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Centre for Innovative Structures and Materials, School of Civil, Environmental and Chemical Engineering, RMIT University, GPO Box 2476, Melbourne 3001, Australia
Faculty of Engineering and Industrial Sciences, Swinburne University of Technology, John Street, Hawthorn, Victoria 3122, Australia
a r t i c l e i n f o
a b s t r a c t
Article history:
Received 11 July 2012
Received in revised form
7 January 2013
Accepted 13 January 2013
Available online 5 February 2013
Luffa sponge is a light-weight natural material which has the potential to be used as an alternative
sustainable material for various engineering applications such as packaging, acoustic and vibration
isolation, and impact energy absorption. The strain rate effect is an important material property for such
applications. In the present study, compressive tests at different strain rates on luffa sponge material
were conducted over a wide density range from 24 to 64 kg m3. A photographic technique was applied
to measure the sectional area which has an irregular shape. The stressestrain curves of luffa sponge
material at various strain rates were calculated based on this measurement. When the dynamic data are
compared with those of quasi-static experiments, it is found that the compressive strength, plateau
stress and specic energy absorption of the luffa sponge material are all sensitive to the rate of loading. It
is also found that the dynamic enhancement for the compressive strength was more prominent than that
for the plateau stress. The underlying mechanism was discussed and claried. Empirical formulae were
proposed for the macroscopic strength, densication strain and specic energy absorption at various
strain rates. A comparison study shows that the luffa sponge has better energy absorption capacity per
unit mass than other cellular materials with similar plateau stress at various strain rates.
2013 Elsevier Ltd. All rights reserved.
Keywords:
Luffa sponge
Energy absorption
Strain rate
Biological material
Sustainability
1. Introduction
Cellular materials are commonly used as packaging and cladding materials to protect products and personnel during collision
and impact events [1]. The mechanical characterization of those
cellular materials at varying strain rates is essential for their efcient use in dynamic loading applications. As we approach the limit
of non-renewable natural resources, there is an increasingly urgent
need to nd alternative materials that full not only the mechanical
stability but also some integrated multi-functional properties with
low environmental impact and renewable source of reproduction
[2]. The fruits of Luffa Cylindrica (LC) have a netting-like brous
vascular system. When they are dried, the brous network structure serves like an open cell foam material. In a recent research [3],
it has been proved that the luffa sponge is potential to be used as an
alternative sustainable material for various practical applications
such as packaging, acoustic and vibration isolation, and impact
energy absorption. The luffa sponge material can be derived from
fruit of the LC plant and has recycling capability and triggered
biodegradability [4,5]. The importance of the luffa sponge material
is growing in our society because of the search for sustainable solutions using new materials. In a recent study [3], the authors
discovered that under quasi-static loading the luffa sponge material
exhibits remarkable stiffness, strength and energy absorption capacities that are comparable to those of a variety of metallic cellular
materials.
A limited amount of research has been conducted on the luffa
sponge as a source of bio-bres and bio-composites in the last ten
years. The previous research indicated that it is a potential alternative material for water absorption [6,7], and waste water treatment [8,9]. The luffa bres were also used as reinforcement bre for
other materials [10e14] and cell immobilization for biotechnology
[15e18]. At the same time, the sponge gourd of LC, the origin of luffa
sponge material, has not yet had their potential fully explored. With
regard to the industrial and technological development, the cost of
fuel is on the increase. Oil is extracted from seeds for industrial use
[6]. The seed of LC is used as oil sources. The oil extracted from LC is
nding increasing use in the production of biodiesel which is now
gaining acceptance because of low CO2 emission and other considerations [19].
However, there is a lack of scientic data on the mechanical
properties of luffa sponge material because up to now its main
practical use has been as a body scrub in the bathroom. The luffa
sponge material and luffa bres have so far found very limited
18
Fig. 1. A luffa sponge specimen with a diameter of 64 mm and illustration of its hierarchical microstructures. The photographs in the middle indicate the orientation of the luffa
bre; and the photographs at the right present the microstructures of luffa bres. Those photographs were taken from different specimens.
Fig. 2. Experimental setup for dynamic compressive tests on luffa sponge material (the
specimens shown are only for the test group with a strain rate of 1 s1).
