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2. The mixture will cool down as it hits the funnel and from vacuum filtration, the
mixture will turn to and produce crystals of the mixture.
7. The sulfanilamide will probably come out as a liquid or oil out rather than a crystalline
because the boiling point of the ethyl alcohol is much higher than the melting point of the
sulfanilamide during that experiment. The sulfanilamide will not crystallize and may come out
as a supercooled liquid rather than a crystal.
Distillation Questions
2. A. 2-Bromopropionic acid could be resolved using pure basic substances, which would
create diastereomer salts.
b. C11H15N is pretty neutral and amphoteric as an amine and could use either a basic or
acidic resolving agent.
c. C8H9OH would act basic with the OH group attached which would mean that we
could use acids like the tartaric acid we used in our experiment to protonate the impure
enantiomer. This creates diasteromer salts, which means it is easier to separate.