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A-96.250.531 / 241013
Customer Support
SWAN and its representatives maintain a fully trained staff of technical specialists
around the world. For any technical question, contact your nearest
SWAN representative, or the manufacturer:
SWAN ANALYTISCHE INSTRUMENTE AG
Studbachstrasse 13
8340 Hinwil
Switzerland
Internet: www.swan.ch
E-mail: support@swan.ch
Document Status
Title:
ID:
A-96.250.531
Revision
Issue
00
Jan. 2008
First Edition
01
Nov. 2008
02
July 2011
03
Oct. 2013
Table of Contents
1.
1.1.
1.2.
Safety Instructions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Warning Notices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
General Safety Regulations . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
4
5
7
2.
2.1.
2.2.
2.3.
2.4.
2.4.1
2.4.2
2.4.3
2.4.4
Product Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Description of the System. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Technical Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Instrument Overview. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Single Components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Sensor OXYTRACE G . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QV-Flow PMMA OTG . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QV-Flow PMMA OTG-QED . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
B-Flow SS316L OTG . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
8
8
12
14
16
16
17
18
19
3.
3.1.
3.2.
3.3.
3.3.1
3.3.2
3.4
3.5.
3.5.1
3.5.2
3.5.3
3.6.
3.7.
3.7.1
3.7.2
3.8.
3.8.1
3.8.2
3.9.
3.9.1
3.9.2
3.9.3
Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Installation Check List. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Mounting of Instrument Panel. . . . . . . . . . . . . . . . . . . . . . . . . . . .
Connecting Sample Inlet and Outlet . . . . . . . . . . . . . . . . . . . . . . .
Swagelok Fitting Stainless Steel at Sample Inlet . . . . . . . . . . . . .
FEP Tube at Sample Outlet . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Install the Swansensor Oxytrace G . . . . . . . . . . . . . . . . . . . . . . .
Electrical Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Electrical Connection Diagram AMI Oxytrace . . . . . . . . . . . . . . .
Electrical Connection Diagram AMI Oxytrace QED . . . . . . . . . . .
Power Supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Relay Contacts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Alarm Relay . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Relay 1 and 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Signal Outputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Signal output 1 and 2 (current outputs) . . . . . . . . . . . . . . . . . . . .
Signal output 3 (optional) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Interface RS232 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Interface RS485 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
USB Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
20
20
21
22
22
23
23
24
25
26
27
28
28
28
28
31
31
31
32
32
32
33
4.
4.1.
4.2.
Instrument Setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Establish Sample Flow . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Programming . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
34
34
34
A-96.250.531 / 241013
5.
5.1.
5.2.
5.3.
5.4.
Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Keys . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Software Structure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Changing Parameters and values. . . . . . . . . . . . . . . . . . . . . . . . .
35
35
36
37
38
6.
6.1
6.2
6.3
6.3.1
6.3.2
6.4
6.5
6.6
6.7
6.8
6.8.1
6.8.2
6.8.3
6.8.4
6.8.5
6.9
6.10
Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Maintenance Table . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Stop of Operation for Maintenance . . . . . . . . . . . . . . . . . . . . . . . .
Maintenance of the Oxygen Sensor . . . . . . . . . . . . . . . . . . . . . . .
Electrolyte exchange. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Clean Swansensor Oxytrace G and Flow Cell . . . . . . . . . . . . . . .
Maintenance of the Faraday electrode . . . . . . . . . . . . . . . . . . . . .
Calibration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Zero-Verification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Faraday Verification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Quality Assurance of the Instrument. . . . . . . . . . . . . . . . . . . . . . .
Activate SWAN Quality assurance procedure . . . . . . . . . . . . . . .
Pre-test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Connect the sample lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Carry out comparison measurement. . . . . . . . . . . . . . . . . . . . . . .
Completion of the measurement. . . . . . . . . . . . . . . . . . . . . . . . . .
Replacing Fuses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Longer Stop of Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
39
39
39
40
40
42
42
44
46
47
48
49
50
50
52
53
54
55
7.
Error List . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
56
8.
8.1.
8.2.
8.3.
8.4.
8.5.
Program Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Messages (Main Menu 1) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Diagnostics (Main Menu 2) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Maintenance (Main Menu 3) . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Operation (Main Menu 4) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Installation (Main Menu 5). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
60
60
61
62
63
64
9.
66
66
66
68
70
71
10.
Material Safety Data sheets . . . . . . . . . . . . . . . . . . . . . . . . . . . .
10.1. Reagents. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
86
86
A-96.250.531 / 241013
11.
Default Values. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
87
12.
Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
90
13.
Notes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
91
A-96.250.531 / 241013
1.
Safety Instructions
General
Target
audience
OM Location
Qualification,
Training
A-96.250.531 / 241013
1.1.
Warning Notices
The symbols used for safety-related notices have the following significance:
DANGER
Your life or physical wellbeing are in serious danger if such
warnings are ignored.
Follow the prevention instructions carefully.
WARNING
Severe injuries or damage to the equipment can occur if such
warnings are ignored.
Follow the prevention instructions carefully.
CAUTION
Damage to the equipment, minor injury, malfunctions or incorrect process can be the consequence if such warnings are ignored.
Follow the prevention instructions carefully.
Mandatory
Signs
Safety gloves
A-96.250.531 / 241013
Warning Signs
Corrosive
Harmful to health
Flammable
Warning general
Attention general
A-96.250.531 / 241013
1.2.
Legal
Requirements
Spare Parts
and
Disposables
Use only official SWAN spare parts and disposables. If other parts
are used during the normal warranty period, the manufacturers
warranty is voided.
Modifications
WARNING
Only SWAN trained and authorized personnel shall perform the
tasks described in this document.
A-96.250.531 / 241013
2.
Product Description
This manual describes the functions of the monitors AMI Oxytrace
and AMI Oxytrace QED. Both monitors are mainly identical except
that AMI Oxytrace QED includes a faraday verification. AMI Oxytrace cannot be upgraded with the faraday verification.
2.1.
