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Bruker AXS

D8 ADVANCE
X-ray Diffractometer

Pre-installation Guide
(North America)
System Requirements
The following specifications are general system
requirements. Use this information to make an initial
decision on the suitability of your proposed site. Refer to
later sections of this Pre-installation Guide for more
details.

Power (pages 4 - 5)

Purpose
This Pre-installation Guide will aid you and any required
personnel in site preparation prior to installation of the
D8 ADVANCE X-ray diffractometer.
Read these instructions carefully and thoroughly to
prepare for the installation of your D8 ADVANCE. Proper
site planning will ensure optimum efficiency,
maintenance access, proper instrument performance,
and avoidance of unnecessary delays during installation.

Responsibility
The customer is responsible for making certain that the
basic site requirements for the D8 ADVANCE are
fulfilled. These instructions are to be followed by the
customer and by personally contracted tradespeople,
except where otherwise noted.
When the basic site requirements are fulfilled, it is the
customers responsibility to complete the attached Preinstallation Checklist and return it to Bruker AXS via fax.

System

208-240V, 60Hz, 1-phase, 40A

Computer/peripherals

100-120V, 60Hz, 1-phase, 15A

Haskris R100C water


recirculator

208-240V, 60Hz (isolated),


1-phase, 15A

Cooling Capacity

3850W (13125 btu/hr) or greater

Temperature

50-68F 2F (10-20C 1C)

Pressure

60-90 psi (4-6 bar)

Quantity*

6 gal (23 L)

*Quantity specified is for Haskris R100C. Use distilled water.

Communications (Figure 2 and Table 5)


Optional RJ-11 line near system for voice connection
Ethernet network connection (Table 5)
Table 1.

Pre-installation Overview

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M88-E04046

18 February 2009

D8 ADVANCE Dimensions

D8 ADVANCE Dimensions

D8 ADVANCE
dimensions
and weight

Shipping Dimensions

Height

82.5 (209.5 cm)

Width

55.1 (140.0 cm)

Depth

49.4 (125.5 cm)

Weight

approx. 1190 lbs


(540 kg)

Floor load
capacity

146.9 lbs/ft2 (717.0 kg/m2) minimum. The floor


should be level and as rigid as possible to avoid
vibration.

Doorway
clearance
required

Largest sub-assembly
(unboxed/uncrated), if
mounted parts are
removed

36.0 (91.4 cm)

27.5 (70.0 cm)


minimum

Although the
instrument has
wheels, it should be
accessible from all
sides for proper
servicing and airflow.

Wall-to rear of
instrument
clearance

Table 2.

The D8 ADVANCE shipment includes two large boxes


from Bruker AXS factories (Table 3). To account for
variation in box size, maximum dimensions are given in
the Table. Additional small boxes may arrive with the
shipment, given the configuration of the system.

Base Box (on pallet)

Top Box (on pallet)

Height

58.3 (148 cm)

44.5 (113 cm)

Width

57.1 (145 cm)

43.3 (110 cm)

Depth

66.1 (168 cm)

55.1 (140 cm)

Weight

1030 lbs (467 kg)

710 lbs (322 kg)

Table 3.

Maximum dimensions of instrument boxes from factory

Actual instrument dimensions, weights, and clearances

33.3" (84.7 cm)


(enclosure rear removed*)
55.1" (140.0 cm)

46.7" (118.7 cm)

Side View
46.0"
(116.8 cm)

43.6"
(111 cm)

Front View

(light bar
removed*)

82.5"
(209.5 cm)

3.1"
(8 cm)
35.1"
(89.2 cm)

33.7" (85.6 cm)


(front and rear panels removed*)

Dolly - 2.4"
(6.0 cm)

46.3" (117.7 cm)


(side panels removed*)

*NOTE: Dimensions with portions temporarily removed for transportation

Figure 1. D8 ADVANCE dimensions

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M88-E04046

Environmental Considerations

Environmental Considerations
Room/Instrument

Requirements

Optimal room temperature

75.2F (24.0C)

Room operation-range temperature

57.2 - 93.2F (14.0 - 34.0C)

Maximum temperature gradient

1.8F (1C) per hour for highest stability of measuring values

Relative humidity

20%-80%, non-condensing

Heat dissipation to the air by the


diffractometer (with temperature stabilizer,
electronics measuring, X-ray generator, and
vacuum pump).

