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To: ChE 141 CORPORATION

Attention : Mr. Antonio Y. Rivera


E-mail : ayrivera.ph@gmail.com
From :
Email :
Telephone :
Date : May 29, 2015
Company CO2 Proposal : 70tpd liquid CO2 recovery
For : ChE 141 CORPORATION
Dear Sirs,
Thank you for your interest in our products and services. As a result of your request we are
pleased to present our proposal for one Company CO2 CO2 recovery plant for your evaluation and
purchasing purposes.
In this revision we have changed the following:
1) We include a NOx removal filter
2) We reviewed the power consumption on the ACF/Dryer.
3) Added optional variable speed drives for Booster, CO2 & NH3 compressors
Once you have had the opportunity to study our proposal, I would be pleased to discuss it with
you and your colleagues so that we can fine-tune the offered scope to suit to your needs. In the
meantime, should you or your colleagues have any questions or require additional information
please feel free to contact us so that we can be of further service to you.
Trusting we have made you an interesting offer and I look forward to again have the honor of
realizing this project in the near future.
With best regards,
Company CO2

INDEX
1. Introduction Company CO2......................................................................................... 6.4
2. Benefits & Advantages.................................................................................................... 4
2.1. CO2 Food Grade Quality...............................................................................................4
2.2. Water Savings...............................................................................................................5
2.3. CO2 Service & Support.................................................................................................5
2.4. CO2 Know-How & Expertise.........................................................................................5
3. One (1) Foam separator OPTION................................................................................... 8
4. One (1) Foam Trap OPTION .......................................................................................... 9
5. One (1) Inline O2 Measurement OPTION......................................................................10
6. One (1) CO2 Gas Booster system..................................................................................11
6.1. One (1) Booster after cooler........................................................................................12
6.2. One (1) CO2 Compressor Pre-Cooler.........................................................................13
7. Two (2) Dry-Running CO2 Compressor units..................................................................14
7.1. One (1) Pre-Cooler.......................................................................................................15
8. One (1) High Efficiency HIGH Pressure Gas Washer.....................................................16
9. One (1) Activated Carbon Filter Dryer Unit.....................................................................17
1. One (1) NOx Filter...........................................................................................................18
2. One (1) CO2 Gas Liquefaction system ..........................................................................19
2.1. One (1) Refrigerant compressor..................................................................................19
2.2. One (1) Economizer with side load .............................................................................20
2.3. One (1) Refrigerant condenser.................................................................................. .20
2.4. One (1) Refrigerant evaporator / CO2 Condenser..................................................... .21
3. One (1) Water Cooling Circuit .......................................................................................22
4. One (1) Purification Unit (stripping system) ...................................................................23
5. One (1) Electrical Hardware & Control System .............................................................24
6. One (1) Turnkey materials (Pipes, Cables, Insulation) ..................................................25
6.1. On Site Piping Materials66...................................................................................... 25
6.2. On Site Insulation Materials...................................................................................... ..25
6.3. On Site Electrical Materials..........................................................................................25
7. One (1) First set of Preventive Maintenance Parts OPTION...........................................26

8. One (1) Home Based Engineering, Design & Project Management 66666666...27
8.1. One (1) Project Manager On Site Visit 66666666666666666666.27
8.2. Design, Approvals & Certification 6666666666666666666666.27
9. One (1) Supervisor for Mounting, installation, Commissioning & Training666666.28
10. One (1) Turnkey Design Package6666666666666666666666...29
11. Utility Requirements6666666666666666666666666666..30
12. General .........................................................................................................................31
12.1. Includes......................................................................................................................31
12.2. Excludes......................................................................................,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,31
13. Guarantees....................................................................................................................32
13.1. Warranty ....................................................................................................................32
13.2. Design Data
13.2.1. Raw gas inlet...........................................................................................................32
13.2.2. Utilities ....................................................................................................................32
13.2.3. Engine room............................................................................................................33
13.3. Performance test protocol..........................................................................................33
14. Standard Accessories List.............................................................................................34
15. Commercial Summary.................................................................................................. 35
15.1. Scope overview and pricing.......................................................................................35
15.2. Options...................................................................................................................... 35
15.4. Terms & Conditions ...................................................................................................36

1. Introduction Company CO2

Company CO2 is a market leader in state of-the-art technology and custom-made solutions for
the recovery and management of CO2. The company belongs to Company CO2s Global
Business Unit Filtration Solutions.
Company CO2, Inc. is a global diversified industrial company headquartered in XXX City, YYY
Country. With 2012 estimated revenues of $7.0 billion, Company CO2 employs over 30,000
people worldwide.
Company CO2 was founded in 19YY and has its roots in total carbon dioxide (CO2) and oxygen
(O2) management and quality control for the brewing and beverage industries. Over the years our
company has grown from a supplier of raw material to developing, manufacturing and servicing,
focusing on quality control equipment,units for carbonation, blending, de-aeration and of course,
CO2 recovery.
Based on our long-term experience in the area of total CO2 and O2 management, Company CO2
has succeeded to continuously expand its existing market presence in the brewing and beverage
industries and successfully enter new markets like the wine and soft drink markets and the
bioethanol/distillery market.
The latest innovation is a solution for upgrading biogas into biomethane, using a technique, which
makes it possible to recover 100 % of the methane and at the same time recover the CO2 byproduct.
Company CO2 is a multinational company, with a strong focus on innovation and customer
satisfaction, and a presence in more than 150 countries around the world. All of our companys
technologies are designed with the same principles in mind: protect the environment and reduce
operating expenses at the same time. In other words: Do more with less.
When it comes to customer satisfaction Company CO2 continuously strives to realize a best of
the best standard, not just meeting but anticipating and exceeding customers requirements. We
offer unparalleled customer service and technical support for all our products through custommade service plans that range from maintenance contracts to comprehensive service level
agreements. Our highly motivated and skilled team of specialists in Country WWW is supported
by a worldwide professional network of agents, distributors and Sales & Service Offices. To help
you achieve maximum plant efficiency, our professionals provide 24/7 technical support by
phone, e-mail or remote service.