Application
AMI Oxytrace is used to measure low levels of oxygen in high-purity water. Especially in power plant water cycles (e.g. feedwater), a
very low level of oxygen is needed to prevent corrosion.
Measuring
principle
Clark principle:
The sensor consists of one noble metal electrode (e.g. platinum or
gold), a reference electrode (mostly Ag/AgCl) and optionally a metal guard electrode.
The Clark-type electrode is the most used frequently oxygen sensor for measuring oxygen dissolved in a liquid. The basic principle
is that there is a cathode and an anode submersed in an electrolyte
and a voltage is applied between the two parts. Oxygen enters the
sensor through a permeable membrane by diffusion, and is reduced at the cathode, creating a measurable electrical current.
O2 + 2 e- + 2 H2O --> H2O2 + 2 OHThere is a linear correlation between the oxygen concentration and
the electrical current.
The guard electrode is on the same voltage level as the cathode
but there is no current measurement. Oxygen which diffuses from
the electrolyte to the cathode is consumed by the guard electrode.
As a consequence, residual oxygen in the electrolyte will no more
disturb the measurement signal and the response time to low oxygen levels will be shorter.
Temperature
compensation
A-96.250.531 / 241013
Faraday
Verification
40
35
operational sensor
30
25
20
15
defective sensor
10
5
0
30
60
90
120
150
180
210
240
270
300
330
Time [Sec]
Unusual sensor performance is recognized immediately and gives
also a maintenance indication to the operator/user. The faraday
verification is therefore an excellent QA/QC tool.
A-96.250.531 / 241013
Signal
Outputs
Two signal outputs programmable for measured values (freely scaleable, linear or bilinear) or as continuous control output (control
parameters programmable).
Current loop:
0/420 mA
Maximal burden:
510
Third signal output with the same specifications as option.
(Only possible if no communication interface is used.)
Relay
Alarm Relay
Input
For potential-free contact to freeze the measuring value or to interrupt control in automated installations (hold function or remote-off)
Safety
Features
Communication Interface
(optional)
10
A-96.250.531 / 241013
Fluidics
B
C
D
E
G
A
B
C
D
A-96.250.531 / 241013
Oxygen sensor
Flow sensor
Flow cell
Flow regulating valve
E Sample outlet
F Drain funnel
G Sample inlet
11
2.2.
Power Supply
Technical Data
Voltage:
Power consumption:
Electronics
housing
Sample
requirements
8 to 25 l/h
1545 C
QV-flow: 0.2 to 1 bar
B-flow: max. 3 bar
QV-flow: pressure free
B-flow: max. 3 bar
not lower than pH 4
less than 10 ppm
Flow cell made of acrylic glass with built-in flow adjustment valve
and digital sample flow meter
Sample inlet:
1/4 Swagelok tube adapter
Sample outlet:
for flexible tube 20x15 mm
On-Site
requirements
Sample inlet:
Accuracy
Reproducibility
Measuring
Range
Temperature
Sample Flow
Measurement
12
A-96.250.531 / 241013
Dimensions
Panel:
Mounting hole distance
Screws:
Weight:
Stainless steel
280x850x150 mm
254x824
5 mm or 6 mm diameter
12.0 kg
280 mm/ 11
A-96.250.531 / 241013
850 mm / 33
13 mm /
824 mm / 32 7/16
AMI Oxytryce
4 x dia. 6.5 mm /
254 mm/ 10
13
2.3.
Instrument Overview
AMI Oxytrace
A
B
C
D
E
F
G
H
A
B
C
D
E
14
Panel
AMI Transmitter
Oxygen sensor
Flow sensor
Flow cell
F
G
H
I
A-96.250.531 / 241013
A
B
C
D
E
F
G
H
I
J
A
B
C
D
E
F
A-96.250.531 / 241013
Panel
AMI Transmitter
Faraday control unit
Oxygen sensor
Sample outlet
Flow sensor
G
H
I
J
K
Flow cell
Flow regulating valve
Faraday electrode
Drain funnel
Sample inlet
15
2.4.
Single Components
2.4.1
Sensor OXYTRACE G
Sensor for the measurement of dissolved oxygen in ultra pure water. Precise oxygen measuring cell with integrated temperature
sensor and guard electrode for faster initial response time after
maintenance.
31.9
38.3
59
100
Technical data:
Measuring
range:
Temp. sensor:
Accuracy:
Precision:
Response time:
Minimal flow:
Operating temp.:
Material:
Protection:
Weight:
16
A-96.250.531 / 241013
2.4.2
Flow cell
Sample temp.
max. 45 C
Inlet pressure
max. 1 bar
Outlet pressure
Sample flow
Process connection inlet
Outlet
Dimensions
Pressure free
625 l/h
Swagelok connection for 1/4 tube
SERTO angle for 6mm flexible tube
see picture below
80
A-96.250.531 / 241013
9.2
138
164
178.5
217.7
40
17
2.4.3
Flow cell
Sample temp.
Inlet pressure
Outlet pressure
Sample flow
Process connection inlet
Outlet
Dimensions
80
138
164
178.5
217.7
40
75
18
A-96.250.531 / 241013
2.4.4
Flow cell
Operating temp.
Sensor
Operating
pressure
Sensor
Outlet pressure
Sample flow
Flow cell
connection
Dimensions
A-96.250.531 / 241013
138
100
154
71
52
40
19
3.
Installation
The first part of this chapter describes the preparing and placing of
the system in position for use. The second part describes the wiring
and the properties of the signal outputs and relay.
Restrictions
on use
3.1.
Check
On site
requirements
Installation
Electrical
Connections
Connect all external devices like limit switches, current loops and
pumps, see Electrical Connections, p. 24.
Connect the power cord, do not switch on power until all external
devices are connected.
20
A-96.250.531 / 241013
Turn-on
power
Switch on power.
First, the analyzer performs a self test, displays the firmware version and then starts normal operation
Run-in Period
Calibration
Leave the sensor at the air. The sensor has to run-in for at least
30 min, better 1 h. During this time it has to be at air with a dry and
clean membrane and has to be connected to the powered instrumenty. Calibrate the sensor after this time, see Calibration, p. 44.
and mount it into the flow cell afterwards.
