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19, 1954
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2 Sheets-Sheet 1
H. o. FoLKlNs ETAL
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2 sheets-sheet 2
_ ww
| tl
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CARBON DISULFIDE
(Cl. 23-206)
n. ,
have beenrfound to cause Vsevere catalyst con- .-. - is extremely advantageous in a reaction of this
with tars and polymers.
'
stoichiometric
requirements,
preheating
the
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4
In coil 22 of heater t, the molten sulfur is
heated to a sufficiently high temperature to vap
orize it, as for example, 850 to 12%o F. under
given operating pressures. Preheated charge gas
leaves coil S by line 24, controlled by valve 25, and
passes to line 225 Where it joins and uidizes the
tion 46.
high `chromium content, Vand 4cliromiuzneniclcel 70 scribed in Figure 5.2. The vreaction products may
stainless steels stabilized ywith molybdenum, etc.
contain considerable amounts 4ofinesulfur par
.have proved eiective. Other -materials 'of con
.struction include :aluminum coated steels, ire
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the system.
'
i f
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is reduced to 31019112- 'or less, to accumulator 22.6.
f'gas and/'or vapor which vremains "uncon
DIOCBSS.
of constituents
to .form
'
lessened.
-Having thusdescribed `the apparatus useful in .175 when used according to the methods outlined
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operation.
ing processes.
'
the invention:
'
the catalyst.
_,
60
volume calculated at 0
IIYhe regeneration-of used agglomerating ma-_ vterial is' eifected by suspension ofthe particles.
in an oxygen-containing gas and passage,V of the
suspension> through a regeneration zone under
conditions adapted to cause combustion of the
acca-,69o
l2
ll
. What is claimed
glomerating. material being capable of occluding 40 in which the agglom'erating matei'ialisv selected
saidisulurecontaining by-products and-said reac
tion zone being maintained under conditions to
promote. the formation of , carbon disulfide and
'
Y'
to reaction temperature._
to10:1.A
__
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14
phere.
17. The method in accordance with claim 16 in 5
Number
Name
Date
2,187,393
which the oxidizing atmosphere is an'oxygen
2,330,934
containing gas.
Y
2,389,810
18. The method in accordance kwith claim 16
2,480,639
in which said agglomerating material is a cat
alyst capable of promoting the formation of car- l0 2,487,039
2,530,243
2,556,177
HARVEY HENNIG.
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