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Article history:
Received 18 January 2011
Received in revised form 3 March 2011
Accepted 4 March 2011
Available online 27 April 2011
Keywords:
Physic nut
Oilseed
Biofuel
Screw press
Vegetable oil
a b s t r a c t
The objective of this study was to optimize the mechanical oil extraction of Jatropha curcas seeds by
increasing the efciency of oil recovery and decreasing oil residues in press cake. The experiments were
carried out with mechanical screw press type Komet D85-1G. Four setups were created by parameter
combination of two different screws (16 and 21.5 mm choke ring size), with two different press cylinders
(1 and 1.5 mm bore size), three different nozzles (8, 10 and 12 mm nozzle diameter) and three rotational
speeds (low, medium and high). Oil recovery reduced when rotational speed increases for all setups;
highest oil was 89.4% (m/m). The oil recovery was increasing when energy input increased and decreasing when seed material throughput increased. The relations between energy input and seed material
throughput followed a strict pattern, which correlated with oil recovery. This correlation can be used for
determining the optimal operation parameters.
2011 Elsevier B.V. All rights reserved.
1. Introduction
Jatropha curcas L., belonging to the family Euphorbiaceae is a
shrub or tree that is propagated by cuttings and is widely planted
as a hedge to protect elds from browsing animals (Heller, 1996;
Sirisomboon et al., 2007). The plant produces toxic seeds and is
therefore non-edible to animals and humans. Toxicity of seeds is
due to the presence of curcine and diterpenes, mainly phorbol ester
(Heller, 1996; Makkar and Becker, 1997; Makkar et al., 1998, 2008;
Jongschaap et al., 2007).
J. curcas can be utilized for different purposes: erosion control, living fence, ornamental plant or source of re wood. The
bark is rich in tannin and produces a dark blue dye. Leaves have
been used for rearing of silkworm, in dyeing and in medicine as
anti-inammatory substance (Openshaw, 2000; Basha et al., 2009).
Seeds have been used as insecticide, soap and varnish production.
Seed cakes have been used as fertilizer, solid fuel or in biogas production. Non toxic varieties or detoxied press cake has been used
as feed for animal (Openshaw, 2000; Sirisomboon et al., 2007).
Due to depletion of fossil fuels and the green-house effect, the
application as biofuel is probably the most interesting from both
economical and ecological points of view (Beerens, 2007). Less
awareness was raised to possible human health hazard by using
biogenic fuels until it was found that strong mutagenic compounds
can be released from biofuel combustion (Krahl et al., 2009).
Corresponding author. Tel.: +49 711 459 22840; fax: +49 711 459 23298.
E-mail address: shkelqim karaj@uni-hohenheim.de (S. Karaj).
0926-6690/$ see front matter 2011 Elsevier B.V. All rights reserved.
doi:10.1016/j.indcrop.2011.03.009
1011
limit range for different screws was determined through preliminary tests. Screw R11 allowed for the application of lower speeds
than screw R8 without jamming during pressing. Therefore, the
speed levels for screw press R11 were set lower than for screw
press R8. The dependent variables such as oil content, oil recovery, system temperatures and time required for pressing as well as
torque and pressure in the pressing chamber were monitored via
weight measurements and sensor control (Table 1). Data was collected by a data acquisition switch unit (34970A Agilent, Hewlett
Packard, Palo Alto, CA) and transferred via BenchLink Datalogger
software to a laboratory computer.
Oil recovery efciency was the most important dependent variable considered in this study. The effects of independent variables
on oil recovery optimization could be explained by considering
the dependent variables. For increasing the extraction efciency
increased temperature is benecial. Since friction inside the press
cylinders generates heat which is passed in the oil, reducing the viscosity of the crushed seed material and facilitating oil brake point,
which is the applied pressure for deliberating oil from crushed
seed material (Sukumaran and Singh, 1989). For optimization of oil
recovery, pressure is the most interesting variable to monitor. Pressure is expected to alter when independent variables are changing
and a general hypothesis is that higher pressure will lead to higher
temperature generation and higher oil recovery efciency (Willems
et al., 2008, 2009).
Oil recovery efciency was calculated by comparing the oil content in the press cake to the initial oil content in the seeds extracted
by Soxhlet apparatus, three replicates respectively, and using the
following formula (Beerens, 2007):
O = 1
OC /(1 OC )
OS /(1 OS )
100
(1)
S
t
(2)
(3)
Et
S
(4)
Four different experiment setups were carried out with combinations of different design parameters in order to determine the
effect of independent variables on dependent variables (Table 2).
