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Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.
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BharthariNtiatakam
IS 263:lWO
Indian Standard
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( Reaffirmed 2005 )
UDC
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661651 : 66558
@ BIS 1990
BUREAU
MANAK
OctobeY1990
OF INDIAN
BHAVAN,
STANDARDS
9 BAHADUR SHAH
NEW DELHI 110002
ZAFAR
MARG
Price Group 3
CosmeticsSectional
Committee,
PCD 19
FOREWORD
This Indian Standard (Fifth Revision ) was adopted by the Bureau of Indian Standards
on
5 March 1990, after the draft finalized by the Cosmetics Sectional Committee had been approved
by the Petroleum, Coal and Related Products Division Council.
Boric acid is used as a preservative
in cosmetic formulations.
It finds use in aftershave
preparations, bath preparations, deodorants, mouth washes, in nail bleaches and in skin powders.
In this revision,
This standard covers requirements of boric acid for cosmetic industry only.
cosmetic use has been covered by a separate standard, IS 10116 : 1982.
Boric
IS263:1S!Ml
Indian Standard
are neces-
acid
( third
revision )
266 : 1977
323 : 1959
1070 : 1977
2088
: 1983
4905
: 1968
10116 : 1982
4 SAMPLING
4.1 The method
of drawing
representative
samples of the material and the criteria for
conformity, shall be as prescribed in Annex B.
5 PACKING
Title
Hydrochloric
to the methods
prescribed
in Annex
A.
Reference to the relevant clauses of Annex A is
given in co1 4 of the Table 1.
of
Boric acid
AND
MARKING
5.1 Packing
5.1.1 The material shall be packed in suitable
containers of appropriate
capacity,
so as to
ensure satisfactory stability and exclude contamination by extraneous matter, or in a manner
as agreed to between the purchaser
and the
supplier.
5.2 Marking
5.2.1 The containers shall be securely closed and
marked with the following information:
3 REQUIREMENTS
b)
Indication
3.1 Description
c>Batch
Date of manufacture;
3.2 The material shall comply with the requirements given in Table I when tested according
Table
Requirements
far Boric
(Clauses
3.2
Ac$d
far Cosmetic
.ri
Industry
'
and B-5.2 )
ii)
(4)
A-2
), ppm, MUX
10
A-3
20
A-4
iii)
Heavy
iv)
05
005
v)
vi)
Solubility in water
vii)
Solubility
viji)
Fineness
ix)
of Test
in
( Ref_t;teLyj
(2)
(1)
i)
Method
Characteristic
Sl
No.
A-6
1
in alcohol
A-5
A-7
A-8
As agreed to between
buyer and seller
A-9
A-10
Sulphates
ANNEX
QUALITY
OF TEST
FOR BORIC
ACID
OF BORIC
ACID
A-2.1 Reagents
Mannitol
or Sorbitol -
Sodium Hydroxide
PhenoQhthalein
Indicator
Solution -Solution -
1 N.
Boric
acid,
percent
by mass
6184 V
-=- M
Dissolve
INDUSTRY
OF REAGENTS
A-2 DETERMINATION
FOR COSMETIC
a of phenolphthalein
where
V == volume in ml of standard sodium
hydroxide solution used in the
titration; and
A-2.2 Procedure
Accurately weigh about 1 g of the dried material
preserved as prescribed in A-5.2 and dissolve it
M =z mass
3*
18263:1990
A-3 TEST FOR ARSENIC
A-3.1 Preparation
Dissolve
water.
1000
of Solution
g of the material
in 20 ml of
.A-3.2 Carry out the test for arsenic as prescribed in IS 2088 : 1983 with the solution obtained
in A-3.1, using 001 mg of arsenic trioxide for
comparison.
A-4 TEST
FOR
HEAVY
METALS
A-4.1 Apparatus
a) Kessler Cylinders A-4.2
50 ml capacity.
Reagents
Dilute
1 N.
b)
Hydrogen &&hide
Solution pared, saturated solution.
Hydrochloric
Acid -
A-5.3 Calculation
approximately
freshly
pre-
Procedure
ON DRYING
A-5.1 Apparatus
M = mass in g of the
for the test.
A-6 TEST
FOR
material
taken
IRON
A-6.1 Reagents
b)
cl
Ammonium Persulphate -
IS 265 :
solid.
Butanolic Potassium
Thiocyanate Solution Dissolve IO g of potassium thiocyanate in
10 ml of water and add sufficient nbutanol to make up the volume to 100 ml.
