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2016FINAL EXPERIMENT
TITLE: Evaluation of Compressive Strength of Polyester Polymer Concrete with MicroMix as Filler
Objective:
To find best mix of polyester resin and micro-mix filler that will result to polymer
concrete with high strength
To produce fire and water resistant concrete.
To know the best percentage of filler that will improve compressive strength of the
polyester polymer concrete
Discussion :
Introduction
The usage of concrete is very wide. It is one of the most important construction
materials. We cannot deny the fact that concrete has become part of our everyday life. It
is comparatively economical, easy to make, offers continuity and solidity and indeed, it
plays the role of developing and improving our modern society.
Concrete is a composite material which is made of filler and a binder. Typical
concrete is a mixture of fine aggregates (sand), coarse aggregates (rock), cement, and
water. Because of its convenience, it is not only used in building construction but also in
other areas such as road construction, harbors, bridges and many more.
Due to its wide range of application and effectiveness, new technology arises in
order to develop and enhance the quality and properties of the concrete. There are lots of
researches done in order to enhance the concretes workability. One of the technological
advances done is by using polymer resin mixed with hardener as a binder for sand in
creating polymer concrete.
Here in Philippines, there are also lots of researchers who are continuously
studying and researching in order to develop the technology of concrete. There are many
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the polymer binder and the aggregate. A hardener is used to start the hardening process
of the polymer concrete mix. Early studies on polyester resin concrete while taking resin
content as a variable reported that compressive strength of polymer concrete is
dependent upon the resin content.
Properties of Polymer Concrete
The properties of polymer concrete are largely dependent on the amount and
properties of polymer in the concrete. Each type of polymer can impart specific properties
to polymer concrete when incorporated with the aggregates. So depending on the
properties of the Polymer Concrete to be achieved, the nature and quantity of the polymer
composition should be chosen. The adhesive properties of polymer concrete allow
patching of both polymer and conventional cement based concretes. These composites
have some advantages compared to ordinary cement concrete such as: rapid hardening,
high mechanical strengths, chemical resistance, etc.
Advantages of Polymer Concrete
Rapid curing
High tensile, flexural, and compressive strengths when fiber reinforcement is used
Good adhesion to most surfaces
Low permeability to water and aggressive solutions
Good resistance against corrosion
May be vibrated to fill voids in forms
Polymer Concrete Composition
Polymer Concrete Composition of a sample with 25% resin and 0.75% filler
Polymer Concrete Mix Components
Total Mass %
Polyester Resin (R10-103)
25a
MEKP (Methyl Ethyl Ketone Peroxide) Hardener
3b
Oven-Dried Sand
74.06a
Micro Mix Filler
0.75c
a Percentage in relation to the mass (resin + hardener + sand + filler)
b Percentage in relation to the mass of resin
c Percentage in relation to the mass (resin + hardener)
mfiller
mresin
.25
msand =
msand =
2.962275 mresin
msand =
2.962275 mresin
4 mresin
x 100= 74.06%
Polymer Concrete Composition of a sample with 25% resin and 1.5% filler
Polymer Concrete Mix Components
Total Mass %
Polyester Resin (R10-103)
25a
MEKP (Methyl Ethyl Ketone Peroxide) Hardener
3b
Oven-Dried Sand
73.86a
Micro Mix Filler
1.5c
a Percentage in relation to the mass (resin + hardener + sand + filler)
b Percentage in relation to the mass of resin
c Percentage in relation to the mass (resin + hardener)
Computation of mass percentage of oven-dried sand:
mfiller
mresin
.25
msand =
msand =
2.95455 m resin
4 mresin
x 100= 73.86%
Polymer Concrete Composition of a sample with 25% resin and 2.25% filler
Polymer Concrete Mix Components
Total Mass %
Polyester Resin (R10-103)
25a
MEKP (Methyl Ethyl Ketone Peroxide) Hardener
3b
Oven-Dried Sand
73.67a
Micro Mix Filler
2.25c
a Percentage in relation to the mass (resin + hardener + sand + filler)
b Percentage in relation to the mass of resin
c Percentage in relation to the mass (resin + hardener)
Computation of mass percentage of oven-dried sand:
mfiller
mresin
.25
msand =
msand =
2.946825 mresin
msand =
2.946825 mresin
4 mresin
x 100= 73.67%
Polymer Concrete Composition of a sample with 30% resin and 0.75% filler