2.0
1.5
1.0
Normalised data
19
0.5
0.0
0.02
-0.5
0.04
0.06
Time (s)
-1.0
-1.5
-2.0
Fig. 3. Illustration of the overall compression process of high strain rate tests on luffa
sponge specimen (All signals were normalised by an average value for better visual
effect).
3. Experimental results
3.1. Deformation features
Force and displacement histories were obtained from the Instron machine (VHS 8800). A typical force displacement curves are
shown in Fig. 4(a). Similar to other cellular materials, the overall
compressive behaviour can be characterised by a steep elastic region up to compressive strength, a plateau collapse region up to
densication, and a densication region with a sharp increase of
force over displacement. Despite of trivial differences, the curve
also shows clearly a fairly constant compressive force over a long
stroke, which represents an ideal energy absorption feature.
Nominal stress (dened as force over original cross sectional area)
and nominal strain (dened as displacement over original thickness of the luffa sponge specimen) were calculated and shown in
Fig. 4(b) for a different specimen in Fig. 4(a). The deformation
patterns at high strain rate of 102 s1 are shown in Fig. 5. This
conrms that the overall compression of the specimen is axial
(along the longitudinal direction) rather than folding of the wall of
the specimen under dynamic loading. Localised crushing band was
observed in plateau collapse region which is similar to the quasistatic compressive behaviour of luffa sponge material.
The deformation was uniform in the elastic range before it
reached compressive strength. Localised crush bands were observed
in plateau collapse region, and the initial strain for localised
20
Plateau force
to calculate
plateau stress
Peak force to
calculate
compressive
strength
(a) a typical force-displacement curve with three regions for luffa sponge material.
0.0
0.2
0.3
0.4
0.5
0.6
0.7
1.2
1.0
50
40
0.8
0.8
60
Plateau stress
0.52 MPa
30
0.6
20
0.4
Densification strain
10
0.578
0.2
0.0
0.0
0.1
0.2
0.3
0.4
1.4
0.1
0.5
0.6
0.7
0
0.8
Strain
(b) the illustration of using energy efficiency method to determine compressive strength and
calculate plateau stress, densification strain and energy absorption capacity.
Fig. 4. Dynamic compressive history data for luffa sponge material.
plateau stress and energy absorption capacity. The dynamic compressive strength of the luffa sponge material is taken to be the
initial peak stress if it exists. If there is no such peak stress, the
stress at the intersection of two slopes is taken to be the compressive strength, namely, the slope for the initial loading and that
for the stress plateau region. In general, the compressive strength of
the luffa specimen increases with the density. However, for similar
density, the strength varies greatly as well. This is expected,
because other research [3] indicated that the component material
of luffa sponge varied with the weather, maturity, soil etc. For
a traditional rate sensitive material, the strain rate effect is independent on the density of the material. In similar research for
metallic foams [22], it was found that the strength enhancement
ratio with respect to strain rate exhibited a power law relationship.
This relationship is difcult to verify for luffa sponge material due
to the scatter in its mechanical properties. Thus the following formula similar to that for metal foams [22] will be adopted for the
21
Fig. 5. Deformation patterns of luffa sponge under dynamic impact (V0 5.0 m s1, L 52.0 mm; High Speed Cameral settings: frame rate: 10,000 frame per second, shutter speed:
1/50,000, resolution: 512 512 pixels).
r
s0
$P
0
A 1 C
sf
rf
!B
(1)
$P
s0 A 1 C rB0
(2)
22
Za
Ed a
sd
sa
0 a 1
(3)
dEd a
d
Zd
spl
(5)
(6)
(7)
r AL
r v2
m
v 0 v A 0
L
d
t
d
v
r v2
; thus; si 0
d
Ft mv0F
a i
0;
0 i 1
(4)
si A F
0.80
0.65
0.60
0.55
(8)
0.6
0.5
Densification strain
0.70
and
-1
0.75
sd
0.50
0.45
0.40
0.35
0.30
0.4
2
0.2
0.25
0.1
0.20
-1
Strain rate = 10 s
0 -1
Strain rate = 10 s
-3 -1
Strain rate = 10 s
2 -1
Trend line for 10 s
0 -1
Trend line for 10 s
-3 -1
Trend line for 10 s
0.3
0.15
0.0
0.10
20
25
30
35
40
45
50
55
60
65
70
Density (kg/m )
Fig. 6. Strain rate effect on the dynamic compressive strength of luffa sponge material.
