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Indian Standard
PLASTICS PART 5
METHODS OF TESTING
MECHANICAL
Section 7 Determination
PROPERTIES
of Flexural Properties
ICS 83.080
@ BIS 1996
BUREAUOF
MANAK
April
1996
BHAVAN,
INDIAN
STANDARDS
9 BAHADUR SHAH
NEW DELHI 110002
ZAFAF:
MARG
Price Group
Methods
NATIONAL
Committee,
PCD 23
FOREWORD
This Indian Standard which is identical with IS0 178 : 1993 Plastics - Determination
of flexural
properties, issued by the International Organization for Standardization
(ISO) was adopted by the
Bureau of Indian Standards on the recommendation
of Methods of Test for Plastics Sectional
Committee and approval of the Petroleum, Coal and Related Products Division Council.
The text of IS0 standard has been approved as suitable for publication
deviations. Certain conventions
are, however, not identical to those
Attention is particularly drawn to the following:
a) Wherever the words International
be read as Indian Standard.
Standard
appear referring
to this standard,
they should
In this adopted standard reference appears to certain Internatronal Standards for which Indian
Standards also exist. The corresponding
Indian S!andards which are to be substrtuted in their place
are listed below along with their degree of equivalence for tile editions indicated:
International
Standard
Corresponding
Indian Standard
Degree of
Equivalence
conditions
do
Identical
NIL
NIL
NIL
(Continued
Technically
equivalent
do
on third cover)
PLASTICS -
METHODS OF TESTING
PART 5
MECHANICAL
Section 7 Determination
Scope
the follow-
thermoplastics
moulding and extrusion materials,
including filled and reinforced compounds in addition to unfilled types; rigid thermoplastics
sheets;
thermosetting
moulding materials, including filled
and reinforced compounds; thermosetting
sheets,
including laminates;
fibre-reinforced
thermoset
and thermoplastics
composites,
incorporating
unidirectional
or nonunidirectional
reinforcements
such as mat, woven
fabrics, woven rovings, chopped strands, combination and hybrid reinforcements,
rovings and
milled fibres; sheets made from pre-impregnated
materials (prepregs);
thermotropic
liquid-crystal
178 : 1993
polymers.
PROPERTIES
of Flexural Properties
1.6 Flexural properties can only be used for engineering design purposes for materials with linear
stress/strain behaviour. For non-linear material behaviour the flexural properties
are only nominal. The
bending test should preferentially be used with brittle
materials, for which tensile tests are difficult.
Normative
references
The following
standards contain provisions
which,
through reference in this text, constitute
provisions
of this International
Standard. At the time of publication, the editions indicated were valid. All ztandards
are subject to revision, and parties to agreements
based on this International Standard are encouraged
to investigate the possibility of applying the most recent editions
of the standards
indicated
below.
Members of IEC and IS0 maintain registers of currently valid International Standards.
IS0 291:1977, Plastics conditioning and resting.
Standard
atmospheres
moulding
for
test
176: 1993
IS0 294:-l,
Plastics Injection moulding
specimens of thermoplastic materials.
of test
rigid -
It is expressed
It is expressed
Flexural
It is expressed
It is expressed
3.7
IS0 2557-2:1986, Plastics - Amorphous thermoplastics - Preparation of test specimens with a specified
reversion - Part 2: Plates.
Preparation
Plastics
of test reConfidence
(MPa).
(mm).
in millimetres
(mm).
test speci-
It is expressed
age (o/o).
test equipment
types (constant
as a dimensionless
It is calculated according
9.2, equation (4).
ratio or a percent-
to the relationship
given in
Definitions
in millimetres
conventional
It is expressed
of test speci-
Multipurpose
in megapascals
mens by machining.
IS0 3167:--3,
mens.
(MPa).
IS0 2557-l : 1989, Plastics - Amorphous thermoplastics - Preparation of test specimens with a specified
maximum reversion - Part 7: Bars.
Plastics -
in megapascals
IS0 2818:-2),
(MPa).
of
in megapascals
Standard,
the
It is expressed
age (o/o).
as a dimensionless
ratio or a percent-
3.10 flexural
strain
at flexural
strength,
Flexural strain at maximum
flexural
stress
figure 1, curves a and b).
It is expressed
age (%).
3.11 modulus
of elasticity
in flexure; flexural
modulus, E,: Ratio of the stress difference uf2 - of1
to the
corresponding
strain
difference
values
(&f2= 0,002 5) - (of, = 0,000 5) [see 9.2, equation
!5)1.
It is expressed
as a dimensionless
in megapascals
&fM:
(see
ratio or a percent-
(MPa).
