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Despite the existence of several possible optical pyrometric methodologies, the determination of the
true temperature has still not received a universal and perfect solution. We present here an analysis
of our theoretical simulations and experimental measurements that have been carried out in order to
validate a three-color method. Our goal is to test a pyroreflectometer (working wavelengths 0.84,
1.3, and 1.55 m) equipped with an optical fiber probe. This apparatus has been developed for in
situ measurements in severe conditions (high temperature, difficult accessibility, controlled
atmosphere, vacuum,) to determine the true temperature of opaque materials. The method is based
on three monochromatic measurements proportional to the emitted radiance; three monochromatic
measurements proportional to normal reflectivities; the hypothesis of the same bidirectional
reflectivity distribution function (BRDF) for the instrumented sample at the three working
wavelengths. Using the six simultaneous measurements, the diffuse factor and the apparent
diffuse factor are introduced to determine the convergence temperature T that is assumed to be
equal to the true temperature T. After theoretical simulation, the method has been experimentally
verified on several materials and an analysis of the causes of errors and their impact on the method
accuracy and the operator modus, is discussed. The quality of the results obtained demonstrates the
utility of the tricolor pyroreflectometer in a situation where fundamental parameters, such as the
temperature and radiative properties, are difficult to measure. 2005 American Institute of Physics.
[DOI: 10.1063/1.1851497]
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I. INTRODUCTION
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0034-6748/2005/76(2)/1/0/$22.50
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76, 1-1
D. Hernandez
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1
1
1
+
ln0T, =
+
ln1 0,T,.
=
T TR C2
TR C2
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0,0T,fcosd
fcosd.
fcosd,
=
+
ln1 T,0,0T,.
T TR C2
10
11
SI
T, =
1
1
b
=
+
ln1 T0,0T,b.
T TRb C2
R
02
= 0,0T,
05
0,T,cosd
1
1
r
+
ln1 T0,0T,r,
=
T TRr C2
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In many cases of practical interest in near infrared pyrometry, particularly on a narrow spectral range, the assumption
that is independent of can be considered as valid.7 This
statement constitutes the basic hypothesis of the presented
method. In the case of simultaneous measurements of the
radiance temperature, normal normal reflectivity, and using
the bicolor technique at r and b, the radiance functions
become a solvable system of two equations:
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0,T, =
T,0,0T, 1.
Second it is convenient to introduce for physical and mathematical analysis the color temperature Tc ordinary used in
bichromatic measurements:
L0T,r L0Tc,r
=
.
L0T,b L0Tc,b
12
The relation between the true temperature and the color temperature expressed using the Wien approximation is given by
the following equalities (color function):
1 T0,0T,r
1 1
= + ln
T Tc
1 T0,0T,b
C2
1
1
r b
13
Tc is related to TRr and TRb:
Tricolor pyroreflectometer
Tc = Tc,R =
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1
1
r b
c T Tc if 0,0T,r 0,0T,b.
14
(iii)
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b T Tc if 0,0T,r 0,0T,b,
16
17
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B. Simulation results
1
1
.
rTRr bTRb
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To realize the measurements needed by the above hypotheses and for in situ conditions a novel tricolor pyroreflectometer has been developed. It is an improvement of a
previously reported bicolor pyroreflectometer.8
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A. Description
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(ii)
In the case of a gray surface (Fig. 1), the color temperature is equal to the true temperature so the three
radiance temperatures converge to Tc = T = T. Because
the color function (13) is constant, only one point of
convergence is possible with increasing radiance
functions (9)(11). Classical optical bichromatic pyrometry is sufficient to determine the true surface
temperature.
In the case of a decreasing value of reflectivity versus
wavelength (Fig. 2), the color temperature is higher
than the true temperature and all calculated temperatures converge toward T such as Tc T = T TR.
Because the color function (13) is decreasing, and radiative functions (9) and (10) increasing, only one solution is possible. Bichromatic pyroreflectometry is
sufficient to determine the true temperature of the surface.
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FIG. 4. Pyroreflectometer diagram. (A) Emission device, (B) detection device, (C) probe protection, (E) hostile environment, (P) sample, (Z) measurement area, (OF) optical fibers, (L) lenses, (S) beamsplitter, (M) mirror,
(F) monochromatic filter. (1) Optical fiber coupler to emission (2) separator
for monochromatic detection (3) laser diodes (4) photodiodes (5) laser diode
drivers (6) switch (7) delay generator (8) and (8) analog memories (9)
optical fiber connections (v,b,r) index to distinguish the three wavelengths
(De) emission measurement (Dr) emissionreflection measurement.
(i)
D. Hernandez
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(ii)
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To validate the method and the apparatus, the pyroreflectometer has been used with a solar thermal source. The tested
materials are opaque and all samples are disks (30 mm diameter and 3 mm thick).
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(iii)
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Both the emission and the detection modules are commanded by the same delay generator. Therefore, when the
quantified signals are synchronized with the laser diode
pulses, they correspond to the characteristic measurements of
the reflection from the sample. When they are obtained outside this phase of synchronization, they correspond to the
characteristic measurements of its thermal emission. The signals are selected and then stored in the corresponding analog
memories.
A. Experimental set-up
B. Measurement process
B. Measurement method
Tricolor pyroreflectometer
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Several samples have been tested to validate our pyroreflectometry method. Figures 69 present typical curves obtained for materials taken as examples: AlN (massive ceramic, surface Rq = 1.26 m), Inconel (massive metal alloy,
surface Rq = 0.28 m), Er2O3 (powder coated by plasma process on the rear face of a metal disk, surface Rq = 4.52 m).