2. Benefits & Advantages

Additional benefits specific for this CO2 recovery project, which we will be pleased to elaborate
on, include but not limited to:
2.1. CO2 Foodgrade

Quality

Company CO2 design CO2 Gas Compressor is of the reciprocating type having dry
non-lube cylinder design with all surfaces in contact with wet CO2 gas fully coated and
use of materials resistant to moisture saturated CO2 gas, fully automatic unloaded start,
stop and level controlled condensate removal, each packaged mounted on skid, preassembled to include interconnecting piping.
Company CO2 Liquid CO2 Purification Unit is designed to purify liquid CO2. This system
is energy self sufficient optimally enhancing the CO2 purity up to 0,000% v/v equal to less
than 0 ppm O2.
Company CO2 Activated Carbon Purifier and Dryer Package are fully automatic in
operation to include online and regeneration cycles. The systems are skid mounted on
one base pre-assembled, and pre-piped.
All vessels and piping are of all Stainless Steel construction. Odor removal in
combination with Company CO2 Gas Washer is highly effective for high quality CO2 gas.
Non-condensable purge gas is utilized to regenerate, meaning no contamination with
external media (steam or hot air) and no additional utilities required to be brought into the
engine room.
2.2. Water Savings
The Company CO2 (structured packed) CO2 gas washer (scrubber) is fully automatic in
operation:
- Effective removal of water soluble (ethanol) for more efficient operation of the
active carbon purifiers: 99,75% ethanol removal efficiency
- Having low water consumption & no circulation pump required (no energy
consumption)
- Water spray energized at start of CO2 gas compressors.
2.3. CO2 Service & Support
Additionally Company CO2 has an excellent support structure for our customers needs.
We have technical sales staff worldwide as well as a service technician network
comprising of 15 technical service engineers that travel the world all dedicated to our
systems and that specific to our systems utilized in the brewing industry.
2.4. CO2 Know-How & Expertise
As market leader in the CO2 & O2 management in breweries, Company CO2 provides
technological
advanced and specifically designed CO2 recovery solutions for its customers worldwide.

Company CO2 has its own dedicated R&D department for CO2 recovery to further
develop and optimize the CO2 recovery process:
- The High efficient Gas washer with its low water consumption (0,9L water per
recovered kg CO2) in combination with the active carbon filter & drier concept
successfully applies the best of Company CO2 & Norit Active Carbon know-how
for high efficient ethanol and odor removal.
- Subject to its application, the LiquiVap contributes to further CAPEX and OPEX
reduction for the end user.
- R&D has its own gas chromatograph specially designed to analyze raw
fermentation gas as well as purified CO2 gas.
At the request of clients Company CO2 provides CO2 & Energy audits varying from a
complete audit (incl. total CO2 mass balance) to plant specific energy scans. With the
audits Company CO2 provides customer specific solutions how to upgrade, expand or
improve its CO2 collection, recovery and consumption process.

One (1) Company CO2 CO2 recovery plant


The CO2 recovery plant is designed according below mentioned specifications:
Capacity : 2920 kg/h CO2 based on liquid in tank
Medium : CO2 gas from CO2 from distillery
CO2 raw gas specification :Gas made up to be confirmed with formal raw CO2 gas
analysis
CO2 inlet temperature : 20 C
CO2 inlet pressure : 1011 mbara at 10 mtr. above sea level.
Fermenter turn-in purity : > 98,00 % v/v
CO2 inlet purity to plant : > 98,00 % v/v
Balance consisting of non-condensable O2 and N2, VOCs, minimal Hydrocarbons & < 40
ppm v/v total Sulphur compounds.
Storage conditions : 17,5 barg & -24 C
Seismicity : Not in a seismic relevant zone unless otherwise specified in this quote
Any changes as a consequence of revised inlet conditions, site location etc. will be
reviewed and offered separately.
Built according to the Company CO2 standard to be installed under Company CO2
supervision and in accordance to Company CO2 P&IDs, general arrangement,
instruction and manuals.
The shown pictures in this proposal are indicative

This proposal contains the following items:


3. One (1) Foam separator

OPTION

The Foam Separation System is fully automatic and protects the CO2 recovery plant from foam
carryover. It features a proven CO2 foam separation design where the foam sensor activates
water spray for foam suppression. After secure foam removal the system resets itself for normal
CO2 recovery operation.

Benefits & advantages:


Water saving system:
- Water sprayed only when required
- Automatic water seal refreshment
Safety : Water seal guard warning of possible CO2 emission
Access way and drain valve for maintenance purposes
Fully stainless steel vessel and piping
Foam free CO2 recovery

Scope:
Foam separator vessel with:
- Foam sensor
- Spray nozzle
- Water inlet connection with stop valve, strainer and solenoid valve
- Low-level water sensor
- Water overflow pipe
- Drain valve
- Lifting lugs

Technical specifications:
Capacity : 2920 kg/h CO2
Working pressure : < 40 mbarg
CO2 connections : DN250
Water connections : DN40
Material of construction : 1.403 / AISI 304
Dimensions ( x L) : 1750 x 3153 mm
Location : Tied into CO2 collection line

4. One (1) Foam Trap

OPTION

The foam trap is a foam protection system whereby the foam sensor activates the automatic
foam to drain valve. When the system no longer detects foam, the foam trap will automatically
switch back to normal CO2 recovery operation.

Benefits & advantages:


Foam free CO2 recovery
Compact plug and play design

Scope:
Foam trap comes with:
- Foam sensor
- 2 x Pneumatic butterfly valves, pilot operated

Technical specifications:
Capacity : 2920 kg/h CO2
CO2 connections : DN250
Location : Tied into CO2 collection line

5. One (1) Inline O2 Measurement

OPTION

The inline O2 measurement, is designed to monitor the O2 content in CO2 gas source and
provides a key parameter in the efficient and economic operation of a CO2 recovery system.