In Setup 1, screw and press cylinder sizes (R8 P1) were kept constant, whereas nozzle was varied in combination with speed. The
constant parameters for the other setups were R8 P1.5, R11 P1 and
R11 P1.5 respectively for Setups 2, 3 and 4, where the same variation of nozzle was applied through all setups. Speed was altered on
three levels from 220, 290 and 355 rpm on rst and second setup,
whereas on third and fourth setup speed levels were 115, 180 and
255 rpm, respectively.
I
II
p
III IV
VI
VII
VIII
XIII
XIV
T1
XII
T5
T2
T3
T4
XI
IX
Fig. 1. Mechanical screw press for oil extraction and installed sensors, (I) feeding container, (II) feeding hopper, (III) housing, (IV) screw, (V) press cylinder with oil outlet holes,
(VI) heating, (VII) nozzle, (VIII) press cake, (IX) press head, (X) compression zone, (XI) oil collector, (XII) coupling, (XIII) motor, (XIV) speed alternator, (T1T5) temperature
sensors, (p) pressure sensor, (E) torque transducer sensor.
Table 1
Dependent variables for optimization of oil extraction.
Variable
Symbol
Unit
Method
OS
T1
T2
T3
T4
T5
t
p
C
h
Nm
bar
Manufacturer
Greisinger Electronic GmbH
Greisinger Electronic GmbH
Greisinger Electronic GmbH
Greisinger Electronic GmbH
Raytek TX
ETH messtechnik GmbH
Kistler Instrument, AG
1013
Table 2
Experimental setup: R8 and R11 screw press with 16 and 21.5 mm choke ring; P1
and P1.5 press cylinders with 1 and 1.5 mm hole size; N8, N10 and N12 nozzles with
8, 10 and 12 mm restriction size.
Setup 1
R8 P1
Setup 2
R8 P1.5
Setup 3
R11 P1
Setup 4
R11 P1.5
N8 220
N8 290
N8 355
N10 220
N10 290
N10 355
N12 220
N12 290
N12 355
N8 220
N8 290
N8 355
N10 220
N10 290
N10 355
N12 220
N12 290
N12 355
N8 115
N8 180
N8 255
N10 115
N10 180
N10 255
N12 115
N12 180
N12 255
N8 115
N8 180
N8 255
N10 115
N10 180
N10 255
N12 115
N12 180
N12 255
Fig. 4. Temperature at different points (T1T5) on four setups when using two
different screws (R8, R11) and two different press cylinders (P1, P1.5); error bars
indicate min and max values of each temperature measuring point, and boxes depict
median, mean values and interquartile range from 25-th to 75-th percentiles.
(5)
(6)
Fig. 3. Temperature pattern of the screw press (Thermal Imager Fluke Ti20).
Table 3
Oil recovery efciency, oil residues in press cake, seed material throughput, specic energy, torque and pressure generated during the process of oil extraction.