Polymer Concrete Mix Components
Total Mass %
Polyester Resin (R10-103)
30a
MEKP (Methyl Ethyl Ketone Peroxide) Hardener
3b
Oven-Dried Sand
68.87a
Micro Mix Filler
0.75c
a Percentage in relation to the mass (resin + hardener + sand + filler)
b Percentage in relation to the mass of resin
c Percentage in relation to the mass (resin + hardener)
Computation of mass percentage of oven-dried sand:
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mfiller
mresin
.30
msand =
10 mresin
3
msand =
2.29561 mresin
msand =
2.29561 m resin
10 mresin
3
x 100= 68.87%
Polymer Concrete Composition of a sample with 30% resin and 1.5% filler
Polymer Concrete Mix Components
Total Mass %
Polyester Resin (R10-103)
30a
MEKP (Methyl Ethyl Ketone Peroxide) Hardener
3b
Oven-Dried Sand
68.64a
Micro Mix Filler
1.5c
a Percentage in relation to the mass (resin + hardener + sand + filler)
b Percentage in relation to the mass of resin
c Percentage in relation to the mass (resin + hardener)
Computation of mass percentage of oven-dried sand:
mfiller
mresin
.30
msand =
10 mresin
- m resin - 0.03 mresin 0.01545 mresin
3
msand =
msand =
2.28788 m resin
10 mresin
3
x 100= 68.64%
Polymer Concrete Composition of a sample with 30% resin and 2.25% filler
Polymer Concrete Mix Components
Total Mass %
Polyester Resin (R10-103)
30a
MEKP (Methyl Ethyl Ketone Peroxide) Hardener
3b
Oven-Dried Sand
68.40a
Micro Mix Filler
2.25c
a Percentage in relation to the mass (resin + hardener + sand + filler)
b Percentage in relation to the mass of resin
c Percentage in relation to the mass (resin + hardener)
Computation of mass percentage of oven-dried sand:
mfiller
mresin
.30
msand =
10 mresin
- m resin - 0.03 mresin 0.023175 mresin
3
msand =
msand =
2.28016 m resin
10 mresin
3
x 100= 68.40%
Basins
4 diameter x 8 height cylindrical mold molder for the desired polymer concrete
sample.
Mixing rod/Scoop/Trowel used to mix the components for the polymer concrete.
Digital Balance (For weighing sand) mainly used to weight oven-dried sand.
High Precision Digital Balance (For weighing resin, hardener, filler)- mainly
used to measure accurate amount of resin, hardener, and filler to be used for
the polymer concrete mix.
Small plastic cups (Container for resin, hardener, filler) used as temporary
container when weighing the resin, hardener, and filler.
Sieves using sieve #4 to removed particles of sand that will be retained in it. High Precision
Digital Balance
Balance
Using sieve #100 to removed particles of sand that will pass through it.
Cylindrical
TrowelMold
Procedure:
1. Oven-dry at least 8 kg of sand for about 24 hours. For at
least 4 hours interval within the 24 hours of oven dring,
the sand should be removed from the oven and mixed
from top to bottom to ensure moisture will not be trapped
in the sand. After letting the moisture to evaporate,
placed the sand again in the oven. This amount of sand
is enough for 3 polymer concrete samples.
2. After 24 hours of oven-drying, the sand should be
removed from the oven.
Oven-dried sand
3. Sieve the oven dried sand. Use sieve No. 4 to remove big partcles of sand retained in
it. Use sieve No. 100 to remove very fine particles of sand passing through it.
4. Prepare 3 same 4 x 8 cylindrical mold with tightly
secured based. The bottom edges of the cylindrical mold
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4 by 8 cylindrical mold
mresin=
msand
2.962275
mhardener=0.03 x
mfiller=0.0075{(0.03 x
Mass of
Filler
mresin=
msand
2.29561
mhardener=0.03 x
mresin=
msand
2.95455
Polymer Concrete
Sample with 25% resin
and 2.25% filler
mresin=
msand
2.946825
m sand
msand
msand
mhardener=0.03 x
mhardener=0.03 x
2.962275
2.95455
2.946825
Polymer Concrete
Sample with 30% resin
and 0.75% filler
Mass of
Polyeste
r Resin
Mass of
MEKP
Hardene
r
Polymer Concrete
Sample with 25% resin
and 1.5% filler
msand
msand
m
msand
msand
msand
mfiller =0.015{(0.03
)+
}x msand
)+
} x
)+
filler =0.0225{(0.03
2.962275 2.962275 2.95455 2.95455
2.946825 2.946825
Polymer Concrete
Sample with 30% resin
and 1.5% filler
mresin=
msand
2.28788
Polymer Concrete
Sample with 30% resin
and 2.25% filler
mresin=
msand
2.28016
msand
msand
msand
mhardener=0.03 x
mhardener=0.03 x
2.29561
2.28788
2.28016
mfiller=0.0075{(0.03 x
msand
msand
m sand
m sand
msand
msand
mfiller=0.015{(0.03
)+
} x
mfiller=0.0225{(0.03
)+
} x
)+
}
2.29561 2.29561
2.28788 2.28788
2.28016 2.28016
10. Weigh resin, hardener, and filler equal or approximately near the previously computed
values.
Compressive Strength, fc =
P
A
P
D 2
4
Where:
P - ultimate compressive load of concrete (KN)
A - surface area in contact with the plates (mm2)