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Helmholtz-Zentrum Berlin f
ur Materialien und Energie GmbH, 14109 Berlin, Germany
Former at Max-Planck-Institut f
ur Eisenforschung GmbH, 40237 D
usseldorf, Germany
c
Max-Planck-Institut f
ur Eisenforschung GmbH, 40237 D
usseldorf, Germany
d
Helmholtz-Zentrum Geesthacht GmbH, Zentrum f
ur Materialforschung und K
ustenforschung, Institute of Materials Research, Materials Mechanics, Solid-State Joining Processes,
21502 Geesthacht, Germany
b
a r t i c l e i n f o
abstract
Article history:
Received 2 March 2012
Received in revised form
19 June 2012
Accepted 20 June 2012
Available online 6 July 2012
The use of light-weight materials for industrial applications is a driving force for the development of
joining techniques. Friction stir welding (FSW) inspired joints of dissimilar materials because it does
not involve bulk melting of the basic components. Here, two different grades of high strength steel
(HSS), with different microstructures and strengths, were joined to AA6181-T4 Al alloy by FSW. The
purpose of this study is to clarify the inuence of the distinct HSS base material on the joint efciency.
The joints were produced using the same welding parameter/setup and characterised regarding
microstructure and mechanical properties. Both joints could be produced without any defects.
Microstructure investigations reveal similar microstructure developments in both joints, although
there are differences e.g. in the size and amount of detached steel particles in the aluminium alloy (heat
and thermomechanical affected zone). The weld strengths are similar, showing that the joint efciency
depends foremost on the mechanical properties of the heat and the thermomechanical affected zone of
the aluminium alloy.
& 2012 Elsevier B.V. All rights reserved.
Keywords:
Friction stir welding
Dissimilar joint
Aluminium alloy
High strength steel
Microstructure
EBSD
Mechanical properties
1. Introduction
Energy and environmental issues in transportation systems
have a strong impact on material selection and on the
development of joining techniques [17]. The incorporation of
light-weight materials in many structures (e.g. automotive, shipbuilding and aerospace) allow a reduction of weight and consequently fuel consumption. In this regard, dissimilar joints
between light-weight materials such as aluminium alloys (Al
alloy) and steels are receiving increased interest both in science
and industrial application [820]. However, the substitution of
one material for another is not straightforward and highly
efcient products require appropriate joining processes.
Dissimilar fusion welding between Al alloy and steels is a
challenge in welding control because of the large differences in
melting temperature and physical and mechanical properties of
the alloys involved. The process often results in complex weld
pool shapes, inhomogeneous solidication microstructures and
segregations in addition, the extremely low solubility of Fe in Al
n
Materialien und
Corresponding author at: Helmholtz-Zentrum Berlin fur
Energie GmbH, 14109 Berlin, Germany. Fax: 49 30 8062 15752.
E-mail address: rodrigo.coelho@helmholtz-berlin.de (R.S. Coelho).
0921-5093/$ - see front matter & 2012 Elsevier B.V. All rights reserved.
http://dx.doi.org/10.1016/j.msea.2012.06.076
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R.S. Coelho et al. / Materials Science & Engineering A 556 (2012) 175183
2. Experiments
2.1. Materials
Commercially available materials that are suitable for automotive structures and reinforcement parts were selected for this
study. DP600 and HC260LA HSS plates were chosen to be joined
to AA6181-T4 Al alloy by FSW. The chemical composition and the
mechanical properties of the steels and the Al alloy are presented
in Tables 1 and 2, respectively. It can be seen that the Al alloy
tensile strength is substantially less than those of the HSSs.
The microstructure of the base materials (BMs) is presented in
Fig. 1. The individual microstructural characteristics can be
summarised as following:
(a) the AA6181-T4 Al alloy shows the typical large grains slightly
elongated with a length of about 70 mm;
(b) the HC260LA HSS shows a-Fe (ferrite) grains with a size of
about 40 mm and presence of pearlite on the grain
boundaries;
(c) the dual phase steel DP600 HSS shows a-Fe grains with a size
of about 15 mm (appear dark in Fig. 1c) and the presence of
martensite as a second phase (appears bright in Fig. 1c).
Table 2
Obtained yield, strength and strain values for each material selected for this study.
The values are an average of at least three tensile tests conducted for each
material.
Materials
AA6181-T4 1277 5
HC260LA
3077 1
DP600
3227 5
267 1
317 1
247 1
Table 1
Chemical composition of the materials selected for this study (wt.%).
