding strain design values. This
process should approximate tensile and compressive strain behavior relatively well
but may produce extremely conservative strain values in shear due to the nonlinear
behavior. A more realistic approach for shear strain design allowables is to use a
maximum strain value of 5% (reference MIL-HDBK-17-1E, section 5.7.6). If a
nonlinear analysis of the materials shear behavior is required, the curve-fit of the
shear stress-strain curve may be used. The representative shear stress-strain curve
was obtained by taking the average of all the sample shear curves and determining
the best-fit line through the data. The actual data points are also presented on the
chart to demonstrate material variability.
100
Shear Stress vs. Shear Strain, RTD

25000
Strain Data Points

Best Curve Fit Output
Shear Stress [psi]
20000
15000
10000
y-1 = a + b ln x/x
r2 = 0.99940513
a = 6.4451128 e-05
b = -2.1753988 e-07
5000
0
0
0.02
0.04
0.06
Shear Strain [in/in]
101
0.08
0.1
0.12
3.3. Statistical Results
102
DISTRIBUTION OF DATA & NORMAL CURVES

Mil-17 eg
DISTRIBUTION OF DATA AT INDIVIDUAL TEST

CONDITIONS
1.2
DISTRIBUTION OF POOLED DATA

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
0.7
Probability of Survival
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL CURVE
+ 10%
- 10%
0
0.5
0.0
0
200
400
600
800
1000
1200
0.6
0.7
0.8
0.9
Normalized Data
0 Measured Tension Strength
103
1.1
1.2

Mil-17 eg

CONDITIONS
1.2

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
0.7
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL
CURVE
+ 10%
0.0
0
200
400
600
800
1000
0.5
1200
0.6
- 10%
0.7
0.8
0.9
Normalized Data
0 Normalized Tension Strength
104
1.1
1.2

Mil-17 eg

CONDITIONS
1.2

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.7
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL
CURVE
+ 10%
0.0
0
200
400
600
800
1000
0.5
1200
0.6
- 10%
0.7
0.8
0.9
Normalized Data
105
1.1
1.2

Mil-17 eg

CONDITIONS
1.2

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.7
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL
CURVE
+ 10%
0.0
0
200
400
600
800
1000
0.5
1200
0.6- 10% 0.7
0.8
0.9
Normalized Data
106
1.1
1.2
1.3

Mil-17 eg

CONDITIONS
1.2

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.7
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL
CURVE
+ 10%
0.0
0
200
400
600
800
0.5
1000
0.6- 10% 0.7
0.8
0.9
Normalized Data
0 Measured Compression Strength
107
1.1
1.2
1.3

Mil-17 eg

CONDITIONS
1.2

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.7
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL
CURVE
+ 10%
0.0
0
200
400
600
800
0.5
1000
0.6- 10% 0.7
0.8
0.9
Normalized Data
0 Normalized Compression Strength
108
1.1
1.2
1.3

Mil-17 eg

CONDITIONS
1.2

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.7
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL
CURVE
+ 10%
0.0
0
200
400
600
800
0.5
1000
0.6
- 10%
0.7
0.8
0.9
Normalized Data
109
1.1
1.2

Mil-17 eg

CONDITIONS
1.2

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.7
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL
CURVE
+ 10%
0.0
0
200
400
600
800
0.5
1000
0.6
- 10%
0.7
0.8
0.9
Normalized Data
110
1.1
1.2

Mil-17 eg

CONDITIONS
1.2

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.7
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL
CURVE
+ 10%
0.0
0
50
100
150
0.5
200
0.6
- 10%
0.7
0.8
0.9
Normalized Data
In-Plane Shear
111
1.1
1.2

Mil-17 eg

CONDITIONS
1.2

1
CTD
RTD
ETD
ETW
0.9
NONE
NORMAL CURVE
1.0
NORMAL CURVE
0.8
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.7
0.8
0.6
0.6
0.5
0.4
0.4
0.3
0.2
POOLED DATA
0.2
0.1
NORMAL
CURVE
+ 10%
0.0
0
20
40
60
80
0.5
100
0.6- 10% 0.7
0.8
0.9
Normalized Data
Apparent Interlaminar Shear
112
1.1
1.2
1.3
APPENDIX A. PHYSICAL AND MECHANICAL TEST PROCEDURES
113
A.1. Physical Properties

A.1.1. Uncured Resin Content
Three (100 mm X 100 mm) uncured samples were taken across the width of the
prepreg ply sheet, from the start and end of the batch. These samples were tested
for resin weight percentage in accordance with TCWIN-Q-P004, using N-Methyl
Pyrrolidone (NMP) solvent to extract the resin matrix, and SACMA SRM 23-94,
Method A.
A.1.2. Uncured Volatile Content
The volatile content weight fraction was determined in accordance with TCWIN-QP001 that meets the intent of ASTM D3530. Three (100 mm X 100 mm) uncured
samples were taken across the width of the prepreg ply sheet, from the start and
end of the batch.
A.1.3. Resin Gel Time
Three (6 mm X 6 mm) uncured samples were taken across the width of the prepreg
ply sheet, from the start and end of the prepreg material batch. The gel time property
was performed in accordance with ASTM D3532 and TCWIN-U-P007.
A.1.4. Resin Flow
The resin flow property was determined in accordance with SACMA SRM 22-94 and
TCWIN-U-P008.
A.1.5. Uncured Fiber Areal Weight
The surface areas of resin content samples tested in accordance with 2.2.1 were
precisely measured in accordance with TCWIN-Q-P004 and SACMA SRM 23R-94.
The fiber areal weight (g/m2) was calculated by dividing the mass of the resin free
fibrous residue by the measured surface area.
A.1.6. Infrared Spectroscopy
The infrared spectroscopy signature tests were performed in accordance with
TCWIN-U-C002 that meets the intent of ASTM D1252 and ASTM D168.
114
A.1.7. High Performance Liquid Chromatography (HPLC)

HPLC signature tests were performed in accordance with TCWIN-U-C004 and
SACMA SRM 20R-94.
A.1.8. Differential Scanning Calorimetry (DSC)
DSC was performed to provide thermal property, specifically onset and peak
temperature, data for prepreg material. The DSC tests were conducted in
accordance with SACMA SRM 25R-94 and TCWIN-U-C003.
A.1.9. Cured Neat Resin Density
Testing the specimens in accordance with ASTM D792 Method A and TCWIN-UM215 determined the cured neat resin density. The density was calculated as
follows:
W1
Re sin = L
W
W
1
2
where:
Resin = Resin density, g/cc

L = density of ethanol or water, g/cc
W1 = weight of sample in air
W2 = weight of sample in ethanol or water
A.1.10. Fiber Volume

The fiber volume of each mechanical test laminate was determined in accordance
with ASTM D3171-90. The calculation was performed in accordance with the
following equation;
W
VF = C * CF
F
where:
VF = calculated fiber volume, %
C = laminate density, g/cc (same method as 2.2.9)
WCF = weight of fibrous carbon fiber residue of acid digestion, g
F = nominal carbon fiber density, g/cc = 1.78 for T700S
A.1.11. Resin Volume
The resin volume of each mechanical test laminate was determined in accordance
following equation;
115
100 WCF
VF = C *
R
where:
VF = calculated fiber volume, %(v)
R = nominal cured neat resin density, g/cc = 1.267
A.1.12. Void Content

The void content of each mechanical test laminate was determined in accordance
following equation;
100 WCF WCF
VV = 100 C *
+
R
F
where:
VV = Void content, %(v)
F = nominal carbon fiber density, g/cc = 1.78 for T700S
R = nominal cured neat resin density, g/cc = 1.267
A.1.13. Cured Laminate Tg by DMA
The dry and wet Tg by DMA was determined on three specimens per batch in
accordance with SACMA SRM 18R-94. The wet Tg specimens were conditioned in
accordance with method described in paragraph 2.1.7.1. The resultant wet Tg data
reflected the plasticization of resin matrix due to moisture absorption that is
anticipated for any operational environment.
A.2. TENSILE PROPERTIES

Note:
The following descriptions below apply to both 0 (Warp) and 90 (Fill)
Tensile specimens unless otherwise specified.
A.2.1. 0 (Warp) and 90 (Fill) Tensile Properties
The 0 (warp) and 90 (fill) tensile tests were conducted in accordance with ASTM
D3039 and TCWIN-U-M201. Six test specimens, 4 for tensile strength & modulus
and 2 for tensile strength only, were tested for each test condition. Test specimens
116
from one batch were tested at -65F (Dry). Test specimens from three batches were
tested at 75F (Dry), 180F (Dry) and 180F (Wet).
Twelve plies were used to fabricate the initial test panels, for zero-degree (warp)12
and ninety-degree (fill) 12 ply orientations. The panels were tabbed in accordance
with para. 2.1.5. The zero-degree and ninety-degree test specimens were wet cut to
9.0 inches nominal length and 1.00 inch nominal width in accordance with TCWINQ-M101.
The widths of the test specimens were measured with digital diameter flat anvil
and spindle micrometer. The thickness of the specimens were measured with digital
diameter hemispherical anvil and spindle micrometer. The measurements were
recorded onto TCFOR-Q-033. The width and thickness measurements were
entered into the test frame computer along with the material type, batch number, test
condition and specimen identification.
The 0 (warp) tensile test specimens were strain gauged with CEA-06-125UT-120
biaxial strain gage, except the 65 F test specimens that were strain gauge with
CEA-06-125UT-350 biaxial strain gage by Intec. The 90 (fill) tensile test specimens
were strain gauged with C-960401-A axial strain gage, except the 65 F test
specimens that were strain gauge with CEA-06-125UW-350 axial strain gage by
Intec. Instron 4505 load frame, operated in stroke control mode, was used to apply
loading to the specimens at a crosshead rate of 0.05 inch/minute. For 0 (warp)
tensile specimens, the loads, crosshead displacements, longitudinal strains and
transverse strains were recorded throughout each test using a calibrated,
computerized data assimilation system. For 90 (fill) tensile specimens, the loads,
crosshead displacements and transverse strains only were recorded throughout
each test using a calibrated, computerized data assimilation system.
A.2.1.1. Tensile Calculations
The ultimate tensile strengths, moduli and the poissons ratio (zero-degree only)
were calculated by transferring the raw data recorded, for example, ultimate loads,
from the Instron computer into a Microsoft Excel spreadsheet program, in
accordance with the following equations:
A.2.1.1.1. Tensile Strength (Un-normalized)
The un-normalized tensile strength was calculated using the following equation:
ULT =
P
b*d
117
where:
ULT = the ultimate tensile stress (MPa)

P = the maximum load, (N)
b = the averaged measured width of the specimen (mm)
d = the averaged measured thickness of the specimen (mm)
A.2.1.1.2. Tensile Strength (Normalized)

The normalized tensile strength was calculated using the following equation:
ULT =
CPTspecimen
P
x
b * d CPTbatchaverage
A.2.1.1.3. Tensile Modulus of Elasticity (Un-normalized)

The un-normalized longitudinal tensile modulus of elasticity was calculated using
the following equation:
E11T =
P0.3% P0.1%
b * d * ( 0.3% 0.1% )
where: E11T = the tensile modulus of elasticity (GPa)

b = the averaged measured width of the specimen (mm)
d = the averaged measured thickness of the specimen (mm)
P0.3% = the applied load at 3000 micron (N)
P0.1% = the applied load at 1000 micron (N)
0.3% = 0.3% measured longitudinal strain = 3000 micron (mm/m)
0.1% = 0.1% measured longitudinal strain = 1000 micron (mm/m)
A.2.1.1.4. Tensile Modulus of Elasticity (Normalized)
The normalized longitudinal tensile modulus of elasticity was calculated using the
following equation:
E11T =
CPTspecimen
P0.3% P0.1%
x
b * d * ( 0.3% 0.1% ) CPTbatchaverage
A.2.1.1.5. 0 (Warp) Tensile Poissons Ratio

The poissons ratio (12) of 0 (warp) tensile specimen was calculated as follows:
118
12 =
where:
Y 2 Y1
0.002
12 = major Poissons ratio

Y1 = transverse strain at stress 1, mm/mm
Y2 = transverse strain at stress 2, mm/mm
0.002 = the longitudinal strain range (X2-X1)=0.0030.001 mm/mm
A.3. COMPRESSIVE STRENGTH

Note: The following description apply to both 0 (Warp) and 90 (Fill) Compressive
Strength specimens unless otherwise specified.
A.3.1. 0 (Warp) and 90 (Fill) Compressive Strength Properties
The 0 (warp) and 90 (fill) compressive strength tests were conducted in
accordance with SACMA SRM 1R-94 and TCWIN-U-M204. Six compressive
strength specimens were tested for each test condition. Test specimens from one
batch were tested at -65F (Dry). Test specimens from three batches were tested at
75F (Dry), 180F (Dry) and 180F (Wet).
Twelve plies were used to fabricate the initial test panels, for zero-degree (warp)12
and ninety-degree (fill) 12 ply orientations. The panels were tabbed in accordance
with para. 2.1.5. The test specimens were wet cut, to nominal length of 3.18 inches
and a nominal width of 0.50 inch. The test specimens were machined at NIAR,
Wichita State University in accordance with SACMA SRM 1-94.
The widths of the specimens were measured with digital diameter flat anvil and
spindle micrometer. The thickness of the specimens used in calculations was the
average of measurements on untabbed test panel with digital diameter
hemispherical anvil and spindle micrometer. The measurements were recorded
onto TCFOR-Q-033. The width and thickness measurements were entered into the
test frame computer along with the material type, batch number, test condition and
specimen identification.
A modified ASTM D695 anti-buckling fixture was used to augment specimen stability
during the compressive tests. Instron 4510 load frame, operated in stroke control
mode, was used to apply loading to the specimens at 0.05 inch/minute crosshead
rate. The loads and displacements were recorded throughout each test using a
calibrated, computerized data assimilation system.
119
A.3.1.1. Compressive Strength Calculations

The ultimate compressive strengths were calculated by transferring the raw data
recorded, for example, ultimate loads, from the Instron 4510 into a Microsoft Excel
spreadsheet program, in accordance with the following equations:
A.3.1.1.1. Compressive Strength Calculation (Un-normalized)
The un-normalized 0 (warp) & 90 (fill) ultimate compressive strengths were
calculated in accordance with the following formula:
F=
where: F
P
b
t
P
b* t
= the ultimate compressive strength (MPa)

= the ultimate compressive load (N)
= the averaged measured specimen width (mm)
= the average thickness measured on untabbed compression panel (mm)
A.3.1.1.2. Compressive Strength Calculation (Normalized)

The 0 (warp) & 90 (fill) compressive strengths were normalized in accordance with
the following formula:
F=
CPTspecimen
P
x
b * t CPTbatchaverage
A.4. COMPRESSIVE MODULUS

Note: The following description apply to both 0 (Warp) and 90 (Fill) Compressive
Modulus specimens unless otherwise specified.
A.4.1. 0 (Warp) and 90 (Fill) Compression Modulus Properties
The 0 (warp) and 90 (fill) compressive modulus tests were conducted in
accordance with SACMA SRM 1R-94 and TCWIN-U-M206. Two test specimens
were tested for each test condition. Test specimens from one batch were tested at 65F (Dry). Test specimens from three batches were tested at 75F (Dry), 180F
(Dry) and 180F (Wet).
120
Fourteen plies were used to fabricate the initial test panels, for zero-degree (warp)14
and ninety-degree (fill) 14 ply orientations. The test specimens were wet cut, to
nominal length of 3.18 inches and a nominal width of 0.50 inch, in accordance with
TCWIN-Q-M103.
The widths of the test specimens were measured with digital diameter flat anvil
and spindle micrometer. The thickness of the specimens were measured with digital
diameter hemispherical anvil and spindle micrometer. The measurements were
recorded onto TCFOR-Q-033. The width and thickness measurements were
entered into the test frame computer along with the material type, batch number, test
condition and specimen identification.
A modified ASTM D695 anti-buckling fixture was used to augment specimen stability
during the compressive tests. Instron 4510 load frame, operated in stroke control
mode, was used to apply the loads. The crosshead displacement rate for each test
was 0.05 in/min (1.27 mm/min) and the strains were measured with a FAE-12S-12S6EL-2 uni-axial strain gauge, except for the 65F test specimens that were strain
gauged with CEA-06-125UW-350 uni-axial strain gauge and tested by Intec. The
loads and strains were recorded throughout each test using computerized data
assimilation system.
A.4.1.1. Compression Modulus Calculations
The compression moduli were calculated by transferring the raw data recorded, for
example, longitudinal strains, from the Instron 4510 into a Microsoft Excel
spreadsheet program, in accordance with the following equations:
A.4.1.1.1. Compressive Modulus Calculation (Un-normalized)
The un-normalized 0 (warp) & 90 (fill) compressive modulus was calculated as
follows:
E=
where:
P0.3% P0.1%
b * d * ( 0.3% 0.1% )
E = compressive modulus (GPa)

P0.3% = applied load at 3000 micron, (N)
P0.1% = applied load at 1000 micron, (N)
b = averaged measured specimen width, (mm)
d = averaged measured specimen thickness, (mm)
0.3% = 0.3% measured strain = 3000 micron (mm/m)
0.1% = 0.1% measured strain = 1000 micron (mm/m)
121
A.4.1.1.2. Compressive Modulus Calculation (Normalized)

The 0 (warp) & 90 (fill) compressive modulus normalization was calculated as
follows:
E=
CPTspecimen
P0.3% P0.1%
x
b * d * ( 0.3% 0.1% ) CPTbatchaverage
A.5. IN-PLANE (IOSIPESCU) SHEAR

The in-plane (iosipescu) shear tests were conducted in accordance with ASTM
D5379-93 and D5379-98 for new calculation range. Six test specimens, 4 for shear
strength & modulus and 2 for shear strength only, were tested for each test
condition. Test specimens from one batch were tested at -65F (Dry). Test
specimens from three batches were tested at 75F (Dry), 180F (Dry) and 180F
(Wet).
Sixteen plies were used to fabricate the initial test panels, in the (Warp/Fill) 4S ply
stacking sequence. The test specimens were wet cut, to nominal length of 3.0
inches and to nominal width of 0.75 inch. The specimen width is further machined to
symmetrical centrally located v-notched width of 0.45 inch, in accordance with ASTM
D5379-93.
The symmetrical centrally notched widths of the test specimens were measured with
digital needlepoint and spindle micrometer. The thickness of the specimens were
measured with digital diameter hemispherical anvil and spindle micrometer. The
measurements were recorded onto TCFOR-Q-033. The width and thickness
measurements were entered into the test frame computer along with the material
type, batch number, test condition and specimen identification.
The test specimens were inserted into the v-notched beam test fixture, with the
notch located along the line-of-action of loading by means of an alignment tool that
referenced the fixture. The notches influence the shear strain along the loading
direction, as the two halves of the fixture were compressed by the load frame while
monitoring load.
Instron 4505 load frame, operated in stroke control mode, was used to apply the
loads. The crosshead displacement rate for each test was 0.05 in/min (1.27
mm/min). The strains were measured with a EA-06-125-TW-120 rosette strain
gauge, except the -65F test specimens that were strain gauged with EA-06-062TV350 and tested by Intec. The loads and strains were recorded throughout each test
using computerized data assimilation system.
122
A.5.1. In-plane (Iosipescu) Shear Strength Calculations

