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Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.
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IS 5610:1993
Indian Standard
CHLORO-FLUORO HYDROCARBONS OF
THE METHANEANDETHANE-SERIESSPECIFICATION
( Second Revision )
1 SCOPE
1.1 This standard prescribes requirements and
methods of sampling and test for chlorofluoro
hydrocarbons
listed in 4 for refrigeration
and
air conditioning purposes and for use as solvents
and for making aerosol.
1.1.1
Other
fluoro
hydrocarbons,
chloro t
hydrocarbons,
bromofluoro
hydrocarbons
and
chlorofluoro
hydrocarbons
used as chemical
intermediates
in polymerisation,
etc, are not
covered by this standard.
2 REFERENCE
The Indian Standards listed below are necessary
adjuncts to this standard:
IS No.
1070 : 1992
K!Xi ( Part 1 ) :
3710 : 1978
4905 : 1968
5297 : 1977
7062 : 1973
Title
Reagent grade water ( third
revision )
Pictorial markings for handling and labelling of goods:
Part I Dangerous
goods
(first revSon )
Filling ratios for low pressure
liquefiable gas ( first revision )
Methods for random sampling
Perchloroethylene
( tetrachloroethylene),
technical (jirst
revision )
Glossary of terms used in gas
industry
3 TERMINOLOGY
For the purpose of this standard, the definitions
given in IS 7062 : 1973 shall apply.
4 TYPES
The main chlorofluoro hydrocarbons of methane
and ethane series which are extensively used in
various industries, are as follows:
Type
R-11
Chemical Name
Trichlorofluoromethane
Formula
CCl,F
R-12
R-21
R-22
R-l 13
R-l 14
-Dichlorodifluoromethane
Dichlorofluoromethane
Chlorodifluoromethane
Trichlorotrifluoroethane
1,2-Dichlorotetrafluoroethane
CCl,F,
CHCl,F
CHCIF,
CC&FCCIFB
CClF,rr1T7
VVlL *
5 REQUIREMENTS
5.1 For Refrigeration and Air Conditioning
Chlorofluoro hydrocarbons for refrigeration and
air conditioning purpose shall comply with the
requirements
given in Table 1 when tested
according to the methods prescribed in Annex A.
5.1.1 When the refrigerant gas cylinder
with a residual gas content for refilling,
not be drained in an open atmosphere,
the material shall be taken to the plant
for reprocessing.
5.2 For Solvents and Aerosols
returns
it shall
instead
system
Chlorofluoro
hydrocarbons
required for use as
solvents and aerosols shall also comply with the
requirement of minimum purity as given below
when tested by the ~method prescribed
in A-8
in addition to those prescribed in Table I:
R-11 R-12 R-113 R-II4 Method of
Test ( Ref
to Cl No.
in Annex A)
Purity, per_ 98.5 98.5 98.5 98.5
A-8
cent
by
volume, Min
6 PACKING
The material shall be supplied compressed and
liquefied in cylinders of approved design and of
suitable capacity
and
complying
with the
requirements
of Gas Cylinder Rules, 1981 with
such modifications as may bz made from time
to time by the Chief Controller
of Explosives,
Government of India, or other duly constituted
authority.
The material shall be filled as per
filling ratios given under IS 3710 : 1978.
Table 1
Requirements
for Chlorofluoro
Hydrocarbons
for Refrigeration
( Clause 5.1 )
SI
Characteristic
No.
Requirement
m----h
R-12
R-21
R-22 R-l 13 --X-Z
R-;
Method of
Test, ( Ref to
Cl No. in
Annex A )
(1)
(2)
evaporation,
(3)
(4)
10
10
23.8
(5)
25
-
I.5
-29.8
0.3
8.9
0.3
0.5
50
50
50
99.8
99.85
(6)
10
1.5
-40.8
0.3
(7)
25
-
(8)
10
1.5
(9)
A-3
A-4
47.6
3.6
A-5
1.0
0.3
A-5
OC MUX
) Acidity
vi) Residue on evaporation,
+----To
-----+
A-6
50
50
A-7
A-8
mglkg, Max
vii) Purity,
percxt
by volume,
Min
99.8
8 INSPECTION
7 MARKING
7.1 The marking, painting,
labelling and
sport of cylinders shall be in accordance
the requirements of the Gas Cylinder Rules,
with such modifications
as may be made
time to time
by the Chief Controller
Explosives, Government of India, or other
constituted
authority.
AND SAMPLING
tranwith
8.1 Inspection
1981
All containers
in a consignment
shall be
examined and any cylinder,
which shows
evidence of leakage, damage or corrosion, shall
be rejected.
from
of
duly
8.2 Sampling
ANNEX A
( Clauses 5.1 and 5.2
METHODS
AND
OF METHANE
analysis.