Materials
*
AA6181-T4
Si
0.85
Fe
0.25
Cu
0.06
Mn
0.09
Mg
0.74
Cr
0.01
Ni
0.002
Zn
0.012
Materials
**
HC260LA
***
DP600
Cmax
0.10
0.10
Mnmax
0.60
1.40
Simax
0.50
0.15
Pmax
0.025
0.07
Smax
0.025
0.008
Almin
0.015
0.02
Timax
0.15
Nmax
0.009
[49]
norm DIN EN 10268, Edition 10.06.
nnn
norm SEW 097 Part 1.
nn
Ti
0.023
Al
Bal.
R.S. Coelho et al. / Materials Science & Engineering A 556 (2012) 175183
177
Fig. 1. Micrographs of the alloy microstructures for each base materials involved in the presented work: (a) AA6181-T4 Al alloy, (b) HC260LA HSS and (c) DP600 HSS.
Fig. 2. Schematic illustration of joint setup studied here (a) Al alloy and steel
joined by FSW in a butt-joint conguration and (b) the relation of real microstructure and tool offset position applied to produce the welds analysed in this
study [14].
Table 3
Welding parameters.
Universal microhardness tests and tensile tests were conducted to assess the mechanical properties of the joints. Regarding the tensile tests, standard at specimens with gauge sections
of 1.5 mm 10 mm 45 mm were extracted by spark erosion
cutting from the base materials and the weld in the transversal
direction of the welding direction. At least three samples from
each base material and from the joints were tested. All welded
specimens were machined on their surface in order to remove the
marks and the crown features left by the tool shoulder and to
avoid any inuences of them on the results. Afterwards, failure
mechanisms of the at tensile test specimens were studied in the
SEM by a fracture surface analysis.
Microhardness was measured on the specimen cross section
according to DIN 50359-1:1997, Universal hardness (HU) standard, applying a 0.02 N load. The measurements were performed
in three different cross section depths in order to check for
through-thickness variance. The measurements crossed all
regions of interest, from the Al alloy side through to the HSS
side. One specimen for each joint setup was tested.
8.0
1600
5.0
5.0
13
1.35
1.0
WRe25
No-threaded
3. Results
3.1. Microstructure of the joints
On the macroscopic scale, the as-welded joints revealed a good
weld surface quality containing neither macro voids/cracks nor
imperfections regarding the weld alignment (Fig. 2b).
Through the weld cross section, both analysed joints revealed
the same microstructure features showing no evidence of mixing
between the Al alloy and the HSS. In both cases, a small amount of
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R.S. Coelho et al. / Materials Science & Engineering A 556 (2012) 175183
Fig. 3. Cross section overview of both investigated joints: (a) Al alloy to HC260LA HSS and (b) the thermo-mechanically deformed interface; (c) Al alloy to DP600 HSS and
(d) the thermo-mechanically deformed interface.
Fig. 4. EDX analysis of element distributions: (a) analysed region, (b) Al distribution in blue, (c) Fe distribution in pink and (d) Zn distribution highlighting the vortex-like
structure on the advancing side in red. (For interpretation of the references to colour in this gure legend, the reader is referred to the web version of this article.)
R.S. Coelho et al. / Materials Science & Engineering A 556 (2012) 175183
179
Fig. 5. Secondary electron SEM micrographs of joint interface highlighting similar features: intermetallic formation and non-smooth interface resulting in mechanical
interlocking between both materials; (a) Al alloy to HC260LA HSS and (b) Al alloy to DP600 HSS.
Fig. 6. TEM investigation of the Al alloyHSS interface: (a) Al alloy to DP600 HSS, (b) Al alloy to HC260LA HSS and (c) selected area electron diffraction pattern from the
Fe2Al5 reaction product on the interface between Al alloy and DP600 HSS.
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R.S. Coelho et al. / Materials Science & Engineering A 556 (2012) 175183
Fig. 7. Universal microhardness measurements horizontally along the Al alloy and the HSS side: (a) Al alloy to HC260LA HSS and (b) Al alloy to DP600 HSS.
Table 4
Obtained yield, strength and strain values for each joint investigated in this study.
Joint
Yield strength
(MPa)
Tensile strength
(MPa)
Elongation
(%)
112 72
119 72
2007 8
211 7 2
87 1
77 1
Al AlloyHC260LA
Al alloyDP600
n
One specimen slide off during the test, therefore only 2 were considered.
in Fig. 8(a) and (b) which have been chosen for improved clarity
in the presentation of results.
Fig. 8. Typical stressstrain curves obtained by tensile test for each BMs (black
and blue curves) and joints (red curves) analysed in this study: (a) Al alloy to
HC260LA HSS and (b) Al alloy to DP600 HSS. (For interpretation of the references
to colour in this gure legend, the reader is referred to the web version of this
article.)