The strains were measured using the bonded strain gauge. The shear cord modulus
was calculated in accordance with ASTM D5379-98, at 6500 microstrain and 2500
microstrain. The ultimate in-plane (iosipescu) shear strength and moduli were
calculated by transferring the raw data recorded, for example, ultimate loads,
measured strains, from the instron computer into a Microsoft Excel spreadsheet, in
accordance with the following equations:
A.5.1.1. In-plane (Iosipescu) Shear, Ultimate Strength Calculation
Ult. =
where:
P
b*d
Ult. = the ultimate in-plane shear strength (MPa)

P = the ultimate load (N)
b = the measured specimen width, in the symmetrical
centrally located notch (mm)
d = the average measured specimen thickness (mm)
A.5.1.2. In-plane (Iosipescu) Shear, Modulus Calculation
G12 =
where:
P0.6% P0.1%
b * d * ( 0.6% 0.1% )
G12 = shear chord modulus of elasticity (GPa)

P0.65% = applied load at 6500 micron (N)
P0.25% = applied load at 2500 micron (N).
b = the measured specimen width, in the symmetrical
centrally located notch (mm)
d = the average measured specimen thickness (mm)
0.65% = +45+-45= shear strain at 6500 micron (mm/m)
0.25% = +45+-45= shear strain at 2500 micron (mm/m)
A.6. SHORT BEAM SHEAR

The short beam shear tests were conducted in accordance with ASTM 2344-89.
Six test specimens from three batches were tested at 75F (Dry) only.
123
Twelve plies were used to fabricate the initial test panels, in the zero-degree ply
stacking sequence, (warp)12. The test specimens were wet cut, to nominal length of
6*average thickness, in inches and to nominal width of 0.25 inch.
Instron 4505 load frame, operated in stroke control mode, was used to apply the
loads. The crosshead displacement rate for each test was 0.05 in/min (1.27
mm/min). The loads and displacements were recorded throughout each test using
computerized data assimilation system.
A.6.1. Short Beam Shear Strength Calculations
The short beam shear strengths were calculated by transferring the raw data
recorded from the Instron 4505 computer into Microsoft Excel spreadsheet program,
in accordance with the following equation:
A.6.1.1. Short Beam Shear Strength Calculation
F=
where:
3* P
4*b*t
F. = the short beam shear strength (MPa)

P = the ultimate load (N)
b = the measured specimen width (mm)
t = the measured specimen thickness (mm)
124
APPENDIX B. MOISTURE CONDITIONING HISTORY CHARTS
125
Traveler #1
Traveler #2
0.50
0.00
1.50
1.00
0.50
0.00
10
10
1/2
1.00
0.50
0.00
8
Time, days 1/2
10
1.50
1.00
0.50
1/2
10
Time, days 1/2
10
1/2
Traveler #11
2.00
1.50
1.00
0.50
1.50
1.00
0.50
0.00
Time, days
126
Time, days
0.00
2
0.50
10
2.00
1.00
Traveler #10
0.00
6
Time, days
% Weight Gain
% Weight Gain
1.50
1.50
0.00
0
2.00
0.50
Traveler #8
2.00
% Weight Gain
Time, days
Traveler #7
1.00
0.00
0
Time, days 1/2
1.50
% Weight Gain
2.00
% Weight Gain
1.00
% Weight Gain
1.50
Traveler #5
2.00
2.00
% Weight Gain
% Weight Gain
2.00
Traveler #4
8
1/2
10
Time, days
8
1/2
10
Traveler #61
Traveler #62
1.00
0.50
0.00
1.50
1.00
0.50
0.00
Time, days
10 12
Time, days
10 12
1.00
0.50
0.00
8
10 12
Time, days 1/2
Time, days
1.50
1.00
0.50
10 12
Time, days
10 12
1/2
Traveler #68
1.50
1.00
0.50
1.50
1.00
0.50
0.00
Time, days
127
2.00
Time, days 1/2
1/2
0.00
2
0.50
10 12
2.00
1.00
Traveler #67
0.00
6
1/2
% Weight Gain
1.50
1.50
0.00
0
2.00
0.50
Traveler #66
% Weight Gain
% Weight Gain
1/2
2.00
1.00
0.00
0
Traveler #65
1.50
% Weight Gain
2.00
% Weight Gain
1.50
Traveler #64
2.00
% Weight Gain
2.00
% Weight Gain
% Weight Gain
2.00
Traveler #63
8
1/2
10 12
10 12
Time, days 1/2
Traveler #69M
Traveler #71M
1.00
0.50
0.00
1.50
1.00
0.50
0.00
8 10 12
Time, days
Time, days
10 12
1.00
0.50
10 12
Time, days 1/2
Time, days
1.50
1.00
0.50
1/2
10 12
10 12
1/2
Traveler #80
1.50
1.00
0.50
1.50
1.00
0.50
0.00
10 12
Time, days 1/2
128
2.00
Time, days 1/2
Time, days
0.00
2
0.50
10 12
2.00
1.00
Traveler #79
0.00
0.00
1/2
% Weight Gain
1.50
1.50
0.00
0
2.00
0.50
Traveler #78
% Weight Gain
% Weight Gain
1/2
2.00
1.00
0.00
0
Traveler #77
1.50
% Weight Gain
2.00
% Weight Gain
1.50
Traveler #75M
2.00
% Weight Gain
2.00
% Weight Gain
% Weight Gain
2.00
Traveler #73M
Time, days
10 12
1/2
Traveler #81
Traveler #82
1.00
0.50
0.00
1.50
1.00
0.50
0.00
Time, days
10
12
Time, days
10 12
1.00
0.50
0.00
8
Time, days
10 12
1/2
Time, days
1.50
1.00
0.50
Time, days
10 12
Time, days
10 12
1/2
Traveler #88
1.50
1.00
0.50
1.50
1.00
0.50
0.00
Time, days
129
2.00
1/2
1/2
0.00
2
0.50
10 12
2.00
1.00
Traveler #87
0.00
6
1/2
% Weight Gain
1.50
1.50
0.00
0
2.00
0.50
Traveler #86
% Weight Gain
% Weight Gain
1/2
2.00
1.00
0.00
0
Traveler #85
1.50
% Weight Gain
2.00
% Weight Gain
1.50
Traveler #84
2.00
% Weight Gain
2.00
% Weight Gain
% Weight Gain
2.00
Traveler #83
10 12
1/2
Time, days
10 12
1/2
Traveler #89M
Traveler #91M
1.00
0.50
0.00
1.50
1.00
0.50
0.00
8 10 12
Time, days
1/2
10 12
1.00
0.50
0.00
8
Time, days 1/2
10
10 12
1.50
1.00
0.50
10
1.50
1.00
0.50
10 12
1.50
1.00
0.50
0.00
Time, days
130
2.00
Time, days 1/2
Traveler #17
0.00
2
Time, days 1/2
2.00
0.50
Traveler #16
0.00
6
1.00
Time, days 1/2
% Weight Gain
1.50
1.50
0.00
0
Traveler #14
% Weight Gain
% Weight Gain
2.00
0.50
Time, days 1/2
2.00
1.00
0.00
0
Traveler #13
1.50
% Weight Gain
2.00
% Weight Gain
1.50
Traveler #95M
2.00
% Weight Gain
2.00
% Weight Gain
% Weight Gain
2.00
Traveler #93M
8
1/2
10
Time, days
8
1/2
10
Traveler #19
Traveler #20
0.50
0.00
1.50
1.00
0.50
0.00
Time, days
10
10
0.50
0.00
8
10 12
Time, days 1/2
10
1.50
1.00
0.50
10 12
1.50
1.00
0.50
10
1/2
1.50
1.00
0.50
0.00
Time, days
131
2.00
Time, days 1/2
Traveler #100
0.00
0
Time, days
2.00
0.00
6
0.50
Traveler #99
% Weight Gain
1.00
1.00
Time, days 1/2
Traveler #98
1.50
1.50
0.00
0
2.00
0.50
Time, days 1/2
% Weight Gain
% Weight Gain
1/2
2.00
1.00
0.00
0
Traveler #97
1.50
% Weight Gain
2.00
% Weight Gain
1.00
% Weight Gain
1.50
Traveler #23
2.00
2.00
% Weight Gain
% Weight Gain
2.00
Traveler #22
10 12
1/2
Time, days
10 12
1/2
Traveler #101
Traveler #102
1.00
0.50
0.00
1.50
1.00
0.50
0.00
10 12
10 12
1.00
0.50
0.00
8
Time, days
10 12
1/2
10 12
1.50
1.00
0.50
Time, days
10 12
1.50
1.00
0.50
10 12
1.50
1.00
0.50
0.00
Time, days
132
2.00
1/2
Traveler #108
0.00
2
Time, days 1/2
2.00
0.50
Traveler #107
0.00
6
1.00
Time, days 1/2
% Weight Gain
1.50
1.50
0.00
0
2.00
% Weight Gain
% Weight Gain
Traveler #106
2.00
0.50
Time, days 1/2
Traveler #105
1.00
0.00
0
Time, days 1/2
1.50
% Weight Gain
2.00
% Weight Gain
1.50
Traveler #104
2.00
% Weight Gain
2.00
% Weight Gain
% Weight Gain
2.00
Traveler #103
10 12
1/2
Time, days
10 12
1/2
Traveler #111M
1.50
1.00
0.50
0.00
1.50
1.00
0.50
0.00
8 10 12
Time, days
Time, days
1.00
0.50
0.00
Time, days
1/2
10
1/2
Time, days
1.50
1.00
0.50
10
Time, days
10 12
1/2
Traveler #29
1.50
1.00
0.50
1.50
1.00
0.50
0.00
Time, days
133
2.00
Time, days 1/2
1/2
0.00
2
0.50
10 12
2.00
1.00
Traveler #28
0.00
8
1.50
0.00
0
% Weight Gain
1.50
0.50
10 12
2.00
1.00
Traveler #26
% Weight Gain
% Weight Gain
1/2
2.00
1.50
0.00
0
Traveler #25
2.00
% Weight Gain
Traveler #115M
2.00
% Weight Gain
2.00
% Weight Gain
% Weight Gain
2.00
Traveler #113M
% Weight Gain
Traveler #109M
8
1/2
10
Time, days
8
1/2
10
Traveler #31
Traveler #32
0.50
0.00
1.50
1.00
0.50
0.00
Time, days
10
Time, days
10
1.00
0.50
Time, days
10 12
1/2
Time, days
1.50
1.00
0.50
10 12
Time, days
10
1/2
Traveler #120
1.50
1.00
0.50
1.50
1.00
0.50
0.00
Time, days
134
2.00
Time, days 1/2
1/2
0.00
2
0.50
10
2.00
1.00
Traveler #119
0.00
0.00
1/2
% Weight Gain
1.50
1.50
0.00
0
2.00
0.50
Traveler #118
% Weight Gain
% Weight Gain
1/2
2.00
1.00
0.00
0
Traveler #117
1.50
% Weight Gain
2.00
% Weight Gain
1.00
% Weight Gain
1.50
Traveler #35
2.00
2.00
% Weight Gain
% Weight Gain
2.00
Traveler #34
10 12
1/2
Time, days
10 12
1/2
APPENDIX C. PHYSICAL TEST RESULTS
135
Summary of Chemical and Physical Tests - Uncured

Material Properties
Material Batch
Uncured
Resin
Content
(%)
Physical
Fiber Prepreg
Areal Volatile
Gel
Resin
Weight Content
Time
Flow
2
(g/m )
(%)
(minutes) (%)
Chemical
IR
HPLC
P1
AF991009
AF991010
AF991011
Grand Average
Requirement
41.5
41.7
41.4
41.5
42 3
194
0.13
190
0.21
193
0.18
192
0.17
193 8 2.0 max
8.0
7.9
9.0
8.3
5 - 25
23.5 scan
23.5
on
23.5
file
23.5
10 min
9.8
10.1
10.4
10.2
DSC
(% Area)
P2 P 3 P4
8.5
8.8
8.9
8.8
5.9
6.4
6.3
6.3
TBD
61.1
59.7
59.8
60.0
P5
14.8
14.9
14.6
14.8
Summary of Chemical and Physical Tests - Cured

Material Properties
Material Batch
Resin
Density
(g/cc)
AF991009
1.267
AF991010
1.267
AF991011
1.266
Grand Average
1.267
Requirement 1.26 0.03
Glass Transition
Temperature
by DMA
(F)
Dry
Wet
290
296
296
294
TBD
264
266
271
267
TBD *
* FAA Recommended Hot/Wet Tg: 230F, Based on Maximum Operation Temperature of 180F + 50F
136
(F)
Onset Peak
280
329
279
330
280
331
280
330
TBD TBD

Material Properties, Batch AF991009
Autoclave
Cured
Cure
Laminate Fiber Resin
Void
Ply
Run
Density Volume Volume Content Thickness
ID
(g/cc) (%vol) (%vol) (%vol)
(in.)
-
Batch No./
Panel ID
Test
Type
AF991009
A1-910-056
A2-910-056
B1-910-056
B2-910-056
A1-910-056
A2-910-056
0 Tens
0 Tens
0 Tens
0 Tens
90 Tens
90 Tens
1.520
1.515
1.500
1.498
1.497
1.505
54.5
51.2
49.6
48.5
51.4
52.2
42.9
47.2
48.3
49.6
45.6
45.0
2.54
1.54
2.11
1.82
3.04
2.75
0.0086
0.0085
0.0087
0.0085
0.0086
0.0086
99-595
99-595
99-596
99-596
99-595
99-595
B1-910-056 90 Tens
1.501
53.2
43.3
3.52
0.0086
99-596
B2-910-056 90 Tens
A1-910-056 0 Comp
A2-910-056 0Comp
B1-910-056 0Comp
B2-910-056 0Comp
A1-910-056 90Comp
A2-910-056 90Comp
B1-910-056 90Comp
B2-910-056 90Comp
A1-910-056
IPS
B1-910-056
IPS
A1-910-056 ILSS
B1-910-056 ILSS
Average
Standard Deviation
COV, %
Requirement
1.505
1.491
1.497
1.506
1.494
1.503
1.484
1.496
1.496
1.497
1.505
1.489
1.543
1.502
0.013
0.85
TBD
47.6
46.8
49.7
48.5
48.2
48.3
48.3
49.1
50.3
49.3
49.6
47.3
53.2
49.8
2.1
4.30
TBD
50.3
51.6
47.9
50.4
49.9
50.3
49.0
48.7
47.1
48.5
48.7
50.4
46.3
48.1
2.4
5.02
TBD
1.30
1.62
2.36
1.13
1.94
1.36
2.77
2.21
2.67
2.18
1.70
2.34
0.47
2.07
0.73
35.09
TBD
0.0086
0.0086
0.0086
0.0086
0.0086
0.0086
0.0086
0.0086
0.0087
0.0087
0.0086
0.0086
0.0082
0.0086
0.0001
1.08
TBD
99-598
99-595
99-595
99-598
99-598
99-597
99-597
99-598
99-598
99-597
99-596
99-601
99-600
-
137

Cured
Void
Ply
(in.)
Autoclave
Cure
Run
ID
-
Batch No./
Panel ID
Test
Type
AF991010
A1-910-057
A2-910-057
B1-910-057
B2-910-057
A1-910-057
A2-910-057
0 Tens
0 Tens
0 Tens
0 Tens
90 Tens
90 Tens
1.488
1.481
1.486
1.498
1.491
1.500
47.8
47.4
47.7
49.1
50.9
51.0
49.6
49.7
49.6
48.6
45.5
46.0
2.55
2.94
2.71
2.35
3.63
2.93
0.0085
0.0086
0.0086
0.0086
0.0086
0.0086
99-626
99-626
99-627
99-627
99-629
99-629
B1-910-057 90 Tens
1.514
52.3
45.4
2.37
0.0085
99-627
B2-910-057 90 Tens
A1-910-057 0 Comp
A2-910-057 0Comp
B1-910-057 0Comp
B2-910-057 0Comp
A1-910-057 90Comp
A2-910-057 90Comp
B1-910-057 90Comp
B2-910-057 90Comp
A1-910-057
IPS
B1-910-057
IPS
A1-910-057 ILSS
B1-910-057 ILSS
Average
Standard Deviation
COV, %
Requirement
1.506
1.499
1.496
1.510
1.504
1.495
1.497
1.485
1.493
1.484
1.501
1.494
1.501
1.496
0.009
0.59
TBD
49.5
50.2
50.6
50.3
50.8
50.2
49.9
49.2
47.9
47.9
49.3
48.0
48.7
49.4
1.4
2.76
TBD
48.6
47.1
46.3
47.9
46.7
46.8
47.4
47.4
49.8
49.2
48.5
49.8
49.3
48.0
1.5
3.14
TBD
1.86
2.69
3.08
1.86
2.54
3.05
2.75
3.41
2.24
2.90
2.19
2.21
1.95
2.61
0.49
18.84
TBD
0.0085
0.0085
0.0086
0.0085
0.0085
0.0085
0.0086
0.0085
0.0085
0.0086
0.0086
0.0086
0.0087
0.0086
0.0000
0.54
TBD
99-627
99-624
99-624
99-625
99-625
99-624
99-624
99-625
99-625
99-629
99-628
99-624
99-625
-
138

Cured
Void
Ply
(in.)
Autoclave
Cure
Run
ID
-
Batch No./
Panel ID
Test
Type
AF991011
A1-910-058
A2-910-058
B1-910-058
B2-910-058
A1-910-058
A2-910-058
0 Tens
0 Tens
0 Tens
0 Tens
90 Tens
90 Tens
1.512
1.514
1.522
1.521
1.502
1.510
49.1
49.0
50.8
51.3
48.7
50.5
49.7
50.0
48.1
47.4
49.5
47.5
1.19
1.06
1.13
1.38
1.84
1.95
0.0086
0.0085
0.0085
0.0085
0.0085
0.0085
99-633
99-633
99-637
99-637
99-633
99-633
B1-910-058 90 Tens
1.497
49.0
48.7
2.34
0.0085
99-630
B2-910-058 90 Tens
A1-910-058 0 Comp
A2-910-058 0Comp
B1-910-058 0Comp
B2-910-058 0Comp
A1-910-058 90Comp
A2-910-058 90Comp
B1-910-058 90Comp
B2-910-058 90Comp
A1-910-058
IPS
B1-910-058
IPS
A1-910-058 ILSS
B1-910-058 ILSS
Average
Standard Deviation
COV, %
Requirement
1.509
1.509
1.498
1.506
1.498
1.489
1.492
1.501
1.508
1.499
1.508
1.500
1.497
1.505
0.009
0.59
TBD
51.3
51.7
49.6
50.2
49.5
47.8
49.4
49.7
49.8
48.4
50.9
50.9
47.0
49.7
1.2
2.49
TBD
46.3
45.7
47.8
47.6
48.0
49.6
47.6
48.0
48.3
49.6
46.9
46.2
51.5
48.2
1.4
3.01
TBD
2.36
2.57
2.56
2.20
2.51
2.55
2.95
2.35
1.83
1.97
2.27
2.91
1.50
2.07
0.58
27.81
TBD
0.0086
0.0085
0.0085
0.0087
0.0087
0.0086
0.0086
0.0086
0.0085
0.0085
0.0085
0.0086
0.0087
0.0086
0.0001
0.76
TBD
99-630
99-631
99-631
99-630
99-630
99-631
99-631
99-630
99-630
99-636
99-637
99-631
99-639
-
139
COMPANY :
MATERIAL SYSTEM :
Toray Composites
DMA Results -- Onset Storage Modulus