Open
Sample Flow
Open the flow regulating valve to allow sample flow into the flow
cell and into the waste. Sample must always overflow into waste
Programming
3.2.
Mounting requirements
A-96.250.531 / 241013
21
3.3.
3.3.1
Preparation
Cut the tube to length and deburr it. The tube must be straight and
free from blemishes for approximately 1,5 x tube diameter from the
end.
Lubrication with lubricating oil, MoS2, Teflon etc. is recommended
for the assembly and reassembly of bigger sized unions (thread,
compression cone).
Installation
Screw on the union nut onto the body, do not tighten it.
Push the stainless steel pipe through the union nut as far as it
reaches the stop of the body.
While holding the fitting body steady, tighten the nut union 1
rotation using an open ended spanner.
C D
12
3
6
A Stainless steel tube
B Union nut
C Compression ferrule
22
D Compression cone
E Body
F Tightened connection
A-96.250.531 / 241013
3.3.2
A Waste funnel
B Hose nozzle
C 1/2 tube
Connect the 1/2 tube [C] to the hose nozzle [B] and place it into a
drain with atmospheric pressure.
3.4
A
B
C
D
E
Fixing sleeve
Transport protection cap
Swansensor Oxytrace G
Sodium sulfit
Sensor cap filled with electrolyte
D
E
Connect the sensor cable to the transmitter, see Electrical Connection Diagram AMI Oxytrace, p. 25.
A-96.250.531 / 241013
23
3.5.
Electrical Connections
WARNING
Always turn off DC power before manipulating electric parts.
Make sure the power specification of the instrument corresponds to the power on site.
Cable
thicknesses
For Relays: Use max. 1.5 mm2 / AWG 14 stranded wire with
end sleeves.
For Signal Outputs and Input: Use 0.25 mm2 / AWG 23
stranded wire with end sleeves.
WARNING
External Voltage.
External supplied devices connected to relay 1 or 2 or to the
alarm relay can cause electrical shocks.
Make sure that the devices connected to the following contacts are disconnected from the power before continuing the
installation.
relay 1
relay 2
alarm relay
24
A-96.250.531 / 241013
3.5.1
CAUTION
Use only the terminals shown in this diagram, and only for the
mentioned purpose. Use of any other terminals will cause short
circuits with possible corresponding consequences to material
and personnel.
A-96.250.531 / 241013
25
3.5.2
CAUTION
Use only the terminals shown in this diagram, and only for the
mentioned purpose. Use of any other terminals will cause short
circuits with possible corresponding consequences to material
and personnel.
26
A-96.250.531 / 241013
3.5.3
Power Supply
WARNING
Risk of electrical shock
Do not perform any work on electrical components if the transmitter is switched on. Failure to follow safety instructions could
result in serious injury or death.
Always turn off AC power before manipulating electric parts.
Installation and maintenance of electrical parts must be performed by professionals.
A
B
C
D
A
B
C
D
Installation
requirements
A-96.250.531 / 241013
27
3.6.
Input
Note: Use only potential-free (dry) contacts.
Terminals 30 and 31
If the signal output is set to hold, the measurement is interrupted if
input is active.
For programming see Menu Installation 5.3.4, p. 94.
3.7.
Relay Contacts
3.7.1
Alarm Relay
Note: Max. load 1 A/250 VAC
Alarm output for system errors.
Error codes see Troubleshooting, p. 46.
NC a)
Terminals
Description
10/11
12/11
Normally
Closed
NO
Normally
Open
a) usual use
3.7.2
Relay 1 and 2
Note: Max. load 1 A/250 VAC
Relay 1 and 2 can be configured as normally open or as normally
closed. Standard for both relays is normally open. To configure a
Relay as normally closed, set the jumper in the upper position.
28
A-96.250.531 / 241013
Relay
config.
Terminals
Jumper
pos.
Description
Normally
Open
6/7: Relay 1
8/9: Relay 2
Open if de-energized.
Closed if energized i.e. triggered by
a programmed limit.
Normally
Closed
6/7: Relay 1
8/9: Relay 2
Closed if de-energized.
Open if energized i.e. triggered by a
programmed limit.
A
B
A-96.250.531 / 241013
29
CAUTION
Risk of damage of the relays in the AMI Transmitter due to
heavy inductive load.
Heavy inductive or directly controlled loads (solenoid valves,
dosing pumps) may destroy the relay contacts.
To switch inductive loads > 0.1 A use an AMI relay box available as an option or suitable external power relays.
Inductive load
Small inductive loads (max 0.1A) as for example the coil of a power
relay can be switched directly. To avoid noise voltage in the
AMI Transmitter it is mandatory to connect a snubber circuit in parallel to the load.
A snubber circuit is not necessary if an AMI relaybox is used.
Resistive load
A
B
C
D
E
A
C
Resistive loads (max. 1A) and control signals for PLC, impulse
pumps and so on can be connected without further measures
B
C
Actuators
AC or DC power supply
AMI Transmitter
External power relay
Snubber
Power relay coil
A AMI Transmitter
B PLC or controlled pulse pump
C Logic
Actuators, like motor valves, are using both relays: One relay contact is used for opening, the other for closing the valve, i.e. with the
2 relay contacts available, only one motor valve can be controlled.
Motors with loads bigger than 0.1A must be controlled via external
power relays or an AMI relay box.
A AC or DC power supply
B AMI Transmitter
C Actuator
A
C
30
A-96.250.531 / 241013
3.8.
Signal Outputs
3.8.1
3.8.2
A-96.250.531 / 241013
31
3.9.
Interface
Note: It is not possible to install more than one of the following
interfaces at the same time.
3.9.1
Interface RS232
Terminal 50, 52, 53
The AMI Interface RS232 PCB is used for Logger down load and
Firmware up load. For detailed information see the corresponding
manual AMI RS232 Interface.