Setup name
S. 1 (R8 P1)b
N8 220
N8 290
N8 355
N10 220
N10 290
N10 355
N12 220
N12 290
N12 355
S. 2 (R8 P1.5)b
N8 220
N8 290
N8 355
N10 220
N10 290
N10 355
N12 220
N12 290
N12 355
S. 3 (R11 P1)b
N8 115
N8 180
N8 255
N10 115
N10 180
N10 255
N12 115
N12 180
N12 255
S. 4 (R11 P1.5)b
N8 115
N8 180
N8 255
N10 115
N10 180
N10 255
N12 115
N12 180
N12 255
a
b
Oil recoverya
O , % (m/m)
Oil residuesa
OC , % (m/m)
Energya ES , kWh/kg
Torque , Nm
Pressure p, bar
84.2
83.9
81.2
83.9
82.7
81.4
84.8
83.6
81.8
8.1
8.3
9.6
8.3
8.8
9.4
7.9
8.0
9.3
3.79
4.72
5.56
3.78
4.96
6.06
3.85
4.63
5.99
0.377
0.393
0.425
0.405
0.360
0.351
0.416
0.431
0.412
58.9
59.0
60.6
61.7
58.3
56.9
70.0
72.7
64.0
4.8
4.6
5.6
4.9
4.9
5.2
5.1
5.5
6.0
78.0
62.9
47.5
67.6
46.1
43.7
49.5
58.6
46.8
7.8
8.0
11.3
5.9
4.8
4.3
6.8
18.4
19.2
89.3
86.8
84.8
85.7
84.9
83.5
84.6
83.8
82.5
5.6
6.9
7.8
7.4
7.8
8.5
8.0
8.3
8.9
4.00
5.19
6.27
3.94
5.13
6.28
4.08
5.18
6.35
0.462
0.445
0.446
0.460
0.432
0.443
0.445
0.423
0.409
79.4
76.4
75.6
77.0
72.6
74.8
74.9
71.1
68.3
4.4
4.9
4.7
4.8
4.7
4.6
5.0
4.9
4.7
71.0
64.4
58.4
84.7
75.5
61.8
57.3
59.1
36.6
19.5
17.0
9.5
14.9
13.2
8.2
7.6
11.3
5.4
84.5
76.3
69.8
81.3
73.7
82.1
76.6
63.2
51.5
8.0
11.8
14.5
9.5
12.9
9.1
11.6
17.1
21.4
5.36
8.55
11.65
5.80
8.94
11.61
5.99
10.19
12.96
0.293
0.284
0.271
0.255
0.262
0.247
0.265
0.251
0.222
131.5
126.0
119.1
119.9
114.1
105.5
131.6
122.4
105.4
15.3
4.9
5.7
7.5
6.2
7.7
5.3
4.9
7.3
85.1
79.7
79.2
42.4
38.8
54.7
67.3
67.9
34.5
21.5
15.8
17.6
14.1
13.6
7.4
18.0
12.4
8.0
83.9
78.4
69.8
76.7
66.6
32.2
65.8
55.8
40.0
8.3
10.8
14.5
11.6
15.8
27.6
16.1
19.9
25.2
6.11
9.56
13.39
6.77
11.88
14.33
7.03
11.56
14.49
0.278
0.261
0.255
0.245
0.237
0.201
0.228
0.202
0.158
141.3
131.1
127.6
138.3
131.1
108.9
133.8
116.2
84.6
4.8
7.0
3.9
5.3
6.0
9.3
5.5
6.8
8.2
75.2
51.6
33.9
40.9
37.3
35.5
44.4
37.3
20.4
22.1
13.6
11.5
9.9
12.6
7.0
9.7
6.0
4.4
(7)
(8)
1.6
3.0
1.4
2.5
1.2
2.0
1.0
0.8
1.5
0.6
1.0
0.4
Oil production
0.5
Energy Efficiency
0.0
10
12
14
0.2
0.0
16
Fig. 5. Correlation between oil temperature (T4) and press cake temperature (T5)
vs. press head temperature (T3) on all analysed setups.
4. Conclusions
Fig. 6. Specic energy input and oil recovery efciency vs. seed material throughput.
The temperature generated on mechanical screw press was created due to resistance of seed material against the press head. Oil
temperature depended on press cylinder and press head temperatures; whereas press cake temperature was only inuenced by heat
generated from the press head. Temperatures up to 140 C were
recorded and highest temperature was generated by using screw
R8 rather than R11.
Oil recovery decreased and oil content in press cake and seed
material throughput was increased when rotational speed of screw
press was higher. Oil extraction with screw press Komet D85-1G
was most efcient by using a screw with 16 mm choke ring size, a
press cylinder with 1.5 mm bore size and a nozzle with 8 mm diameter in contrast to other combinations. Specic energy input and oil
recovery are correlated to seed material throughput. Throughput
can be adjusted by rotational speed of the screw to maximise either
oil production or energy efciency, in which fortunately both maxima where close together. The optimal operation point for screw
press Komet D85-1G was at 11 kg/h Jatropha seed throughput,
resulting in a press capacity of 2.67 kg/h in terms of recovered oil.
The oil extraction efciency was reaching study objectives. Future
studies should focus on analysing different varieties, cultivation
origins and production practices as well as temperature inuence
on oil and press cake quality indentifying threshold temperature
where oil and protein deterioration does not occur.
Acknowledgements
The authors are grateful to the Bundesministerium fr Bildung
und Forschung, Berlin (Germany) for nancial support of Project
0330799A, Optimization of de-shelling and oil extraction of Jatropha curcas L. for direct use in plant oil stoves (01.06.2007 to
30.06.2010).
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