Benefits & advantages:


Optimize overall CO2 collection efficiency.
Cost saving:
- reduction of CO2 losses through short response time
- efficient operation of CO2 recovery system
- no frequent calibration required
- low maintenance
Automating the purging of CO2 gas in combination with foam trap

Scope:
Control unit with O2 sensor
Mounting set (wall / panel)
Signal cable between sensor and unit (15 mtr.)
Welding socket 25mm with cover pin set

Technical specifications:
Type : OGM-LHO Low pressure
Sensor : Optical
CO2 purity set point : > 98,0 % v/v
Detection limit : 0,0...4,2 % v/v O2
Accuracy at STP : 2 % v/v O2 of m.v.
CO2 inlet pressure : 0...400 mbarg
Analogue output : 4...20 mA
Ingress protection : IP 67
Possible locations : Tied into CO2 collection line in fermentation area/ BBT area /
Foam separator / Foam trap /engine room, frost free

10

6. One (1) CO2 Gas Booster system


A booster is designed to boost the raw CO2 fermentation gas pressure to the required CO2
compressor suction pressure.

Scope:
Blower with electric motor and drive guard
Inlet & outlet piping with isolation valves
Suction and discharge pressure gauge
Discharge pressure transmitter
Discharge temperature transmitter
Discharge check valve
Optional variable speed drive 33 kW

Technical specifications:
Type : Centrifugal
Capacity minimum : 1460 kg/h
Capacity maximum : 2920 kg/h
Suction temperature : 30 C
Suction pressure : 1011 mbara
Discharge pressure : 1200 mbara
Location : In engine room, frost free

11

6.1. One (1) Booster after cooler


The CO2 gas will be heated by the booster, this after cools the CO2 by a heat exchanger on
cooling water
.

Benefits & advantages:


Fully automatic
1step cooling before the CO2 compressor
Reduces power consumption at the CO2 compressor
Removes ethanol from the gas (will be collected in the water)

Scope:
Pre-cooler
Automatic condensate drain for water separator by pneumatic maintenance free
valves
System with:
- Temperature indicator
- Strainer
- Stop valves

Technical specifications:
Capacity: 2920 kg/h CO2
Cooling medium : Cooling water
Temp in: 54 C Temp out: 45 C

12

6.2. One (1) CO2 Compressor Pre-Cooler


The CO2 Compressor pre-cooler is designed to reduce the water content in the CO2 through
condensation.This will reduce the water load and to cool the gas before entering the CO2
compressor.This cooler will be cooled by the re-used water from the CO2 scrubber

Benefits & advantages:


Fully automatic
Reduces energy consumption of the CO2 compressor

Scope:
Heat exchanger
Automatic condensate drain for water separator by pneumatic maintenance free
valves
System with:
- Temperature indicator
- Strainer
- Stop valves

Technical specifications:
Capacity: 2920 kg/h CO2
Cooling medium : Re-used cold scrubber water
Temp in : 45 C Temp out: 30 C

13

7. Two (2) Dry-Running CO2 Compressor units


The 2 stage, dry-running, V-belt driven CO2 compressor unit is specifically designed for the
compression of wet CO2 gas.

Benefits & advantages:


Fully automatic unloaded start, stop and level controlled condensate removal.
Below-mentioned parts are skid mounted, pre-assembled, pre-piped and pre-cabled
CO2 piping, coolers and condensate separators in stainless steel.
V-belt drive assembly with slide mounted motor
Modulating temperature control valve to maintain a constant CO2 discharge
temperature

Scope:
Dry running CO2 compressor
Electric motor with V-belt and drive guard
Stainless steel inter- and after cooler
Condensate separator with automatic zero CO2 loss drain after each stage
Temperature switch after each stage and after cooler
Temperature / pressure indicators on both stages
CO2 high pressure switch
Safety valve protecting each stage
CO2 check valve
Cooling utility circulation system with:
- Stop valve
- Strainer
- Solenoid valve
- Temperature control valve
- Temperature indicators
Optional frequency drive (VSD) in optional price overview

Technical specifications (each):


Capacity : 1460 kg/h CO2
Discharge pressure : 18 barg
Coolant Inter cooler : Cooling water
Coolant After cooler : Cooling water
Make Mehrer : TVZ-900
Location : On skid in engine room

14

7.1. One (1) Pre-Cooler


The CO2 gas pre-cooler is designed to reduce the water content in the CO2 gas through
condensation. This will reduce the water load onto the Driers, lowering the chance that the CO2
condenser will freeze and thus improve the CO2 recovery and liquefaction efficiency.

Benefits & advantages:


Fully automatic
Reduces energy consumption of active carbon filters and driers.
Reduces CO2 consumption of active carbon filter and driers.

Scope:
Pre-cooler
Automatic condensate drain for water separator by pneumatic maintenance free valves
System with:
- Temperature indicator
- Strainer
- Stop valves

Technical specifications:
Capacity : 2920 kg/h CO2
Coolant : Integrated in the refrigeration system
CO2 inlet temperature : 40 C
CO2 outlet temperature : 15 C
Location : After CO2 compressors

15

8. One (1) High Efficiency HIGH Pressure Gas Washer


The gas washer is a proven once through water-wash system to remove water-soluble impurities
(such as ethanol & Acetaldehyde) from the raw CO2 gas. Using special stainless steel structured
packing the counter flow design guarantees an optimal scrubbing effect with minimal water
usage.

Benefits & advantages:


Water saving system:
- Water consumed only
when required
- Automatic water seal
refreshment
Safety:
- Water seal guard warning
of possible CO2 emission
- Low flow alarm to switch
off CO2 compressors

Fully stainless steel vessel and piping


Efficient ethanol removal : 99,75 %
Optimal odor removal in combination with Company CO2 Active Carbon Filter

Scope:
Gas washer with:
- Water distributor
- Packing in stainless steel
- Water overflow pipe
- Drain valve
- Low-level water sensor
- 2x CO2 points for _p meter connection
- Lifting lugs
Water inlet connection with:
- High pressure water supply pump (20 bar)
- Stop valve, strainer, solenoid valve & water pressure regulating valve with
pressure gauge
- Needle valve
- Low water flow alarm
Water chiller integrated in offered refrigeration

Technical specifications:
Capacity : 2920 kg/h CO2
Working pressure : 18 bar
CO2 connection : DN150
Water connection : DN15
Water temperature : 15 C
Dimensions ( x H) : 500 x 6800 mm
Material of construction : 1.4301 / AISI 304

16

9. One (1) Activated Carbon Filter Dryer Unit


The Activated Carbon Filter and Drier is a fully automatic CO2 deodorizing and drying system.