DRY
WET
As Fabricated
Tg [C]
142.5
144.0
143.5
148.0
146.5
146.0
144.0
148.0
147.5
Tg [F]
288.5
291.2
290.3
298.4
295.7
294.8
291.2
298.4
297.5
Moisture Equilibrium at 85% RH

Sample #
Tg [C]
Tg [F]
A-1-910-056-4
129.0
264.2
A-1-910-056-5
129.5
265.1
A-1-910-056-6
128.5
263.3
A-1-910-057-4
130.0
266.0
A-1-910-057-5
129.0
264.2
A-1-910-057-6
130.5
266.9
A-1-910-058-4
133.0
271.4
A-1-910-058-5
132.5
270.5
A-1-910-058-6
132.0
269.6
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
294.00
3.78
1.28
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
Sample #
A-1-910-056-1
A-1-910-056-2
A-1-910-056-3
A-1-910-057-1
A-1-910-057-2
A-1-910-057-3
A-1-910-058-1
A-1-910-058-2
A-1-910-058-3
266.80
3.00
1.12
DMA Results - Peak Tan Delta

DRY
WET
As Fabricated
Tg [C]
193.5
196.0
192.5
198.0
198.0
190.5
198.0
197.5
198.0
Tg [F]
380.3
384.8
378.5
388.4
388.4
374.9
388.4
387.5
388.4

Sample #
Tg [C]
Tg [F]
A-1-910-056-4
151.0
303.8
A-1-910-056-5
151.0
303.8
A-1-910-056-6
149.0
300.2
A-1-910-057-4
152.0
305.6
A-1-910-057-5
151.5
304.7
A-1-910-057-6
152.5
306.5
A-1-910-058-4
154.0
309.2
A-1-910-058-5
150.5
302.9
A-1-910-058-6
153.5
308.3
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
384.40
5.19
1.35
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
Sample #
A-1-910-056-1
A-1-910-056-2
A-1-910-056-3
A-1-910-057-1
A-1-910-057-2
A-1-910-057-3
A-1-910-058-1
A-1-910-058-2
A-1-910-058-3
305.00
2.77
0.91
DMA Results -- Peak of Loss Modulus

DRY
WET
As Fabricated
Tg [C]
178.0
186.5
177.5
185.5
186.0
185.5
185.5
188.5
186.0
Tg [F]
352.4
367.7
351.5
365.9
366.8
365.9
365.9
371.3
366.8

Sample #
Tg [C]
Tg [F]
A-1-910-056-4
143.0
289.4
A-1-910-056-5
143.5
290.3
A-1-910-056-6
141.0
285.8
A-1-910-057-4
144.5
292.1
A-1-910-057-5
144.0
291.2
A-1-910-057-6
145.0
293.0
A-1-910-058-4
145.5
293.9
A-1-910-058-5
142.5
288.5
A-1-910-058-6
145.0
293.0
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
363.80
6.93
1.90
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
Sample #
A-1-910-056-1
A-1-910-056-2
A-1-910-056-3
A-1-910-057-1
A-1-910-057-2
A-1-910-057-3
A-1-910-058-1
A-1-910-058-2
A-1-910-058-3
140
290.80
2.59
0.89
141
142
143
144
145
146
147
148
149
150
151
152
153
154
155
156
157
158
159
160
APPENDIX D. STATISTICAL ANALYSIS SUMMARY
161
COMPANY
Toray
MATERIAL
PROPERTY
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
RTD
ETD
ETW
Sample Size
18
18
18
No. of Batches
Mean
747.203
708.869
668.465
472.915
Std.dev
51.276
56.467
58.548
43.159
% Co. Variation
6.862
7.966
8.759
9.126
Minimum
701.885
593.713
580.651
394.658
Maximum
844.971
782.660
774.079
531.983
Kb
2.028
1.758
1.758
1.758
Ka
3.163
2.925
2.925
2.925
Equal C.V. Basis Values

B-Basis Value
621.925
605.822
571.291
404.168
A-Basis Value
551.760
537.415
506.784
358.531
Anderson Darling Test for Normality

O.S.L
Normality is
0.131
0.236
0.314
0.539
Acceptable
Acceptable
Acceptable
Acceptable
O.S.L for pooled data is
0.3941
Normality is Acceptable
Check for Normality based on Normal Scores

r
Normality is
0.880
0.975
0.981
0.986
Questionable
Acceptable
Acceptable
Acceptable
0.9930
r for pooled data is
k-sample Anderson Darling Test ( ADK < ADC for batches from same population)
ADK
1.565
1.179
1.520
1.200
ADC
2.105
1.501
1.501
1.501
YES
YES
NO
YES
SAME POPULATION
N/A
Equality of Coeff. of Variations: Pooled Data ( F CALCULATED < FCRITICAL for equality )
LEVEL
0.05
0.77
0.025
0.01
F CALCULATED
F
2.929
3.524
4.323
CRITICAL
COMMENTS
OUTLIERS EXIST! BASIS VALUES INVALID, Dispose Outliers & rerun Analysis
162
COMPANY
Toray
MATERIAL
PROPERTY
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
RTD
ETD
ETW
Sample Size
18
18
18
No. of Batches
Mean
749.955
708.742
664.143
474.854
Std.dev
51.465
57.768
58.129
45.123
% Co. Variation
6.862
8.151
8.753
9.502
Minimum
704.469
589.686
573.899
396.111
Maximum
848.082
780.970
765.078
539.716
Kb
2.028
1.758
1.758
1.758
Ka
3.163
2.925
2.925
2.925

B-Basis Value
621.623
603.589
565.607
404.402
A-Basis Value
549.748
533.785
500.195
357.633

O.S.L
Normality is
0.131
0.164
0.371
0.543
Acceptable
Acceptable
Acceptable
Acceptable
0.3877

r
Normality is
0.880
0.970
0.984
0.988
Questionable
Acceptable
Acceptable
Acceptable
0.9928
ADK
1.565
1.142
1.489
1.200
ADC
2.105
1.501
1.501
1.501
YES
YES
YES
YES
SAME POPULATION
N/A
LEVEL
0.05
0.96
0.025
0.01
F CALCULATED
F
2.929
3.524
4.323
CRITICAL
COMMENTS
163
COMPANY
Toray
MATERIAL
PROPERTY
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
RTD
ETD
ETW
Sample Size
18
18
18
No. of Batches
Mean
802.874
917.599
968.984
1051.949
Std.dev
37.896
42.177
41.099
30.909
% Co. Variation
4.720
4.596
4.241
2.938
Minimum
752.490
842.606
880.860
1002.461
Maximum
843.194
998.737
1015.816
1106.526
Kb
2.028
1.758
1.758
1.758
Ka
3.163
2.925
2.925
2.925

B-Basis Value
738.480
853.790
901.601
978.797
A-Basis Value
702.415
811.431
856.870
930.236

O.S.L
Normality is
0.531
0.560
0.026
0.429
Acceptable
Acceptable
Acceptable
Acceptable
0.1025

r
Normality is
0.968
0.989
0.951
0.982
Acceptable
Acceptable
Acceptable
Acceptable
0.9896
ADK
0.470
0.890
1.504
1.296
ADC
2.105
1.501
1.501
1.501
YES
YES
NO
YES
SAME POPULATION
N/A
LEVEL
0.05
1.19
0.025
0.01
F CALCULATED
F
2.929
3.524
4.323
CRITICAL
COMMENTS
164
COMPANY
Toray
MATERIAL
PROPERTY
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
RTD
ETD
ETW
Sample Size
18
18
18
No. of Batches
Mean
803.236
912.052
964.970
1049.137
Std.dev
37.526
40.079
44.067
31.952
% Co. Variation
4.672
4.394
4.567
3.046
Minimum
756.865
846.883
864.643
1003.433
Maximum
848.175
994.092
1014.012
1109.689
Kb
2.028
1.758
1.758
1.758
Ka
3.163
2.925
2.925
2.925

B-Basis Value
737.897
847.726
896.912
975.143
A-Basis Value
701.302
805.025
851.733
926.023

O.S.L
Normality is
0.626
0.614
0.033
0.469
Acceptable
Acceptable
Acceptable
Acceptable
0.2087

r
Normality is
0.980
0.989
0.948
0.984
Acceptable
Acceptable
Acceptable
Acceptable
0.9901
ADK
0.470
0.973
0.919
1.169
ADC
2.105
1.501
1.501
1.501
YES
YES
YES
YES
SAME POPULATION
N/A
LEVEL
0.05
1.11
0.025
0.01
F CALCULATED
F
2.929
3.524
4.323
CRITICAL
COMMENTS
165
COMPANY
Toray
MATERIAL
PROPERTY
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
RTD
ETD
ETW
Sample Size
18
18
18
No. of Batches
Mean
744.535
702.974
649.439
479.913
Std.dev
73.620
36.981
40.100
25.188
% Co. Variation
9.888
5.261
6.175
5.249
Minimum
636.880
638.979
556.310
435.238
Maximum
831.167
774.590
707.857
523.323
Kb
2.028
1.758
1.758
1.758
Ka
3.163
2.925
2.925
2.925

B-Basis Value
654.992
629.671
581.719
429.870
A-Basis Value
604.841
581.010
536.764
396.650

O.S.L
Normality is
0.738
0.352
0.416
0.710
Acceptable
Acceptable
Acceptable
Acceptable
0.6440

r
Normality is
0.988
0.985
0.976
0.994
Acceptable
Acceptable
Acceptable
Acceptable
0.9940
ADK
1.565
1.317
1.227
1.362
ADC
2.105
1.501
1.501
1.501
YES
YES
YES
YES
SAME POPULATION
N/A
LEVEL
0.05
1.93
0.025
0.01
F CALCULATED
F
2.929
3.524
4.323
CRITICAL
COMMENTS
166
COMPANY
Toray
MATERIAL
PROPERTY
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
RTD
ETD
ETW
Sample Size
18
18
18
No. of Batches
Mean
741.866
698.158
645.694
478.702
Std.dev
73.356
36.083
39.442
24.823
% Co. Variation
9.888
5.168
6.108
5.185
Minimum
634.596
640.837
555.232
433.678
Maximum
828.187
765.583
703.056
519.773
Kb
2.028
1.758
1.758
1.758
Ka
3.163
2.925
2.925
2.925

B-Basis Value
653.537
626.087
579.039
429.285
A-Basis Value
604.067
578.243
534.790
396.481

O.S.L
Normality is
0.738
0.474
0.479
0.625
Acceptable
Acceptable
Acceptable
Acceptable
0.6505

r
Normality is
0.988
0.987
0.978
0.991
Acceptable
Acceptable
Acceptable
Acceptable
0.9940
ADK
1.565
1.287
1.227
1.294
ADC
2.105
1.501
1.501
1.501
YES
YES
YES
YES
SAME POPULATION
N/A
LEVEL
0.05
2.04
0.025
0.01
F CALCULATED
F
2.929
3.524
4.323
CRITICAL
COMMENTS
167
COMPANY
Toray
MATERIAL
PROPERTY
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
RTD
ETD
ETW
Sample Size
18
18
18
No. of Batches
Mean
718.773
775.382
838.774
893.055
Std.dev
19.586
58.245
65.356
68.559
% Co. Variation
2.725
7.512
7.792
7.677
Minimum
688.155
687.602
728.125
759.543
Maximum
742.458
858.027
942.857
1004.365
Kb
2.028
1.758
1.758
1.758
Ka
3.163
2.925
2.925
2.925

B-Basis Value
614.325
677.690
733.095
780.537
A-Basis Value
555.826
612.839
662.941
705.844

O.S.L
Normality is
0.686
0.062
0.228
0.265
Acceptable
Acceptable
Acceptable
Acceptable
0.5273

r
Normality is
0.979
0.967
0.976
0.979
Acceptable
Acceptable
Acceptable
Acceptable
0.9943
ADK
1.565
1.467
1.916
1.967
ADC
2.105
1.501
1.501
1.501
YES
YES
NO
NO
SAME POPULATION
N/A
LEVEL
0.05
1.83
0.025
0.01
F CALCULATED
F
2.929
3.524
4.323
CRITICAL
COMMENTS
168
COMPANY
Toray
MATERIAL
PROPERTY
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
RTD
ETD
ETW
Sample Size
18
18
18
No. of Batches
Mean
722.602
771.977
833.734
892.276
Std.dev
20.145
56.806
65.826
70.336
% Co. Variation
2.788
7.359
7.895
7.883
Minimum
696.157
688.601
722.975
752.772
Maximum
746.775
852.207
943.274
1008.063
Kb
2.028
1.758
1.758
1.758
Ka
3.163
2.925
2.925
2.925

B-Basis Value
616.820
673.994
727.913
779.024
A-Basis Value
557.575
608.950
657.665
703.844

O.S.L
Normality is
0.622
0.092
0.359
0.268
Acceptable
Acceptable
Acceptable
Acceptable
0.5816

r
Normality is
0.978
0.970
0.983
0.978
Acceptable
Acceptable
Acceptable
Acceptable
0.9953
ADK
1.565
1.702
1.886
2.009
ADC
2.105
1.501
1.501
1.501
YES
NO
NO
NO
SAME POPULATION
N/A
LEVEL
0.05
1.64
0.025
0.01
F CALCULATED
F
2.929
3.524
4.323
CRITICAL
COMMENTS
169
COMPANY
Toray
MATERIAL
PROPERTY
In-Plane Shear
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
RTD
ETD
ETW
Sample Size
18
18
18
No. of Batches
154.888
132.570
106.206
74.569
Std.dev
8.994
4.873
2.904
2.136
% Co. Variation
5.806
3.676
2.735
2.865
Minimum
140.140
119.133
99.529
68.150
Maximum
164.811
139.524
110.741
77.954
Kb
2.028
1.758
1.758
1.758
Ka
3.163
2.925
2.925
2.925
Mean

B-Basis Value
144.345
124.746
99.938
70.168
A-Basis Value
138.440
119.552
95.777
67.247

O.S.L
Normality is
0.343
0.073
0.496
0.072
Acceptable
Acceptable
Acceptable
Acceptable
0.0108

r
Normality is
0.941
0.939
0.978
0.922
Acceptable
Acceptable
Acceptable
Acceptable
0.9642
ADK
0.470
0.764
0.668
1.165
ADC
2.105
1.501
1.501
1.501
YES
YES
YES
YES
SAME POPULATION
N/A
LEVEL
0.05
1.21
0.025
0.01
F CALCULATED
F
2.929
3.524
4.323
CRITICAL
COMMENTS
170
COMPANY
Toray
MATERIAL
PROPERTY
Apparent Interlaminar Shear
COMMENTS
DATE
December 23, 2002
DATA SUMMARY
TEST CONDITION
STATISTIC
CTD
Sample Size
RTD
ETD
ETW
149
No. of Batches
14
Mean
59.935
Std.dev
3.124
% Co. Variation
5.213
Minimum
52.403
Maximum
68.707
Kb
1.478
Ka
2.613

B-Basis Value
55.317
A-Basis Value
51.771

O.S.L
0.489
Normality is
Acceptable
0.4893

r
0.987
Normality is
Acceptable
0.9869
ADK
2.110
ADC
SAME POPULATION
1.364
N/A
NO
N/A
N/A
N/A
LEVEL
F CALCULATED
F
0.05
N/A*
0.025
0.01
CRITICAL
COMMENTS
*. Number of test conditions < 2, equality of c.v not applicable
N/A*
171
APPENDIX E. METHOD FOR TRANSFORMING VARIANCES OF TEST

SAMPLES (SUPPLEMENT TO DOT/FAA/AR-47/00)
172
The following Appendix describes a procedure to supplement the process described

in DOT/FAA/AR-47/00 for the case in which the variances are found to be unequal
per section 5.3.1.3 of that document. A supplemental is given below which provides
guidance in the situation of unequal variances and describes procedures to obtain a
conservative design allowable. Note that these procedures must be combined with
engineering judgment and that the failure modes must remain the same across
environments.
The follow excerpt is taken from DOT/FAA/AR-47/00, section 5.3.1.3 and is used as
the basis for this procedure:
In general, a coefficient of variation between 4% and 10% is typical of
composite materials. Experiences with large data sets have shown that this
range is representative of most composite material systems. Lower
coefficients of variation may be caused by the specimen fabrication and
testing by a single laboratory while higher coefficients may point to lack of
material and processing control. In cases where the coefficients of variation
of the pooled data set are higher or lower than this range, the reason for the
higher or lower coefficient of variation should be investigated before
determining design allowable values from the pooled data set. For the
coefficient of variation lower than 4%, an assigned value of 4% may be
considered as an alternative engineering solution.
Using this philosophy, the data in this report, which demonstrates unequal variances
per section 5.3.1.3 of DOT/FAA/AR-47/00 will be modified by the supplemental
procedure described in this appendix with the revised presented below. The
coefficient of variation to be used in this case will be 4% as suggested by
DOT/FAA/AR-47/00.
173
Check Equality of Variance per

section 5.3.1.3
NO
Variance
Equal ?
Using "engineering judgement",

assess the degree of inequality using
= 0.05, 0.025 and 0.01
ACCEPTABLE
YES
QUESTIONABLE
Identify dataset problem looking at

Coefficients of Variations (CV)
HIGH CV
LOW CV
analyze "problem" dataset using

procedure per supplemental section
5.3.1.4 - substitute with modified
dataset
Proceed with analysis as presented in

section 5.3.1
Use A and B basis allowables as

generated
Figure E.1. Procedures to obtain design allowables in the case of variance

inequality
174
A simple procedure for modifying the variance of a test sample to any desired value
is presented. This procedure is useful in the case in which an environmental pooled
dataset does not pass the equality of variance test per section 5.3.1.3 of
DOT/FAA/AR-47/00. Consider a test sample xi of n specimens with an average
value of x . Let the variance of this sample be CV which is given by
n
CV =
(x
i =1
x)
eq. 1
n 1
Let the desired variance of the sample be CV * . Consider a transformation of the

form
xi* = xi + (xi )
eq. 2
where xi* is the transformed data, is a constant and ( x i ) is a weighting function.