20
30
40
50
60
70
Density (kg/m )
Fig. 7. The strain rate effect on the densication strain of luffa sponge material.
-3
0.55
0.50
value is equal to the area under the stressestrain curve. Fig. 9 shows
that the energy dissipation capacity per unit volume increases
favourably with the strain rate. It indicates that luffa sponge material will dissipate more energy under dynamic loading. Thus the
energy dissipation capacity for the range of strain rates considered
can be written as,
-1
Strain rate=10 s
0 -1
Strain rate=10 s
2 -1
Strain rate=10 s
-3 -1
Eq. (7) (10 s )
0 -1
Eq. (7) (10 s )
2 -1
Eq. (7) (10 s )
0.60
0.45
w 1583 1 0:375_0:14 r0 2:35 103 r2:22
0
0.40
0.30
0.25
0.15
0.10
20
25
30
35
40
45
50
55
60
65
-3
Density (kg/m )
Fig. 8. Strain rate effect on the plateau stress of luffa sponge material.
(9)
0.35
0.20
23
-1
Strain rate = 10 s
0 -1
Strain rate = 10 s
-3 -1
Strain rate = 10 s
0.35
0.30
0.25
0.20
0.15
0.10
0.05
20
30
40
50
60
70
Density (kg/m )
Fig. 9. Strain rate effect on the energy absorption capacity of luffa sponge material.
24
0.8
0.7
0.6
0.5
0.4
Compressive strength
Modified plateau stress (MPS)
Plateau stress (PS)
Linear fit of strength
Linear fit of MPS
Linear fit of PS
0.3
0.2
0.1
20
30
40
50
60
70
Density (kg/m )
Plateau stress
0.447 MPa
0.4
Plateau stress
0.266 MPa
0.2
0.0
0.0
0.2
0.4
0.6
0.8
Strain
(b) stress-strain curves for dynamic and quasi-static tests of luffa sponge with type II
microstructures
Fig. 10. Comparison of the stress enhancement features over strain rate.
Calladine [26] and Su et al. [27,28]. It can be seen from Fig. 1 that the
orientations of the bres vary with their locations on the luffa
sponge specimen and the majority of the bres on the inner surface
of the specimen are along the loading direction. We believe that
those bres contribute more to the larger enhancement in the
compressive strength than that in the plateau stress for the luffa
sponge material. A special experiment was conducted in which the
nal crushing length of specimen was controlled to a strain of 30%
using an aluminium tube as a stopper. After that, the specimen was
cut to review the deformation of longitudinal bres on the inner
surface of the specimen as shown in Fig. 11(a). It can be seen clearly
that some of the bres deform outwards, which is similar to the
deformation mode of a half of the type II structure shown in
Fig. 11(b). Other bres serve as an additional mass along the longitudinal bres. The extra energy dissipated in the dynamic loading
process is caused by the axial plastic deformation of the bres along
the loading direction rather than by the bending of bres in the
quasi-static loading process. The length scale of bres with type II
behaviour varies with the imperfection in the alignment of these
longitudinal bres. Fig. 11(a) also shows the bending length is much
smaller on the other side of the luffa sponge specimen. Furthermore,
the photographic examinations performed on the inner surface of
luffa sponge specimens with various densities shows that the
maximum bre misalignments are highly scattered. Apart from this
imperfection at macroscopic level, individual bre walls as shown in
Fig. 1 possess further imperfections at smaller length scales that are
difcult to quantify such as the waviness or non-uniform thickness
25
Fig. 11. Mechanism of the stress enhancement over strain rate for luffa sponge material.
2 1
Fig. 12. Comparison with other cellular materials. (Strain rate for luffa sponge: 10 s ;
Expanded polypropylene [34]: 60 s1; Balsa wood [35]: 3000 s1; Alporas foam [22]:
103 to 102 s1; Honeycombs [36]: for 103 s1 and * for 102 s1; others are quasistatic data [29]. The data are marked by its density in kg m3).
The strain rate effect of the luffa sponge material was investigated in this paper by conducting experiments at different strain
rates on cylindrical specimens of the luffa sponge with a wide range
26
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