3.9.2
Interface RS485
Terminal 37 PB, Terminal 38 PA
To connect several instruments by means of a network or to configure a PROFIBUS DP connection, consult the PROFIBUS manual.
Use appropriate network cable.
Note: The switch must be ON, if only one instrument is
installed, or on the last instrument in the bus.
81.420.020
Profibus
PB-DPV1 V5.5
ON
OFF
32
A-96.250.531 / 241013
3.9.3
USB Interface
The USB Interface is used to store Logger data and for Firmware
up load. For detailed information see the corresponding installation
instruction.
USB Interface
A-96.250.531 / 241013
33
4.
Instrument Setup
4.1.
4.2.
Open the flow regulating valve and wait until the flow cell is
completely filled.
Switch on power.
Programming
Program all parameters for external devices (interface, recorders,
etc.)
Program all parameters for instrument operation (limits, alarms),
see Program List and Explanations, S. 66
34
A-96.250.531 / 241013
5.
Operation
5.1.
Keys
A
Enter
Exit
Program
Access, Exit
RUN
R1
14:10:45
1.05 ppb
Enter
R2
9 l/h
A-96.250.531 / 241013
25.4C
Exit
Main Menu
Messages
Diagnostics
Maintenance
Operation
Installation
35
5.2.
Display
A B
C D
RUN
15:20:18
R1
0.15 ppm
R2
23 C
12 l/h
E
F
G
A
RUN
normal operation
HOLD
OFF
ERROR
Error
Time
Process values
Sample Temperature
Fatal Error
Relay status
36
A-96.250.531 / 241013
5.3.
Software Structure
Main Menu
Messages
Diagnostics
Maintenance
Operation
Installation
Messages
Pending Errors
Maintenance List
Message List
1.1
Diagnostics
Identification
Sensors
Sample
I/O State
Interface
2.1
3.1
Maintenance
Calibration
Service
Simulation
Set Time 23.09.06 16:30:00
Operation
Sensors
Relay Contacts
Logger
4.1
Installation
Sensors
Signal Outputs
Relay Contacts
Miscellaneous
Interface
5.1
A-96.250.531 / 241013
Menu Messages 1
Reveals pending errors as well as an event history
(time and state of events that have occurred at an
earlier point of time).
It contains user relevant data.
Menu Diagnostics 2
Provides user relevant instrument and sample data.
Menu Maintenance 3
For instrument calibration, relay and signal output
simulation, and to set the instrument time.
It is used by the service personnel.
Menu Operation 4
User relevant parameters that might need to be
modified during daily routine. Normally password
protected and used by the process-operator.
Subset of menu 5 - Installation, but process-related.
Menu Installation 5
For initial instrument set up by SWAN authorized
person, to set all instrument parameters. Can be
protected by means of password.
37
5.4.
Changing
parameters
5.1.2
4.4.1
FOME
30
min
Free chlorine
no
Temperature
Standards
Logger
Log interval
Save ?
Clear logger
Yes
No
Changing
values
Alarm oxygen
Alarm High
Alarm Low
Hysteresis
Delay
Alarm oxygen
Alarm High
Alarm Low
Hysteresis
Delay
38
Press [Enter]
Press [
] or [
] key to
highlight the required parameter.
NT5K
Logger
Log interval Interval.
5 min
Clear logger
10 min
30 min
1 Hour
Logger
Log interval
Clear logger
4.1.3
30min
no
4.1.3
10 min
no
4.1.3
Yes is highlighted.
6
Press [Enter].
Press [Exit].
Yes is highlighted.
no
5.3.1.1.1
10.00 ppm
1.00 ppb
0.10 ppb
5 Sec
5.3.1.1.1
8.00 ppb
1.00 ppb
0.10 pp
5 Sec
Press [Exit].
] or
A-96.250.531 / 241013
6.
Maintenance
Maintenance frequency depends strongly on the water quality. The
AMI Oxytrace QEDn is designed for determination of low level of
dissolved oxygen in high purity water.
It is not suitable for the measurement of dissolved oxygen in waste
water.
6.1
Maintenance Table
Weekly
Monthly
Half a year
Yearly
Every 2nd
year
6.2
A-96.250.531 / 241013
39
6.3
WARNING
Etching liquid
The electrolyte is alkaline and caustic. It contains less than 1%
of potassium hydroxide.
Do not ingest. Wear protective goggles and gloves during
handling. Avoid contact with clothes.
In case of accidental contact with the eyes, wash immediately
with clear water and contact a physician. Show him the label
of the bottle or this section of the manual.
Short contact with skin is harmless, nevertheless wash with
lots of water.
6.3.1
Electrolyte exchange
An electrolyte exchange is indicated in the maintenance list as
soon as the remaining amount is below 10%.
40
A Fixing sleeve
B Sensor
C Flow cell
1
A-96.250.531 / 241013
A
B
C
D
A
B
C
D
E
F
G
H
Swansensor Oxytrace G
Thread
Groove
Guard electrode
Anode
Measuring head
Cathode
Sensor cap with membrane
E
F
G
H
Unscrew and remove the sensor cap [H] from the Swansensor
Oxytrace G [A].
Slowly screw the sensor cap onto the sensor to allow the excess electrolyte to escape without building up too much pressure inside the electrode. Fasten sensor cap tightly.
Switch on power.
A-96.250.531 / 241013
41
6.3.2
6.4
Clean the sensor with a soft tissue and rinse it with water afterwards.
Use a soft brush to remove the dirt which sticks on the walls of
the flow cell.
Switch off the instrument and close the flow regulating valve.
Disconnect and remove the cable from the faraday control unit.
Remove the faraday electrode from the flow cell, do not pull on
the cable.
Remove the washer (C) and the o-ring [D] from the electrode
body (B).
Clean the inner electrode (E) with a tissue and the hollow electrode with a pipe cleaner.
The electrode surfaces should be shining metallic after
cleaning. Use probably a polishing detergent or a small
amount of toothpaste.
