TCP Lab 1

1. Scouring of Cotton : Recipe

NaoH- 2%
Na2CO3 2 %
Lissapol- 0.5%
MLR- 1:50
Temp-Boil(100C)
Time- 2 hours
WASHING(NEUTRALIZATION):
Ch3COOH- 1%
Temp-Room Temp
Time- 5-10 mins
2. Scouring of Polyester:
Recipe:
Na2CO3- 2%
Non ionic detergent-0.5%
MLR-1:50
Temp-85C
Time-2Hours
Washing:
With simple water
3. Scouring of wool:
Recipe:
Na2CO3-0.5% owf
Soap-0.5% owf
MLR-1:50
Temp- 55-60C
Time-2hours
Washing:
CH3COOH-0.5%
MLR-1:50
Temp-Room Temp
Time-5-10 min

4. Degumming of Silk:
Recipe:
Neutral Soap-10%
MLR-1:50
Temp-Boil
Time-1 Hour
Washing :
With simple water
5. Scouring of P/C blend
Na2CO3- 1%
Non-Ionic Detergent-0.5%
MLR-1:50
Time-2.5 hours
Washing:
Ch3COOH-1%
6. Bleaching of Cotton with NaOClNaOCl-20ml/l available chlorine
Temp- Room temp
MLR-1:50
Time-2hours
Neutralisation:
CH3COOH-0.1%
MLR-1:50
Temp-Room Temp
Time-1-15 mins
7. Bleaching of cotton NaClO2
NaClO2-0.5%
CH3COOH- PH 4
MLR-1:50
Temp-85C
Time-2 hours
Washing: Anti chlor treatment
NaHSO4-2%
MLR- 1:50
Temp- Room temp
Time-10-15 min

8. Bleaching of Cotton with H2O2

H2O2-(35%)- 3%
Na2CO3- 1% (PH 9.5-10.5)
Na2SiO3- 6.5%
MLR-1:50
Temp-95C
Time-2 hours
Neutralisation:
CH3COOH- 0.5%
MLR-1:50
Temp-Room temp
Time-10-15 mins
9. Dyeing of Cotton with Direct Dye
Dye x% owf
NaCl- 50 gm/lt
MLR-1:50
30 min

40C

2C/min

15 min

15 min

Dye Sample

NaCl

10. Dyeing of cotton with Cold Brand dye:

Dye-x% owf
NaCl-50gpl
Na2CO3 -6 gpl
NaOH-25gpl
MLR-1:50
Temp- Room temp-40C

10 min

dye

10 min

dye

10 min

dye

10 min

dye

alkali

30 min

alkali

Soaping:
Na2CO3- 2gp
Anionic detergent-0.5 gpl
MLR-1:50
Temp-Boil
Time-15 min

11. Dyeing of Cotton with Sulpher dye

Dye- 5% 10% owm
Na2S-10%
NaCl-20gpl
MLR-1:50
Temp-Boil
15 min

45 min

95 C
10 min

Na2S

Dye+Sample

Oxidation:
CH3COOH-1ml/l
K2Cr2O7-1gm/l
Soap-1gm/l
Temp-Boil
Time-1/2 hour
MLR-1:50

12. After treatment of Direct dye

K2Cr2O7- 1gpl
Or
CuSO4- 1gpl
Or
K2Cr2O7-0.5gpl
CuSO4-0.5gpl
PH-4.5
Temp-60C
Time-30 min

NaCl

TCP 2 Lab
1.

Dyeing of Cotton with Vat Dye

Recipe:
Dye-1%(Narian Red)
NaOH-10%
Na2SO4- 10%
NaCl-20gpl
MLR-1:30
Soaping:
Non ionic Detergent-0.5ml
Na2CO3-0.5gpl
Temp-at boil
Time-15 min
Oxidation:
H2O2-1 ml
MLR- 1:30
Temp-50C
Time-15 min
Temp:
Vatting-50-60C
Dyeing-50-55C
Time-1.5hours

2.

Dyeing of Cotton with Insoluble azoic colours:

STEP1. Solubalisation of Naphthol
Naphthol-10gpl
NaOH-65% AS , 35%ASG
TR oil- small quantity
Time-1-20min
STEP2. Naphtholation of cellulose
NaCl-20 gpl
Temp-at boil
Time-1-1.5 hours
MLR-1:30
STEP3. Diazotizaton of base
Base-10gpl
HCL-5ml/l
NaNO2-3gpl
Temp-0-5C
Time-15-20 min
MLR-1:30

3.

Dyeing of Wool with Acid Dyes

Acid Dye-1% shade
Acetic acid-To adjust PH- 4.5-5.5
NaCl-50 gpl
Temp-initially 40C raised to 90C
Time-2 hours
MLR-1:30
Soaping:
Non ionic detergent- 1gpl
MLR- 1:50
Temp-boil
Time-15min

4.

Dyeing of Nylon with Metal Complex Dye:

Dye-1%
Acetic acid-1gpl(to adjust PH 4.5-5.5)
MLR- 1:30
Time-2 hours
Temp-at boil
Soaping:
Na2CO3- 1gpl
Non Ionic Detergent-1gpl
Temp-at boil
MLR-1:50

5.

Dyeing of Cotton with Solubalised Vat Dye(Arlindone Pink IR)

Dye- 1%
Na2CO3- 1%
NaNO2-2%
TR oil- a little
NaCl- 20gpl
Temp- at boil
Time- 1.5 hours
MLR- 1:30
Oxidation
H2SO4- 5ml/l
Temp- 50-60C
40-80C (Blue)
Time-30 min
MLR- 1:30
Soaping
Na2CO3-1gpl
MLR-1:30
Temp-Boil

Time- 15 min
Non Ionic Detergent-1ml/l