Let the weighting function be
(xi ) = (xi x)
eq. 3
The new variance for the transformed data is then given by
(x
n
CV * =
i =1
*
i
x*
eq. 4
n 1
where x * is the average value of the transformed sample. Substituting equations (2)
and (3) into equation (4) we obtain
[{x + (x x )} x ]
n
CV * =
i =1
* 2
n 1
If we further let x * = x , equation (5) reduces to
175
eq. 5
CV * =
(1 + )2 ( xi x )2
i =1
eq. 6
n 1
which gives
CV *
=
1
CV
eq. 7
Thus, a sample with a known variance CV can be transformed using equation (2) to
obtain the desired variance CV*. The constant for transformation , can be
calculated using equation (7).
For example, consider a typical test sample of size n=10 with an average value of
146.27 and a corresponding CV of 0.0184 as shown in the table E.1. The sample is
transformed as per the previous discussions to obtain a transformed sample with a
CV* of 0.04 (desired value). The transformation is illustrated using a probability of
survival plot shown in Figure E.2. It can be observed that the original normal curve
has been rotated and stretched due to the transformation.
Table E.1: A typical data sample and transformed data.
i
xi
xi x
x*i
1
2
3
4
5
6
7
8
9
10
142.3
143.2
144.1
144.8
145.9
146.8
147.5
148.2
149.6
150.3
-3.97
-3.07
-2.17
-1.47
-0.37
0.53
1.23
1.93
3.33
4.03
137.63
139.59
141.55
143.07
145.46
147.42
148.95
150.47
153.52
155.04
146.27
CV
0.0184
x*
CV*
0 .040
1 = 1.174
0. 0184
146.27
0.040
In order to further investigate the effects of the above transformation on

normality of the data, the Anderson- Darling test for normality was conducted
both the original and transformed data. The test indicated no change in
Observed Significance Level (O.S.L = 0.758) for both the samples. Thus,
176
the
for
the
the
transformation not only maintains the average value of the sample but also retains
the normality of the sample.
1
ORIGINAL DATA
TRANSFORMED DATA
PROBABIL ITY OF SURVIVAL
0.8
0.6
0.4
( xi x )
0.2
0
130
140
150
160
PROPERTY
Figure E.2: Original and transformed data points
Once this sample has been transformed to the desired coefficient of variation, it may
replaced and the data analyzed per the method described in section 5.3.1 of
DOT/FAA/AR-47/00. It should be noted that this replacement is only for the
calculation of basis values and the original data should be retained for all follow-on
testing concerning material equivalence and acceptance.
177
APPENDIX F. RAW TESTING SUMMARIES

[Raw test sheets report data in US units only. Please refer to Section 3 for data in SI units]
178
0 (Warp) Tension Properties, -65F (Dry)
Material Type: F6273C-07M

Batch Number: AF991009
Test Method: ASTM D3039
Test Operator: Bryan Mines

Test Frame: I
Test Speed: 0.05 in/min
Control Mode: Stroke
Strain Gage: One biaxial gage (CEA-06-125UT-350)
Specimen Preconditioning: as machined

Test Conditions: -65F/Dry
Ply Orientation: (warp)12
Testing Facility: Intec
Test Date: 12/29/99, 2/23/00
Specimen
Number
Specimen
Thickness
A1-910-056-1-7
A2-910-056-1-7
B1-910-056-1-7
B2-910-056-1-7
A2-910-056-1-8
B2-910-056-1-8
Average
Std. Dev.
COV, %
(in.)
0.1026
0.1030
0.1035
0.1039
0.1027
0.1038
0.1033
0.0006
0.54
Specimen Ultimate
Width
Tensile
Load
(in.)
(lbs.)
1.0010
12560
1.0020
11460
1.0010
12180
0.9980
12670
1.0000
11960
1.0010
11340
1.0005
12028
0.0014
551
0.14
4.58
CPT (batch average):

Fiber Volume(batch average):
Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
122
122
111
111
118
118
122
123
116
116
109
110
116
116
5.5
5.4
4.72
4.67
Load @
0.1%
Strain
(lbs.)
839.2
768.4
845.3
802.0
-
179
Load @
0.3%
Strain
(lbs.)
2631
2423
2497
2537
-
0.0086 in.
49.8%
Tensile Modulus
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.68
8.63
8.02
8.00
8.12
8.14
8.31
8.37
8.28
8.29
0.29
0.27
3.51
3.30
Poisson's
Failure Location
Ratio
&
(0.1-0.3%)
Comments
strain)
0.110
Lateral failure under tab
0.070
Lateral failure at tab
0.090
Lateral failure in gage
0.070
Lateral failure under tab
Tensile failure inside/end of tab
Tensile failure inside/end of tab
0.085
0.019
22.53
0 (Warp) Tension Properties, 75F (Dry)

Test Operator: John Smith
Test Frame: Instron 4505
Test Conditions: RT/Dry
Ply Orientation: (warp) 12

Testing Facility: Toray Composites (America)
Test Date: 1/1/2000, 2/14/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-1
A2-910-056-1-1
B1-910-056-1-1
B2-910-056-1-1
A1-910-056-1-6
B1-910-056-1-6
Average
Std. Dev.
COV, %
(in.)
0.1027
0.1023
0.1033
0.0999
0.1027
0.1051
0.1027
0.0017
1.66
(in.)
1.0010
1.0011
0.9997
0.9983
0.9980
0.9971
0.9992
0.0017
0.17
Ultimate
Tensile
Load
(lbs.)
13880
12690
13500
13460
14850
12810
13532
787
5.81
0.0086 in.
Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
135
134
124
123
131
131
135
131
145
144
122
124
132
131
8.3
7.7
6.31
5.84
Load @
0.1%
Strain
(lbs.)
895.2
807.7
838.3
825.8
-
Load @
0.3%
Strain
(lbs.)
2523
2451
2461
2471
-
49.8%
Tensile Modulus
(0.1-0.3% strain)
Actual Norm.
(msi)
(msi)
7.92
7.88
8.02
7.95
7.86
7.86
8.25
7.98
8.01
7.92
0.17
0.06
2.17
0.73
Poisson's
Ratio
(0.1-0.3%)
strain)
0.025
0.015
0.020
0.040
0.025
0.011
43.20
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area

Test Date: 1/1/2000, 2/14/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-1
A2-910-057-1-1
B1-910-057-1-1
B2-910-057-1-1
A1-910-057-1-6
B1-910-057-1-6
Average
Std. Dev.
COV, %
(in.)
0.1025
0.1025
0.1026
0.1033
0.1029
0.1025
0.1027
0.0003
0.30
(in.)
1.0010
1.0013
1.0014
1.0014
1.0011
1.0010
1.0012
0.0002
0.02
Ultimate
Tensile
Load
(lbs.)
13770
14130
14060
13380
13550
13120
13668
394
2.88

Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
134
133
138
137
137
136
129
129
132
131
128
127
133
132
4.0
3.8
2.99
2.87
Load @
0.1%
Strain
(lbs.)
882.0
849.4
920.2
863.7
-
Test Date: 1/1/2000, 2/14/00
(in.)
1.0009
1.0013
1.0013
1.0013
0.9981
0.9972
1.0000
0.0019
0.19
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area

(in.)
0.1027
0.1024
0.1017
0.1016
0.1031
0.1029
0.1024
0.0006
0.60
Failure
Failure
Failure
Failure
Failure
Failure
A1-910-058-1-7
A2-910-058-1-7
B1-910-058-1-7
B2-910-058-1-7
A1-910-058-1-6
B1-910-058-1-6
Average
Std. Dev.
COV, %
Failure Location
&
Comments
Specimen
Width
Poisson's
Ratio
(0.1-0.3%)
strain)
0.025
0.040
0.045
0.025
0.034
0.010
30.54
Specimen
Thickness
Tensile Modulus
(0.1-0.3% strain)
Actual Norm.
(msi)
(msi)
8.21
8.16
8.15
8.10
8.30
8.25
8.12
8.12
8.20
8.16
0.08
0.07
0.98
0.84
Specimen
Number
Load @
0.3%
Strain
(lbs.)
2568
2523
2626
2542
-
0.0086 in.
49.4%
Ultimate
Tensile
Load
(lbs.)
14170
13980
14440
12820
14070
13080
13760
651
4.73
Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
138
137
136
135
142
140
126
124
137
137
128
127
134
133
6.2
6.2
4.61
4.69
Load @
0.1%
Strain
(lbs.)
841.0
916.6
894.7
992.5
-
180
Load @
0.3%
Strain
(lbs.)
2451
2613
2539
2809
-
0.0086 in.
49.7%
Tensile Modulus
(0.1-0.3% strain)
Actual Norm.
(msi)
(msi)
7.83
7.79
8.27
8.21
8.07
7.96
8.93
8.79
8.28
8.19
0.47
0.44
5.70
5.33
Poisson's
Ratio
(0.1-0.3%)
strain)
0.050
0.135
0.045
0.035
0.066
0.046
69.82
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
0 (Warp) Tension Properties, 180F (Dry)


Test Conditions: 180F/Dry


Test Date: 1/1/2000, 2/22/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-2
A2-910-056-1-2
B1-910-056-1-2
B2-910-056-1-2
A2-910-056-1-6
B2-910-056-1-6
Average
Std. Dev.
COV, %
(in.)
0.1030
0.1027
0.1040
0.1010
0.1053
0.1041
0.1033
0.0015
1.42
(in.)
1.0010
1.0016
1.0011
0.9987
0.9983
0.9982
0.9998
0.0016
0.16
Ultimate
Tensile
Load
(lbs.)
14490
14770
14140
13330
15020
15150
14483
673
4.64
0.0086 in.
Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
141
140
144
143
136
137
132
129
143
146
146
147
140
140
5.2
6.6
3.70
4.67
Load @
0.1%
Strain
(lbs.)
849.8
812.6
870.4
912.5
-
Load @
0.3%
Strain
(lbs.)
2457
2461
2490
2569
-
49.8%
Tensile Modulus
(0.1-0.3% strain)
Actual Norm.
(msi)
(msi)
7.80
7.78
8.01
7.97
7.78
7.84
8.21
8.04
7.95
7.91
0.20
0.12
2.56
1.50
Poisson's
Ratio
(0.1-0.3%)
strain)
0.035
0.065
0.035
0.020
0.039
0.019
48.71
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area

Test Date: 1/1/2000, 2/22/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-2
A2-910-057-1-2
B1-910-057-1-2
B2-910-057-1-2
A2-910-057-1-6
B2-910-057-1-6
Average
Std. Dev.
COV, %
(in.)
0.1029
0.1033
0.1033
0.1033
0.1035
0.1032
0.1032
0.0002
0.18
(in.)
1.0012
1.0006
1.0014
1.0015
0.9982
1.0011
1.0007
0.0013
0.13
Ultimate
Tensile
Load
(lbs.)
13590
13970
15030
14860
14940
14080
14412
607
4.21

Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
132
132
135
135
145
145
144
144
145
145
136
136
139
140
5.8
5.9
4.13
4.25
Load @
0.1%
Strain
(lbs.)
1035.0
846.3
896.8
893.2
-
Test Date: 1/1/2000, 2/22/00
(in.)
1.0029
1.0012
1.0009
1.0014
0.9981
0.9988
1.0006
0.0018
0.18
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
(in.)
0.1019
0.1023
0.1007
0.1013
0.1023
0.1017
0.1017
0.0006
0.60
Failure
Failure
Failure
Failure
Failure
Failure

A1-910-058-1-8
A2-910-058-1-8
B1-910-058-1-8
B2-910-058-1-8
A2-910-058-1-6
B2-910-058-1-6
Average
Std. Dev.
COV, %
Failure Location
&
Comments
Specimen
Width
Poisson's
Ratio
(0.1-0.3%)
strain)
0.070
0.025
0.015
0.025
0.034
0.025
72.95
Specimen
Thickness
Tensile Modulus
(0.1-0.3% strain)
Actual Norm.
(msi)
(msi)
9.10
9.07
8.13
8.14
8.37
8.38
8.16
8.17
8.44
8.44
0.45
0.44
5.36
5.18
Specimen
Number
Load @
0.3%
Strain
(lbs.)
2910
2527
2628
2581
-
0.0086 in.
49.4%
Ultimate
Tensile
Load
(lbs.)
14970
14950
14620
12960
15040
14160
14450
800
5.54
Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
146
145
146
145
145
142
128
125
147
146
139
137
142
140
7.5
7.8
5.30
5.55
Load @
0.1%
Strain
(lbs.)
873.4
853.1
845.2
914.4
-
181
Load @
0.3%
Strain
(lbs.)
2554
2434
2489
2608
-
0.0086 in.
49.7%
Tensile Modulus
(0.1-0.3% strain)
Actual Norm.
(msi)
(msi)
8.22
8.12
7.72
7.65
8.15
7.96
8.35
8.19
8.11
7.98
0.27
0.24
3.36
3.02
Poisson's
Ratio
(0.1-0.3%)
strain)
0.045
0.050
0.050
0.005
0.038
0.022
58.12
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
0 (Warp) Tension Properties, 180F (Wet)

Specimen Preconditioning: per Section 3.2 of AGATE Methodology
Test Conditions: 180F

Test Date: 4/28/00, 4/27/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-3
A2-910-056-1-3
B1-910-056-1-3
B2-910-056-1-3
A1-910-056-1-4
B1-910-056-1-4
Average
Std. Dev.
COV, %
(in.)
0.1035
0.1025
0.1040
0.1007
0.1036
0.1047
0.1032
0.0014
1.37
(in.)
0.9984
0.9984
0.9979
1.0010
1.0006
1.0007
0.9995
0.0014
0.14
Ultimate
Tensile
Load
(lbs.)
15420
16420
16160
15070
16620
16060
15958
597
3.74
0.0086 in.
Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
149
150
160
159
156
157
150
146
160
161
153
156
155
155
5.0
5.8
3.22
3.76
Load @
0.1%
Strain
(lbs.)
872.5
873.1
976.0
825.6
-
Load @
0.3%
Strain
(lbs.)
2494
2679
2866
2419
-
49.8%
Tensile Modulus
(0.1-0.3% strain)
Actual Norm.
(msi)
(msi)
7.85
7.87
8.83
8.77
9.11
9.18
7.90
7.71
8.42
8.38
0.64
0.71
7.62
8.42
Poisson's
Ratio
(0.1-0.3%)
strain)
0.029
0.026
0.035
0.033
0.031
0.004
12.60
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area

Test Date: 4/28/00, 4/27/00, 5/3/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-3
A2-910-047-1-3
B1-910-057-1-5
B2-910-057-1-3
A1-910-057-1-4
B1-910-057-1-4
Average
Std. Dev.
COV, %
(in.)
0.1025
0.1034
0.1033
0.1033
0.1018
0.1032
0.1029
0.0006
0.62
(in.)
1.0011
0.9986
1.0016
1.0014
1.0017
1.0014
1.0010
0.0012
0.12
Ultimate
Tensile
Load
(lbs.)
15990
15930
15050
15780
15740
15100
15598
416
2.67

Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
156
155
154
155
145
146
153
153
154
152
146
146
151
151
4.5
4.1
2.97
2.72
Load @
0.1%
Strain
(lbs.)
874.2
882.6
921.5
946.5
-
Fiber Volume(normalizing):
Test Date: 4/28/00, 4/27/00
(in.)
0.1031
0.1023
0.1025
0.1018
0.1032
0.1033
0.1027
0.0006
0.59
(in.)
0.9981
0.9985
0.9987
0.9985
1.0011
1.0014
0.9994
0.0014
0.14
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area

A1-910-058-1-3
A2-910-058-1-3
B1-910-058-1-3
B2-910-058-1-3
A1-910-058-1-4
B1-910-058-1-4
Average
Std. Dev.
COV, %
Failure Location
&
Comments

Specimen
Width
Poisson's
Ratio
(0.1-0.3%)
strain)
0.036
0.029
0.038
0.017
0.030
0.010
32.20
Specimen
Thickness
Tensile Modulus
(0.1-0.3% strain)
Actual Norm.
(msi)
(msi)
8.33
8.27
8.19
8.20
8.59
8.60
8.34
8.35
8.36
8.36
0.17
0.17
2.03
2.09
Specimen
Number
Load @
0.3%
Strain
(lbs.)
2582
2573
2700
2672
-
0.0086 in.
49.4%
Ultimate
Tensile
Load
(lbs.)
15620
15640
16000
15600
15400
15040
15550
316
2.03
Ultimate Tensile
Strength
Actual Norm.
(ksi)
(ksi)
152
152
153
152
156
155
154
151
149
149
145
146
152
151
3.8
3.2
2.52
2.15
Load @
0.1%
Strain
(lbs.)
887.9
972.1
899.2
974.5
-
182
Load @
0.3%
Strain
(lbs.)
2593
2727
2658
2720
-
49.8%
0.0086 in.
49.7%
Tensile Modulus
(0.1-0.3% strain)
Actual Norm.
(msi)
(msi)
8.29
8.28
8.59
8.51
8.59
8.53
8.59
8.47
8.51
8.45
0.15
0.12
1.79
1.40
Poisson's
Ratio
(0.1-0.3%)
strain)
0.028
0.032
0.041
0.011
0.028
0.013
45.50
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
90 (Fill) Tension Properties, -65F (Dry)

Test Operator: Joel Patterson, Bryan Mines

Test Frame: I
Strain Gage: One axial gage (CEA-06-250UW-350)
Ply Orientation: (fill)1 2

Test Date: 12/29/99, 2/23/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-7
A2-910-056-1-7
B1-910-056-1-7
B2-910-056-1-7
A1-910-056-1-8
B1-910-056-1-8
Average
Std. Dev.
COV, %
(in.)
0.1038
0.1044
0.1044
0.1038
0.1029
0.1032
0.1038
0.0006
0.59
(in.)
1.0020
1.0010
1.0000
1.0010
1.0010
1.0000
1.0008
0.0008
0.08
Ultimate
Tensile
Load
(lbs.)
11200
11160
10420
10840
10730
10600
10825
309
2.85
Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
108
108
107
108
100
101
104
105
104
104
103
103
104
105
2.84
2.92
2.72
2.79
Load @
0.1%
Strain
(lbs.)
801
756
843
773
-
183
Load @
0.3%
Strain
(lbs.)
2507
2459
2578
2459
-
0.0086 in.
49.8%
Tensile Modulus
(0.1-0.3% strain)
Actual
(msi)
8.23
7.96
8.18
8.04
8.10
0.12
1.54
Norm.
(msi)
8.28
8.05
8.28
8.09
8.17
0.12
1.47
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
90 (Fill) Tension Properties, 75F (Dry)



Strain Gage: One axial gage (C-960401-A)