1.0 kW (3412 btu/hr) maximum


Dissipated heat must be removed by a ventilation or air conditioning system. Cooling air
should flow around the instrument without restriction. If possible, locate the air conditioning
and heating ducts so that their airflow is not aimed directly at the instrument.

This configuration assumes that an external


water recirculator is installed in a separate
room.

NOTE: We recommend a clean, dust-free environment.

Static electricity elimination (to avoid adverse


effects on instrument electronics)

Any carpeting in the area should be of a conductive variety. If the area is carpeted with nonconductive carpet, we recommend that you place anti-static mats over the conventional
carpeting in the area around the instrument.

Table 4.

Environmental considerations

External water recirculator


(Haskris R100C)

28' (8.5 m) maximum


cable distance between
instrument and computer.
Allow for routing of cables
along baseboards.

27.5"
(70 cm)

Generator

Electronics

RJ-45 jack
for internet
connection
(optional)

RJ-11 jack
for voice
connection
(optional)

27.5"
(70 cm)

27.5"
(70 cm)
Minimum
clearance

Table (not factory-supplied)

NOTE: For plumbing and electrical details,


see the other Figures and Tables in
this Pre-installation Guide.

Figure 2. Typical D8 ADVANCE floor plan

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M88-E04046

Communications

Communications

Electrical Power
See Table 6 for power requirements for the D8

Connection

Connector

Purpose

Telephone
(optional)

RJ-11

Voice connection near


instrument

RJ-45 (Ethernet)

Remote diagnosis over


the internet

Internet
connection
Table 5.

Communications: connections

We strongly recommend that you install a telephone


connection (for voice communications) near the
instrument.
NOTE: Bruker AXS Remote Diagnosis features are now
available over the internet (i.e., WebEx). Check
with your IT administrator to find out how
Remote Diagnosis may affect your IT policy.

ADVANCE (including the computer and peripherals).


Note the lengths of the various cables.
On the wall behind the instrument, connect power

from the building mains to a plug-type wall outlet or


to a direct-wired circuit breaker/disconnect box, so
that power to the instrument can be interrupted if
necessary.
NOTE: Outlet and plug not factory-supplied.

NOTE: If the power line voltage at your site fluctuates


outside the values in Table 6, a compatible line
voltage conditioner or regulator may be
necessary. Check with your sites electrical
coordinator.
Wire the room air conditioner and any external

pumps to a different electrical circuit than that used


for the instrument. High starting currents from their
motors may adversely affect line voltage stability.
Additionally, provide a separate electrical power circuit for the Haskris water recirculator (if purchased).

208 VAC, 40A


Circuit breaker, disconnect box, or
outlet for plug (not factory-supplied).
Secure to wall.

208 VAC, 15A


(isolated from system)
Haskris
R100C
water
recirculator

110 VAC, 15A


Ground cable
(factory-supplied)

six-outlet power strip


(included)

Generator

Electronics

Figure 3. D8 ADVANCE electrical connections

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M88-E04046

Electrical Power

Instrument
(left side)
Electronics & Generator

Cable to
chassis ground
(factory-supplied)

3-conductor, 8-gauge
power cable (factory-supplied).
Cable is 20 feet (6.1 m) long,
4 feet (1.5 m) of which are
enclosed inside the instrument.

Fuse or
breaker
40 A (2)

Electrical Box
House Power
208 VAC

L1
L2

Earth Ground

Figure 4. D8 ADVANCE electrical connections (schematic)

Component

Current rating

Voltage and frequency

Power cable lengths

D8 ADVANCE diffractometer
unit

40A

208-240V, 60Hz, 1-phase

8-gauge, 3-conductor power cable


(factory-supplied), about 15 ft (4.6 m)*

Computer and peripherals

15A

100-120V, 60Hz, 1-phase

6 ft (1.8 m)**
Data cables: about 28 ft (8.5 m)

External water recirculator,


Haskris R100C

15A

208-240V, 60Hz, 1-phase

About 8 ft (2.4 m)***

* Customer supplies plug to match wall receptacle (if used).


