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General Rules
1. No student is allowed to work in the lab without the supervision of an instructor (your TA
or a designated person with qualifications).
2. Only the scheduled experiment can be performed in the lab. No unauthorized experiment
is permitted; alteration/modification of the lab procedure is not allowed unless it has been
checked and okay-ed by your instructor.
3. Eating, drinking, and chewing gum are not allowed in the lab. Chewing gum may absorb
chemicals from the laboratory. During the lab period, store your books and bags under
your bench, do not put them on top of the bench.
4. Keep your work area (fuming hood etc) orderly and clean. Keep shared areas of the
laboratory clean; this includes areas such as the balance area, sink area, side supply bench
facing the window and the storage fuming hood where the reagents, waste
containers/bottles are kept. It is especially important to keep the balance clean and free of
chemical spills.
5. Hands must be completely dry when handling electric plugs, grasp the electrical plug (not
the cord) when removing it from the socket. When using a hot plate, make sure that the
cord is not touching the hot surface of the hot plate, the cord will melt and expose
electrical wires. Unplug the hot plate before you leave the lab.
6. Avoid using any faulty equipment or damaged electric cords; damaged or exposed
electric cords could cause electrocution if touched, or trigger a fire if exposed to water,
report it immediately to your TA.
7. Experiments must be monitored while reactions are taking place or when heating, notify
your TA immediately if you notice unexpected chemical reaction of your experiment or
any unsafe condition. Report all accidents (chemical spill, broken glass, etc.) or/and
injuries (burn, cut, chemical splash etc.), no matter how minor to your TA immediately.
8. Do not run or walk quickly through the lab, before you back up, look behind you to make
sure no one is behind you that you might bump into.
9. Do not get involved in social conversation in the lab; focus on your work and avoid
distraction. No noise and any disruptive behavior will be tolerated.
10. Wash your hands before leaving the lab, be careful not to touch your eyes or other body
areas without thoroughly washing your hands first.
Personal Protection
1. Safety eyewear (goggle, safety glasses) must be worn at all times. Contact lenses
should not be worn during the organic lab period, as vapors and toxic fumes may get
trapped beneath the contact lenses and harm your eyes.
2. You must wear closed-toe shoes. Wear clothes that are made of cotton and can cover
your torso and legs at least to the knees. Short clothes and sandals are not allowed.
3. Long hair should be tied back so it does not fall into chemicals or onto a heating device.
2. Be careful not to contaminate the chemicals. Dont put your spatula directly to take
the solid from the supply bottle , you will be contaminating the chemical. Instead,
pour solid directly into your container by tilting the bottle and rotating it to control
the amount dispensed. If the solid seems to be tightly packed and would not pour off,
close the container and then gently tap the bottle with the palm of your hand to loosen
up the caked solid.
3. Never to dip your medicine dropper directly into the supply reagent container.
Instead, transfer small amount into your container and then working with it using
your medicine dropper.
4. Dispose any left-over chemicals into the labeled waste container. Check with
your TA if you dont know how to dispose it.
5. Keep the flammable solvents, such as diethyl ether, acetone, hexanes, benzene,
toluene, ethyl acetate, ethanol, methanol, etc., away from your heating device. If
highly flammable solvents, such as diethyl ether, hexanes, are used, make sure no
open flame is present in the lab.
6. Make sure to re-cap ALL containers, including the reagent bottles and the waste
containers after each use!
7. Always hold the chemicals away from you; NEVER look directly over reaction flask,
separatory funnel (during work-up, after vigorous shaking), etc.
3. Any broken glass must be cleaned up immediately, but dont attempt to clean it up
without notifying your TA first.
4. If ground glass stopper is stuck, report it to your TA. If you force the stopper off the
bottle or separatory funnel, you may experience chemical splash, burn and injuries.
5. Do not shake a thermometer after melting-point measurement. Lay thermometer on a
towel to cool, away from the edge of the lab bench.
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