42
A-96.250.531 / 241013
14 Feed the electrode cable through the cable gland of the faraday
control unit.
15 Connect the electrode cable to terminal 5 (green) and terminal 6
(white).
16 Switch the instrument on.
17 Open the flow regulating valve and adjust the sample flow between 8 and 25 l/h.
A
B
C
D
E
F
G
Fixing sleeve
Electrode body
Washer
O-ring
Inner electrode
O-ring
Hollow electrode
B
C
D
F
G
A-96.250.531 / 241013
43
6.5
Calibration
The sensing part of the sensor must not be in direct contact with
water!
In the wet flow cell, the atmosphere will be saturated with water vapor. This atmosphere will produce the most accurate calibration results.
The required time for a calibration depends mainly on the difference between temperature and oxygen content in the sample and
in the air. It can take 15 20 minutes. This is also the case, if the
electrolyte was exchanged.
As soon as the reading is stable, the microprocessor will store the
calibration data in the memory.The end of the calibration is indicated on the display.
To perform a calibration proceed as follows:
1
2
<Enter> to continue
3.1.5
Calibration
Take sensor out of
flow cell and dry
membrane and sensor
5
6
Unscrew and remove the threaded sleeve [A], see Electrolyte exchange, p. 40.
Remove the oxygen sensor [B]
from the flow cell [C].
Dry the sensor membrane and the
flow cell with a soft paper tissue.
<Enter> to continue
44
A-96.250.531 / 241013
3.1.5
Calibration
Place the electrode into
the wet flow cell at
a slightly tilted angle.
<Enter> to continue
A Tilted sensor
B Flow cell
Calibration
Saturation
Sat. Current
3.1.1
98.7 %
3.35 A
Progress
Calibration
Saturation
Sat. Current
3.1.1
98.7 %
3.35 A
Calibration Successful
A-96.250.531 / 241013
45
6.6
Zero-Verification
SWANSENSOR OXYTRACE G for the measurement of low oxygen content (< 1 ppb).
1
Put the electrode into the sodium sulfite solution afterwards. Assure that there are no air bubbles in front of the sensor.
Depending on the state of the electrode this process can take several hours. In case of an electrode-refill, this can take days until the
measured value is lower than 1 ppb.
46
A-96.250.531 / 241013
6.7
Faraday Verification
The Faraday verification works only for oxygen concentrations below 200 ppb. If automatic Faraday verification is enabled, a periodic
check of the system is performed. A manual verification can be
started for test purposes.
Automatic
Verification
Per default the instrument performs an automatic faraday verification every 3 hours. To change the settings for automatic verification
go to menu Faraday Parameter- Timer mode, see menu 4.1.3, p.
70 for details.
Possible settings are:
off
interval
daily
weekly
Manual
Verification
<Enter> to stop
3.3
Faraday Verification
Efficiency
91.5 %
Faraday Conc.
12.85 ppb
Progress
Done
A-96.250.531 / 241013
47
6.8
Quality
assurance
level
48
A-96.250.531 / 241013
max. deviation
temperature [C] a)
max. deviation
result [%]
Off
Off
1: Trend
0.5 C
10 %
annual
2: Standard
0.4 C
5%
quarterly
3: Crucial
0.3 C
5%
monthly
4: User
0 - 2C
0 - 20%
Quality Level
0: Off
min. inspection
interval
Off
annual, quarterly,
monthly
Procedure
Pre-test
Connect instruments
6.8.1
A-96.250.531 / 241013
49
6.8.2
Pre-test
Reference instrument: AMI Oxytrace QED:
Check certificate; reference instrument certificate not older
then one year.
Check battery; Battery of the AAMI Oxytrace QED should
be completely charged. Remaining operating time on
display minimum 20 hours.
Make sure, that both instruments are set to the same
temperature compensation.
Sensor is in working condition
On-line instrument: Monitor AMI oxygen:
Good order and condition; Flow cell free of particles,
Sensor surface free of deposits.
Check message list; Review the message list in menu 1.3
and check for frequently alarms (as for example flow
alarms). If alarms occur frequently remove cause before
starting the procedure.
6.8.3
Example
50
A-96.250.531 / 241013
B
C
D
E
G
A
B
C
D
Stop sample flow to the monitor AMI Oxygen by closing the appropriate valve, e.g. back pressure regulator, sample preparation or flow regulating valve at flow cell.
Connect sample line of the monitor AMI Oxygen [A] with the
sample inlet of the reference instrument AMI Oxytrace QED [B].
Use the supplied tube, made of FEP.
Connect sample outlet of the reference instrument AMI Oxytrace QED to the sample outlet funnel of the monitor.
A-96.250.531 / 241013
E Sample outlet
F Sample inlet
G T-fitting
51
6.8.4
Press [Enter].
<Enter> to continue
3.5.5
Quality Assurance
Value H2
0.05 ppb
Value Temp.
25.00 C
Wait 10 Minutes
Read the ppb value of the reference instrument and enter under
Inspector. by using the [
] or
[
] keys.
Read temperature value of the reference instrument and enter under Inspector Temp. by using the
[
] or [
] keys.
<Enter> to continue
Quality Assurance
Value H2
Value Temp.
Inspector H2
Inspector Temp.
3.5.3
0.05 ppb
25.00 C
0.06 ppb
25.0 C
<Enter> to continue
Quality Assurance
Value H2
Value Temp.
Inspector
Inspector Temp.
3.5.4
0.05 ppb
25.00 C
0.06 ppm
25.0 C
<Enter> to continue
Quality Assurance
Max. Dev. H2
Max. Dev. Temp.
Dev. H2
Dev. Temp.
3.5.5
0.5 %
0.4 C
0.1 %
0.4 C
QA-Check succesful
52
A-96.250.531 / 241013
6.8.5
Stop the sample flow to the AMI Oxytrace QED by closing the
appropriate valve, e.g. back pressure regulator, sample preparation or flow regulating valve at flow cell again.
Disconnect the AMI Inspector by removing the tubes and connect the sample outlet of the Monitor AMI Oxytrace QED to the
sample outlet funnel again.