Shake vigorously until the solution is clear.
Standard Iron Solution - Dissolve 0702 g of
ferrous
ammonium
sulphate
[ FeS04.
in water in a I-litre
(NH&.SDI.GH~O]
flask, add 4 ml of concentrated sulphuric
acid (see IS 266 : 1977 ) and dilute with
water to the mark. When required for
test, dilute 10 ml of this solution to 100 ml
in a graduated flask. One millilitre of the
diluted solution contains 001 mg of iron
( as Fe).
A-6.2 Procedure
made
of
glass
or
a) Dish - Circular,
aluminium,
100 mm in diameter
and
10 mm deep, with tight-fitting cover or lid.
A-5.2
1OOm
by mass = 7
where
Procedure
IS 263 : 1990
test with 5 ml standard iron solution in place of
the material and the same quantities of other
reagents. Compare the colour of the butanol
layers.
A-6.2.1 The limit prescribe.d in Table 1 shall be
taken as not having been exceeded
if the
intensity of the colour of the butanol layer in
the test with the material is not greater than
that of the colour produced in the control test.
A-7
A-7.1
TEST
FOR
SOLUBILITY
IN WATER
Calculations
where
Procedure
FOR
SOLUBILITY
IN ALCOHOL
A-10
OF SIEVE
Apparatus
taken
for
OF SULPHATES
Reagents
Barium Chloride Solution - 05 M. Dissolve
1221 g of barium chloride ( BaCl,.2Hz0
)
b)
4
Procedure
A-9 DETERMINATION
ANALYSIS
DETERMINATION
A-10.1
A-9.2
test.
a)
Reagent
A-9.1
retained
IS 265 : 1976.
A-10.2
Procedure
ANNEX
( Clause 5.1 )
SAMPLING
B-l GENERAL
SAMPLING
REQUIREMENTS
OF BORIC ACID
OF
pre-
Starting
from any container,
count
as
1, 2, 3 . . . . . . ) etc, up to r and so on where r
is equal to the integral part of JV/n. Every rth
container thus counted shall be taken out to
give a sample for test..
sampling
instrument
shall be clean
Table
Lot Si!ze
Upto
4
5 to 50
51 to 200
201 to 400
401 to 650
651 to 1 000
1 001 and above
B-3 TEST
SAMPLE
Lot
container
3
4
5
6
AND REFEREE
of Test Samples
B-3.1.2 Thoroughly
mix
all portions
of the
material drawn from the same container.
Out
of these portions, equal quantity shall be taken
from each selected container and shall be well
mixed up together so as to form a composite
sample weighing not less than 500. This composite sample shall be divided into three equal
parts, one for the purchaser,
another for the
supplier and the third for the referee.
lot
to
from
SAMPLES
Each
B-2.3
(nl
(2)
B-3.1 Preparation
OF SAMPLING
No. of Containers
to be Selected
(Jv)
(1)
B-2.1
to be
( ClauseB-2.2 )
B-2 SCALE
Number of Containers
Selected for Sampling
parts
shall be immediately
transferred
to
thoroughly dried-bottles which are than sealed
airtight with stoppers and labelled with all the
particulars of sampling given under B-1.7. The
material in each such sealed bottle shall conThese
stitute
an individual
test sample.
individual samples shall be separated into three
identical sets of samples in such a way that each
set has an individual test sample representing
each container selected. One of these three sets
shall be sent to the purchaser, another to the
supplier and the third shall be used as referee
sample.
B-3.2
Referee Sample
OF TESTS
FOR
CONFORMITY
The lot shall be declared to have satisrequirement for boric acid if the value
expression (X - 06R) is equal to or
than the value specified in Table 1.
For Composite
Sample
Standmd
Mark
The use of the Standard Mark is governed by the provisions of the Bureau ofIndian Standards
made thereunder.
The Standard Mark on products
covered by an Indian Standard conveys the assurance that they have been produced to comply with
the requirements of that standard under a well defined system of inspection, testing and quality
control which is devised and supervised by BIS and operated by the producer.
Standard marked
products are also continuously checked by BIS for conformity to that standard as a further safeguard. Details of conditions under which a licence for the use of the Standard Mark may be granted
to manufacturers or producers may be obtained from the Bureau of Indian Standards.
.
/
4;
in
in
or
),
Amendmenta
Immrad@ncc Publication
Date of Issue
Amend No.
BUREAU
OF INDIAN
Tea
Affected
STANDARDS
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