** Factory-supplied 6-position AC outlet strip (110V).
*** For the recommended Haskris model (R100C), customer supplies plug to match wall receptacle (if used).
If fuses are used, use slow-blow fuses.
Table 6.

D8 ADVANCE electrical specifications

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M88-E04046

Cooling Requirements

Cooling Requirements
Cooling capacity
when water source
is 65F (18C):

3850W (13125 btu/hr)

Water pump
capacity

3.7 gal/min (14.1 L/min)

Water reservoir
volume

6 gal (23 L)

Temperature
stability

2F (1.1C)

Refrigerant

R134a

Unit weight

325 lbs (148 kg)


(approximate shipping
weight without water in
the tank)

Unit dimensions

31H 21W 29D


(79 cm 53 cm 74 cm)

Coolant required

Clean, potable, distilled


water. Do not use
deionized water.

When temp. is:


65F (18C)
75F (24C)
85F (29C)

Flow rate required is:


1.0 gal/min (3.8 L/min)
1.5 gal/min (5.7 L/min)
3.1 gal/min (11.8 L/min)

Minimum required
pressure differential
from condenser
water inlet to outlet:

25 psi (1.7 bar)

During installation, the Bruker AXS Field Service


Engineer will connect factory-supplied 1/2 (12mm)
inside diameter hoses between the Haskris R100C and
piping, and then between the piping and instrument (the
unit and instrument having customer-supplied barbed
fittings). The Engineer will then fasten the water hoses
to the barbed fittings with hose clamps.

Maximum pressure
differential from
condenser water
inlet to outlet:

60 psi (4.1 bar)

Maximum
condenser water
inlet pressure:

125 psi (8.6 bar)

NOTE: The Haskris R100C needs supply water and a


drain to remove heat that it emits. However, it
keeps water consumption to a minimum using a
water valve that opens and closes as required.

Must be installed in
a clean, indoor
environment. If
possible, install the
Haskris in a
separate room to
minimize noise and
heat emission.

We recommend access to
the:
TOP for routine
maintenance, such as
changing water in the
reservoir.
FRONT for visibility of
controls and readouts.
ONE SIDE for convenient
servicing should a spare
part be required.

An external cooling-water system is required to


dissipate heat produced by the D8 ADVANCE. The
cooling-water system must be fed with a closed-circuit
cooling system.
To minimize difficulties with cooling water (e.g.,
suspended solids, low pressure, and extreme water
temperature variations), we recommend installing a
Haskris R100C closed-circuit water recirculator as
shown in Figures 5 and 6. Other cooling system
arrangements are not recommended as they will
inevitably fail to minimize the aforementioned difficulties
and result in cooling problems.

Technical
features

NOTE: If you do not wish to install a Haskris closedcircuit water recirculator, contact Bruker AXS for
more information.

CAUTION

The X-ray tubes warranty does not cover damage


resulting from improper cooling water.
Install two 3/4 copper lines, each maximum length of
48 ft (15m), with a shut-off valve near each end of each
pipe. Install 1/2 barbed fittings (not supplied) at each
end of the pipes. These copper lines are intended for
transporting the cooling water over long distances. The
barbed fittings at the end of the pipes will connect to the
short, factory-supplied hoses attached to the instrument.

NOTE: To protect the Haskris R100C, ensure that the


water is free of suspended matter. Also, ensure
that water hardness does not exceed 300 mg/
liter CaO, while remaining at neutral pH (7).

Condenser
cooling water
requirements

Location

Table 7.

Haskris R100C recirculator specifications

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M88-E04046

Cooling Requirements

Haskris Model R100C


TECHNICAL SPECIFICATIONS
1. Power Requirements: 208/230V-1-60Hz
2. F.L.A. Rating: 9.9A
3. Recommended Fuse Size: 15A (time delay)

Water Level
Indicator

Note:
Supply and return connections are
1/2" Hand Valves with 1/2" Hose Barbs.