A-2 TEST SAMPLE
A-2.1 The test samples from the cylinders
sampled from a consignment
( see 8.2 ) shall be
taken as prescribed in A-2.1.1.
IS 5610 : 1993
A-3 DETERMINATION
OF MOISTURE
A-3.0 General
Principle
Preparation
MAGIC
BALL
JOINT\
SILICA
VENT
GEL
1:!SE-
SLIOAC
ELECTRIC
MOlOR
FOR STIRRER(l120HP)
EVE
IS 5610 : 1993
A-3.1.3.2
Sampling
A-3.2.1 Apparatus -
A-3.2.2 Procedure
of the
Titration
A-3.2.3 Calculation
x lo6
Moisture
content,
=ppm(r)
where
C = volume in ml of Karl Fischer reagent
consumed,
I; = factor of Karl Fischer reagent ( H,O
g/ml ), and
S = mass in g of the sample.
ppm ( MI)
Molecular mass of water
Molecular mass of
carrier gas
where
v = in ppm, is determined From the Hygrometric Unit Equivalence
Table given
in Annex C.
to all refrigerants
A-4 DETERMINATION
ABSORBABLE GASES
Principle
OF NON
P
I
GLASS
WOOL
SILICA
GEL
200
700
l_sJ
SAMPLE
BOTTLE
SAMPLE
INLET
TUBE
DTKNERt
All dimensions
FIG. 2
TWO
BULB
SPRAY
sATMUPBLkNG
in millimetrcs.
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IS 5610:1993
DOUBLE WALLED
EVACUATED FLASK
A-5.2.4 As soon as the reading on the thermometer is constant, record the temperature as
the initial boiling point of the refrigerant.
A-5.2.5 Continue heating the flask kept in the
water bath and record the temperature when
5 ml of the refrigerant has evaporated.
A-5.2.6 Continue
the test and take down
readings at an interval of every 3 minutes till
15 ml of the refrigerant
is left. Note down
this end point.
Fill the boiling range flask with lOO_ml A-5.2.7 Observe the barometric pressure at the
refrigerant
and add 2 to 3 crystals of end.
carbide or silica gel of about 800
A-5.3 Calculation
size.
A-5.2.2 Suspend the thermometer in such a way A-5.3.1 Boiling Range from 5 to 85 Percent
that it does not touch the walls of the tip of Evaporation
the flask.
Find out the difference in temperature recorded
in A-5.2.5 and A-5.2.6 and report as the boiling
A-5.2.3 Immerse the tip of the boiling range
flask in the water bath at a temperature 35C range from 5 percent to 85 percent evaporation
of the refrigerant.
above the boiling point of the refrigerant.
IS 5610 : 1993,
A-5.3.2 Calculate
the corrected initial boiling
point of the refrigerant by adding to the reading
obtained in A-5.2.4, 0.03lC for each miilimetre
of difference of average barometric
pressure
below 760 mm Hg and vice versa.
A-6 DETERMINATION
A-7 RESIDUE
A-7.0 General
Two
OF ACIDITY
A-6.1 Reagent
A-6.1.1
A-6.2
ON EVAPORATION
A-7.1 Method I
Procedure
A-7.1 .l Apparatus
A-6.2.1
_4-7.1.X1
Platinum dish -
A-7.1.1.2 Water
0*2x!.
A-7.1.1.3 Oven controlled.
bath -
Controlled
Thermostatic,
at
100 f
electrically
FIG. 6
100 ml capacity.
As
IS 5610 : 1993
A-7.1.2 Procedure
A-7.1.2.1
A-7.2.2
A-7.2 Method II
A-7.2.1 Apparatus
As shown in Fig. 7, consisting
A-7.2.1.1 Jacketed
glass
of the following.
container
A-7.2.3 Calculation
with ground
Residue on
evaporation,
glass stopper
A-7.2.1.2
joint
Detatchable
element
Procedure
mg/kg = Ooo$
Mr
where
M, = mass in mg of the residue weighed,
and
M = mass in g of the test portion.
A-8 DETERMINATION
A-g.1 Apparatus
A-0.1.1 Dual
Fitted with ------e--e_
--_----____
----------m-e
------m-m_
-----___-
_-
Column
OF PURITY
Gas
Chromatograph ~-
__-_
A-8.1.2 Column
4 meter long copper/stainless
steel tube of
uniform internal diameter ( 4 to 6 mm ), packed
with porapak-Q between 250 micron to 180
micron IS sieve.
A-8.2 Conditions of Test
A-8.2.1 Column Temperature
PIG. 7
100C.
IS 5610 : 1993
A-8.3 Procedure
A-S.4 Calculation
A-8.4.1
where
Am, Aa, Ab = Peak areas of main component
m and other components a, b,
etc ( cm2 ); and
Sm, Sa, Sb = Recorded sensitivities of main
component
m and other components a, b, etc.