A-96.250.531 / 241013
53
6.9
Replacing Fuses
WARNING
External Voltage.
External supplied devices connected to relay 1 or 2 or to the
alarm relay can cause electrical shocks.
Make sure that the devices connected to the following contacts are disconnected from the power before continuing the
installation.
relay 1
relay 2
alarm relay
When a fuse has blown, find out the cause and fix it before
replacing it with a new one.
Use tweezers or needle-nosed pliers to remove the defective fuse.
Use original fuses provided by SWAN only.
A
B
C
D
E
F
54
D E F
A-96.250.531 / 241013
Clean the sensor with a soft tissue and rinse it with water afterwards.
Use a soft brush to remove the dirt which sticks on the walls of
the flow cell.
A-96.250.531 / 241013
55
7.
Error List
Error
Non-fatal Error. Indicates an alarm if a programmed value is exceeded.
Such Errors are marked E0xx (bold and black).
Fatal Error
(blinking symbol)
Control of dosing devices is interrupted.
The indicated measured values are possibly incorrect.
Fatal Errors are divided in the following two categories:
Errors which disappear if correct measuring conditions are recovered (i.e. Sample Flow low).
Such Errors are marked E0xx (bold and orange)
Errors which indicate a hardware failure of the instrument.
Such Errors are marked E0xx (bold and red)
HOLD
R1
14:10:45
7.04 ppm
R2
8 l/h
25.4C
Main Menu
Messages
Diagnostics
Maintenance
Operation
Installation
Messages
Pending Errors
Maintenance List
Message List
Pending Errors
Error Code
1.1
1.1.5
E002
Alarm low
<Enter> to Acknowledge
56
Error or
fatal Error
Error not yet acknowledged.
Check Pending Errors 1.1.5 * and
take corrective action.
Press [ENTER].
Navigate to menu Messages.
Press [ENTER].
A-96.250.531 / 241013
Error
Description
Corrective action
E001
check process
check programmed value,
see 5.3.1.1.1, S. 76
E002
check process
check programmed value,
see 5.3.1.1.25, S. 76
E003
check process
check programmed value,
see 5.3.1.4, S. 77
E004
check process
check programmed value,
see 5.3.1.4, S. 77
E007
check process
check programmed value,
see 5.3.1.3.1, S. 77
E008
check process
check programmed value,
see 5.3.1.3.25, S. 77
E009
E010
E011
Temp. shorted
E012
Temp. disconnected
A-96.250.531 / 241013
57
Error
58
Description
Corrective action
E013
E014
E017
Control Timeout
E018
Faraday Efficiency
E019
Quality Assurance
E024
Input active
E025
IC MK41T56
call service
E026
IC LM75
call service
E027
IC PCF8574
call service
E028
EEProm Microcon
call service
E029
EEProm Motherboard
call service
E030
EEProm Frontend
call service
E031
Calibration Recout
call service
A-96.250.531 / 241013
Error
Description
Corrective action
E032
Wrong Frontend
call service
E033
Power-on
E034
Power-down
E065
Electrolyte depleted
A-96.250.531 / 241013
59
8.
Program Overview
For explanations about each parameter of the menus see Program
List and Explanations, S. 66.
Menu 1 Messages is always accessible for everybody. No
password protection. No settings can be modified.
Menu 2 Diagnostics is always accessible for everybody. No
password protection. No settings can be modified.
Menu 3 Maintenance is for service: Calibration, simulation of
outputs and set time/date. Please protect with password.
Menu 4 Operation is for the user, allowing to set limits, alarm
values, etc. The presetting is done in the menu Installation
(only for the System engineer). Please protect with password.
Menu 5 Installation: Defining assignment of all inputs and
outputs, measuring parameters, interface, passwords, etc.
Menu for the system engineer. Password strongly recommended.
8.1.
Pending Errors
1.1.5*
Maintenance List
1.2.5*
Message List
Number
1.3.1*
1.3*
Date, Time
* Menu numbers
1.1*
Maintenance List
1.2*
60
A-96.250.531 / 241013
8.2.
Identification
Desig.
AMI Oxytrace
2.1*
Version
5.40-03/13
Factory Test
Instrument
2.1.3*
Motherboard
* Menu numbers
2.1.3.1*
Front End
Operating Time
2.1.4.1*
2.1.4*
Sensors
Oxytrace G
Current Value
2.2*
2.2.1*
Number
2.2.1.5*
Date, Time
2.2.1.5.1*
Sat. Current
Air pressure
Miscellaneous
Case Temp.
2.2.2*
Air pressure
QA History
QA History
2.2.2.1*
2.2.3.1*
2.2.3*
Sample
Sample ID
2.3*
Temperature C
2.3.1*
Nt5K Ohm
I/O State
Alarm Relay
2.4.1*
2.4*
Relay 1/2
2.4.2*
Input
Signal Output 1/2
Interface
Protocol
2.5*
USB Stick
A-96.250.531 / 241013
2.5.1*
61
8.3.
Calibration
3.1.5
Service
Electrolyte
Last filling
3.2*
3.2.1*
Remaining amount
* Menu numbers
3.1*
Remaining time
New Filling
Faraday Verification
Current Value
3.2.2
Faraday Conc.
3.2.1.5*
Progress
Simulation
Alarm Relay
3.2.1*
3.3*
Relay 1
3.2.2*
Relay 2
3.2.3*
Signal Output 1
3.2.4*
Signal Output 2
3.2.5*
Set Time
(Date), (Time)
3.4*
Quality Assurance
Quality Assurance
3.5.5*
3.5*
62
A-96.250.531 / 241013
8.4.