Test Date: 12/18/99, 2/14/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-6
A2-910-056-1-1
B1-910-056-1-1
B2-910-056-1-1
A1-910-056-1-9
B1-910-056-1-9
Average
Std. Dev.
COV, %
(in.)
0.1041
0.1007
0.1036
0.1031
0.1024
0.1025
0.1027
0.0012
1.16
(in.)
1.0014
1.0011
1.0015
0.9980
0.9998
0.9996
1.0002
0.0014
0.14
Ultimate
Tensile
Load
(lbs.)
11290
12440
12710
12710
11980
12750
12313
580
4.71
0.0086 in.
Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
108
109
123
120
122
123
124
123
117
116
124
124
120
119
6.25
5.68
5.21
4.76
Load @
0.1%
Strain
(lbs.)
822
861
913
854
-
Load @
0.3%
Strain
(lbs.)
2429
2497
2583
2514
-
49.8%
Tensile Modulus
(0.1-0.3% strain)
Actual
(msi)
7.71
8.12
8.05
8.07
7.99
0.19
2.34
Norm.
(msi)
7.77
7.92
8.08
8.06
7.96
0.14
1.77
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area

Test Date: 12/31/99, 2/14/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-1
A2-910-057-1-1
B1-910-057-1-1
B2-910-057-1-1
A1-910-057-1-6
B1-910-057-1-6
Average
Std. Dev.
COV, %
(in.)
0.1025
0.1023
0.1031
0.1020
0.1034
0.1026
0.1026
0.0005
0.50
(in.)
1.0006
0.9999
1.0011
1.0010
1.0013
1.0007
1.0008
0.0005
0.05
Ultimate
Tensile
Load
(lbs.)
12570
10700
11420
10900
10320
10920
11138
787
7.06

Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
123
122
105
104
111
111
107
106
100
100
106
106
108
108
7.78
7.62
7.17
7.07
Load @
0.1%
Strain
(lbs.)
871
877
875
843
-
Test Date: 1/1/00, 2/14/00
A1-910-058-1-7
A2-910-058-1-7
B1-910-058-1-7
B2-910-058-1-7
A1-910-058-1-6
B1-910-058-1-6
Average
Std. Dev.
COV, %
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
(in.)
1.0005
0.9992
1.0015
1.0015
1.0004
0.9995
1.0004
0.0010
0.10
Failure
Failure
Failure
Failure
Failure
Failure

(in.)
0.1024
0.1017
0.1028
0.1033
0.1039
0.1036
0.1029
0.0008
0.78
Norm.
(msi)
7.78
7.89
7.97
7.78
7.86
0.10
1.21
Specimen
Width
Actual
(msi)
7.83
7.96
7.98
7.87
7.91
0.07
0.89
Failure Location
&
Comments
Specimen
Thickness
Tensile Modulus
(0.1-0.3% strain)
Specimen
Number
Load @
0.3%
Strain
(lbs.)
2477
2506
2522
2451
-
0.0086 in.
49.4%
Ultimate
Tensile
Load
(lbs.)
10480
11590
11200
11100
10660
12340
11228
673
6.00
Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
102
101
114
112
109
108
107
107
103
103
119
120
109
109
6.60
6.58
6.06
6.05
Load @
0.1%
Strain
(lbs.)
877
849
849
873
-
184
Load @
0.3%
Strain
(lbs.)
2534
2470
2502
2489
-
0.0086 in.
49.7%
Tensile Modulus
(0.1-0.3% strain)
Actual
(msi)
8.09
7.98
8.03
7.82
7.98
0.12
1.47
Norm.
(msi)
8.03
7.86
8.00
7.82
7.93
0.10
1.27
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
90 (Fill) Tension Properties, 180F (Dry)




Test Date: 1/4/00, 2/22/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-2
A2-910-056-1-2
B1-910-056-1-2
B2-910-056-1-2
A1-910-056-1-9
B1-910-056-1-9
Average
Std. Dev.
COV, %
(in.)
0.1033
0.1014
0.1024
0.1020
0.1023
0.1037
0.1025
0.0008
0.81
(in.)
1.0015
1.0012
1.0012
1.0006
0.9993
1.0009
1.0008
0.0008
0.08
0.0086 in.
Ultimate
Tensile
Load
(lbs.)
14140
13850
12650
12400
13980
13740
13460
741
5.50
Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
137
137
136
134
123
122
122
120
137
136
132
133
131
130
7.00
7.18
5.33
5.51
Load @
0.1%
Strain
(lbs.)
846
831
914
897
-
Load @
0.3%
Strain
(lbs.)
2463
2425
2563
2552
-
49.8%
Tensile Modulus
(0.1-0.3% strain)
Actual
(msi)
7.82
7.85
8.04
8.11
7.95
0.14
1.80
Norm.
(msi)
7.82
7.71
7.98
8.01
7.88
0.14
1.78
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area

Test Date: 1/4/00, 2/22/00
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-2
A2-910-057-1-2
B1-910-057-1-2
B2-910-057-1-2
B2-910-057-1-6
A2-910-057-1-6
Average
Std. Dev.
COV, %
(in.)
0.1031
0.1025
0.1032
0.1024
0.1032
0.1030
0.1029
0.0004
0.35
(in.)
1.0008
0.9999
1.0011
1.0013
1.0011
1.0001
1.0007
0.0006
0.06
Ultimate
Tensile
Load
(lbs.)
11190
10820
12570
11700
12600
12840
11953
839
7.02

Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
108
108
106
105
122
122
114
113
122
122
125
124
116
116
7.89
8.11
6.80
7.00
Load @
0.1%
Strain
(lbs.)
896
802
861
840
-
Test Date: 1/4/00, 2/22/00
A1-910-058-1-8
A2-910-058-1-8
B1-910-058-1-8
B2-910-058-1-8
A2-910-058-1-6
B2-910-058-1-6
Average
Std. Dev.
COV, %
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
(in.)
0.9975
1.0014
1.0016
0.9994
1.0012
1.0012
1.0004
0.0016
0.16
Failure
Failure
Failure
Failure
Failure
Failure

(in.)
0.1017
0.1027
0.1018
0.1028
0.1017
0.1033
0.1023
0.0007
0.69
Norm.
(msi)
8.07
7.54
7.80
7.87
7.82
0.22
2.84
Specimen
Width
Actual
(msi)
8.08
7.59
7.80
7.93
7.85
0.21
2.66
Failure Location
&
Comments
Specimen
Thickness
Tensile Modulus
(0.1-0.3% strain)
Specimen
Number
Load @
0.3%
Strain
(lbs.)
2564
2357
2473
2467
-
0.0086 in.
49.4%
Ultimate
Tensile
Load
(lbs.)
11190
11550
12170
12540
12040
12800
12048
601
4.99
Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
110
109
112
112
119
118
122
122
118
117
124
124
118
117
5.34
5.74
4.54
4.92
Load @
0.1%
Strain
(lbs.)
848
909
898
840
-
185
Load @
0.3%
Strain
(lbs.)
2449
2574
2582
2475
-
0.0086 in.
49.7%
Tensile Modulus
(0.1-0.3% strain)
Actual
(msi)
7.89
8.09
8.26
7.96
8.05
0.16
2.03
Norm.
(msi)
7.78
8.06
8.15
7.93
7.98
0.16
2.03
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
90 (Fill) Tension Properties, 180F (Wet)




Test Date: 4/27/2000
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-3
A2-910-056-1-3
B1-910-056-1-3
B2-910-056-1-3
A1-910-056-1-4
B1-910-056-1-4
Average
Std. Dev.
COV, %
(in.)
0.1036
0.1031
0.1042
0.1020
0.1040
0.1041
0.1035
0.0009
0.82
(in.)
1.0014
1.0014
1.0012
1.0009
1.0012
1.0007
1.0011
0.0003
0.03
0.0086 in.
Ultimate
Tensile
Load
(lbs.)
15110
13630
13510
13910
14480
13010
13942
749
5.37
Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
146
146
132
132
130
131
136
135
139
140
125
126
135
135
7.39
7.23
5.49
5.36
Load @
0.1%
Strain
(lbs.)
796
883
980
864
-
Load @
0.3%
Strain
(lbs.)
2415
2495
2710
2498
-
49.8%
Tensile Modulus
(0.1-0.3% strain)
Actual
(msi)
7.81
7.81
8.29
8.00
7.98
0.23
2.87
Norm.
(msi)
7.84
7.80
8.37
7.91
7.98
0.27
3.34
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area

Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-3
A2-910-057-1-3
B1-910-057-1-3
B2-910-057-1-3
A1-910-057-1-4
B1-910-057-1-4
Average
Std. Dev.
COV, %
(in.)
0.1031
0.1028
0.1033
0.1028
0.1031
0.1031
0.1030
0.0002
0.20
(in.)
1.0010
1.0000
0.9996
1.0012
0.9983
1.0007
1.0001
0.0011
0.11
Ultimate
Tensile
Load
(lbs.)
13810
13810
14080
14276
14390
13720
14014
277
1.98

Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
134
134
134
134
136
136
139
138
140
140
133
133
136
136
2.77
2.76
2.03
2.03
Load @
0.1%
Strain
(lbs.)
845
837
840
874
-
Test Date: 4/28/2000, 4/27/00
A1-910-058-1-3
A2-910-058-1-3
B1-910-058-1-3
B2-910-058-1-3
A1-910-058-1-4
B1-910-058-1-4
Average
Std. Dev.
COV, %
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
(in.)
1.0002
0.9994
0.9969
1.0016
1.0005
1.0015
1.0000
0.0017
0.17
Failure
Failure
Failure
Failure
Failure
Failure

(in.)
0.1023
0.1014
0.1033
0.1033
0.1036
0.1028
0.1028
0.0008
0.81
Norm.
(msi)
7.68
8.09
7.89
7.89
7.89
0.17
2.14
Specimen
Width
Actual
(msi)
7.69
8.13
7.88
7.92
7.90
0.18
2.30
Failure Location
&
Comments
Specimen
Thickness
Tensile Modulus
(0.1-0.3% strain)
Specimen
Number
Load @
0.3%
Strain
(lbs.)
2432
2508
2468
2504
-
0.0086 in.
49.4%
Ultimate
Tensile
Load
(lbs.)
11270
11590
12940
12120
12130
12720
12128
638
5.26
Ultimate Tensile
Strength
Actual
Norm.
(ksi)
(ksi)
110
109
114
112
126
126
117
117
117
117
124
123
118
118
5.75
6.25
4.87
5.32
Load @
0.1%
Strain
(lbs.)
940
780
820
884
-
186
Load @
0.3%
Strain
(lbs.)
2548
2303
2445
2510
-
0.0086 in.
49.7%
Tensile Modulus
(0.1-0.3% strain)
Actual
(msi)
7.86
7.52
7.89
7.85
7.78
0.17
2.25
Norm.
(msi)
7.79
7.38
7.89
7.86
7.73
0.24
3.06
Failure Location
&
Comments
Failure
Failure
Failure
Failure
Failure
Failure
in
in
in
in
in
in
gage
gage
gage
gage
gage
gage
area
area
area
area
area
area
0 (Warp) Compression Properties, -65F (Dry)

Test Method: SACMA SRM 1-94
Preconditioning: as machined
Testing Facility: TCA

Specimen
Number
A1-910-056-1-4
A1-910-056-1-5
A2-910-056-1-4
B1-910-056-1-4
B2-910-056-1-4
B2-910-056-1-5
Average
Std. Dev.
COV, %
FV(batch average):
Specimen Specimen Ult.

Thickness
Width Comp.
Load
(in.)
(in.)
(kips)
0.1036
0.5000
5.43
0.1036
0.5002
5.27
0.1036
0.5002
5.50
0.1036
0.5000
6.35
0.1036
0.4997
5.69
0.1036
0.4998
5.43
0.1036
0.5000
5.61
0.0000
0.0002
0.38
0.00
0.04
6.86
Strain Gage: N/A

Test Frame: I

FV(normalizing):
Test Operator: Joel Patterson


49.8%
0.0086 in.
49.8%
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
105
105
102
102
106
107
123
123
110
111
105
105
108
109
7.44
7.47
6.86
6.86
Test Date: 12/29/1999
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage

FV(normalizing):
FV(batch average):
Specimen
Number
Specimen Specimen Load @

Thickness
Width
0.1%
Strain
(in.)
(in.)
(lbs.)
A2-910-056-1-6 0.1209
0.4980
686.0
B2-910-056-1-6 0.1209
0.4990
684.7
Average
Std. Dev.
COV, %
187
0.1209
0.0000
0.00
0.4985
0.0007
0.14
49.8%
0.0086 in.
49.8%
Load @
0.3%
Strain
(lbs.)
1628
1649
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.82
7.86
8.00
8.03
7.91
0.12
1.53
7.94
0.12
1.53
0 (Warp) Compression Properties, 75F (Dry)



Loading Rate: 0.05 in/min

Strain Gage: N/A
FV(normalizing):
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-8
A2-910-056-1-5
B1-910-056-1-5
B2-910-056-1-7
B2-910-056-1-8
A1-910-056-1-10
Average
Std. Dev.
COV, %
(in.)
0.1030
0.1030
0.1030
0.1030
0.1030
0.1030
0.1030
0.0000
0.00
(in.)
0.5001
0.5001
0.5000
0.4996
0.4999
0.5002
0.5000
0.0002
0.04

Ult.
Comp.
Load
(kips)
5.06
4.95
5.78
5.41
5.29
4.78
5.21
0.36
6.84

Test Date: 12/27/1999
49.8%
49.8%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage

FV(normalizing):

FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-5
A2-910-057-1-7
A2-910-057-1-8
B1-910-057-1-5
B2-910-057-1-7
B2-910-057-1-8
Average
Std. Dev.
COV, %
(in.)
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.0000
0.00
(in.)
0.4991
0.5019
0.5016
0.5000
0.4998
0.5000
0.5004
0.0011
0.21

Ult.
Comp.
Load
(kips)
4.89
5.68
5.66
5.82
4.58
4.41
5.17
0.62
11.98
49.4%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
FV(normalizing):
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-058-1-4
A1-910-058-1-5
A2-910-058-1-4
B1-910-058-1-4
B1-910-058-1-5
B2-910-058-1-4
Average
Std. Dev.
COV, %
(in.)
0.1040
0.1040
0.1040
0.1040
0.1040
0.1040
0.1040
0.0000
0.00
(in.)
0.5005
0.5004
0.5004
0.5004
0.5004
0.4998
0.5003
0.0003
0.05
Ult.
Comp.
Load
(kips)
5.85
5.47
5.39
5.42
5.40
5.70
5.54
0.19
3.45
(in.)
0.4991
0.4989
Average
Std. Dev.
COV, %
0.1185
0.0001
0.06
0.4990
0.0001
0.03
Specimen
Number
49.7%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
188
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.18
8.05
8.12
8.00
8.02
0.04
0.44

Strain Gage: One axial gage (FAE-12S-AS-S6EL-2)
FV(normalizing):
FV(batch average):
A2-910-057-1-1
B2-910-057-1-1
(in.)
0.1189
0.1175
(in.)
0.4989
0.4986
Average
Std. Dev.
COV, %
0.1182
0.0009
0.80
0.4987
0.0002
0.05
Specimen
Number
49.8%
Load @
0.3%
Strain
(lbs.)
1513
1506

Specimen Specimen
Thickness
Width

Test Date: 12/31/1999
49.8%
Load @
0.1%
Strain
(lbs.)
545.8
545.2
49.8% in.
0.0086
8.15
0.04
0.50
Load @
0.1%
Strain
(lbs.)
564.7
552.5
49.8%
0.0086 in.
49.4%
Load @
0.3%
Strain
(lbs.)
1525
1520
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.10
7.99
8.26
8.06
8.18
0.11
1.38
8.03
0.05
0.57

0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
112
113
105
106
104
104
104
105
104
105
110
110
106
107
3.69
3.72
3.46
3.46
(in.)
0.1185
0.1186


Strain Gage: N/A

A2-910-056-1-1
B2-910-056-1-1

Test Date: 12/27/1999
49.8%

FV(batch average):
Specimen Specimen
Thickness
Width
0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
95.6
95.0
110
110
110
109
114
113
89.4
88.8
86.1
85.5
101
100
12.0
11.9
11.85
11.85
Specimen
Number
FV(normalizing):


Strain Gage: N/A

0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
98.2
98.0
96.1
95.9
112
112
105
105
103
102
92.9
92.7
101
101
6.94
6.93
6.86
6.86

FV(normalizing):
FV(batch average):
Specimen Specimen
Thickness
Width
B2-910-058-1-1
A2-910-058-1-1
(in.)
0.1186
0.1201
(in.)
0.4986
0.4988
Average
Std. Dev.
COV, %
0.1194
0.0011
0.89
0.4987
0.0001
0.03
Load @
0.1%
Strain
(lbs.)
532.4
527.7
49.8%
0.0086 in.
49.7%
Load @
0.3%
Strain
(lbs.)
1524
1423
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.38
8.26
7.47
7.45
7.93
0.64
8.13
7.86
0.57
7.25
0 (Warp) Compression Properties, 180F (Dry)




Strain Gage: N/A
FV(normalizing):
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-9
A2-910-056-1-8
A2-910-056-1-9
B1-910-056-1-8
B1-910-056-1-9
B2-910-056-1-9
Average
Std. Dev.
COV, %
(in.)
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.0000
0.00
(in.)
0.5002
0.5006
0.5004
0.5000
0.5000
0.4995
0.5001
0.0004
0.07

Ult.
Comp.
Load
(kips)
4.40
4.41
4.37
4.91
4.92
4.98
4.66
0.30
6.41
49.8%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
FV(normalizing):
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-8
A1-910-057-1-9
A2-910-057-1-9
B1-910-057-1-8
B1-910-057-1-9
B2-910-057-1-9
Average
Std. Dev.
COV, %
(in.)
0.1020
0.1020
0.1020
0.1020
0.1020
0.1020
0.1020
0.0000
0.00
(in.)
0.4989
0.4986
0.5017
0.4999
0.5000
0.4999
0.4998
0.0011
0.22

Ult.
Comp.
Load
(kips)
5.01
5.71
4.88
5.34
5.46
4.29
5.12
0.50
9.83
FV(normalizing):
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-058-1-9
A2-910-058-1-5
A2-910-058-1-9
B1-910-058-1-9
B2-910-058-1-5
B2-910-058-1-9
Average
Std. Dev.
COV, %
(in.)
0.1031
0.1031
0.1031
0.1031
0.1031
0.1031
0.1031
0.0000
0.00
(in.)
0.5004
0.5000
0.5002
0.5005
0.4998
0.4995
0.5001
0.0004
0.08
Ult.
Comp.
Load
(kips)
4.94
5.09
4.58
5.25
5.36
5.57
5.13
0.35
6.81
Specimen
Width
A2-910-056-1-2
B2-910-056-1-2
(in.)
0.1188
0.1192
(in.)
0.5005
0.5004
Average
Std. Dev.
COV, %
0.1190
0.0003
0.26
0.5005
0.0001
0.02
0.0086 in.
49.4%

Test Date: 1/5/2000
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
49.7%
Ult. Comp.
Strength
Actual
Norm.
(ksi)
(ksi)
95.7
95.6
98.7
98.6
88.7
88.6
102
102
104
104
108
108
100
99
6.8
6.8
6.86
6.86
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
189
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.00
7.89
7.84
7.77
7.83
0.09
1.12

FV(normalizing):
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A2-910-057-1-2
B2-910-057-1-2
(in.)
0.1197
0.1178
(in.)
0.5003
0.5000
Average
Std. Dev.
COV, %
0.1187
0.0014
1.15
0.5001
0.0002
0.05

Test Date: 1/5/2000
0.0086 in.
49.8%
Load @
0.3%
Strain
(lbs.)
1479
1451

Load @
0.1%
Strain
(lbs.)
548.5
565.5
49.8%
0.0086 in.
49.4%
Load @
0.3%
Strain
(lbs.)
1534
1626
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.23
8.18
9.01
8.81
8.62
0.55
6.38
8.49
0.44
5.23


49.8%
Load @
0.1%
Strain
(lbs.)
528.0
515.2
49.8%
0.0086 in.
7.92
0.11
1.38


Strain Gage: N/A

Specimen
Thickness


FV(batch average):
Specimen
Number
49.8%
Ult. Comp.
Strength
Actual
Norm.
(ksi)
(ksi)
98.5
97.3
112
111
95.4
94.3
105
104
107
106
84.2
83.2
100
99
10.0
9.8
9.91
9.91


Strain Gage: N/A

FV(normalizing):

Test Date: 1/4/2000
0.0086 in.