NOTES
1 Inert Gas - Tch,r;;e,rmanent
gases (oxygen,
nitromonoxide
and
methane )
gen, argon,
connectively
present in a chlorofluoro
hydrocarbon
and which should be totalled.
2 In case of refrigerants
with higher boiling points
such as R-113, the sample ( 10 micro litre ) is injected
by means of microsyringe
through aseptum
into the
column
through
pre-column
heating
block.
The
chromatogram
is obtained as usual.
3 If the gas chromatograph
has got built in computing integrator
or outside
connecting
integrator,
then the peak area and percent volume will automatically come on the printer/screen.
Sm Am x 100
SmAm+SaAa+SbAb+...
A-0.4.2
sensitivities
P, = recorded
component m and other
a, b, c, etc.
10
of
main
components
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IS 5610 :1993
ANNEX D
( Foreword)
COMMITTEE COMPOSITION
Industrial
Gases Sectional
Committee,
CHD 006
Representing
Chairman
SHRI I. MOOKHERJEE
Members
SHRI P. K. AQARWALA
SHRIKAILASHA~ARWAL(Alternate )
SHRIA. K. ANEJA
SHRI M. P. DHANUKA( Alternate )
SHRID. BANDHYOPADHAY
SHRI N. G. BASAK
SHRIK. P. DOHARE( Alternate )
SHRI H. P. DUBEY
DR S. RAHUT( Aknate
)
SHRI T. GARCJ
SHRIN. K. RAI ( Ahernate )
SHRI L. R. GARG( Alternate )
SHRID. R . GHOSAL
SHRI M. KALYANARAMAN
(Alternate )
SHRI SYKALYANAM
SHRI R. P. KHATOR
DR K. N. NINAN
SHRIA. K. MUKHOPADHYAY
( Alternate )
DR U. C. PANDEY
DR BADRIPRASAD
DY CHIEF CHEMIST( Alternate )
SHRIB. N. QANUN~O
SHRI N. V. RAMANI
SHRI S. GOSWAMY
( Alternate )
REPRESENTATIVE
New Delhi
REPRESENTATIVE
REPRESENTATIVE
SHRI R. S. SAIC+AL
DR P. L. BHATIA( Akerrrate )
SHRIM. V. SHAH
SHRI R. N. CHOKHSI( Alternate )
SHRI N. SIKKA
SHRIS. K . KAPOOR( Alternate )
SHRIA. K. SRIVASTAVA
SHRIS. P. SIN~H ( Altertiute )
( Continued on page 14 )
13
( Continuedfrom
page 13 )
Sulphur Dioxide,
Convener
The Chemicals
SHRI M. R.SOMAYAII
& PIastics
Dam
Members
DR B. K. GUHA
DR K K. BAVEJA (Alternate )
DR P %JESALPURA
SHRI P. S. PAPMESHWARAN( Alternate )
SHRIM. KOCHUKRISHNAN
SHRIS K. LAGHATE
SHRI R. N. BANERJEE ( AIternate)
SHRIM.K.MANEK
SHRI S. KRISHNAN (dhwzate
)
SHRI H.K.NAGAR
SHRI SANDEEP BHATIA (Alternate)
DR D.C. PARASHAR
SHRIPRABHATK.GUPTA
(Alternate)
hd5an
Institute
Gujrat
Fluoro
of Technology,
Chemicals
New Delhi
Limited,
Industries
Industries,
Physical
14
Limited.
Vadodara
Ltd, Udyogmanhal
Bombay
Bhestan
Laboratory,
New DeIhi
Standard
Mark
The use of the Standard Mark is governed by the provisions of the Eureau of Indian
Standurds Act, 1986 and the Rules and Regulations made thereunder. The Standard Mark
on products covered by an Indian Standard conveys the assurance that they have been
produced to comply with the requirements
of that standard under a well defined system
of inspection, testing and quality control which is devised and supervised by BIS and
operated by the producer.
Standard marked products are also continuously cheked by
Details of conditions under
BIS for conformity to that standard as a further safeguard.
which a licence for the use of the Standard Mark may be granted to manufacturers or
producers may be obtained from the Bureau of Indian Standards.
Bureau of Indian
Standards
BIS is a statutory
institution
established
under
the
Bureau oj Indian
of standardization,
promote
harmonious
development
of the activities
certification
of goods and attending
to connected
matters
in the country.
Srandards
Acr,
1986
to
and quality
marking
Copyright
No part of these publications
may be reproduced
BIS has the copyright
of all its publications.
This does not preclude
the free use,
Ian any form without the prior permission
in writing of BlS.
in the course of implementing
the standard,
of necessary
details,
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