Benefits & advantages:


Fully automatic operation and
regeneration cycle
Below-mentioned parts are skid
mounted, preassembled, pre-piped,
pre-cabled and pre-insulated
Fully stainless steel vessels and
piping
Specially developed NoritCompany CO2 activated carbon for
optimal odor removal
Only non-condensable purge gas used for regeneration
No contamination with external media (steam or hot air)
No additional utilities required to be brought into the engine room
Simple construction with two 4-way valves
Low maintenance system e.g. no check valves, no steam valves, no air blower
Unique heating system for heating during regeneration
Energy saving system: temperature control based regeneration
Easy access for filling exchange
Easy access to external heaters: no process interruption such as decompression is
required

Scope:
Activated carbon filter / dryer vessels each with in- and outlet filter
2x 4-way actuated ball valves with valve position confirmation
2x Pressure gauges
2x Safety valves
Purge gas connection with flow indicator and control valve
Actuated purge valve with valve position confirmation
Particulate filter after drier
Heating elements
Temperature switches
Insulation with aluminum cladding
Pressure transmitter
Production MASS flow meter
Inline dew point transmitter

Technical specifications:
Capacity : 2920 kg/h CO2
Dew point at working pressure : _ -40 C
Dew point at 1 atmosphere : _ -60 C
Inlet temperature : 15 C
Cycle time : 24 hours
Material vessel : 1.4571 AISI 316
Location : On skid in engine room

17

1. One (1) NOx Filter


For filtration of NOx from the CO2 gas , we install a Purafil filter between the ACF & Dryer.
This filter is filled with a media which removes the NO2 & NO out of the gas and includes a
stainless steel vessel including safety valves, pressure gauge, insulation valve. The unit will be
skid mounted,

Technical specifications:
Max. Capacity : 2920 CO2/h
Operating pres. : approx. 16 barg
(max 20 barg)
Position : Between AC filter and
Dryer
Inlet NOx : 1 ppm
Media life span : 12 months

18

2. One (1) CO2 Gas Liquefaction system


The purpose of the refrigeration unit in the CO2 recovery plant is to provide sufficient condensing
capacity to liquefy the dry CO2 gas through a CO2 condenser.

Benefits & advantages:


Fully automatic operation
Optimal and automatic purging of non-condensable gasses for optimal CO2 recovery
efficiency
The system contains the following items:
2.1. One (1) Refrigerant compressor
The compressor compresses the low pressure and low temperature refrigerant gas into
a high pressure and high temperature gas.

Scope:
Compressor incl. electric motor with drive assembly mounted on base frame
Oil separator with oil return and lubrication system
Oil cooler
Oil strainer
Capacity control 0-100
Stop valve on suction and discharge side
Suction and discharge pressure switch
Optional frequency drive (VSD) in optional price overview

Technical specifications:
Total cooling capacity : 2920 kg/h CO2
Refrigerant : NH3
Compressor make : Sabroe
Compressor type : Screw
Refrigerant condensing temperature : 35 C
Refrigerant evaporating temperature : -34 C
Cooling medium Oil cooler : Cooling water
Location : In CO2 engine room

19

2.2. One (1) Economizer

with side load

This economizer is a special design that increases the efficiency of the cooling compressor by
sub cooling the liquid refrigerant prior to entering the refrigerant evaporator and compressing the
suction gas created from an intermediate pressure to the condensation pressure.

Benefits & advantages:


Fully automatic operation
Increased refrigeration capacity
No additional chillers for the side load needed

Scope:
Heat exchanger
Valves and accessories
Pressure maintaining valve

Technical specifications:
Refrigerant : NH3
Side load : 88,0 kW
Side load description : Water chiller gas washer and Precooler after
CO2 compressor
Location : In CO2 engine room
2.3. One (1) Refrigerant condenser
The refrigerant condenser is a heat exchanger designed to liquefy the high pressure refrigerant
gas from the refrigerant compressor. The heat of condensation is removed from the refrigerant
gas by heat transfer to a cooling medium.

Scope:
Refrigerant condenser
In- & Outlet isolation valves
Coolant inlet filter
Pressure gauge & stop valve

Technical specifications:
Refrigerant : NH3
Refrigerant condensing capacity : 480 kW
Refrigerant condensing temperature : 35 C
Cooling medium condenser : Cooling water
Location : Outside

20

2.4. One (1) Refrigerant evaporator / CO2 Condenser


The refrigerant evaporates in the CO2 condenser (Refrigerant evaporator) and produces the
required cooling capacity to liquefy the incoming CO2 gas. The system is optimally designed to
separate the noncondensable gasses (N2, O2) from the liquefied CO2 meaning less CO2 is lost
from the system during automatic purging.