49.8%
Ult. Comp.
Strength
Actual
Norm.
(ksi)
(ksi)
85.8
85.3
85.9
85.3
85.1
84.6
95.8
95.2
95.9
95.3
97.2
96.5
91.0
90.4
5.9
5.9
6.48
6.48

FV(normalizing):
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A2-910-058-1-2
B2-910-058-1-6
(in.)
0.1198
0.1214
(in.)
0.5002
0.4985
Average
Std. Dev.
COV, %
0.1206
0.0012
0.96
0.4994
0.0012
0.25
Load @
0.1%
Strain
(lbs.)
520.9
529.7
49.8%
0.0086 in.
49.7%
Load @
0.3%
Strain
(lbs.)
1479
1477
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.00
7.95
7.83
7.89
7.91
0.12
1.51
7.92
0.04
0.55
0 (Warp) Compression Properties, 180F (Wet)

Preconditioning: Section 3.2 of AGATE
Test Date: 7/6/2000
Specimen
Number
Specimen
Thickness
A1-910-056-1-1
A1-910-056-1-2
A2-910-056-1-1
B1-910-056-1-2
B1-910-056-1-1
B2-910-056-1-1
Average
Std. Dev.
COV, %
(in.)
0.1036
0.1036
0.1036
0.1036
0.1036
0.1036
0.1036
0.0000
0.00
FV(batch average):
Specimen Ult.
Width
Comp.
Load
(in.)
(kips)
0.4999
3.43
0.5000
3.56
0.4999
2.96
0.4999
3.15
0.4999
3.01
0.4995
3.99
0.4999
3.35
0.0002
0.39
0.03
11.67

(in.)
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.0000
0.00
FV(batch average):
Specimen Ult.
Width
Comp.
Load
(in.)
(kips)
0.4991
3.58
0.4990
3.44
0.5021
3.28
0.4996
3.92
0.5000
3.32
0.5000
3.32
0.5000
3.47
0.0011
0.24
0.23
6.98

Specimen
Number
Specimen
Thickness
A1-910-058-1-1
A2-910-058-1-1
A2-910-058-1-2
B1-910-058-1-1
B2-910-058-1-1
B2-910-058-1-2
Average
Std. Dev.
COV, %
(in.)
0.1047
0.1047
0.1047
0.1047
0.1047
0.1047
0.1047
0.0000
0.00
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Specimen
Number
FV(batch average):
Specimen Ult.
Width
Comp.
Load
(in.)
(kips)
0.5005
3.98
0.5000
3.83
0.4999
3.71
0.5005
4.04
0.4997
3.71
0.4997
3.75
0.5000
3.84
0.0003
0.15
0.07
3.79
Specimen Specimen
Thickness
Width
Average
Std. Dev.
COV, %
0.1197
0.0002
0.16
0.4997
0.0001
0.02


Specimen
Number
FV(batch average):
Specimen Specimen
Thickness
Width
(in.)
0.1201
0.1186
(in.)
0.4996
0.4994
Average
Std. Dev.
COV, %
0.1193
0.0011
0.89
0.4995
0.0001
0.03

49.7%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Specimen
Number
Load @
0.1%
Strain
(lbs.)
515.9
588.0
0.0086 in.
49.4%
Load @
0.3%
Strain
(lbs.)
1406
1665
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.42
7.40
9.10
8.96
8.26
1.18
14.34
8.18
1.10
13.46

FV(batch average):
Specimen Specimen
Thickness
Width
A2-910-058-1-3
B2-910-058-1-3
(in.)
0.1198
0.1197
(in.)
0.4994
0.4993
Average
Std. Dev.
COV, %
0.1198
0.0000
0.03
0.4994
0.0001
0.01
190
7.85
0.52
6.59


Test Date: 5/1/2000
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.28
8.22
7.52
7.49

A2-910-057-1-3
B2-910-057-1-3
0.0086 in.
49.8%
Load @
0.3%
Strain
(lbs.)
1530
1398
7.90
0.53
6.75
Test Date: 5/1/2000
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Load @
0.1%
Strain
(lbs.)
540.4
497.0
0.0086 in.


49.4%
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
76.0
77.1
73.2
74.3
70.9
71.9
77.2
78.3
70.8
71.9
71.6
72.6
73.3
74.4
2.73
2.77
3.72
3.72
FV(batch average):
(in.)
0.4997
0.4996

Strain Gage: N/A
(in.)
0.1196
0.1198
0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
69.9
69.5
67.2
66.7
63.7
63.3
76.5
75.9
64.7
64.3
64.7
64.3
67.8
67.3
4.81
4.77
7.09
7.09

A2-910-056-1-3
B2-910-056-1-3


Test Date: 7/6/2000
49.8%

Strain Gage: N/A
Test Date: 7/6/2000
A1-910-057-1-1
A1-910-057-1-2
A2-910-057-1-1
B1-910-057-1-1
B1-910-057-1-2
B2-910-057-1-1
Average
Std. Dev.
COV, %

Test Date: 5/1/2000
0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
66.3
66.5
68.7
68.9
57.2
57.5
60.8
61.1
58.1
58.3
77.1
77.4
64.7
64.9
7.57
7.59
11.70
11.70




Specimen
Thickness


Strain Gage: N/A

Specimen
Number

Load @
0.1%
Strain
(lbs.)
527.5
514.7
0.0086 in.
49.7%
Load @
0.3%
Strain
(lbs.)
1488
1427
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.03
7.99
7.63
7.59
7.83
0.28
3.60
7.79
0.28
3.63
90 (Fill) Compression Properties, -65F (Dry)


Specimen
Number
A1-910-056-1-4
A2-910-056-1-4
A2-910-056-1-5
B1-910-056-1-3
B1-910-056-1-4
B2-910-056-1-3
Average
Std. Dev.
COV, %
Strain Gage: N/A
Ply Orientation: (fill)12

Test Operator: Joel Patterson

FV(batch average):
Specimen Specimen Ult.

Thickness
Width Comp.
Load
(in.)
(in.)
(kips)
0.1028
0.4995
5.64
0.1028
0.5000
4.75
0.1028
0.5000
5.19
0.1028
0.4996
5.44
0.1028
0.4998
6.20
0.1028
0.4999
6.09
0.1028
0.4998
5.55
0.0000
0.0002
0.55
0.00
0.04
9.88
0.0086 in.
49.8%
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
110
109
92.4
92.1
101
101
106
106
121
120
118
118
108
108
10.7
10.7
9.89
9.89
Test Date: 12/29/1999
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage

FV(batch average):
Specimen
Number
Specimen Specimen Load @

Thickness
Width
0.1%
Strain
(in.)
(in.)
(lbs.)
A2-910-056-1-6 0.1206
0.4980
659.4
B2-910-056-1-6 0.1222
0.4980
650.9
Average
Std. Dev.
COV, %
191
0.1214
0.0011
0.93
0.4980
0.0000
0.00
0.0086 in.
49.8%
Load @
0.3%
Strain
(lbs.)
1514
1491
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.12
7.13
6.90
7.00
7.01
0.15
2.19
7.07
0.09
1.26
90 (Fill) Compression Properties, 75F (Dry)




Strain Gage: N/A
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-5
A2-910-056-1-8
A2-910-056-1-9
B1-910-056-1-5
B1-910-056-1-8
B2-910-056-1-4
Average
Std. Dev.
COV, %
(in.)
0.1020
0.1020
0.1020
0.1020
0.1020
0.1020
0.1020
0.0000
0.00
(in.)
0.4998
0.5003
0.5003
0.4994
0.4997
0.4996
0.4999
0.0004
0.07

Ult.
Comp.
Load
(kips)
4.98
4.88
4.81
4.93
5.35
5.73
5.11
0.36
6.95

Test Date: 12/27/1999
49.8%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage



FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-8
A2-910-057-1-4
A2-910-057-1-5
B1-910-057-1-7
B2-910-057-1-4
B2-910-057-1-5
Average
Std. Dev.
COV, %
(in.)
0.1020
0.1020
0.1020
0.1020
0.1020
0.1020
0.1020
0.0000
0.00
(in.)
0.4988
0.5006
0.5009
0.4995
0.4994
0.4997
0.4998
0.0008
0.16

Ult.
Comp.
Load
(kips)
5.28
5.37
5.22
5.39
5.51
5.38
5.36
0.10
1.86
49.4%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage

FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-058-1-4
A1-910-058-1-5
A2-910-058-1-4
B1-910-058-1-4
B1-910-058-1-5
B2-910-058-1-4
Average
Std. Dev.
COV, %
(in.)
0.1035
0.1035
0.1035
0.1035
0.1035
0.1035
0.1035
0.0000
0.00
(in.)
0.4994
0.4995
0.5014
0.5016
0.5018
0.4996
0.5005
0.0012
0.23
Ult.
Comp.
Load
(kips)
5.50
4.79
5.09
5.24
5.15
5.47
5.21
0.26
5.09
(in.)
0.4988
0.4988
Average
Std. Dev.
COV, %
0.1202
0.0011
0.88
0.4988
0.0000
0.00
Specimen
Number
49.7%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
192
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.42
7.36
7.52
7.55
7.47
0.07
0.89

FV(batch average):
A2-910-057-1-1
B2-910-057-1-1
(in.)
0.1206
0.1193
(in.)
0.4987
0.4985
Average
Std. Dev.
COV, %
0.1199
0.0010
0.80
0.4986
0.0001
0.03
Specimen
Number
49.8%
Load @
0.3%
Strain
(lbs.)
1431
1432
7.46
0.13
1.77

Specimen Specimen
Thickness
Width

Test Date: 12/31/1999
Load @
0.1%
Strain
(lbs.)
546.6
525.1
0.0086

Load @
0.1%
Strain
(lbs.)
525.9
518.7
0.0086 in.
49.4%
Load @
0.3%
Strain
(lbs.)
1464
1430
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.80
7.81
7.66
7.59
7.73
0.09
1.23
7.70
0.16
2.02

0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
106
107
92.7
93
98.0
98
101
101
99.2
100
106
106
101
101
5.17
5.19
5.15
5.15
(in.)
0.1194
0.1209


Strain Gage: N/A

A2-910-056-1-1
B2-910-056-1-1

Test Date: 12/27/1999

FV(batch average):
Specimen Specimen
Thickness
Width
0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
104
103
105
104
102
101
106
105
108
107
106
104
105
104
2.0
2.0
1.92
1.92
Specimen
Number
in.


Strain Gage: N/A

0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
97.6
96.5
95.6
94.5
94.2
93.1
96.7
95.6
105
103.7
112
111.0
100
99.1
7.01
6.93
6.99
6.99


FV(batch average):
Specimen Specimen
Thickness
Width
A2-910-058-1-1
B2-910-058-1-1
(in.)
0.1206
0.1192
(in.)
0.4984
0.4987
Average
Std. Dev.
COV, %
0.1199
0.0010
0.80
0.4986
0.0002
0.04
Load @
0.1%
Strain
(lbs.)
542.0
554.5
0.0086 in.
49.7%
Load @
0.3%
Strain
(lbs.)
1497
1536
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.95
7.96
8.26
8.17
8.10
0.22
2.69
8.06
0.15
1.89
90 (Fill) Compression Properties, 180F (Dry)




Strain Gage: N/A
Ply Orientation: (fill) 12
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-056-1-7
A1-910-056-1-8
A2-910-056-1-10
B1-910-056-1-9
B2-910-056-1-5
B2-910-056-1-9
Average
Std. Dev.
COV, %
(in.)
0.1030
0.1030
0.1030
0.1030
0.1030
0.1030
0.1030
0.0000
0.00
(in.)
0.4999
0.4997
0.5003
0.4998
0.4998
0.5000
0.4999
0.0002
0.04

Ult.
Comp.
Load
(kips)
4.88
4.15
4.41
4.48
5.10
5.26
4.71
0.43
9.19

Test Date: 1/4/2000
49.8%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage



FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-057-1-10
A2-910-057-1-8
A2-910-057-1-9
B1-910-057-1-8
B2-910-057-1-10
B2-910-057-1-11
Average
Std. Dev.
COV, %
(in.)
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.0000
0.00
(in.)
0.4988
0.5008
0.5007
0.4993
0.4995
0.4995
0.4998
0.0008
0.16

Ult.
Comp.
Load
(kips)
4.69
5.22
5.27
4.80
4.82
4.74
4.92
0.25
5.16
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A1-910-058-1-9
A2-910-058-1-8
A2-910-058-1-9
B1-910-058-1-9
B2-910-058-1-8
B2-910-058-1-9
Average
Std. Dev.
COV, %
(in.)
0.1023
0.1023
0.1023
0.1023
0.1023
0.1023
0.1023
0.0000
0.00
(in.)
0.4994
0.5016
0.5017
0.5021
0.4994
0.4992
0.5006
0.0014
0.27
Ult.
Comp.
Load
(kips)
4.99
4.85
4.62
4.85
4.92
4.95
4.86
0.13
2.71
Specimen
Width
A2-910-056-1-2
B2-910-056-1-2
(in.)
0.1197
0.1211
(in.)
0.5002
0.5003
Average
Std. Dev.
COV, %
0.1204
0.0010
0.81
0.5002
0.0001
0.02
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
193
49.8%
Load @
0.3%
Strain
(lbs.)
1420
1436
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.56
7.51
7.69
7.73
7.63
0.09
1.22
7.62
0.16
2.03

FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
A2-910-057-1-2
B2-910-057-1-2
(in.)
0.1205
0.1193
(in.)
0.5003
0.5000
Average
Std. Dev.
COV, %
0.1199
0.0009
0.73
0.5001
0.0002
0.04

Test Date: 1/5/2000
49.7%
Load @
0.1%
Strain
(lbs.)
515.1
504.4
0.0086 in.

Load @
0.1%
Strain
(lbs.)
491.4
526.2
0.0086 in.
49.4%
Load @
0.3%
Strain
(lbs.)
1405
1498
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.58
7.58
8.15
8.07
7.86
0.40
5.13
7.83
0.34
4.40


0.0086 in.
Ult. Comp.
Strength
Actual
Norm.
(ksi)
(ksi)
97.6
96.8
94.4
93.6
90.0
89.2
94.4
93.6
96.3
95.5
96.8
96.0
94.9
94.1
2.8
2.7
2.91
2.91
Specimen
Thickness


Strain Gage: N/A

Specimen
Number

Test Date: 1/5/2000

FV(batch average):

0.0086 in.
49.4%
Ult. Comp.
Strength
Actual
Norm.
(ksi)
(ksi)
91.8
91.2
102
101
103
102
93.8
93.2
94.1
93.4
92.6
92.0
96.1
95.5
4.8
4.8
5.00
5.00


Strain Gage: N/A


0.0086 in.
Ult. Comp.
Strength
Actual
Norm.
(ksi)
(ksi)
94.8
94.6
80.7
80.5
85.5
85.3
87.0
86.9
99.1
98.9
102
102
91.5
91.4
8.4
8.4
9.19
9.19


FV(batch average):
Specimen
Number
Specimen
Thickness
Specimen
Width
B2-910-058-1-2
A2-910-058-1-6
(in.)
0.1194
0.1202
(in.)
0.5003
0.4982
Average
Std. Dev.
COV, %
0.1198
0.0005
0.44
0.4992
0.0015
0.30
Load @
0.1%
Strain
(lbs.)
484.4
507.5
0.0086 in.
49.7%
Load @
0.3%
Strain
(lbs.)
1384
1432
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.53
7.47
7.72
7.71
7.63
0.14
1.79
7.59
0.17
2.23
90 (Fill) Compression Properties, 180F (Wet)

Test Date: 7/6/2000
Specimen
Thickness
A1-910-056-1-1
A2-910-056-1-1
A2-910-056-1-2
B1-910-056-1-1
B2-910-056-1-1
B2-910-056-1-2
Average
Std. Dev.
COV, %
(in.)
0.1028
0.1028
0.1028
0.1028
0.1028
0.1028
0.1028
0.0000
0.00
FV(batch average):
Specimen Ult.
Width
Comp.
Load
(in.)
(kips)
0.4993
3.30
0.5001
3.59
0.4998
3.38
0.4998
3.24
0.4998
3.67
0.4994
3.57
0.4997
3.46
0.0003
0.17
0.06
5.03


FV(normalizing):
Test Date: 7/6/2000
Specimen
Thickness
A1-910-057-1-1
A1-910-057-1-2
A2-910-057-1-1
B1-910-057-1-1
B2-910-057-1-1
B2-910-057-1-2
Average
Std. Dev.
COV, %
(in.)
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.1025
0.0000
0.00
FV(batch average):
Specimen Ult.
Width
Comp.
Load
(in.)
(kips)
0.4994
3.68
0.4993
3.85
0.5008
3.47
0.4996
3.50
0.4990
3.72
0.4996
3.89
0.4996
3.68
0.0006
0.17
0.13
4.66

Test Date: 7/6/2000
Specimen
Number
Specimen
Thickness
A1-910-058-1-1
A2-910-058-1-1
A2-910-058-1-2
B1-910-058-1-1
B2-910-058-1-1
B2-910-058-1-2
Average
Std. Dev.
COV, %
(in.)
0.1035
0.1035
0.1035
0.1035
0.1035
0.1035
0.1035
0.0000
0.00
Specimen
Number
(in.)
0.1199
0.1213
(in.)
0.4995
0.4996
Average
Std. Dev.
COV, %
0.1206
0.0010
0.79
0.4995
0.0000
0.01