Sensors
4.1.1*
4.1*
4.1.2*
Faraday Parameter
Mode
4.1.3.1*
4.1.3*
Interval
4.1.3.20*
Delay
4.1.3.3*
Signal Outputs
4.1.3.4*
Output/Control
4.1.3.5*
Relay Contacts
Alarm Relay
Alarm oxygene
Alarm High
4.2.1.1.1*
4.2*
4.2.1*
4.2.1.1*
Alarm Low
4.2.1.1.25*
Hysteresis
4.2.1.1.35*
Delay
4.2.1.1.45*
Alarm Saturation
Alarm High
4.2.1.2.1*
4.2.1.2*
Alarm Low
4.2.1.2.25*
Hysteresis
4.2.1.2.35*
Delay
4.2.1.2.45*
Logger
4.3*
A-96.250.531 / 241013
Relay 1/2
Setpoint
4.2.x.100*
4.2.2* - 4.2.3*
Hysteresis
4.2.x.200*
Delay
4.2.x.30*
Input
Active
4.2.4.1*
4.2.4*
Signal Outputs
4.2.4.2*
Output / Control
4.2.4.3*
Fault
4.2.4.4*
Delay
4.2.4.5*
Log Interval
4.3.1*
Clear Logger
4.3.2*
4.3.3*
* Menu numbers
63
8.5.
Sensors
Miscellaneous
Flow
5.1.1.1*
5.1*
5.1.1*
Offset
5.1.1.2*
Quality Assurance
Level
5.1.2.1*
* Menu numbers
5.1.2*
Signal Outputs
Parameter
5.2.1.1 - 5.2.2.1*
5.2*
5.2.1* - 5.2.2*
Current Loop
5.2.1.2 - 5.2.2.2*
Function
5.2.1.3 - 5.2.2.3*
Scaling
Range Low
5.2.x.40.10/11*
5.2.x.40
Range High
5.2.x.40.20/21*
Relay Contacts
Alarm Relay
Alarm oxygen
Alarm High
5.3.1.1.1*
5.3*
5.3.1*
5.3.1.1*
Alarm Low
5.3.1.1.25
Hysteresis
5.3.1.1.35
Delay
5.3.1.1.45
Sample Flow
Flow Alarm
5.3.1.2.1
5.3.1.2*
Alarm High
5.3.1.2.2*
Sample Temp.
Relay 1 and 2
5.3.2* and 5.3.3*
64
Alarm Low
5.3.1.2.35*
Alarm High
5.3.1.3.1*
5.3.1.3*
Alarm Low
5.3.1.3.25*
Alarm Saturation
Alarm High
5.3.1.4.1*
5.3.1.4*
Alarm Low
5.3.1.4.25
Hysteresis
5.3.1.4.35
Delay
5.3.1.4.45
Case Temp.
5.3.1.5.1*
5.3.1.5*
5.3.1.5.2*
Function
5.3.2.15.3.3.1*
Parameter
5.3.2.205.3.3.20*
Setpoint
5.3.2.3005.3.3.301*
Hysteresis
5.3.2.4005.3.3.401*
Delay
5.3.2.505.3.3.50*
Input
Active
5.3.4.1*
5.3.4*
Signal Outputs
5.3.4.2*
Output/Control
5.3.4.3*
Fault
5.3.4.4*
Delay
5.3.4.5*
A-96.250.531 / 241013
Miscellaneous
Language
5.4.1*
5.4*
Set defaults
5.4.2*
Load Firmware
5.4.3*
Password
Messages
5.4.4.1*
5.4.4*
Maintenance
5.4.4.2*
Operation
5.4.4.3*
Installation
5.4.4.4*
Sample ID
5.4.5*
Interface
Protocol
Hyperterminal
5.5*
5.5.1*
A-96.250.531 / 241013
* Menu numbers
65
9.
1 Messages
1.1 Pending Errors
1.1.5
Provides the list of active errors with their status (active, acknowledged). If an active error is acknowledged, the alarm relay opens
again. Cleared errors are moved to the Message list.
Shows the error history: Error code, date / time of issue and status
(active, acknowledged, cleared). 65 errors are memorized. Then
the oldest error is cleared to save the newest error (circular buffer)..
2 Diagnostics
In diagnostics mode, the values can only be viewed, not modified.
2.1 Identification
Desig.: Designation of the instrument.
Version: Firmware of instrument (e.g. 5.40-04/13)
2.1.3
2.1.4
2.2 Sensors
2.2.1
Oxytrace G
Current value: Shows the actual measuring value in ppb.
66
Saturation
A-96.250.531 / 241013
2.2.1.4
Cal. History
Review the diagnostic values of the last calibration of the oxygen
sensor. Max. 64 data records are memorized.
Number: Calibration counter.
Date, Time: Date and time of the calibration.
Sat. Current: Saturation current at that time of calibration.
Air pressure: Air pressure at that time of calibration.
2.2.2
2.2.2.1
Miscellaneous:
Case Temp: Shows the actual temperature in C inside the transmitter.
Air pressure: Shows the actual air pressure in hPa
2.2.3
QA History
Review QA values (Number, Date, Time, Deviation oxygen, Deviation Temperature, Status of QA check) of the last quality assurance
procedures.
2.3 Sample
2.3.301
Sample ID: Shows the assigned sample identification. This identification is defined by the user to identify the location of the sample
Temperature: Shows temperature in C.
(Nt5K): Shows raw value of the temperature in
Sample Flow: Shows the sample flow in l/h
(Raw value) Shows the sample flow in Hz
Alarm Relay:
Relay 1 and 2:
Input:
Signal Output 1 and 2:
Signal Output 3:
Open or closed.
Open or closed.
Open or closed.
Actual current in mA
Actual current in mA (if option is installed)
2.5 Interface
2.5.1
A-96.250.531 / 241013
67
3 Maintenance
3.1 Calibration
3.1.1
Start a calibration and follow the instructions on the screen. Displayed values are saturation in % and the saturation current in mA.
The indication bar shows the progress. Detailed explanation see
Calibration, p. 44.
3.2 Service
3.2.1
3.2.1.5
3.2.2
68
Electrolyte
Last Filling: Shows the date of the last filling of electrolyte.
Remaining Amount: Remaining amount of electrolyte in %.
Remaining Time: Remaining time in days until electrolyte exchange
recommended.