IS
IS0
NOTES
value
force
Apparatus
5.1
5.1 .l
Testing
machine
General
The machine shall comply with IS0 5893 and the requirements given in 5.1.2 to 5.1.4, as follows.
Principle
51.2
Speed of testing
The testing
machine
the speed of testing
Specimen
Curve b
Specimen
:urve c
Specimen
that neither has a yield point nor breaks before the conventional
Figure
the
of
3 With computer-aided
equipment, the determination
of
the modulus E, using two distinct stress/strain points can
be replaced by a linear regression procedure applied on the
part of the curve between these two points.
Lrve
178 : 1993
determined
value.
During this procedure
applied to the specimen
is measured.
13360
1 -
deflection
deflection
sc
s,
IS
13360
178:1993
IS0
lame
i -
necommenaea
values ror me speea
of testing
Speed
mm/min
Tolerance
%
1 1)
f 20 2)
2
5
f 20 2)
f 20
of the test
of the test
10
f 20
20
50
f 10
f 10
100
f 10
200
500
f 10
f 10
5.1.4
Indicators
2)
and
Micrometers
and gauges
5.2.1 Micrometer,
or
equivalent,
G 0,Ol mm (for measuring the thickness
b of the test specimen, see figure3).
reading
to
h and width
52.2
Vernier caliper, or equivalent,
accurate to
within k 0,l % of the span L, for determining
the
span (see 8.2 and figure 2).
5.1.3
Supports
and striking
edge
Applied
Striking
Test specimens
6.1
6.1 .l
The
with
with
shall
force
Shape
and dimensions
General
dimensions of the test specimens
the relevant material standard and,
6.1.2 or 6.1.3. Otherwise, the type
be agreed between the interested
edgeT./-,7
Test specimen
c
Figure 2 -
shall comply
as applicable,
of specimen
parties.
IS
IS0
Preferred specimen
6.1.2
dimensions,
7 ) : 1996
( Part 5/Set
178 : 1993
type
Table 2 -
The preferred
13360
in millimetres,
shall be
b, in relation
Dimensions
length:
1=80f2
width:
b = 10,o f 0,2
thickness:
h = 4,0 f 0,2
Nominal
thickness, h
NOTE 4
The preferred specimen may be machined from
the central part of a multi-purpose test specimen complying
with IS0 3167.
Other test specimens
When it is not possible or desirable to use the preferred test specimen, the following limits shall apply.
unless affected
8.2 c).
given in table2
3<h<5
10,o
5<h<lO
15,0
lO<h<20
20,o
30,o
20<h
Q 35
35,0
50,o
35<h
< 50
50,o
80,O
entation.
6.3
shall
6.3.1
6.2
Anisotropic
15,o
1
NOTE 7
If, because of the application, this material is
subjected to stress at some specific orientation to the principal direction, it is desirable to test the material in that ori-
width
25,0
6.2.2 When the material shows a significant difference in flexural properties in two principal directions,
it shall be tested in these two directions. The orientation of the test specimens relative to the principal
directions shall be recorded (see figure 3).
NOTE 5
Certain specifications require that test specimens from sheets of thickness greater than a specified upper limit shall be reduced to a standard thickness by
machining one face only. In such cases, it is conventional
l<h<3
Textile
and
long-fibrs
reinforced
plastics
materials
NOTE 6
The position or orientation and the dimensions
of the test specimens sometimes have a very significant
influence on the test results. This is particularly true for
laminates.
...
by the provisions
Moulding and
extrusion
compounds,
thermoplastic and
thermosetting
sheets
in millimetres
Width b f 0,5 1)
6.1.3
to
materials
Preparation
of test
specimens
Moulding
or extrusion
compounds
6.2.1 In the case of materials having physical properties that depend on direction, e.g. elasticity, the test
specimens shall be chosen so that the flexural stress
in the test procedure will be applied in the same direction as that to which products (moulded articles,
sheets, tubes, etc.) will be subjected in service. The
relationship of the test specimen to the application
will determine the possibility of using standard test
specimens (see 6.1 and 8.2).
6.3.2
Sheets
from sheets
in accord-
IS
13360
IS0
( Part 5/Set
7 ) : 1996
178 : 1993
Position
Figure
E3.3
3 -
of specimen
Direction
length
width
length
width
Long-fibre-reinforced
of test specimen
of force
normal
I 1
in relation to direction
6.5
plastics materials
A panel of the material shall be prepared in accordance with IS0 1268 or another specified or agreedupon preparation
procedure.
Specimens
shall be
machined in accordance with IS0 2818.
6.4
of the product
Direction
of product
Position
Width direction
parallel
of product
and direction
of force
Checking
Conditioning
Specimens showing measurable or observable departure from one or more of these requirements shall be
rejected or machined to proper size and shape before
testing.
