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Article history:
Received 9 November 2012
Accepted in revised form 21 February 2013
Available online 5 March 2013
Keywords:
Laser rapid manufacturing on
vertical surfaces
Track geometry
Analytical modelling
Gravity effect
a b s t r a c t
Analytical and experimental studies on geometrical aspects of the deposited tracks were carried out at different
processing parameters for laser rapid manufacturing (LRM) in vertical surface conguration using AISI type 304
stainless steel powder on the substrate of the same material. The vertical downward shift of the deposited track
and its peak due to the gravity ow of the melt were found to follow quadratic dependence on the track height.
The downward rounded bulging was found to be quite signicant for the scan speeds lesser than 200 mm/min,
while this was insignicant for the scan speeds more than 400 mm/min. A set of consolidated processing parameters for continuous material deposition was identied. The threshold value of laser energy and powder fed, both per
unit traverse length for the continuous deposition were found to be ~96 J/mm and ~0.006 g/mm respectively. The
maximum powder catchment efciency was ~42% for stand-off distances in the range of 1518 mm. The surface
waviness factor was found to decrease from ~0.95 to ~0.05 when the overlap index was increased from 30% to
80%. The study provides a deeper insight into the ensuing geometrical aspects of the tracks using LRM in vertical
conguration.
2013 Elsevier B.V. All rights reserved.
1. Introduction
Laser rapid manufacturing (LRM) is one of the advanced additive
manufacturing processes. It is similar to laser cladding/alloying at the process end with an extended capability of fabricating three-dimensional object directly from a solid model. LRM employs a high power laser beam as
a heat source to melt a thin layer on the surface of the substrate/deposited
material and fed material to deposit a new layer as per shape and dimensions dened in numerical control code as per the solid model. A number
of such layers are deposited one over another resulting in three dimensional (3D) components. LRM offers many advantages over conventional
subtractive techniques, such as reduced production time, better process
control and capability to form functionally graded parts [1]. It employs a
high power laser like CO2, Nd:YAG, diode and bre as energy source to
melt and deposit a layer of the desired material in the form of powder
or wire onto the substrates/previously deposited layers forming a sound
metallurgical bond [2]. A wide variety of the deposit materials and substrates are reported in literature for various applications in automotive,
aerospace, machinery, petrochemical, power generation and shipbuilding
industries [16]. Since most of the laser rapid manufacturing applications
involve deposition of materials on the horizontal surfaces, there have
been theoretical and experimental studies of laser rapid manufacturing
process in the horizontal conguration [713]. The technology is
also being investigated for the laser rapid manufacturing of porous
Corresponding author. Tel.: +91 731 248 8384; fax: +91 731 248 8380.
E-mail address: paulcp@rrcat.gov.in (C.P. Paul).
0257-8972/$ see front matter 2013 Elsevier B.V. All rights reserved.
http://dx.doi.org/10.1016/j.surfcoat.2013.02.044
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828
Nomenclature
ai
A
Cp
D
El
g
hc
H0
hmax
hmin
i
j
k
k1
L1
L2
Lm
M
md
_p
m
mp/l
PL
Pp
Rg
rl
rp
st
s
T
Tamb
Tm
U(z)
V
v
W
w
wmax
X
Y
Z
Greek symbols
l
laser absorptivity
density, kg/m 3
L
density of liquid metal, kg/m 3
tendency before solidication for prediction of track geometry. The consolidated processing parameters for various values of laser energy per
unit length of track, powder fed per unit length of track and overlapping
indices for this process were experimentally identied. The effect of
19
20
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828
Fig. 1. Schematic arrangement of laser cladding head for processing vertical surfaces.
laser beam passes away [18]. For better laser energy deployment
and improved powder utilization, the width of powder stream should
nearly be laser beam diameter. For this, the maximum height of track
may be written as
l P L P p
T x; y; z
f x; y; z; v
kr l
h max
f x; y; z; v 0
ExpH
p3 d
2
1 2
2 2
Y 2
X2
Z2
H
2:
2
2 1
2
"
2r2l
r 2p
#!
