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Computer chip-cyclic
thermal loading.
Fig. 22.30(b), Callister 7e. (Fig. 22.30(b) is
courtesy of National Semiconductor Corp.)
Hip implant-cyclic
loading from walking.
Fig. 22.26(b), Callister 7e.
ISSUES TO ADDRESS...
How do cracks that lead to failure form?
How is fracture resistance quantified? How do the fracture
resistances of the different material classes compare?
How do we estimate the stress to fracture?
How do loading rate, loading history, and temperature
affect the failure behavior of materials?
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
Fracture mechanisms
Ductile fracture
Accompanied by significant plastic deformation
Brittle fracture
Little or no plastic deformation
Catastrophic
Usually strain is < 5%.
Classification:
Fracture
behavior:
Very
Ductile
Moderately
Ductile
Brittle
Large
Moderate
Small
%RA or %EL
Ductile fracture is
usually more desirable
than brittle fracture!
Ductile:
Warning before
fracture
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MatSE 280: Introduction to Engineering Materials
Brittle:
No
warning
4
Ductile failure:
Stress-strain curve
--one piece
--large deformation
BCC iron
%C
Brittle failure:
--many pieces
--small deformation
Figures from V.J. Colangelo and F.A.
Heiser, Analysis of Metallurgical
Failures (2nd ed.), Fig. 4.1(a) and (b),
p. 66 John Wiley and Sons, Inc., 1987.
Used with permission.
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MatSE 280: Introduction to Engineering Materials
Impact loading:
-- severe testing case
-- makes material more brittle
-- decreases toughness
Impact Energy
(Charpy)
More Ductile
High strength materials ( y > E/150)
Temperature
Ductile-to-brittle
transition temperature
final height
initial height
Adapted from Fig. 9.18(b), Callister & Rethwisch 3e. (Fig. 9.18(b)
is adapted from H.W. Hayden, W.G. Moffatt, and J. Wulff, The
Structure and Properties of Materials, Vol. III, Mechanical
Behavior, John Wiley and Sons, Inc. (1965) p. 13.)
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
http://www.uh.edu/liberty/photos/liberty_summary.html
For Liberty Ships it was in the process of steel that was issue for they
made up to 1 ship every 3 days at one point!
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
Very
crack + plastic
Evolution to failure:
Moderately Brittle
necking
fracture
surfaces
Plastic region
Note:
Remnant of
microvoid
formation and
coalescence.
Brittle fracture:
no warning.
void
nucleation
void growth
and linkage
shearing
at surface
fracture
50
50m
m
(steel)
100 m
particles
serve as void
nucleation sites.
Cup-cone fracture in Al
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
Intergranular
(within grains)
(between grains)
304 S. Steel (metal)
Reprinted w/permission from
"Metals Handbook", 9th ed,
Fig. 633, p. 650. Copyright
1985, ASM International,
Materials Park, OH.
(Micrograph by J.R. Keiser
and A.R. Olsen, Oak Ridge
National Lab.)
spherical
dimples
parabolic
dimples
316 S. Steel
(metal)
Reprinted w/ permission
from "Metals Handbook",
9th ed, Fig. 650, p. 357.
Copyright 1985, ASM
International, Materials
Park, OH. (Micrograph by
D.R. Diercks, Argonne
National Lab.)
Polypropylene
(polymer)
Al Oxide
(ceramic)
Reprinted w/ permission
from R.W. Hertzberg,
"Defor-mation and
Fracture Mechanics of
Engineering Materials",
(4th ed.) Fig. 7.35(d), p.
303, John Wiley and Sons,
Inc., 1996.
Reprinted w/ permission
from "Failure Analysis of
Brittle Materials", p. 78.
Copyright 1990, The
American Ceramic
Society, Westerville, OH.
(Micrograph by R.M.
Gruver and H. Kirchner.)
160m
3m
1 mm
Tensile loading
Shear loading
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MatSE 280: Introduction to Engineering Materials
Brittleness of Ceramics
Restricted slip planes (reduced plasticity)
Stress concentrators (voids, pores, cracks, oh, my!)
Chevron marks
From brittle fracture
e.g, MgO
Mg2+
Origin of crack
O2Fan-shaped ridges
coming from crack
Mg2+
O2-
O2Mg2+
O2Mg2+
Mg2+
O2-
O2-
Mg2+
Mg2+
O2-
O2-
Mg2+
What is restriction?
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
Al203
100
0.0
1.0
Plasticity increased
with temperature,
more due to viscous
flow less from slip.