Unit ON/OFF
Switch

65
FULL
MENU

2.25"
Flowmeter

SUPPLY

Power
Indicator

31.0"
(78.7 cm)

RETURN

Water Temp
Control & Display

DEPTH = 29.0"
(73.7 cm)

POWER CORD (7 ft., no plug furnished)

24"

21"

Ventilation grille

18.5"
2.5"
2.5"

3"

City Water "IN"


3/8" FPT Brass
City Water "OUT"
3/8" FPT Brass

Leveling Legs
(adjustable from 1/2" To 2")

21.0"
(53.3 cm)

FRONT
VIEW

REAR
VIEW

NOT DRAWN
TO SCALE

NOT DRAWN
TO SCALE

Figure 5. Haskris R100C recirculator specifications

Water supply

Haskris
R100C

Drain

Reinforced industrial water hose


Return from
instrument

Supply to
instrument

3/4" copper tubing


Shut-off valves (wall-mounted)
1/2" barbed fitting

NOTE: 25 (7.6 m) of water hose comes


with the Haskris R100C.
Generator

Electronics

65 (20.0 m) of usable water


hose comes with the D8
ADVANCE.

Figure 6. Cooling water with the Haskris R100C closed-circuit water recirculator

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M88-E04046

Plumbing Requirements

Plumbing Requirements
Material supplied with D8
ADVANCE

Tubing/hose ID sizes for


barbed fittings

Tubing/hose lengths

Counter tube gas


(P10for MBraun positionsensitive detector only)

Inlet: Black Viton tubing

0.125 (0.32cm)

23 ft (7m)

Outlet: Blue polymer tubing

0.25 (0.64cm)

23 ft (7m)

Helium

Blue Polymer tubing

0.125 (0.32cm)

23 ft (7m)

Cooling water hoses

Pressure water hose

0.5 (1.27cm)

65 ft (20.0m)

Vacuum exhaust*

Plastic hose

0.5 (1.27cm)

17 ft (5.2m)

* Mist elimination is installed; exhausting vacuum is an option. You must provide an outlet for the vacuum exhaust (see Figure 2).
Table 8.

Tubing and hose sizes for supplied barbed fittings on D8 ADVANCE and Haskris R100C water recirculator

Gas Specifications
Position-sensitive Detector Gas Supply
(optionalfor MBraun PSD only)

Helium Supply (optional)


For equipment with a helium or nitrogen flush option

If an MBraun PSD (position-sensitive detector) is

used with the D8 ADVANCE, install a P10 gas cylinder and regulator as noted in Table 9.
Install a cylinder of gas with a two-stage regulator

(for the flow counter) as noted in Table 9. We recommend indoor installation of the gas cylinder.

(required for liquid or loose powder analysis), install a


helium or nitrogen cylinder with a two-stage regulator as noted in Table 9.
Secure the cylinder with a mounting support to avoid

accidental tipping.

Ensure that the cylinder is securely mounted to avoid

tipping. Observe all safety regulations for flammable


gases. We recommend that you keep a reserve cylinder.
Install as short a line as possible from the gas cylin-

der to the instrument. Use factory-supplied Viton tubing (length as noted in Table 8). If your supply line
must exceed the supplied length, use oxygen-free
(high-purity) copper or stainless-steel piping. Ensure
that the lines are clean and free of water, solvents,
and particulate matter. Avoid exposing the gas lines
to extreme temperatures (such as heating vents).
Operate the flow counters only with a commercial-

grade mixture of P10 gas (i.e., 90% Argon, 10%


methane, impurities less than 0.5% by volume).

Gas

Cylinder/Regulator
(not factory-supplied)

P10

Compressed-gas cylinder with T-size


cylinder filling pressure, 2900 psi (180
bar), with regulator such as AGA model
SGVHPT272B-350 or equivalent.*

Helium or nitrogen
(optional; use if
ordered)

Compressed-gas cylinder with T-size


cylinder filling pressure, 2900 psi (180
bar), with regulator such as AGA model
SGVHPT270B-580 or equivalent.*

* Securely mount the cylinders to a wall or table. Observe safety


regulations for all flammable gases.
Table 9.

Gas specifications

Install a separate exhaust line leading to an outside

discharge for the spent gas.