Scope:
Refrigerant evaporator / CO2 condenser
HP float
Shut off valves
Safety valves CO2 and refrigerant side
Pressure gauge
Oil drain vessel with accessories
One (1) Automated purge system for optimize CO2 recovery efficiency
Drain valve

Technical specifications:
Capacity : 2920 kg/h CO2
Refrigerant : NH3
CO2 condensing pressure : 17,5 barg
Location : At sufficient height to enable gravity feed into
stripping system or CO2 storage

21

3. One (1) Water Cooling Circuit


The fully automated cooling circuit is designed to cool the following CO2 recover plant parts:
Inter cooler of the CO2 compressor
After cooler of he CO2 compressor
Refrigerant condenser
Refrigerant oil cooler
The collected heat is rejected to
environment through a cooling tower

Benefits & advantages:


Stand alone operation
Fully automatic operation
Low operational costs

Scope:
Open cooling tower comes with:
- Fan with frequency controlled motor
- Drift eliminators
- Low water level cut out switch
- Water supply system with stop valve, strainer and water flow meter at inlet
- Drain
- Junction box
- Water treatment (anti-corrosion & -scaling) system
- Biocide dosing system
- Trace heating for water pan & circulation pump
Coolant circuit comes with:
- Circulation pump with strainer and block in valves
- Safety valve, overflow valve and drain
- Pressure gauge

Technical specifications:
Make : Evapco or BAC
Type : AT 19-68 or VXC C380
Cooling capacity : 1082 kW
Circuit coolant : Water
Circuit coolant flow : 135 m3/h
Circuit coolant inlet temperature : 40 C
Circuit coolant outlet temperature : 33 C
Wet bulb temperature : _ 28 C
Dimensions (L x W x H) : 5385 x 2245 x 3620 mm
Ambient temperature : min 24 max 32C
Location : wihtin 10 meters of the CO2 plant

Notes & recommendations:


Cooling circuit calculations are based on above mentioned wet bulb temperature which
customer is to confirm. Any changes as a consequence of revised local conditions will be
reviewed and offered separately.
Coolant filling is care of customer

22

4. One (1) Purification Unit (stripping system)


This Liquid Stripping System type is designed to increase the end purity of the liquefied gas. The
automatic Stripping system includes an integrated management system to optimize CO2 recovery.

Benefits & advantages:


Fully automatic operation
Enhances CO2 purity
Energy neutral system: CO2 gas to
the CO2 condenser is pre-cooled in
the re-boiler to generate the
required stripping gas. No additional
heat or energy in terms of
refrigeration is required to generate
stripping gas
Heating element to compensate
during start/stops and partial load
Special stainless steel packing for
optimal stripping of O2

Scope:
Stripping & management system
Stripping column with packings
Reboiler
Heating element
Safety valve
Level measurement reboiler
Pressure transmitter
Flow meter
Two(2) CO2 liquid transfer pump from reboiler to CO2
storage tank
Pre-insulated

Technical specifications:
System capacity : 2920 kg/h CO2
Maximum turn down : 50 %
Location : In engine room under CO2 condenser

23

5. One (1) Electrical Hardware & Control System


The electric control panel is executed according to the Company CO2 standard and thus
designed for the automatic control of the offered parts if not specifically mentioned otherwise. The
control panel is equipped with a control system including a Human Machine Interface (HMI) for
control, status and alarm messages of the system.

Benefits & advantages:


Full automatic operation of the
controlled parts
Motor-starters: Direct On Line _
7,5 kW, Star-Delta > 7,5 kW , > 55
kW soft starter
Electrical drawings are according
Company CO2 standard in EPLAN
which is AutoCAD compatible
Panel layout with main voltage
segregated from control voltage
Pre-wired and pre-tested

Scope:
Control panel with internal lighting
and power outlet
Lockable door on which easy
accessible HMI, emergency stop
and main switch are mounted
PLC based control system consisting of:
- CPU
- HMI
- All necessary digital-inputs + outputs
- All necessary analogue input + outputs
Digitally stabilized 24VDC control voltage supply
One potential-free contact is foreseen for general alarm
All necessary software for the control of the offered parts
All necessary (automatic) fuses for control voltage, in/outlets and instruments
All necessary Motor starter relays and fuses
PLC includes Profibus connections
PLC includes Ethernet connections

Technical specifications:
HMI Control Panel : Siemens TP 12"
PLC in Control Panel : Siemens S7 300 Compatible
Control voltage (common) : 24 VDC
Design : IEC 60204-1
Ingress Protection : IP 54
Name plates : English
HMI text : English
PLC program : English
Material panel : Coated steel
Location of main panel : Engine room

24

6. One(1) Turnkey materials (Pipes, Cables, Insulation)


Company CO2 will deliver Turnkey materials (Pipes, Cables, Insulation) for the installation of the
offered CO2 recovery plant.
For the successful realization of on site works:
Mounting of goods is to be done directly when goods arrive
Brewery to provide on site a secure and lockable area for offered parts
CO2 recovery plant will be set up in an engine room (closed layout)
Available room is free of obstacles and easily accessible especially for the installation
of the offered parts and its connections
Offered parts outside are to be installed in close proximity of the CO2 recoverys engine
room
All utilities are available and ready to be connected.
6.1. On Site Piping Materials
The following piping materials (pipes, elbows, tees and reducers) are included in the scope of
supply:
Interconnecting CO2 and refrigerant piping between the offered parts within the
boundary of the CO2 engine room
Utility piping from one point in engine room to offered parts within the boundary of the
engine room
Pipe clamps and pipe supports for the piping within the boundary of the engine room
Special insulation clamps for cold piping
CO2 and utility piping are executed in stainless steel
Refrigerant piping executed in carbon steel
Piping materials not specified, to/from not offered parts and to/from parts located
outside CO2 engine room are not included. Specifically the CO2 collection line from the
fermenters to the engine room, blow off lines, drains and the CO2 piping to/from the
storage tanks, vaporizers and to the CO2 consumers are not included.
6.2. On Site Insulation Materials
For the following units insulation materials will be supplied:
CO2 condenser (cold)
Stripper & re-boiler (cold)
CO2 & refrigerant piping (cold)
Water piping (cold).
CO2 pre-coolers & water chiller (cold)
ACF/Dryer (hot)
Insulation is PU or similar and where necessary aluminum cladding and vapor barriers
will be applied.
6.3. On Site Electrical Materials
This includes the following:
Interconnecting cable materials between the offered parts within the boundary of the
engine room and to CO2 storage tank mounted next to engine room
Cable trays (zink coated steel) and protection pipes for the offered cable materials
Communication cable to start/stop the control panel of the existing CO2 recovery plant
Cabling materials not specified, to/from not offered parts and to/from parts located
outside engine room are not included. Specifically the power supply cable from the site
plant power distribution to the Company CO2 control panels is not included.