High T
Viscous flow
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MatSE 280: Introduction to Engineering Materials
materials
materials
Craze: microvoids expand and form fibrilar bridges, then coalesce to form crack.
Fig. 9.20
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
a 1/ 2
m = 2 o = Kt o
t
where
t = radius of curvature
o = applied stress
m = stress at crack tip
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MatSE 280: Introduction to Engineering Materials
Surface cracks
a
2 crack fronts
to propagate
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MatSE 280: Introduction to Engineering Materials
1 crack front
to propagate
2a
Internal cracks
0
Surface crack are worse!
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MatSE 280: Introduction to Engineering Materials
A=A=A etc.
Mode I
Mode II
Mode III
A B
A
B
A B
Tensile
Sliding
Tearing
s + P ) = EGc
= 2E(
a
a
Griffiths Criteria
(Tensile mode I)
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MatSE 280: Introduction to Engineering Materials
Fast-Fracture Condition
K = a = EG
c
= constant!!
Fracture Toughness
Gc 2 s
Surface energy
Units of MPam
Hard to measure
stress intensity factor Internal flaws
Measureable (fixed)
materials properties
increasing
LHS of equation => fast fracture will occur when (in a material
subjected to stress s) a crack reaches some critical size a; or, when a
material constains cracks of size a is subjected to some critical stress s.
Point is that the critical combination of stress and crack length at which
fast fracture occurs is a MATERIAL CONSTANT!
FAST Fracture will occur when
K Kc = EG
= constant
c
Fracture Toughness, Kc
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MatSE 280: Introduction to Engineering Materials
Tearing
Sliding
KIc
K = K Ic = XY c
Materials
selection
K = a K = EGc = constant
Ic
K = K = a
Ic
Materials
selection
Design
stress
Geometric factor
mostly 0.5 < Y < 2
Allowable interior or
surface flaw size or
NDT flaw detection
c = 1/2 a interior
or c = asurface
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MatSE 280: Introduction to Engineering Materials
z ~ 0
city building nearby, where employees were at lunch, collapsed burying a number of victims
z ~ 0
and a firehouse was crushed in by a section of the tank, killing and injuring a number of
z ~ ( x + y )
firemen.1
On collapsing, a side of the tank was carried against one of the columns supporting the
elevated structure [of the Boston Elevated Railway Co.] This column was completely
sheared offand forced back under the structure. the track was pushed out of alignment
and the superstructure dropped several feet Twelve persons lost their lives either by
K Ic
Experimentally, the plane-strain condition is found for B 2.5
ys
Plane-strain fracture toughness is K = XY c
Ic
drowning in molasses, smothering, or by wreckage. Forty more were injured. Many horses
belonging to the paving department were drowned, and others had to be shot.2
1. Scientific American 120 (1919) 99.
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
K Kc
XY a
--largest flaw is 9 mm
--failure stress = 112 MPa
design <
Kc
Y amax
Use:
c =
amax <
1 Kc
Y design
NOTE:
only K Ic /
is critical
for design!
Kc
Y amax
112 MPa
9 mm
c amax
4 mm
) (
A
= c amax
Answer:
Reducing flaw size pays off!
( )
c B
= 168MPa
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
F(XY )
Kc =
amax
WB
XY
a /W
Two issues to consider...
1. Does condition of plane-strain hold? If so, use fast-fracture criterion.
2. Use fast-fracture criterion for the correct plate and crack geometry!
Kc =
F(XY )
amax
WB
XY
a /W
With
K
Ic
ys
K
B 2.5 Ic = 4.6 mm, hence, B = 6 mm > 4.6 mm (Plane-strain holds!)
ys
a 16 mm
=
= 0.4 figure gives
W 40 mm
XY = 2.12
With K > KIc, we must expect fracture to occur by fast-fracture in the plate.
We may use fast-fracture criterion: K = XY amax > K c
What would be the largest surface crack in plate to prevent failure by this mode?
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MatSE 280: Introduction to Engineering Materials
Thus,
For yielding, = ys .
For fast fracture,
= pr
2t
if t <<r.
or
If the critical flaw size is less than the wall thickness, t, then fast
fracture can occur without warning (catastrophically).
If critical crack length is ac = t, then the gas will leak out through
the crack before crack can run (no catastrophic failure!).
With
Y a =K
Ic
KIc =Y ac
= Ic
Y a
K
Ic
Hence: ac = S
Y 2 ys
KIc
is key !