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M88-E04046

Final Check

Final Check

When the System Arrives

You, the customer, are responsible for meeting all


applicable building and safety codes. Once the preinstallation utilities are connected, get certification (from
an approved authority) that the installation meets all
local building and safety codes.

When the system arrives, check it for damage with

When all pre-installation work is finished, complete the


attached D8 ADVANCE Pre-installation Checklist and fax
it to Bruker AXS.
Fax:

1 (608) 276-9162 or 1 (608) 276-3015

the delivery driver. Contact the carriers office and


Bruker AXS immediately if you find any damage.
Compare the packing list (i.e., the number of boxes

received) with your order invoice and contact Bruker


AXS if you find any discrepancies.
Move boxes or crates to the installation site (if possi-

ble) to facilitate timely installation. Wait until a Bruker


AXS Field Service Engineer opens the boxes to
check their contents against your invoice. Do not
open or uncrate any boxes.
If uncrating is required, call Bruker AXS for authoriza-

Also, contact the Bruker AXS Service Department by


telephone to confirm that your site is ready for
installation.
Tel:

1 (800) 234-XRAY [9729] or 1 (608) 276-3087

tion at 1 (800) 234-XRAY [9729] extension 3087. If


you are authorized to uncrate the shipment, save all
packing material until the Bruker AXS Field Service
Engineer completes the installation.
Installation must be performed by a Bruker AXS Field

Service Engineer.
Save all packing materials for the system until the

Upon receiving confirmation that your site is ready,


Bruker AXS personnel will schedule the instrument
installation.

Bruker AXS Field Service Engineer has completed


the installation.
NOTE: Installation of the system typically requires three
to four working days. Optional attachments
require additional time for installation and
testing.

Bruker BioSciences

Bruker AXS Inc.

40 Manning Road
Billerica, MA USA

5465 East Cheryl Parkway


Madison, WI 53711-5373 USA

Phone +1 (978) 663-3660


Fax: +1 (978) 667-5993

Phone +1 (800) 234-XRAY [9729]


Fax +1 (608) 276-3006

E-mail: info@bruker-biosciences.com
www.bruker-biosciences.com

E-mail: info@bruker-axs.com
www.bruker-axs.com

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D8 ADVANCE Pre-installation Checklist

D8 ADVANCE Pre-installation Checklist


Please complete the checklist below and fax it to the Bruker AXS Service Department:

FAX
FROM:

TO:

Contact Name

Phone

Company/Organization

Fax

Bruker AXS,
Attn: Service Dept.
1 (608) 276-9162 or
1 (608) 276-3015

Email

Component

YES/NO

Value/remark

Initial/date

Room Location
Floor load capacity exceeds 146.9 lbs/ft2 (717.0 kg/m2)
(see Table 2)
Room height exceeds 82.5 (209.5 cm) (see Table 2)
Floor space for D8 ADVANCE free of equipment and clean (see
Figures 1 and 2, Table 2)
Doors and hallways from loading dock to location have adequate
clearance for moving the D8 ADVANCE in its shipping crates;
freight elevator available (see Table 3)
Clearance on all sides of uncrated unit exceeds 27.5 (70.0 cm)
(see Figure 2, Table 2)
Computer table within 13.0 (4.0 m) of instrument

Environment (see Table 4)


System is not exposed to direct sunlight
Temperature between 57.2 - 93.2F (14.0 - 34.0C)
Temperature gradient less than 1.8F (1C) per hour
Heat removal capacity exceeds 1.0 kW (3412 btu/hr)
Relative humidity between 20% - 80%, no condensation
Carpeted rooms: anti-static carpeting or mats installed

Communications (see page 4)


Optional voice line (near instrument)
Internet connection for remote diagnostics

Electrical Power (see Figure 4, Table 6)


208 VAC, 60 Hz 3 Hz, 40A (D8 ADVANCE)
208 VAC, 60 Hz 3 Hz, 15A (Haskris R100C)
110 VAC, 60 Hz 3 Hz, 15A (Computer and peripherals)

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D8 ADVANCE Pre-installation Checklist