Test Date: 5/1/2000
49.4%
Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Specimen
Number
FV(normalizing):
FV(batch average):
Specimen Ult.
Width
Comp.
Load
(in.)
(kips)
0.4994
3.85
0.5014
3.62
0.5014
3.73
0.5020
3.51
0.4996
3.46
0.4996
3.46
0.5006
3.60
0.0012
0.16
0.23
4.41
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.15
7.12
7.93
7.99
7.55
0.61
8.13

FV(normalizing):
FV(batch average):
Specimen Specimen
Thickness
Width
A2-910-057-1-3
B2-910-057-1-3
(in.)
0.1241
0.1192
(in.)
0.4994
0.4995
Average
Std. Dev.
COV, %
0.1216
0.0035
2.87
0.4995
0.0001
0.02

Load @
0.1%
Strain
(lbs.)
518.8
554.4
49.8%
0.0086 in.
49.4%
Load @
0.3%
Strain
(lbs.)
1482
1573
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
7.77
8.01
8.56
8.47
8.16
0.55
6.77
8.24
0.32
3.90


Preconditioning: per Section 3.2 of AGATE Methodology
FV(normalizing):
49.8%
49.8%

Test Date: 5/1/2000
0.0086 in.
49.7%
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
74.4
74.7
69.8
70.0
71.9
72.1
67.5
67.7
67.0
67.2
66.9
67.1
69.6
69.8
3.08
3.09
4.43
4.43
49.8%
Load @
0.3%
Strain
(lbs.)
1372
1488


49.8%
Load @
0.1%
Strain
(lbs.)
516.1
526.9
49.8%
0.0086 in.
7.54
0.55
7.34


Strain Gage: N/A
FV(batch average):
Specimen Specimen
Thickness
Width
A2-910-056-1-3
B2-910-056-1-3


Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
71.9
71.4
75.1
74.6
67.6
67.2
68.4
67.9
72.7
72.2
75.9
75.4
71.9
71.5
3.40
3.38
4.73
4.73
Test Date: 5/1/2000
49.8%

Strain Gage: N/A

FV(normalizing):

49.8%
0.0086 in.
Ult. Comp.
Strength
Actual Norm.
(ksi)
(ksi)
64.3
64.0
69.8
69.5
65.7
65.5
63.1
62.9
71.4
71.1
69.6
69.3
67.3
67.1
3.38
3.37
5.02
5.02




Specimen
Number


Strain Gage: N/A
FV(normalizing):

Specimen
Number

Failure
Location
&
Comments
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Failure in gage
Specimen
Number

FV(batch average):
Specimen Specimen
Thickness
Width
A2-910-058-1-3
B2-910-058-1-3
(in.)
0.1205
0.1195
(in.)
0.4993
0.4998
Average
Std. Dev.
COV, %
0.1200
0.0007
0.60
0.4995
0.0004
0.08
194
Load @
0.1%
Strain
(lbs.)
545.4
533.9
0.0086 in.
49.7%
Load @
0.3%
Strain
(lbs.)
1518
1486
Comp. Mod.
(0.1-0.3% strain)
Actual
Norm.
(msi)
(msi)
8.08
8.09
7.97
7.91
8.03
0.08
0.98
8.00
0.13
1.57
In-plane Shear (Iosipescu) Properties, -65F (Dry)
Test Operator: Bryan Mines
Test Frame: H
Strain Gage: One biaxial gage (EA-06-062TV-350)
Ply Orientation: (0/90) 4S

Test Date: 12/29/99, 2/23/00
0.0086 in.
49.8%
Specimen
Specimen
Notch
Ultimate
In-plane Shear
IPS Modulus (1)
Failure Location
Number
Thickness
Width
Load
(0.25-0.65%) (2)
&
Comments
A1-910-056-1-1
A2-910-056-1-2
B1-910-056-1-1
B2-910-056-1-2
A1-910-056-1-3
B1-910-056-1-3
Average
Std. Dev.
COV, %
(in.)
0.1388
0.1385
0.1388
0.1389
0.1387
0.1391
0.1388
0.0002
0.14
(in.)
0.4520
0.4500
0.4460
0.4480
0.4510
0.4480
0.4492
0.0022
0.50
(lbs.)
1499
1429
1430
1431
1270
1340
1400
81
5.80
Strength
Actual
(ksi)
23.9
22.9
23.1
23.0
20.3
21.5
22.5
1.31
5.82
(1)
(2)
(msi)
0.665
0.689
0.573
0.563
0.623
0.064
10.25
Modulus is determined to be the slope of the Stress-Shear Strain curve.

0.25 ~ 0.65% strain range per ASTM D5379-98, Section 12.3.1
195
Shear failure in gage

In-plane Shear (Iosipescu) Properties, 75F (Dry)

Strain Gage: One biaxial gage (EA-06-125-TW-120)
Ply Orientation: (0/90)4S

Test Date: 12/31/1999, 2/14/00
Specimen
Number
Specimen
Thickness
Notch
Width
Ultimate
Load
A1-910-056-1-5
A1-910-056-1-6
B1-910-056-1-5
B1-910-056-1-6
A1-910-056-1-27
B1-910-056-1-27
Average
Std. Dev.
COV, %
(in.)
0.1390
0.1393
0.1390
0.1387
0.1387
0.1377
0.1387
0.0005
0.38
(in.)
0.4513
0.4526
0.4481
0.4477
0.4518
0.4493
0.4501
0.0021
0.46
(lbs.)
1209
1200
1219
1256
1083
1140
1185
62
5.26
0.0086 in.
In-plane Shear
Strength
Actual
(ksi)
19.3
19.0
19.6
20.2
17.3
18.4
19.0
1.02
5.39
49.8%
IPS Modulus (1)

(0.25-0.65%) (2)
(msi)
0.619
0.667
0.598
0.587
0.618
0.035
5.73
Failure Location
&
Comments

Test Date: 12/31/1999, 2/14/00

Specimen
Specimen
Notch
Ultimate
In-plane Shear
Number
Thickness
Width
Load
A1-910-057-1-1
A1-910-057-1-2
B1-910-057-1-1
B1-910-057-1-2
A1-910-057-1-11
B1-910-057-1-11
Average
Std. Dev.
COV, %
(in.)
0.1380
0.1377
0.1363
0.1376
0.1371
0.1362
0.1372
0.0007
0.55
(in.)
0.4498
0.4499
0.4522
0.4514
0.4501
0.4505
0.4506
0.0009
0.21
(lbs.)
1183
1223
1182
1191
1162
1171
1185
21
1.78
Strength
Actual
(ksi)
19.1
19.7
19.2
19.2
18.8
19.1
19.2
0.30
1.58
0.0086 in.
49.4%
IPS Modulus (1)

(0.25-0.65%) (2)
(msi)
0.628
0.596
0.593
0.601
0.605
0.016
2.65
Failure Location
&
Comments

Test Date: 12/31/99, 2/14/00

Specimen
Specimen
Notch
Ultimate
In-plane Shear
Number
Thickness
Width
Load
A1-910-058-1-1
A1-910-058-1-2
B1-910-058-1-1
B1-910-058-1-2
A1-910-058-1-11
B1-910-058-1-11
Average
Std. Dev.
COV, %
(in.)
0.1354
0.1359
0.1356
0.1361
0.1357
0.1356
0.1357
0.0003
0.20
(in.)
0.4484
0.4484
0.4566
0.4548
0.4488
0.4534
0.4517
0.0037
0.81
(lbs.)
1227
1221
1177
1182
1148
1228
1197
33
2.76
Strength
Actual
(ksi)
20.2
20.0
19.0
19.1
18.9
20.0
19.5
0.61
3.11
(1)
(2)
0.0086 in.
49.7%
(1)
IPS Modulus
(0.25-0.65%) (2)
(msi)
0.603
0.575
0.679
0.588
0.611
0.047
7.62

196
Failure Location
&
Comments
In-plane Shear (Iosipescu) Properties, 180F (Dry)


Test Date: 1/5/2000, 2/14/00
0.0086 in.
Specimen
Number
Specimen
Thickness
Notch
Width
Ultimate
Load
A1-910-056-1-7
A1-910-056-1-8
B1-910-056-1-7
B1-910-056-1-8
A1-910-056-1-28
B1-910-056-1-28
Average
Std. Dev.
COV, %
(in.)
0.1392
0.1395
0.1383
0.1378
0.1387
0.1380
0.1386
0.0007
0.48
(in.)
0.4511
0.4514
0.4492
0.4543
0.4514
0.4549
0.4520
0.0022
0.48
(lbs.)
980
971
983
1001
922
906
961
38
3.91
49.8%
IPS Modulus (1)
In-plane Shear
Strength
Actual
(ksi)
15.6
15.4
15.8
16.0
14.7
14.4
15.3
0.62
4.06
(0.25-0.65%) (2)
(msi)
0.524
0.507
0.498
0.493
0.506
0.014
2.70
Failure Location
&
Comments

Test Date: 1/5/2000

Specimen
Specimen
Notch
Ultimate
In-plane Shear
Number
Thickness
Width
Load
A1-910-057-1-3
A1-910-057-1-4
B1-910-057-1-3
B1-910-057-1-4
A1-910-057-1-12
B1-910-057-1-12
Average
Std. Dev.
COV, %
(in.)
0.1378
0.1381
0.1376
0.1372
0.1365
0.1362
0.1372
0.0007
0.55
(in.)
0.4501
0.4491
0.4510
0.4501
0.4498
0.4504
0.4501
0.0006
0.14
(lbs.)
961
978
953
938
934
937
950
17
1.81
Strength
Actual
(ksi)
15.5
15.8
15.4
15.2
15.2
15.3
15.4
0.22
1.43
0.0086 in.
49.4%
(1)
IPS Modulus
(0.25-0.65%) (2)
(msi)
0.513
0.537
0.491
0.521
0.516
0.019
3.71
Failure Location
&
Comments

Test Date: 1/5/2000
0.0086 in.
49.7%
Specimen
Specimen
Notch
Ultimate
In-plane Shear
IPS Modulus (1)
Failure Location
Number
Thickness
Width
Load
(0.25-0.65%) (2)
&
Comments
A1-910-058-1-3
A1-910-058-1-4
B1-910-058-1-3
B1-910-058-1-4
A1-910-058-1-12
B1-910-058-1-12
Average
Std. Dev.
COV, %
(in.)
0.1361
0.1365
0.1365
0.1366
0.1358
0.1350
0.1361
0.0006
0.46
(in.)
0.4484
0.4546
0.4529
0.4569
0.4541
0.4416
0.4514
0.0056
1.23
(lbs.)
980
962
940
954
929
945
951
18
1.90
Strength
Actual
(ksi)
16.1
15.5
15.2
15.3
15.1
15.8
15.5
0.39
2.52
(1)
(2)
(msi)
0.584
0.495
0.514
0.530
0.531
0.038
7.21

197

In-plane Shear (Iosipescu) Properties, 180F (Wet)


Test Date: 5/2/2000
0.0086 in.
Specimen
Number
Specimen
Thickness
Notch
Width
Ultimate
Load
A1-910-056-1-10
B1-910-056-1-9
B1-910-056-1-10
A1-910-056-1-13
A1-910-056-1-9
B1-910-056-1-11
Average
Std. Dev.
COV, %
(in.)
0.1391
0.1371
0.1363
0.1363
0.1393
0.1353
0.1372
0.0016
1.20
(in.)
0.4508
0.4489
0.4494
0.4465
0.4508
0.4491
0.4492
0.0016
0.35
(lbs.)
680
671
677
688
666
649
672
14
2.03
49.8%
IPS Modulus (1)
In-plane Shear
Strength
Actual
(ksi)
10.8
10.9
11.1
11.3
10.6
10.7
10.9
0.26
2.36
(0.25-0.65%) (2)
(msi)
0.443
0.457
0.470
0.455
0.456
0.011
2.42
Failure Location
&
Comments

Test Date: 5/2/2000

Specimen
Specimen
Notch
Ultimate
In-plane Shear
Number
Thickness
Width
Load
A1-910-057-1-5
A1-910-057-1-6
B1-910-057-1-5
B1-910-057-1-6
A1-910-057-1-7
B1-910-057-1-7
Average
Std. Dev.
COV, %
(in.)
0.1382
0.1382
0.1370
0.1374
0.1383
0.1371
0.1377
0.0006
0.43
(in.)
0.4511
0.4999
0.4508
0.4517
0.4492
0.4505
0.4589
0.0201
4.38
(lbs.)
690
683
668
671
660
670
674
11
1.62
Strength
Actual
(ksi)
11.1
9.88
10.8
10.8
10.6
10.8
10.7
0.41
3.85
0.0086 in.
49.4%
(1)
IPS Modulus
(0.25-0.65%) (2)
(msi)
0.489
0.436
0.481
0.420
0.457
0.034
7.38
Failure Location
&
Comments

Test Date: 5/2/2000
0.0086 in.
49.7%
Specimen
Specimen
Notch
Ultimate
In-plane Shear
IPS Modulus (1)
Failure Location
Number
Thickness
Width
Load
(0.25-0.65%) (2)
&
Comments
A1-910-058-1-5
A1-910-058-1-6
B1-910-058-1-5
B1-910-058-1-6
A1-910-058-1-7
B1-910-058-1-7
Average
Std. Dev.
COV, %
(in.)
0.1368
0.1367
0.1369
0.1374
0.1366
0.1373
0.1369
0.0003
0.25
(in.)
0.4486
0.4479
0.4560
0.4559
0.4486
0.4543
0.4519
0.0039
0.86
(lbs.)
676
678
665
660
679
678
673
8
1.20
Strength
Actual
(ksi)
11.0
11.1
10.7
10.5
11.1
10.9
10.9
0.23
2.14
(1)
(2)
(msi)
0.540
0.451
0.429
0.447
0.467
0.050
10.66

198

In-plane Shear (Iosipescu) Strength, Fluid Sensitivity

Fluid: Jet Fuel
Specimen Preconditioning: at RT for 500 hrs
Test Temperature: 180F
Strain Gage: N/A

Test Date: 1/5/2000
Specimen
Number
Specimen
Thickness
Notch
Width
Ultimate
Load
A1-910-056-1-15
A1-910-056-1-16
B1-910-056-1-16
B1-910-056-1-17
B1-910-056-1-18
Average
Std. Dev.
COV, %
(in.)
0.1375
0.1376
0.1384
0.1386
0.1389
0.1382
0.0006
0.45
(in.)
0.4502
0.4510
0.4487
0.4559
0.4496
0.4511
0.0028
0.62
(lbs.)
883
878
889
931
906
897
22
2.42
0.0086 in.
49.8%
In-plane Shear
Strength
Actual
(ksi)
14.3
14.1
14.3
14.7
14.5
14.4
0.23
1.61
Failure Location
&
Comments
Fluid: Hydraulic Fluid

Specimen Preconditioning: at RT for 60 - 90 minutes
Test Temperature: 180F
Strain Gage: N/A

Test Date: 12/30/1999
Specimen
Number
Specimen
Thickness
Notch
Width
Ultimate
Load
A1-910-056-1-19
A1-910-056-1-20
A1-910-056-1-21
B1-910-056-1-19
B1-910-056-1-20
Average
Std. Dev.
COV, %
(in.)
0.1382
0.1384
0.1384
0.1390
0.1390
0.1386
0.0004
0.28
(in.)
0.4513
0.4509
0.4517
0.4491
0.4493
0.4505
0.0012
0.26
(lbs.)
967
961
961
949
969
961
8
0.83
0.0086 in.
49.8%
In-plane Shear
Strength
Actual
(ksi)
15.5
15.4
15.4
15.2
15.5
15.4
0.13
0.85
Failure Location
&
Comments
Fluid: MEK Solvent

Specimen Preconditioning: at RT for 60 - 90 minutes
Test Temperature: RT
Strain Gage: N/A

Test Date: 12/30/1999
Specimen
Number
Specimen
Thickness
Notch
Width
Ultimate
Load
A1-910-056-1-23
A1-910-056-1-24
B1-910-056-1-23
B1-910-056-1-24
B1-910-056-1-25
Average
Std. Dev.
COV, %
(in.)
0.1374
0.1364
0.1380
0.1376
0.1366
0.1372
0.0007
0.52
(in.)
0.4489
0.4490
0.4491
0.4490
0.4490
0.4490
0.0001
0.02
(lbs.)
1174
1165
1151
1129
1130
1150
20
1.76
0.0086 in.
49.8%
In-plane Shear
Strength
Actual
(ksi)
19.0
19.0
18.6
18.3
18.4
18.7
0.35
1.86
199
Failure Location
&
Comments
Apparent Interlaminar Shear Strength, 75F (Dry)

Strain Gage: N/A

Test Date: 12/27/1999
Specimen
Number
Specimen
Depth
Specimen
Width
A1-910-056-1-1
A1-910-056-1-2
A1-910-056-1-3
B1-910-056-1-1
B1-910-056-1-2
B1-910-056-1-3
Average
Std. Dev.
COV, %
(in.)
0.1040
0.1040
0.1044
0.0968
0.0950
0.0934
0.0996
0.0051
5.11
(in.)
0.2523
0.2523
0.2527
0.2516
0.2514
0.2514
0.2519
0.0006
0.22
Span:
Thickness
Ratio
0.0086 in.
49.8%
Ultimate
Load
Short Beam
Shear
Strength
(ksi)
8.40
8.49
8.38
8.75
8.81
8.47
8.55
0.184
2.15
(kips)
294
297
295
284
281
265
286
12
4.25
4:1
4:1
4:1
4:1
4:1
4:1
Failure Location
&
Comments
Shear Failure
Shear Failure
Shear Failure
Shear Failure
Shear Failure
Shear Failure
Strain Gage: N/A

Test Date: 12/31/1999
Specimen
Number
Specimen
Depth
Specimen
Width
A1-910-057-1-1
A1-910-057-1-2
A1-910-057-1-3
B1-910-057-1-1
B1-910-057-1-2
B1-910-057-1-3
Average
Std. Dev.
COV, %
(in.)
0.1031
0.1036
0.1038
0.1043
0.1044
0.1043
0.1039
0.0005
0.47
(in.)
0.2519
0.2522
0.2523
0.2512
0.2507
0.2512
0.2516
0.0006
0.25
Span:
Thickness
Ratio
0.0086 in.
49.4%
Ultimate
Load
Short Beam
Shear
Strength
(ksi)
8.79
8.61
8.95
8.76
7.93
8.32
8.56
0.375
4.38
(kips)
304
300
313
306
277
290
298
13
4.32
4:1
4:1
4:1
4:1
4:1
4:1
Failure Location
&
Comments
Shear Failure
Shear Failure
Shear Failure
Shear Failure
Shear Failure
Shear Failure
Strain Gage: N/A