Ratio
ys
Now
(See Ex.9.1 Callister)
K Ic
ys
is now important!
37
D.D.
Johnson 2004,2006-2008
=pr/2t
K Ic
Y a
yielding
Steel
400 MN/m 2
Al
fast fracture
(w/ safety)
No yielding
=pr/2t
1000 MN/m 2
ys
fracture
ys/S
w/ safety
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MatSE 280: Introduction to Engineering Materials
2
1 K
1 170MPa m
a = Ic ~
Y 1000MPa
a=
2
1 K Ic
1 23MPa m
~
Y 400MPa
In Aluminum: 1 mm
p= 2 Ic
2
Y r ys
Y t
t = pr
2
K Ic
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MatSE 280: Introduction to Engineering Materials
10
p=
2
2 K Ic
Y r Y
2
ac =
S 2 K Ic
Y 2 Y
Note:
For permissible stress, there is a
penalty to be paid for extra safety.
Either p is lowered or t is increased!
K Ic
Y t
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MatSE 280: Introduction to Engineering Materials
log-log
1. Yield-before-Break
2
K
ac = M ~ Ic
Y
Slope = 1
K Ic2
2. Leak-before-Break
p =M ~
n
1
log K Ic = log Y + logM
m
m
Y = 320 MPa
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MatSE 280: Introduction to Engineering Materials
Slope = 1/2
Increasing temperature...
-increases %EL and K c
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
11
Another is Fatigue:
Failure from dynamic or fluctuating stresses from
Lengthy period of repeated stress or strain cycles.
motor
counter
S = stress amplitude
Sfat
safe
max
m
min
+ min
= max
m
2
= max min = 2 a = 2S
r
R = max
min
time
case for
steel (typ.)
unsafe
flex coupling
tension on bottom
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MatSE 280: Introduction to Engineering Materials
10 3
mean stress
Range of stress
and amplitude
Stress ratio
10 5
10 7
10 9
N = Cycles to failure
S = stress amplitude
10
case for
Al (typ.)
unsafe
S-N behavior
S1
Fe- and Ti-based alloys, fatigue limit
is 35-60% of TS.
safe
3
10
10
10
N = Cycles to failure
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
12
S = stress amplitude
Fatigue
unsafe
S1
S-N Curves
Fatigue limit:
safe
Failure
103
case for
Al (typ.)
- PMMA, PP, PE
105
107
109
N = Cycles to failure
No fatigue limit:
- PET, Nylon (dry)
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
Fatigue Mechanisms
1. Impose a compressive
surface stress(to suppress
typ. 1 to 6
da
m
= K
dN
~
( )
( )
--Method 2: carburizing
shot
put
surface
into
compression
increases
crack gets longer
loading freq. increases.
2. Remove stress
concentrators.
Fig. 9.34
C-rich gas
bad
better
bad
better
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
13
Anelastic - Effects
Adiabatic
load
increase
Adiabatic
load release
No heat transfer
during (un)loading.
Anelastic - Effects
Elastic type
hysteresis loop
Isothermal
load increase
No T during
(un)loading.
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
Creep Failure
Creep
primary
tertiary
secondary
elastic
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MatSE 280: Introduction to Engineering Materials
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Secondary Creep
Tertiary creep
accelerated creep rate
and failure!
Q
& s = K 2 n exp c
RT
strain rate
material const.
applied stress
200
Stress (MPa)
40
427C
538 C
Rupture time
20
10
Short-life creep:
turbine blades, rocket nozzles.
10 -2
10 -1
1
Steady state creep rate (%/1000hr)
649 C
Adapted from
Fig. 9.38, Callister &
Rethwisch 3e.
(Fig. 9.38 is from Metals
Handbook: Properties and
Selection: Stainless Steels,
Tool Materials, and Special
Purpose Metals, Vol. 3, 9th
ed., D. Benjamin (Senior
Ed.), American Society for
Metals, 1980, p. 131.)
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
g.b. cavities
Adapted from
Fig. 8.45, Callister 6e.
applied
stress
Time to rupture, tr
T(20 + log tr ) = L
temperature
function of
applied stress
time to failure (rupture)
24x10 3 K-log hr
T(20 + log tr ) = L
1073K
Ans: tr = 233hr
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MatSE 280: Introduction to Engineering Materials
15
Summary
climb
precipitate
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MatSE 280: Introduction to Engineering Materials
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MatSE 280: Introduction to Engineering Materials
16