C p T m T amb Lm :
Assuming that the track height has parabolic cross section along
xz plane [23] and deriving w(y) from the melt-pool geometry on
the top layer of the substrate, the track height at any point (x, y) is
given by
"
hx; y hmax 1
y L2 2
L1 L2 2
#"
1
x2
wy2
#
6
where,
_p
c m
:
2L r l v
The melt pool boundary was estimated by calculating the temperature prole for T > Tmelt from Eq. (1). Thus obtained moving melt
pool is divided into two regions, one representing the front part of
the pool and another representing the rear part of the pool. As described by Ahsan and Pinkerton [22], the boundaries of these regions
of pool may be approximated as half ellipses dened by the melt pool
width (w) and the melt pool length in the forward direction, L1, and
the melt pool length in the rear direction, L2 (refer to Fig. 2). The
melt pool has asymmetry about the x-axis that increases with the
scanning speed. The maximum height of track can be deduced by following the principle of conservation of energy and mass for powder
particle ow, as described in our previous work. It may be noted
that Marangoni ow is important for the prediction of melt pool
boundaries. In the present study, the effect of uid motion due to
the thermo-capillary (Marangoni) phenomena is incorporated by
modifying the thermal conductivity K for the estimation of track geometry. Since the track material is just above the melting point during
LRM, other phenomena, like gravity, surface tension, viscous forces,
predominate for the shape of the molten metal drop as the moving
s
y2
wy r l 1 2 for y > 0
L
s1
2
y
rl 1 2 for yb0:
L2
Once the powder particles reach the molten pool on the vertical surface, it gets melted and trapped by the surface tension and viscous
forces (both temperature dependent) and counter acting gravity force.
The details of temperature dependence of the material properties are
Fig. 2. Schematic diagram of a moving melt pool in y-direction during LRM on vertical
surface.
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828
discussed in the later part of this section (in Eqs. 1517). In the present
section, a simplied model is presented in 2-D conguration where the
shape of the molten metal drop is resulted from the downward ow
under gravity, surface tension, viscous forces as the moving laser
beam passes away. Fig. 3(a) and (b) show the schematics of the molten
metal proles under gravity of melt-pool at time t = 0 at a point in xz
plane and at time t = (2rl/v), i.e. at the time when laser passed through
that point. As the molten metal is viscous and gets solidied as the moving laser beam passes away, the ow of molten metal is in laminar regime. This ow of molten metal due to gravity is resisted by the
viscosity and the surface tension at the free surface of liquid metal. Following Newtonian uid relationship for viscosity incorporating the
gravity and Kim and Na [24], the ow of molten metal may be described
as
L
U z
d T
L gz
dT s
z
One can substitute values of 1 and DTS from Eqs. (9) and (11) into
Eq. (8). After integrating it, one obtains
L U z L g
d
Kai
s H 0
1 A Rg s ln1 Kai
dT
1 Kai T
"
#
rl
z2
L g 1 DTS z :
v L
2
14
Eq. (14) can be solved to get the loci of the top boundary of the
track. In the above, time of solidication of deposit is the same as
that of laser interaction time. It is to be noted here that the local
layer uid displacement (x) is less at higher scan speeds due to
lower laser interaction time and subsequently lower time of local solidication. Material properties of AISI 304 stainless steel used in the
calculations are taken from Kim and Na [24] and they are given in
Table 1.
The temperature dependence of the density [29] and viscosity [30]
of liquid metal is incorporated as follows:
L T b
!
10
1 A1 A3 1
1A2
15
where,
and
TT m
T b T m
A1 1:829
A2 0:03MT m =T b 0:5 2:7 104 MT m =T b 2 A1 1
A3 m 1A2 1A1 :
b
T
h TT amb
:
DTS c
k
s
11
13
where
H0
Rg T
z2
1 DTS z:
2
K k1 exp
21
1:61
12
16
Here, subscripts m, b, and s in Eqs. (15) and (16) refer to the melting point, boiling point, and saturation state, respectively. Further,
L T A:
1=2
M
T
1=2
:T : exp B: m
2=3
T
V
Fig. 3. Schematic diagram of deposited clad prole at (a) t = 0 and (b) t = (2rl/v).
17
22
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828
Table 1
Material properties of AISI 304 stainless steel.
Parameter
Unit
Value
ai
A
Rg
Tm
H0
s
k
wt.%
N/(m K)
kg/m3
kg/(m s)
J/(kg mol K)
K
J/(kg.mol)
J/(kg mol m2)
W/(m K)
0.001
1.0 104
7200
0.05
0.9
8314.3
1723
1.88 108
1.3 108
580
where,
1=2
A 1:80 0:38 108 J=Kmol1=3
B 2:34 0:2:
downward shift of the deposit and its peak. The height (z) of the
deposit is a function of powder feed per unit length for given laser
power and the same stand-off distance. Also, higher height of the
track results in higher uid velocity at farthest layer, where z = hmax.
Thus, the higher powder feed per unit length leads to higher shift of deposit and its peak for the same system conguration.