25

7. One (1) First set of Preventive Maintenance Parts

OPTION

The preventive maintenance is to be carried out after CO2 recovery plant's 1st year of operation.
Below mentioned parts are for preventive maintenance to warrantee optimal 2nd year of plant
operation.

Benefits & advantages:


Original parts
Maintenance parts onsite

Scope:
Two (2) Maintenance sets Maintenance sets CO2 compressors, including:
- Set of suction- and delivery valves
- Set of piston- and guide rings
- Set of inner-parts piston rod sealing
- Set of gaskets and O-rings
One (1) Maintenance set Active Carbon & Drier Unit, including:
- Basic set of seals & filters
One (1) Maintenance set Maintenance set CO2 liquefaction Unit, including:
- Basic set of seals & filters

26

8. One (1) Home Based Engineering, Design & Project Management


This includes:
Management and coordination of the project
Engineering of the offered parts
Preparation and supply of an agreed Project Program
Detailed list of requirements to the customer before sending the supervisor for
installation and commissioning
Documentation (2x digital, English) according to Company CO2 standard:
- Parts, Accessories and Instrument schedule
- Operation Instructions, Maintenance Manuals & Spare parts Lists
- Project drawings:
o Engineering diagrams (PID)
o Layout & above ground foundation drawings
o Electrical diagrams + panel layout drawings (in EPLAN)
o General assembly drawings.

Notes & recommendations:


The documentation will be prepared according to relevant Good Engineering Practice.
Differences or specifications requested by the customer will be charged according to expenses.
8.1. One (1) Project Manager On Site Visit
To discuss the project with the local project team and review the local conditions we offer an on
site visit by the Project Manager.
This includes costs for:
Tickets
Visa
Hotels
Local transportation
Travel hours
Working hours
8.2. Design, Approvals & Certification
The supplied equipment will be designed and produced in accordance with the following EEC
Directives
Machine Directive 2006/42/EC,
Electro Magnetic Compatibility Directive 2004/108/EC
Pressure Equipment Directive 97/23/EC
Unless specifically specified otherwise:
all pressure vessels will be designed according to CE-PED and approved by TV
(German NoBo) or similar.
electrical design & approvals will be in accordance with IEC 60204-1.

27

9. One (1) Supervisor for Mounting, installation, Commissioning & Training


Company CO2 provides one qualified engineer/supervisor for a period of 8 weeks, 6 days per
week, 50 on site workings hours per week to:
Supervise mounting and erection of all delivered items
Supervise installation of interconnecting piping, cabling and insulation
Commission (start-up) the offered parts, directly after erection
Test run and fine tune the system for acceptance
Train the local personnel (during commissioning) in English (translation care of
customer).

Scope:
One (1) round-trip for the supervisor
Daily Allowances and Local Transport.
local costs, hotel and board (acc. to western standard) are care of customer.
In case the supervision of the installation and commissioning takes longer than the above
mentioned period of time due to no fault of Company CO2, the additional supervision
costs will be charged separately according to Company CO2 Service Department terms
and conditions.
Should there be conditions where in the Company CO2 engineer/supervisor assigned
and on site for installation supervision and start up is deemed not qualified to execute
certain job/task according to local regulations, laws or customer rules then the customer
is to and will be responsible to arrange/pay for a qualified specialist to meet this
requirement at no expense to Company CO2.
To prevent any unnecessary project delays the customer will provide and put at the
disposal of the Company CO2 engineer/supervisor :
Sufficient amount of skilled workers including equipment, tools etc. Company CO2
cannot be held responsible for the damage or delay caused by others. The Company
CO2 supervisor has the right to reject supplied workers and their tools, which are to be
replaced by the customer
English speaking translator
All necessary utilities such as CO2, glycol, compressed air, water, electricity, etc.
On site phone and Internet connection.
Company CO2 will provide a schedule for the onsite works indicating necessary labor,
crane etc.
It is assumed that supervision of the installation works and commissioning of the offered
parts will take place within 1 year after Ex-works WWW City/Manufacturer

28

10. One (1) Turnkey Design Package


Company CO2 will supply a Design Package (DP) for the interconnecting piping, cabling and
insulation. The design package includes:
Piping isometrics
Piping bill of materials
Cable bill of materials
Cable tray bill of materials
Piping support drawings
Insulation specification

Notes & recommendations:


Documentation will be prepared according to relevant Good Engineering Practice.
Differences or specifications requested by the customer will be charged according to
expenses.
The customer is to provide, as built PID, layout & other documents relevant for a proper
design and speedy installation of the offered scope of supply.
Project planning is based on speedy reply and/or confirmation by the customer: PIDs,
layout & other engineering data need to be approval within 5 working days of receipt.

29

11. Utility Requirements


Approximate utility consumption of offered parts based on 24-hour continuous foam free
operation at maximum capacity. Values are estimates with tolerance 5% and are subject to
further detailed engineering.

Power consumption 3x 460 VAC (+/- 5%) /60 Hz


Booster
CO2 Compressor
Pump Ethanol washer to chiller
Active carbon filter dryer (per line)
Refrigeration
Cooling tower + cooling water pumps
CO2 pump

Power
consumption
32,0 kW
274,0 kW
2,2 kW
18,5 kW
180,4 kW
41 kW
2.2 kW

Installed
capacity
37,00 kW
320,0 kW
3,0 kW
73,5 kW
250,0 kW
44 kW
4.4 kW

Specific power consumption (0,189 kW/kgCO2, incl Cooling tower, 0,175 KW/kgCO2 excl.
cooling tower)

Food-grade water - inlet conditions: chloride < 3ppm w/w 20...30C, 1...4 barg
High pressure Gas Washer

0,75 m3/h

Process water - inlet conditions: 25...35C, 1...4 barg


Cooling tower water

2,2 m3/h

Cooling water - inlet conditions: 32...34C, 1...4 barg


CO2 Compressor
Refrigeration

248,4 kW
594,0 kW

Compressed air inlet conditions : clean, oil & NH3-free, 6 barg with dew point < -20C
(acc. to ISO 8573.1 class 3)
Compressed air

1 Nm3/h

Notes:
Foam separator will only consume water when foam is detected. Foaming is not
considered normal operation.
CO2 compressor will only consume utilities when CO2 compressor is running.
Reboiler heating element 33kW will only consume at start / stop of the Liquefaction
System.
Utility consumption figures are confirmed during the detailed engineering phase
of the project.