For AlN (Fig. 6) we approach the case of a gray body. The
color temperature can be taken as the true temperature with
respect to the error measurements. The second sample (Fig.
7) is a metallic alloy used in aeronautical applications. The
26
C. Experimental results
D. Hernandez
Sample
Tc C
TRr C
TRb C
TRv C
0,0T , r
0,0T , b
0,0T , v
Rq
m
T C
T*
LaCr2O3
Plasma
coating
Plasma
coating
Plasma
coating
Plasma
coating
Plasma
coating
Ceramic
Ceramic
Ceramic
Metal
alloy
1026
1049
1047
1045
0.026
0.027
0.031
4.40
1042
1079
1079
1079
1086
0.048
0.047
0.043
4.35
1081
1283
1036
1063
1138
0.273
0.276
0.311
2.33
4.83
1326
30
1202
1155
1161
1145
0.052
0.050
0.091
2.25
4.61
1188
614
1046
971
1014
0.072
0.216
0.205
2.16
4.52
1089
965
953
882
770
802
916
829
737
819
921
834
742
911
938
853
753
0.325
0.262
0.166
0.265
0.329
0.268
0.168
0.239
0.280
0.217
0.174
0.220
2.04
0.77
1.79
0.65
3.01
1.02
1.26
0.28
1003
960
889
758
3
2
2
3
Cr2O
Al2TiO5
FeO
Er2O3
ZrO2
Si3N4
AlN
Inconel
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Product
V. ANALYSIS OF ERRORS
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For a correct determination of the reflectivities, the observation distance x between the head of the optical fiber
probe must be the same during the calibration on a reflectivity reference, and along the measurements. For a variation
dx, the measurements of the reflected fluxes DE+RT , have
the identical proportional error and the emitted fluxes
DET , keep the same value. Consequently the normal normal reflectivities are not true and color, radiance and convergence temperatures and emissivities are correct (second line).
The diffusivity factor determined by convergence is not
the true value. It is worth noting that the method accounts for
variation of the reflectivity factors. Thus the emivissivities
0 , T = 1 T0,0 , T are right.
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T TR,
T
T, + 0,0T,.
=
+
T
TR,
C20T,
26
(i)
Surface
TR,
T ,
0,0T ,
0,0T ,
T / T for
T , = 0
T , / equivalent to
T , = 0.05
S.D.R.
S.D.E.
S.S.
10
10
10
0.01
0.01
0.01
2.53
2.53
0.6
0.3
0.02
1.2
0.24
0.95
0.28
6%
1.8%
2.4%
10% on T / T 5%
2.3% on T / T 30%
8.5% on T / T 6%
Tricolor pyroreflectometer
Tc C
TRr C
TRb C
T Rv C
0,0T , r
0,0T , b
0,0T , v
T C
Ideal
Variation dx = 0.1 mm
for x = 8 mm
Grey/Absorption
r , v , b : 2%
Selective/Absorption
r , v : 2 % -b : 4%
Selective/Absorption
r , v : 4 % -b : 2%
Parasitic/Radiation
r : 0 % -b , v : 20%
1000
1000
889
889
902
902
938
928
0.2
0.195
0.2
0.195
0.2
0.195
2.5
2.56
1000
1000
1000
886
900
936
0.19
0.19
0.19
2.69
1000
977
886
897
936
0.19
0.18
0.19
1.78
954
1024
883
900
934
0.18
0.19
0.18
3.08
1039
1249
889
927
953
0.2
0.2
0.2
1105
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We obtain the same kind of results when the transmission of the thermal radiation is affected in the same proportion (third line). In this case, the reflectivities, the radiance
temperatures and the diffuse factor are erroneous while the
color temperature, the emissivities and the convergence temperature are true.
When the transmissions of the thermal radiations are selectively affected versus the wavelength, all the parameters
are in error (fourth and fifth line). The convergence method
always delivers erroneous values.
When the effective thermal radiation is hampered by a
parasitic flux, the method is not applicable. In Fig. 9 we
present experimental results obtained on a sample semitransparent to the solar radiation: the convergence temperature
cannot be determined.
In all cases, careful attention have to be implemented
during the application of the convergence method. The nature and the evolution of the surrounding conditions have to
be strongly controlled. Errors can be detected when: Tc
Tc,R (parasitic fluxes, erroneous calibrations, ); there is a
significant variation of the signal DR0 T0 , (evolution of the
transmission on the optical path or/and the optical face of the
fibers).
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L0 blackbody radiance
r index when working wavelength is equal to
1.55 m
Rq surface roughness parameter: root mean square
S.D.R. reflective and diffuse sample
S.D.E. emissive and diffuse sample
S.S. specular sample
T samples temperature
TR radiance temperature determined after calibration of the radiometer
Tc color temperature determined after calibration of
the radiometer
Tc,R color temperature determined with radiance
temperatures [Eq. (14)]
T temperature determined with a convergence
method
T0 ambient temperature
T* max. of T* TTR , 0,0T , , T absolute
value for the three working wavelengths
index when working wavelength is equal to
0.84 m
x observation distance between the probe and the
sample (dx variation of x)
0,
d
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0,
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NOMENCLATURE
BRDF bidirectional reflectivity distribution function
b index when working wavelength is equal to
1.3 m
C2 second Planck constant
DE+R samples measurement related to thermal emission and reflection phenomena
DE samples measurement related to thermal emission phenomena
DR0 references measurement related to reflection
phenomena at ambient temperature
L0 samples radiance in the normal direction
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ACKNOWLEDGMENTS
Greek
0
*
0,0