Fig. 4(a)(d) present the analytical results showing the effect of
gravity at various scan speeds on the track geometry for a set of
laser processing parameters (laser power = 1.6 kW and powder
feed rate = 10 g/min). It is evident that the deposit shifts downward
at lower scan speeds (v = 200 mm/min). Little shift is observed for
scan speed of 400 mm/min and it is insignicant for higher scan
speeds (v 700 mm/min). It is because for higher scan speeds, the
interaction time is also small and hence, the time period for deposit
to remain in molten state is small. As a result, higher effective viscosity counters the ow of molten deposit under gravity. On the contrary, at lower scan speeds leads to higher interaction time and
longer time period for deposit to remain in molten state. The lower
4. Experimental studies
AISI type 304 stainless steel is general purpose austenitic stainless
steel with a face centred cubic structure. It derives its stainless characteristics through the formation of an invisible and adherent Chromium
rich oxide lm. It is essentially non-magnetic in the annealed condition
and can only be hardened by cold working. As this material is used
widely for various industrial applications, it has been selected as the
feed material for present study. Comprehensive experimental study
was carried out on the substrate of the same material (size: 75 mm
diameter and 12 mm thick) to study the effect of different processing
parameters on the track geometry. Initially, a number of single tracks
were deposited at various combination of laser power, scan speed and
powder feed rate. Table 2 summarizes the experimental trials and subsequent deposited track geometries. The cross sections of these tracks
were examined using optical microscopy. The images of these tracks
were used to measure track dimensions, i.e., width and height. The single tracks were also deposited at various stand-off distances. The powder catchment efciency was evaluated experimentally by measuring
the weight of the substrate before and after single track deposition
using precision electronic balance having least count of 1 mg. The effect
of overlapping parameter on the surface roughness and waviness of
the overlapped tracks was experimentally determined by measuring the surface nish using TaylorHobson make surface roughness
tester model: Surtronic 3 + and height gauge with puppy dial and
9pt?>sub-millimetre probe respectively. To demonstrate LRM on vertical
surfaces applications, the developed LRM head was used on concave and
convex surfaces of tubular geometry.
5. Results and discussion
5.1. Effect of laser processing parameters on deposited track geometry
Experiments were carried out with bre laser of beam diameter
2.0 mm. As illustrated in Eq. (14), the local uid displacement in the
molten pool due to gravity depends primarily on interaction time
[=laser beam diameter (2.rl)/scan speed (v)] and consequently on
the solidication rate. The larger interaction time allows more period
for uid to ow downward resulting in shifted deposit and its peak.
The uid properties, i.e., density, viscosity and surface tension of molten metal govern the ow tendency under gravity of the deposit. As
these properties are the functions of the molten pool temperature,
the lower interaction time results in lower bulk mean average temperature of molten pool and consequently, it leads to higher average
density and extremely high viscosity. Subsequently, it results in little
Table 2
Experimental trials and measured dimensions of deposits.
Laser power
Scan speed
m/min
g/min
Height
Width
Remark
mm
mm
800
800
800
200
400
700
6
6
6
0.815
0.325
0.225
2.375
1.75
1.61825
800
1000
0.17
1.2525
1200
400
0.085
1.378
1200
1200
1200
400
700
1000
6
6
6
0.5
0.33
0.285
2.195
1.9475
1.96
1600
700
0.31
3.131
1600
1600
1600
800
800
800
400
700
1000
200
400
700
6
6
6
10
10
10
0.64
0.42
0.38
1.105
0.56
0.285
2.71
2.2425
2.915
2.265
1.9225
1.7225
800
1000
10
0.175
1.6225
1200
1200
1200
400
700
1000
10
10
10
0.655
0.335
0.27
2.5675
2.41
2.245
1600
1600
1600
800
800
800
400
700
1000
200
400
700
10
10
10
14
14
14
0.725
0.515
0.425
1.44
0.81
0.41
2.96
2.71
2.5725
2.4675
1.905
1.7325
800
1000
14
0.27
1.5875
800
400
18
1.89
2.623
1200
400
14
0.95
2.4075
1200
1200
700
1000
14
14
0.5
0.355
2.395
2.2425
1600
1600
1600
400
700
1000
14
14
14
0.955
0.525
0.43
3.1475
2.5025
2.635
Regular deposit
Regular deposit
Non-uniform
deposit
Non-uniform
deposit
Non-uniform
deposit
Regular deposit
Regular deposit
Non-uniform
deposit
Non-uniform
deposit
Regular deposit
Regular deposit
Regular deposit
Regular deposit
Regular deposit
Non-uniform
deposit
Non-uniform
deposit
Regular deposit
Regular deposit
Non-uniform
deposit
Regular deposit
Regular deposit
Regular deposit
Regular deposit
Regular deposit
Non-uniform
deposit
Non-uniform
deposit
Non-uniform
deposit
Non-uniform
deposit
Regular deposit
Non-uniform
deposit
Regular deposit
Regular deposit
Regular deposit
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828
23
Fig. 4. Vertical transverse cross section of track as per analytical model with laser power of 800 W and powder feed rate of 10 g/min at various scan speeds: (a) 200 mm/min, (b)
400 mm/min, (c) 700 mm/min, and (d) 1000 mm/min.
uid velocity results in higher shift of deposit's peak for the same interaction time. Fig. 7(a)(c) presents the experimental results for the
above sets of laser processing parameters. The effect of gravity at various powder feed rates on the track geometry is evident in both analytical and experimental results.