6
IS
13360
Determine
all relevant
stresses,
deflections
strains defined in clause 4 from a force/deflection
a stress/deflection
curve or equivalent data.
8.2
Measure the width b of the test specimens to
the nearest 0,l mm and the thickness h to the nearest 0,Ol mm in the centre of_ the test specimens.
Calculate the mean thickness h for the set of specimens.
L=(16
comply
with
the
the
(2) shall
resulting
be used
span
except
to
the
of results
expressed
OfI
equation:
3FL
in
. . . (3)
2bh2
where
nearest
in the following
fibre-reinforced
test specimens, if necessary to avoid delamination
in shear, use a distance between supports calculated on a higher ratio of L/h.
is the width,
men;
is the thickness,
specimen.
9.2
and
or
Flexural stress
Of
following
and expression
Calculate
the
flexural
stress
megapascals, using the following
. . (2)
+ 1)h
and measure
0,5 %.
Equation
cases.
L to
Calculation
9.1
7 ) : 1996
8.5
Record the force and the corresponding
deflection of the specimen during the test, using, if
practicable, an automatic recording system that yields
a complete flexural stress/deflection
curve for this
operation [see 9.1, equation (3)].
Procedure
Adjust the
equation:
( Part 5/Set
178 : 1993
IS0
in millimetres,
of the speci-
in millimetres,
of the
Flexural modulus
For the measurement of the flexural modulus, calculate the deflections s, and s2, which correspond to the
given values of flexural
strain Ef, = 0,000 5 and
q2 = 0,002 5, by the following equation:
if necessary to prevent
into the test specimen,
s=~
G2
(i=
...
1;2)
where
8.3
Set the speed of testing according to the standard for the material being tested. In the absence of
this information, select a value from table 1 that gives
a strain rate as near as possible to 1 % per minute.
This gives a testing speed that produces the deflection closest to 0,4 times the specimen thickness
in 1 min, e.g. 2 mm/min for the preferred specimen
complying with 6.1.2.
is an individual
deflection,
in millimetres;
Efi
is the thickness,
specimen.
in millimetres,
of the
in
IS
13360
( Part 5/Set
7 ) : 1996
178 : 1993
IS0
a) a reference
where
Bfl
is the
flexural
stress,
expressed
in
megapascals, measured at the deflection
s1;
Qf2
is the
flexural
stress,
expressed
in
megapascals, measured at the deflection
s2.
For computer-aided
equipment,
NOTE 8
All equations referring to flexural properties hold
exactly for linear stress/strain behaviour only (see 1.6); thus
for most plastics they are accurate at small deflections only.
to this International
9.3
Statistical parameters
f)
Significant figures
Calculate the stresses and the modulus to three significant figures. Calculate the deflections to two significant figures.
and conditioning
9.4
Standard;
procedures,
tested;
i)
i)
the accuracy
IS0 5893);
grading
of the
test
machine
(see
10
Precision
1) the individual
11
Test report
test results,
if required;
results;
information:
if
do
do
Multipur-
NIL
NIL
Technically
equivalent
In the case of IS0 1209-1, IS0 1209-2, IS0 2557-1, IS0 3167 and IS0 5893, the Technical Committee
responsible for the preparation of this standard has reviewed its contents and has decided that they
are acceptable for use in conjunction with this standard.
For tropical countries like India, the standard
as 27 + 2C and 65 + 5 percent respectively.
temperature
shall be taken
In reporting the results of a test or analysis in accordance with this standard, if the final value,
observed or calculated, is to be rounded off, it shall be done in accordance with IS 2 : 1960 Rules
for rounding off numerical values (revised).
BIS is a statutory institution est.ablished under the Bureau of Indian Standards Act, I986 to promote
harmonious development of the activities of standardization, marking and quality certification of goods
and attending to connected matters in the country.
Copyright
BIS has the copyright of all its publications. No part of these publications may be reproduced in any form
without the prior permission in writing of BIS. This does not preclude the free use, in the course of
implementing the standard, of necessary details, such as symbols and sizes, type or grade designations.
Enquiries relating to copyright be addressed to the Director (Publications), BIS.
Review of Indian Standards
Amendments are issued to standards as the need arises on the basis of comments. Standards are also
reviewed periodically; a standard along with amendments is reaffirmed when such review indicates that
no changes are needed; if the review indicates that changes are needed, it is taken up for revision. Users
of Indian Standards should ascertain that they are in possession of the latest amendments or edition by
referring to the latest issue of BIS Handbook and Standards Monthly Additions.
This Indian Standard has been developed from Dot : No. PCD 23 ( 1394 ).
Amendments
Text Affected
Date of Issue
Amend No.
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