R.S. Coelho et al. / Materials Science & Engineering A 556 (2012) 175183
181
Fig. 9. SEM micrographs showing the fractured tensile test specimen: (a) the schematic illustration of the relationship sample and tool position; (bc) the microscopic
analysis of the fractured surface and (dg) the EDX element distribution analysis highlighting the cracking presence close to the joint interface (dg).
Fig. 10. Inverse pole gures maps from the critical interface Al alloy BM-HAZTMAZ-SZ: (a) cross section and (b) top analysis [14]. The arrows highlight the
gradient in grains characteristics.
4. Discussion
In this study, dissimilar joints between Al alloy and two grades of
HSS were investigated in terms of microstructure and mechanical
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R.S. Coelho et al. / Materials Science & Engineering A 556 (2012) 175183
revealed that the joint curves (red in Fig. 8) follow the tendency of
the Al alloy curve showing almost the same yield and strength. By
evaluating the results presented in Tables 2 and 4, it becomes
clear that the measured ultimate tensile strength for the joints
does not reach the yield strength of the HSS. This fact suggests
that all deformation during the tensile test took place solely in the
Al alloy. Additionally, no evidence of plastic deformation was
observed in micrographs of the tensile specimens, which suggests
once again that the Al alloy is responsible for the overall efciency
of the joint.
Fractography analysis showed that failure always occurs far
away from the joint interface on the retreating side crossing the
interface of the Al alloy BM-HAZ-TMAZ-SZ (Fig. 9). Those regions
(arrow in Fig. 10a) reveal the presence of highly deformed grains
and evidence of sub-grain development. No signicant differences
in hardness were observed crossing those regions (Fig. 7). The
strong differences in a grain size distribution and grain shape
shown in Fig. 10 originate from each region of the joint (BM-HAZTMAZ-SZ) being exposed to different thermo-mechanical cycles.
The gradual accumulation of strain accompanied by the frictional
heating leads to the nucleation and growth of new grains during the
ongoing deformation process (non-homogeneous dynamic recrystallisation). While accumulated plastic deformation increases the
mechanical strength of the TMAZ and SZ, the grains located in the
HAZ reveal relatively small defect densities (concentration of
dislocations and sub-grains) and control the mechanical behaviour
of the joint as the weakest elements of the structure.
Additionally, the fracture analysis suggests that the crack
propagation follows the HSS inclusions. These ne-grained HSS
inclusions are surrounded by the intermetallic compound and act
as stress concentrators upon load. The control of their amount is
crucial for joint efciency. Hence, the welding setup and parameter chosen in this study were crucial for the good acquired
mechanical properties by controlling the tool pin position and
consequently the amount of HSS detached particles and the
interface formation (Figs. 3 and 5) [13].
Acknowledgements
The authors gratefully acknowledge the Helmholtz Association
of German Research Centres for nancial support via the virtual
institute Improving Performance and Productivity of Integral
Structures through Fundamental Understanding of Metallurgical
Reactions in Metallic Joints (VI-IPSUS). The authors also would
like to thank Mr. Martin Preilowski for help in sample preparation
during his undergraduate studies at MPIE.
References
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]
[9]
[10]
[11]
[12]
[13]
[14]
[15]
[16]
5. Conclusions
In the present study, friction-stir dissimilar joints between two
grades of HSS (DP600 and HC260LA) and AA6181-T4 Al alloy were
produced applying the same welding parameters and setup (tool
offset position). The studies focussed on the inuence of distinct
HSS BMs on the joint efciency. The conducted analysis can be
summarised as follows:
[17]
[18]
[19]
[20]
[21]
[22]
[23]
[24]
[25]
[26]
[27]
[28]
[29]
[30]
[31]
[32]
[33]
[34]
[35]
[36]
[37]
R.S. Coelho et al. / Materials Science & Engineering A 556 (2012) 175183
[38] T. DebRoy, H.K.D.H. Bhadeshia, Sci. Technol. Weld. Join. 15 (4) (2010)
266270.
[39] R.S. Coelho, A. Kostka, H. Pinto, A. Rothkirch, J. Dos Santos, A.R. Pyzalla.
Proceedings of the 2008 Denver X-ray Conference, Colorado, USA, 48 August
2008 (manuscript for electronic publication).
[40] A. Kostka, R.S. Coelho, J. dos Santos, A.R. Pyzalla, Scr. Mater. 60 (2009) 953956.
[41] Y. Yong, Z. Da-tong, Q. Cheng, Z. Wen, Trans. Nonferrous Met. Soc. China 20
(2010) s619s623.
[42] P. Venkateswaran, Z.-H. Xu, X. Li, A.P. Reynolds, J. Mater. Sci. 44 (2009)
41404147.
[43] M.A. Mod, A. Abdollah-zadeh, F. Malek Ghaini, Mater. Des. 36 (2012)
161167.
[44]
[45]
[46]
[47]
183