The maximum displacement of deposit's peak (i.e., at z = hmax)
for various scan speeds was obtained from Eq. (14) and their comparison with experimental data is presented in Fig. 8. It clearly indicates
that the shift of deposit's peak is the cumulative effect of surface tension, viscous force against gravity, scan speed and deposit's maximum
height. The term exhibiting the effect of surface tension, viscous force
against gravity is due to vertical orientation of the surface for LRM. It
may be noted that the shift of deposit's peak increases with decrease
in the scan speed for the same deposit height and it is parabolic for
lower scan speeds (v b 200 mm/min). At relatively higher scan
speed (e.g. v ~ 400 mm/min), the shift of deposit's peak tends to be
a straight line for various deposit heights, while it is negligible for
higher scan speeds (v 700 mm/min). The experimental results for
the shift of deposit's peak for various deposit heights are in agreement with that of analytical modelling.
24
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828
Fig. 5. Vertical transverse cross section of track as per experimental model with laser power of 800 W and powder feed rate of 10 g/min at various scan speeds: (a) 200 mm/min,
(b) 400 mm/min, (c) 700 mm/min, and (d) 1000 mm/min.
Scan Speed v
Laser Power P L
Scan Speed v
18
19
The parameters laser energy per unit traverse length and powder fed per unit traverse length governs the laser energy and the material available for the single track deposition, respectively. Fig. 9
presents the consolidated processing parameters for LRM on the vertical surface for the experimental range of parameters under investigation. At extremely high laser energy per unit traverse length and
lower powder fed per unit traverse length, there may be vaporization
of the feed material. As a result, there may be very thin or no track
formation. On the contrary, at extremely low laser energy per unit
traverse length and higher powder fed per unit traverse length, the
feed material may not fuse and form a discontinuous irregular track.
Hence, there is processing zone, where a balance of both the parameters, results in fused continuous track. The threshold value of laser energy and powder fed, both per unit traverse length for the continuous
deposition were found to be ~96 J/mm and ~0.006 g/mm respectively.
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828
25
Fig. 6. Vertical transverse cross section of track as per analytical model with laser power of 800 W and scan speed of 200 mm/min at various powder feed rates: (a) 6 g/min,
(b) 10 g/min, and (c) 14 g/min.
Our experimental study with other material depicts a similar trend. The
obtained consolidated processing parameters are found to be closer in
terms of trend and values to the earlier published similar work for
laser rapid manufacturing in horizontal conguration [31,32].
5.3. Powder catchment efciency
The powder catchment efciency is one of the important processing
parameters for high quality track geometry and economical viability of
the process. It is the ratio of the powder deposited to the powder fed for
the deposition during the LRM process. Mathematically,
c
20
Fig. 7. Vertical transverse cross section of track as per experimental model with laser power of 800 W and scan speed of 200 mm/min at various powder feed rates: (a) 6 g/min,
(b) 10 g/min, and (c) 14 g/min.
26
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828
Fig. 10. Powder catchment efciency as a function of stand-off distance between nozzle tip and substrate during LRM on vertical surfaces.
overlap index i
The surface characteristics of the track geometry on vertical substrate play an important role as it denes the manufacturing tolerance
and post processing of the deposits. Generally, multi-layer overlapped
tracks are used for the fabrication of any engineering components on
the surfaces. Higher waviness and poor surface roughness means less
effective deposition to achieve on the plane surface. The LRM surfaces
have two distinct characteristics surface roughness and surface waviness. The surface roughness is primarily due to semi-molten powder
particles adhered on the deposit, while overlapping parameter governs
the surface waviness to a great extent.
st
100
W
waviness factor j
h max h min
:
h max
21
22
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828
27
Fig. 13. Laser vertical surface cladding on (a) internal and (b) external surface of tubular
geometry.
Fig. 11. Schematic diagram for various parameters for overlapped deposition.
surface nish was also measured in the samples across and along the
track. The surface nish was found to be 1214 m Ra and 912 m Ra
across and along the track, respectively. A similar trend is observed for
surface nish along and across the tracks for LRM on horizontal surfaces
[3335]. The surface nish during LRM on horizontal surfaces with the
28
C.P. Paul et al. / Surface & Coatings Technology 224 (2013) 1828