Component

YES/NO

Value/remark

Initial/date

All electrical power for the system must be isolated from circuits
that have high starting currents (e.g., air conditioners, pumps,
furnaces)
Electrical connection of instrument to mains power supply is
provided with automatic circuit breakers for all phases
It is possible to disconnect the D8 ADVANCE completely from the
mains power supply, using either a labeled switch or a circuit
breaker located near the system
Power cable connected directly to switchboard
Socket outlet according to DIN49462, VDE 0623, IEC 309-1
(Approved plug connector supplied by customer)

Cooling Requirements (see page 6)


Closed cooling system (Haskris R100C recommended)
(see Figures 2 and 6)
Plumbing/piping complete
(for recommended Haskris unit)
Customer-supplied cooling system (not recommended)
The Haskris R100C water recirculator meets the cooling water requirements of the system. If you provide your own water supply, it must
meet the following requirements.
Flow rate greater than 1 gal/min (3.6 L/min). Recommended rate:
1.1 gal/min (4.0 L/min)
Pressure 60-110 psi (4-7.5 bar) and pressure-free drain
Temperature 59-68F (15-20C). Room temperature must be high
enough to avoid condensation.
Bruker AXS recommends the use of distilled or reverse osmosis (RO) water for cooling the X-ray tube and generator. Use of deionized water
is NOT recommended. If building water is used, it must meet the following requirements.
Hardness less than:
300mg/L CaO, or
30 CaO (German scale), or
53.7 CaO (French scale), or
37.5 CaO (UK scale)
pH of 7.0 1
Adequate filtering to remove suspended solids (50 m)

Plumbing Requirements (see page 8)


Distance to water supply less than 26 (8 m), less than 48 (15 m)
if Haskris used
Shutoff valves installed on both lines (not required if discharging
into drain)
Elevation difference between Haskris and instrument less than 20
(6 m)
NW hose barb fittings for supply and return of cooling water

Supply Gases (the optional helium mode requires helium gas cylinders and regulators, not factory-supplied) (see
Tables 9 and 8, Figure 2)

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D8 ADVANCE Pre-installation Checklist

Component

YES/NO

Value/remark

Initial/date

P10 Gas (for MBraun PSD only):


Commercial-grade P10 gas (90% Argon, 10% methane, less than
0.5% impurities by volume) in T-size gas cylinder, e.g., 50 L, 200
bar (2900 psi)
Cylinder/regulator securely mounted to wall within 6 (2 m) of the
D8 ADVANCE
If mounted further away than the supplied hose length, correct
tubing/piping line installed (see Table 8)
Local safety requirements for flammable gases fulfilled
Exhaust gas vents to the outside, or a fume hood is present
(if mandated by local safety requirements)

Helium Gas (if applicable):


Cylinder/regulator securely mounted to wall within 6 (2 m) of the
D8 ADVANCE
If mounted farther away than the supplied hose length, correct
tubing/piping line installed (see Table 8)

Vacuum
Exhaust to outside (optional)

Final Check
All local safety codes are met
Fax a copy of this form to: Bruker AXS, Attention: Service
Department 1 (608) 276-9162
Call for installation: 1 (800) 234-XRAY [9729] extension 3087
When system arrives: Check packing crates for shipping damage. If there is damage, contact your Carriers Office and Bruker AXS. Compare
the packing list (the number of boxes) with your invoice. If possible, move boxes (crates) to installation site or storage area.
Do not open crates or boxes. If uncrating is required, call Bruker AXS for authorization at 1 (800) 234-XRAY [9729] extension 3087.
If authorized to uncrate, save all packing material until the Bruker AXS Field Service Engineer completes installation.

3 of 3
Bruker BioSciences

Bruker AXS Inc.

40 Manning Road
Billerica, MA USA

5465 East Cheryl Parkway


Madison, WI 53711-5373 USA

Phone +1 (978) 663-3660


Fax: +1 (978) 667-5993

Phone +1 (800) 234-XRAY [9729]


Fax +1 (608) 276-3006

E-mail: info@bruker-biosciences.com
www.bruker-biosciences.com

E-mail: info@bruker-axs.com
www.bruker-axs.com

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