30

12. General
12.1. Includes
The first filling of:
CO2 compressor oil
Refrigerant compressor oil
Active carbon
Sorbead SW Dryer agent
Remark: NH3 is never included and is to be supplied by the customer.
12.2. Excludes
The items or services listed below are excluded from the scope of supply. Wherever
possible we are prepared to submit a quotation for such items upon request. All items
and services not explicitly mentioned are not included in the price. In particular not:
Local transport, hotel and board for offered Company CO2 supervisor
All local labor, tools & equipment on site
Unloading, storage and placing of the offered parts
All piping, piping bridges, cables & cable trays outside of skids
All insulation work of the cold and warm parts of the installation (materials delivered)
Integration of existing system/parts
Control and integration of offered parts into customers central control system
Painting and labeling of piping and cables
Dismounting and removal of the replaced and/or existing parts
All civil works and mounting/support constructions, platforms, ladders & walkways.
Drains, connections, blow-off lines and gullies
Onsite X-ray welding checks
All health and safety certificates
All local approvals, technical translations, RTN Technical Passports of pressure
vessels, Permission to Use, Permission to Operate, etc. are care of client
All approvals by the local authorities, such as permits, certificate of inspection,
permission to use, license to operate
All certificates (except CE/PED certificates for the pressure vessels) unless otherwise
mentioned
All required utilities (water, glycol, electricity, CO2 etc.). Connection point in engine
room
All refrigerant & CO2 detection, ventilation systems etc. in engine room.
Municipal fees, field inspection, or related local authority fees
Duties, vat, taxes or fees
Custom clearance, related works ((un)loading, storage etc.) & consequential delays
Liquidated and/or consequential damages due to loss of production. This includes costs
relating from the loss of product during the commissioning phase
Spare parts
Wind, and seismic calculations and cost implications.
Any item not specifically mentioned in the quotation.

31

13. Guarantees
When the offered parts are installed and operated according to the Company CO2 instructions
and commissioned by a Company CO2 supervisor within 12 months after date Ex-Works WWW
City, Company CO2
guarantees the following:
13.1. Warranty
The offered parts have a warranty period of 12 months from start-up, however, not longer than 18
months from date of Ex-Works Company CO2, WWW City. Parts that are subject to wear and
tear (e.g. gaskets, coils) are not covered by this warranty. During the warranty period Company
CO2 will replace defective parts free of charge, however we reserve the right to charge for labor,
lodging and traveling costs. Not covered by the guarantee are liquidated and/or consequential
damages due to loss of production.
13.2. Design Data
The offered guarantee and parts are based on the above-mentioned technical specifications and
the following designed data:
13.2.1. Raw gas inlet
As per gas analyses from Airborne labs 19 November 2014 (exluding Hexanes +)
CO2 source :
fermentation gas
1100 mbar
CO2 pressure :
CO2 temperature :
30 C
min. 98,00 vol %
CO2 purity at fermenter turn-in :
CO2 purity to plant :
min. 98,00 vol %
CO2 Condensing pressure :
17,50 barg
Relative humidity :
100 %
13.2.2. Utilities
Foodgrade / tap water 2 :

Circulation (cooling) water

3+4

In addition to meeting WHO guidelines or EU


regulations, the water needs to meet the
following specifications:
Chloride (Cl-) < 2 mg/l
Chlorine, free < 0.1 mg/l
: pH 7.5 8.5
: Hardness < 8 dH
: Chloride (Cl-) < 100 mg/l @ T< 40C or
Chloride (Cl-) < 250 mg/l @ T< 20C
: Iron (Fe) < 1 mg/l
: Silicon Dioxide (SiO2) < 200 mg/l
: Sulfate (SO4 ) < 100 mg/l
: Tot.Diss.Solids (TDS) < 600 mg/l
: Corrosion inhibitors to be dosed & monitored
: Same as Circulation water incl. site dosing and
monitoring of the following:
Corrosion inhibitors
Anti-scale measures
Anti-biocide measures
: Corrosion inhibitors to be dosed monitored
2-

Make up water for cooling tower

Glycol-water

32

13.2.3. Engine room


Ambient temperature in engine room (frost free) : min. 20 C
: max. 35 C
Ambient temperature outside
: min. 24 C
: max. 36 C
Environment and utilities incl CO2 raw gas
: Not aggressive to carbon steel and
stainless steel. e.g. AISI 304

Notes & recommendations:


1) A peak is defined as a max. concentration over a time period of max. 15 min. during 12 compressor
running hours.
2) Water which comes in contact with CO2-fermentation gas, f.e. foam separator and gas washer.
3) Water which does not come in contact with CO2-fermentation gas, and used in various CO2 plant heat
exchangers.
4) Higher concentrations requires professional water treatment. Please consult your water treatment
specialist.

Company CO2 reserves the right to adapt specifications for engineering purposes.
13.3. Performance test protocol
A detailed performance test protocol for acceptance is subject to scope of supply. Test protocol is
based on max. 48hr continuous operation, and will be fine-tuned during detailed engineering
stage of the project. The following points will be tested:
The guaranteed capacities refer to the in this quotation mentioned Design Data.
Capacity of the offered parts are according to the VDI-rules for compressors (DIN 2045
and DIN 1945) with a tolerance of 5%.
- The capacity of produced liquid CO2 into tank is measured by means of mass
flow meter from reboiler to tank and/or level sensor in tank.
The dew point is measured in the CO2 gas phase after the Driers. Measurement is done
with a manual Dew Point Tester (DPT), which can be offered optionally.
CO2 & O2 outlet values are measured in the liquid phase after the reboiler.
Measurement is done with an inline OGM O2 monitor which can be offered optionally.
For the quantification of organic and/or sulfur components, a gas sample after the
Driers can be taken for analysis. A CO2 sampling and sampling service (CAS) can be
offered optionally.