Test Date: 12/31/1999
Specimen
Number
Specimen
Depth
Specimen
Width
A1-910-058-1-1
A1-910-058-1-2
A1-910-058-1-3
B1-910-058-1-1
B1-910-058-1-2
B1-910-058-1-3
Average
Std. Dev.
COV, %
(in.)
0.1028
0.1023
0.1044
0.1037
0.1035
0.1036
0.1034
0.0008
0.73
(in.)
0.2519
0.2528
0.2526
0.2515
0.2514
0.2516
0.2520
0.0006
0.23
Span:
Thickness
Ratio
Ultimate
Load
(kips)
298
299
301
288
300
279
294
9
2.96
4:1
4:1
4:1
4:1
4:1
4:1
200
0.0086 in.
49.7%
Short Beam
Shear
Strength
(ksi)
8.63
8.68
8.57
8.28
8.64
8.04
8.47
0.256
3.02
Failure Location
&
Comments
Shear Failure
Shear Failure
Shear Failure
Shear Failure
Shear Failure
Shear Failure
Apparent Interlaminar Shear Strength, 75F (Dry) - continued

Test Method: ASTM D2344-00
Specimen Specimen
Specimen
Panel
Coupon
Depth
Width
(in.)
(in.)
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
A-49
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
B-50
1-1
1-3
1-5
4-7
4-9
4-11
8-13
8-15
1-2
1-4
1-6
4-8
4-10
4-12
8-14
8-16
8-18
1-1
1-3
1-5
4-7
4-9
4-11
8-13
8-15
1-2
1-4
1-6
4-8
4-10
4-12
8-14
8-16
8-18
Average
Std, Dev.
COV, %
0.10070
0.10035
0.10055
0.10190
0.10220
0.10180
0.10380
0.10370
0.10055
0.10045
0.10165
0.10175
0.10160
0.10205
0.10350
0.10380
0.10405
0.10120
0.10130
0.10165
0.10005
0.10055
0.10030
0.10025
0.10035
0.10130
0.10140
0.10095
0.10020
0.10030
0.10030
0.10035
0.10025
0.10045
0.25060
0.25065
0.25000
0.25005
0.25005
0.24995
0.24890
0.24890
0.25075
0.25025
0.25030
0.25005
0.25015
0.25005
0.24915
0.24870
0.24885
0.25065
0.25065
0.25050
0.24990
0.24970
0.24970
0.24930
0.24940
0.25080
0.25060
0.25045
0.24985
0.24970
0.24970
0.24940
0.24945
0.24955
Span
(in.)
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
Panel Fabrication: TCA - vacuum bagged at 270F

Ultimate
Initial
Total
SBS
Failure
Load
Load
Load
Strength
Location
(lbs)
(lbs)
(lbs)
(ksi)
301.9
303.5
307.2
274.7
276.9
304.4
279.6
269.9
275.5
279.4
288.0
268.7
263.7
302.1
282.1
264.6
278.6
296.2
293.2
291.0
300.3
324.7
305.6
302.8
302.4
291.4
287.9
298.5
287.5
291.0
299.4
271.9
282.3
292.9
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
301.9
303.5
307.2
274.7
276.9
304.4
279.6
269.9
280.7
284.6
293.2
273.9
268.9
307.3
287.3
269.8
283.8
296.2
293.2
291.0
300.3
324.7
305.6
302.8
302.4
296.6
293.1
303.7
292.7
296.2
304.6
277.1
287.5
298.1
8.97
9.05
9.17
8.09
8.13
8.97
8.12
7.84
8.35
8.49
8.64
8.07
7.93
9.03
8.35
7.84
8.22
8.76
8.66
8.57
9.01
9.70
9.15
9.09
9.06
8.75
8.65
9.01
8.77
8.87
9.12
8.30
8.62
8.92
8.65
0.450
5.20
201
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Specimen Preconditioning:
Loading Rate:
Control Mode:
Testing
Test Conditions
Facility
Temp
RH
(F)
(%)
TCA
TCA
TCA
TCA
TCA
TCA
TCA
TCA
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
TCA
TCA
TCA
TCA
TCA
TCA
TCA
TCA
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
73
73
73
73
73
73
73
73
81
81
81
81
81
81
81
81
81
73
73
73
73
73
73
73
73
81
81
81
81
81
81
81
81
81
50
50
50
50
50
50
50
50
62
62
62
62
62
62
62
62
62
50
50
50
50
50
50
50
50
61
61
61
61
61
61
61
61
61
as machined
0.05 in/min
Stroke
Test
Test
Operator Frame
John S.
John S.
John S.
John S.
John S.
Debra W.
Debra W.
Debra W.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Debra W.
Debra W.
Debra W.
Debra W.
John S.
John S.
John S.
John S.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
Test
Date
5/21/2002
5/21/2002
5/21/2002
5/21/2002
5/21/2002
5/17/2002
5/17/2002
5/17/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
5/17/2002
5/17/2002
5/17/2002
5/17/2002
5/21/2002
5/21/2002
5/21/2002
5/21/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002

Specimen
Specimen Specimen
Panel
Coupon
Depth
Width
(in.)
(in.)
A-51
A-51
A-51
A-51
A-51
A-51
A-51
A-51
A-51
A-51
A-51
A-51
A-51
A-51
A-51
A-51
B-52
B-52
B-52
B-52
B-52
B-52
B-52
B-52
B-52
B-52
B-52
B-52
B-52
B-52
B-52
B-52
2-1
2-3
2-5
5-7
5-9
5-11
8-13
8-15
2-2
2-4
2-6
5-8
5-10
5-12
8-14
8-16
2-1
2-3
2-5
5-7
5-9
5-11
8-13
8-15
2-2
2-4
2-6
5-8
5-10
5-12
8-14
8-16
Average
Std, Dev.
COV, %
0.10270
0.10235
0.10205
0.10165
0.10135
0.10135
0.10090
0.10035
0.10260
0.10210
0.10220
0.10145
0.10110
0.10100
0.10055
0.10050
0.10350
0.10360
0.10385
0.10130
0.10125
0.10155
0.09825
0.09825
0.10355
0.10400
0.10370
0.10145
0.10130
0.10160
0.09825
0.09835
0.25030
0.25065
0.25025
0.25060
0.25030
0.25030
0.24980
0.24955
0.25085
0.25045
0.25030
0.25025
0.25005
0.24990
0.24965
0.24965
0.24955
0.24955
0.24945
0.24950
0.24945
0.24945
0.25000
0.24980
0.24905
0.24965
0.24950
0.24960
0.24930
0.24940
0.24985
0.24975
Span
(in.)
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413

Ultimate
Initial
Total
SBS
Failure
Load
Load
Load
Strength
Location
(lbs)
(lbs)
(lbs)
(ksi)
291.2
277.9
263.5
295.2
288.3
278.2
290.2
278.0
275.7
270.8
288.5
286.4
272.4
287.5
291.0
271.7
293.9
312.9
295.5
287.5
311.6
305.2
287.7
270.8
272.2
276.8
276.3
283.5
282.7
276.7
284.0
276.8
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
291.2
277.9
263.5
295.2
288.3
278.2
290.2
278.0
280.9
276.0
293.7
291.6
277.6
292.7
296.2
276.9
293.9
312.9
295.5
287.5
311.6
305.2
287.7
270.8
277.4
282.0
281.5
288.7
287.9
281.9
289.2
282.0
8.50
8.12
7.74
8.69
8.52
8.22
8.64
8.33
8.18
8.09
8.61
8.61
8.23
8.70
8.85
8.28
8.53
9.08
8.56
8.53
9.25
9.04
8.78
8.28
8.07
8.14
8.16
8.55
8.55
8.34
8.83
8.61
8.49
0.329
3.88
202
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Loading Rate:
Control Mode:
Testing
Test Conditions
Facility
Temp
RH
(F)
(%)
TCA
TCA
TCA
TCA
TCA
TCA
TCA
TCA
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
TCA
TCA
TCA
TCA
TCA
TCA
TCA
TCA
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
73
73
73
73
73
73
73
73
81
81
81
81
81
81
81
81
73
73
73
73
73
73
73
73
80
80
80
80
80
80
80
80
50
50
50
50
50
50
50
50
62
62
62
62
62
62
62
62
50
50
50
50
50
50
50
50
63
63
63
63
63
63
63
63
as machined
0.05 in/min
Stroke
Test
Test
Operator Frame
Debra W.
Debra W.
Debra W.
Debra W.
John S.
John S.
John S.
John S.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
John S.
John S.
John S.
John S.
Debra W.
Debra W.
Debra W.
Debra W.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
Inst 4510
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
Test
Date
5/17/2002
5/17/2002
5/17/2002
5/17/2002
5/21/2002
5/21/2002
5/21/2002
5/21/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
5/21/2002
5/21/2002
5/21/2002
5/21/2002
5/17/2002
5/17/2002
5/17/2002
5/17/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002

Specimen
Specimen Specimen
Panel
Coupon
Depth
Width
(in.)
(in.)
A-53
A-53
A-53
A-53
A-53
A-53
A-53
A-53
A-53
A-53
A-53
A-53
A-53
A-53
A-53
A-53
B-54
B-54
B-54
B-54
B-54
B-54
B-54
B-54
B-54
B-54
B-54
B-54
B-54
B-54
B-54
B-54
1-1
1-3
1-5
6-7
6-9
6-11
7-13
7-15
1-2
1-4
1-6
6-8
6-10
6-12
7-14
7-16
1-1
1-3
1-5
6-7
6-9
6-11
7-13
7-15
1-2
1-4
1-6
6-8
6-10
6-12
7-14
7-16
Average
Std, Dev.
COV, %
0.10105
0.10090
0.10135
0.10355
0.10345
0.10375
0.10375
0.10370
0.10085
0.10105
0.10125
0.10355
0.10360
0.10395
0.10385
0.10390
0.10080
0.10110
0.10130
0.10195
0.10200
0.10180
0.10205
0.10215
0.10095
0.10120
0.10120
0.10195
0.10210
0.10200
0.10195
0.10210
0.24840
0.24850
0.24905
0.24910
0.24955
0.24940
0.24905
0.24900
0.24825
0.24880
0.24920
0.24920
0.24960
0.24935
0.24900
0.24915
0.24695
0.25020
0.25050
0.24985
0.24955
0.24945
0.24940
0.24955
0.25000
0.25040
0.25030
0.24955
0.24945
0.24920
0.24950
0.24965
Span
(in.)
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413

Ultimate
Initial
Total
SBS
Failure
Load
Load
Load
Strength
Location
(lbs)
(lbs)
(lbs)
(ksi)
266.7
310.3
289.7
314.2
332.8
308.2
301.0
294.9
288.3
280.7
298.1
317.5
304.7
311.3
284.2
282.1
279.6
296.9
316.5
324.5
301.7
312.1
300.5
280.3
276.7
283.1
305.1
310.5
300.2
295.6
278.4
278.3
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
266.7
310.3
289.7
314.2
332.8
308.2
301.0
294.9
293.5
285.9
303.3
322.7
309.9
316.5
289.4
287.3
279.6
296.9
316.5
324.5
301.7
312.1
300.5
280.3
281.9
288.3
310.3
315.7
305.4
300.8
283.6
283.5
7.97
9.28
8.61
9.14
9.67
8.93
8.74
8.57
8.79
8.53
9.01
9.38
8.99
9.16
8.39
8.32
8.42
8.80
9.35
9.55
8.89
9.22
8.86
8.25
8.38
8.53
9.19
9.31
8.99
8.87
8.36
8.34
8.84
0.421
4.76
203
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Loading Rate:
Control Mode:
Testing
Test Conditions
Facility
Temp
RH
(F)
(%)
TCA
TCA
TCA
TCA
TCA
TCA
TCA
TCA
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
TCA
TCA
TCA
TCA
TCA
TCA
TCA
TCA
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
73
73
73
73
73
73
73
73
79
79
79
79
79
79
79
79
73
73
73
73
73
73
73
73
79
79
79
79
79
79
79
79
50
50
50
50
50
50
50
50
64
64
64
64
64
64
64
64
50
50
50
50
50
50
50
50
65
65
65
65
65
65
65
65
as machined
0.05 in/min
Stroke
Test
Test
Operator Frame
John S.
John S.
John S.
John S.
Debra W.
Debra W.
Debra W.
Debra W.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Debra W.
Debra W.
Debra W.
Debra W.
John S.
John S.
John S.
John S.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
Test
Date
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002

Specimen
Specimen Specimen
Panel
Coupon
Depth
Width
(in.)
(in.)
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
A-55
B-56
B-56
B-56
B-56
B-56
B-56
B-56
B-56
B-56
B-56
B-56
B-56
B-56
B-56
B-56
B-56
1-1
1-3
1-5
3-7
3-9
3-11
8-13
8-15
1-2
1-4
1-6
3-8
3-10
3-12
8-14
8-16
8-18
1-1
1-3
1-5
3-7
3-9
3-11
8-13
8-15
1-2
1-4
1-6
3-8
3-10
3-12
8-14
8-16
Average
Std, Dev.
COV, %
0.10115
0.10020
0.10145
0.10095
0.09955
0.10075
0.09870
0.09870
0.10045
0.10075
0.10160
0.10000
0.10020
0.10125
0.09850
0.09895
0.09980
0.10070
0.10095
0.10075
0.10135
0.10165
0.10125
0.10370
0.10400
0.10080
0.10095
0.10025
0.10145
0.10150
0.10075
0.10375
0.10405
0.25100
0.25085
0.25065
0.25075
0.25070
0.25065
0.24960
0.24965
0.25080
0.25075
0.25040
0.25060
0.25060
0.25040
0.24950
0.24965
0.24960
0.24895
0.25050
0.25025
0.25065
0.25060
0.25065
0.24950
0.24955
0.25050
0.25040
0.25010
0.25070
0.25060
0.25050
0.24950
0.24940
Span
(in.)
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.401
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413
0.413

Ultimate
Initial
Total
SBS
Failure
Load
Load
Load
Strength
Location
(lbs)
(lbs)
(lbs)
(ksi)
293.1
283.1
285.1
332.5
331.6
321.2
287.3
282.2
270.7
272.4
267.7
310.4
283.7
305.7
243.9
270.4
264.8
292.1
315.1
301.6
326.2
320.6
316.4
309.4
315.0
297.2
302.4
289.5
323.8
290.3
282.0
300.1
297.7
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
293.1
283.1
285.1
332.5
331.6
321.2
287.3
282.2
275.9
277.6
272.9
315.6
288.9
310.9
249.1
275.6
270.0
292.1
315.1
301.6
326.2
320.6
316.4
309.4
315.0
302.4
307.6
294.7
329.0
295.5
287.2
305.3
302.9
8.66
8.45
8.41
9.85
9.97
9.54
8.75
8.59
8.21
8.24
8.04
9.44
8.63
9.20
7.60
8.37
8.13
8.74
9.35
8.97
9.63
9.44
9.35
8.97
9.10
8.98
9.13
8.81
9.70
8.71
8.53
8.84
8.75
8.88
0.557
6.27
204
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Interlaminar Shear
Loading Rate:
Control Mode:
Testing
Test Conditions
Facility
Temp
RH
(F)
(%)
TCA
TCA
TCA
TCA
TCA
TCA
TCA
TCA
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
TCA
TCA
TCA
TCA
TCA
TCA
TCA
TCA
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
NIAR
73
73
73
73
73
73
73
73
81
81
81
81
81
81
81
81
81
73
73
73
73
73
73
73
73
78
79
79
79
79
79
79
79
50
50
50
50
50
50
50
50
62
62
62
62
62
62
62
62
62
50
50
50
50
50
50
50
50
65
66
66
66
66
66
66
66
as machined
0.05 in/min
Stroke
Test
Test
Operator Frame
Debra W.
Debra W.
Debra W.
Debra W.
John S.
John S.
John S.
John S.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
John S.
John S.
John S.
John S.
Debra W.
Debra W.
Debra W.
Debra W.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Ken G.
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
Inst 4505
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
MTS 318.1
Test
Date
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
5/20/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
6/3/2002
APPENDIX G. DATES OF PANEL MANUFACTURE AND COPY OF FAA FORM

8130-3
205
206
207
208
209
210
211
212
213
214
215
216
217
218
219
220
221
222
223
224
225
226
227
228
229
230
231
232
233
234
235
236
237
238
239
240
241
242
243
244
245
246
247
248
249
250
251
252

A - Basis and B - Basis

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A - Basis and B - Basis

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Advanced General

A Basis and B Basis

J. Tomblin, J. Sherraden, W. Seneviratne, K. S. Raju

Symbols Used ..................................................................................3

Acronyms and Definitions ..................................................................4

Environmental Conditioning .......................................................11

Fluid Sensitivity Screening .........................................................11

Statistical Analysis ....................................................................14

Material Performance Envelope and Interpolation........................14

Non-Destructive Inspection (NDI) ...............................................20

FAA Test Coupon Conformity and Test Witness ..........................23

Test Coupon Conformity.........................................................23

Test Witness .........................................................................24

Prepreg Documentation by Prepreg Lot............................................25

Data Documentation .......................................................................28

TORAY T700SC-12K-50C/#2510 LAMINA PROPERTIES...........................31

Test Results ...................................................................................32

Individual Test Summaries.........................................................33

Tension, 1-axis ......................................................................34

Tension, 2-axis ......................................................................35

Compression, 1-axis ..............................................................36

Compression, 2-axis ..............................................................37

Shear, 12 axis .......................................................................38

Shear, 13 axis .......................................................................39

Individual Test Charts................................................................40

Tension, 1-axis ......................................................................41

Tension, 2-axis ......................................................................42

Compression, 1-axis ..............................................................43

Compression, 2-axis ..............................................................44

Shear, 12 axis .......................................................................45

Shear, 13 axis .......................................................................46

Raw Data .......................................................................................47

Raw Data Spreadsheets and Scatter Charts ...............................48

Fluid Sensitivity Raw Data Spreadsheets and Scatter Charts .......95

Representative Shear Stress-Strain Curve ................................ 100

3.3. Statistical Results ............................................................................. 102

A.1.10. Fiber Volume ............................................................................ 115

APPENDIX E. METHOD FOR TRANSFORMING VARIANCES OF TEST

major Poissons ratio, tension

Acronyms and Definitions

95% lower confidence limit on the first population

Standard Test Method for Density and Specific Gravity of

Standard Test Method for Apparent Interlaminar Shear

Standard Test Method for Void Content of Reinforced

Standard Test Method for Tensile Properties of Polymeric

Standard Test Method for Fiber Content of Resin-Matrix

Standard Test Method for Volatiles Content of Epoxy Matrix

Standard Test Method for Gel Time of Carbon Fiber-Epoxy

Standard Practice for Determining and Reporting Dynamic

Standard Practice for Determining Cure Behavior of

Shear Properties of Composite Materials by the V-Notched

General Techniques of Infrared Quantitative Analysis,

Standard Practice for General Techniques for Qualitative

Glass Transition Termperature by Differential Scanning

Thermoset Prepreg with Destructive Technique," Suppliers

Material Process Specification for Torayca Plain

Fourier Transform Infrared Analysis," Toray

Differential Scanning Calorimetry," Toray Composites

High Performance Liquid Chromatography," Toray

Lay-up/Vacuum Debulking, Toray Composites

Autoclave Curing, Toray Composites

Panel Tabbing, Toray Composites (America), Inc.,

Tensile Specimen Machining," Toray Composites