33

14. Standard Accessories List


The following accessories and instruments have been foreseen in the CO2 Recovery Plant where
applicable. Depending on the type of equipment offered some components may not be delivered.
Description
Actuators
Butterfly valve
Ball valve
Check valves
CO2 tank valves
R507 valves
R507 safety valves
R507 bursting disks
R507 change-over valves
3-Way valves
4-Way valves
Control Valves
Pneumatic valves
Electro Pneumatic valves
Solenoid valves
Safety valves
Pressure reducing valve
Temp. control valves
Temperature indicators
Temperature switches
Temperature transmitters
Level switch
Level transmitter
Flow indicator
Flow switch
Flow transmitter
Pressure gauge
Pressure switches
Pressure transmitters
Pressure diff. transmitter
Filters / Strainers
Dust filters
Spray ball
Electric motors
Foam detectors

Make
El-o-matic / Econ(osto) / Tyco
Keystone / Econ(osto)
Meca inox / Haitima / Econ(osto)
Meca Inox / EDS / Herl / Gestra / Econ(osto)
OEM Standard / Herl / Econ(osto) / Herose
KMP / Castel
Hansa
Henry
Henry
Meca Inox
BAC / Econ(osto)
Samson / Brkert / End
Festo
End Armaturen / Econ(osto)
Danfoss / Alco / Econ(osto)
Leser / Herl / Henry / Generali
Brkert / Tescom / Econ(osto) / Norgren
Danfoss / Thermoreg / Samson
Econosto
Jumo
Endress & Hauser
Endress & Hauser / Hansen
RTK /IFM
Yokogawa
Honsberg / End/ IFM
Endress & Hauser
Econosto / Wika / VDH
Danfoss
Danfoss / Endress & Hauser
Endress & Hauser /
Meca Inox / Econ(osto) / Hansa / KMP / Alco
Amafilter / Donaldson
Schlick / Hake
WEG / Hoyer / OEM Standard
Endress & Hauser

Company CO2 reserves the right to make alterations to the above mentioned accessories list for
engineering purposes. Alternatives may be supplied subject to revised quotation. OEM supplied
accessories are OEM standard.

34

15. Commercial Summary


15.1. Scope overview

and pricing

Quantity
Description
Currency
One (1)
Booster 3240 kg/h
EUR
One (1)
Booster after cooler - 3240 kg/h
EUR
One (1)
Compressor pre-cooler - 3240 kg/h
EUR
Two (2)
CO2 compressor - 1460 kg/h
EUR
One (1)
Pre Cooler - 3137 kg/h
EUR
One (1)
Gas washer - 1800 kg/h
EUR
One (1)
Pump Ethanol washer to chiller
EUR
One (1)
Active carbon filter dryer - 2920 kg/h
EUR
One (1)
NOx Filter
EUR
One (1)
Refrigeration - 2920 kg/h
EUR
One (1)
Cooling Tower Circuit 1082 kW
EUR
One (1)
Stripping system - 2920 kg/h
EUR
One (1)
Control System
EUR
One (1)
Turnkey materials (Pipes, Cables, Insulation)
EUR
One (1)
Design approvals and certification
One (1)
Home based engineering, Design & Project management
Total project price, EXW unpacked WWW City/Manufacturer
EUR
1.598.370

Price
44.660
31.330
40.540
347.720
13.410
57.780
9.550
188.920
41.840
276.870
92.380
113.530
107.890
231.950
Included
Included

Packing included, CIF Manila Philippines container liners owned

EUR

47.720

TOTAL EQUIPMENT AND TRANSPORT

EUR

1.646.090

One (1) On site visit Project Manager


One (1) Supervisor for Mounting, installation, Commissioning & Training
One (1) Turnkey Design Package
TOTAL SERVICES

EUR
EUR
EUR
EUR

8.540
55.550
14.350

78.440

TOTAL PROJECT PRICE:EQUIPMENT + SERVICES

EUR

1.724.530

15.2. Options
Quantity
Description
One (1) Foam separation system - 2920 kg/h
One (1) Foam trap - 2920 kg/h
One (1) Inline O2 Measurement OGM - LHO LP
One (1) Variable Speed Drive Booster
Two (2) Variable Speed Drive CO2 Compressor
One (1) Variable Speed Drive NH3 Compressor
One (1) Set of Spare parts

35

Currency
EUR
EUR
EUR
EUR
EUR
EUR
EUR

Price
24.660
5.640
6.950
4.880
33.760
23.970
23.740

15.3. Terms
General

& Conditions

Delivery
Delivery time
Delivery conditions
Terms and conditions

Payment

Currency
Duties
Validity

36

: The above-mentioned prices are calculated in accordance with the


actual costs basis at date of issue of this proposal and under the
condition that there is no partial delivery or variance from the scope of
supply.
: Packing included, CIF Manila Philippines container liners owned
: To be agreed upon subject to time of order.
: According to ICC Incoterms 2010
: To this proposal the 'General Terms and Conditions of Sale Of
Company CO2 Water Proces Technologie Holding B.V. and its
subsidiaries' apply, filed at the office of the Trade Register of the
Chamber of Commerce for East WWW Country, under the number
06032084., a copy of which is enclosed. Company CO2 B.V. expressly
rejects the applicability of any of the customer's general terms and
conditions.
: Payment 100% by Letter of Credit, of which:
30% will be payable at order
60% at delivery against documents.
10% after signing SAT protocol
: All prices stated on this proposal are in EURO
: All required duty, excise, VAT etc. payments with respect to this
proposal are care of customer.
: 2 months as from proposal date.
Project pricing and Ex-Works delivery times are subject to the price and
availability of steel at the time of manufacturing.

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