New Filling: Select Yes after electrolyte exchange to reset the
counter.
Faraday Verification
Start a manual faraday verification. Displayed values are current
value in ppb and the faraday concentration in %.
Current value: Measuring value in ppb
Faraday conc.: Oxygen concentration in % after activating the faraday verification.
Progress: The progress bar shows the progress of the faraday verification.
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3.3 Simulation
In this menu the following relays and signal outputs can be tested:
Alarm relay
Relay 1 and 2
Signal output 1 and 2
Signal output 3 (if option is installed)
Select a relay or signal output with the [
] or [
] keys,
press the [Enter]> key to confirm. Then change the value with the
[
] or [
] keys. After confirming the setting with the [Enter]
key, the value is simulated by the relay/signal output.
Alarm Relay:
Relay 1 and 2:
Input:
Signal Output 1 and 2:
Signal Output 3:
Open or closed.
Open or closed.
Open or closed.
Current in mA
Current in mA (if option is installed)
At the absence of any key activities, the instrument will switch back
to normal mode after 20 min. If you quit the menu, all simulated values will be reset.
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69
4 Operation
4.1 Sensors
4.1.1
4.1.2
4.1.3
4.1.3.1
4.1.3.20
4.1.3.21
4.1.3.22
4.1.3.3
4.1.3.4
Filter Time Constant: Used to damp noisy signals. The higher the
filter time constant, the slower the system reacts to changes of the
measured value.
Range: 5300 Sec
Hold after Cal: Delay permitting the instrument to stabilize again after calibration. During calibration plus hold-time, the signal outputs
are frozen (held on last valid value), alarm values, limits are not active.
Range: 06000 Sec
Faraday Parameter
Mode: The can be set to Interval, daily, weekly or off. If Mode is set
to Off, no further settings are available. The Faraday Verification
has to be started manually.
Interval: The interval can be set between 1h and 12h
Start Time: Start time appears if Mode is set to daily, how to set the
start time see 5.3.2.341, p. 81.
Calendar: Calendar appears if Mode is set to weekly, how to set
the Calendar see 5.3.2.342, p. 82.
Delay: during Faraday Verification plus the delay time the signal
and control outputs are held in the operating mode programmed
below.
Range: 06000 Sec.
Signal Outputs: Select operating mode of the signal output:
Cont.:
Hold:
Off:
4.1.3.5
70
Hold:
Off:
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4.3 Logger
4.3.1
Interval
1s
5s
1 min
5 min
10 min
30 min
1h
Time
25 min
2h
25 h
5d
10 d
31 d
62 d
4.3.2
Clear Logger: If confirmed with yes, the complete logger data is deleted. A new data series is started.
5 Installation
5.1 Sensors
5.1.1
5.1.1.1
5.1.1.2
5.1.2
5.1.2.1
Miscellaneous
Flow: If a flow cell without flow measurement (e.g. B-Flow) is used,
choose none. With flow measurement select Q-Flow
O2 Offset: Manual, small correction of the offset. Range 03 ppb.
Quality Assurance: Switch the Quality Assurance on or off.
Level: Select quality level:
Level 0: Off
Quality assurance procedure switched off. Any additional QA
menus are hidden.
Level 1: Trend
Level 2: Standard
Level 3: Crucial
Level 4: User
Edit user specific limits in menu 5.1.2.2
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71
5.2.1.2
5.2.1.3
As process
values
(4 - 20 [mA])
(0 - 20 [mA])
20
10
0/4
0.0
X
0.1
A linear
B bilinear
72
12
0.2
0.3
0.4
0.5
X Measured value
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[mA]
10
12
(4 - 20 [mA])
(0 - 20 [mA])
20
4 6
0/4
1
0
10
1
100
2
1000
3
10000
4
Scaling: Enter beginning and end point (Range low & high) of the
linear or logarithmic scale. In addition, the midpoint for the bilinear
scale.
Parameter: Oxygen.
Range low: 0.00 ppb 20.00 ppm
Range high: 0.00 ppb 20.00 ppm
Parameter: Temperature
Range low: -30 to + 130 C
Range high: -30 to + 130 C
Parameter: Saturation
Range low: 0200 %
Range high: 0200 %
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73
As control
output
a
L
74
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5.2.1.43.3
5.2.1.43.4
5.2.1.43.5
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75
5.3.1.1
5.3.1.1.1
5.3.1.1.25
5.3.1.1.35
5.3.1.1.45
76
Alarm oxygen
Alarm High: If the measured value rises above the alarm high value, the alarm relay is activated and E001, is displayed in the message list.
Range: 0.00 ppb 20.00 ppm
Alarm Low: If the measured value falls below the alarm low value,
the alarm relay is activated and E002 is displayed in the message
list.
Range: 0.00 ppb 20.00 ppm
Hysteresis: Within the hyst. range, the relay does not switch. This
prevents damage of relays contacts when the measured value fluctuates around the alarm value.
Range. 0.00 ppb 20.00 ppm
Delay: Duration, the activation of the alarm relay is retarded after
the measuring value has risen above/fallen below the programmed
alarm.
Range: 028800 Sec
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5.3.1.2
5.3.1.2.1
5.3.1.2.2
5.3.1.2.35
5.3.1.3
5.3.1.3.1
5.3.1.3.25
5.3.1.4
5.3.1.4.1
5.3.1.4.25
5.3.1.4.35
5.3.1.4.45
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77
5.3.1.5
5.3.1.5.1
5.3.1.5.2
Case Temp.
Case Temp. high: Set the alarm high value for temperature of electronics housing. If the value rises above the programmed value
E013 is issued.
Range: 3075 C
Case Temp. low: Set the alarm low value for temperature of electronics housing. If the value falls below the programmed value
E014 is issued.
Range: -10 to + 20 C
Relay 1 and 2: The function of relay contacts 1 or 2 are defined by
the user
Note: The navigation in the menu <Relay 1> and <Relay 2> is
equal. For reason of simplicity only the menu numbers of
Relay 1 are used in the following.
5.3.2.1
5.3.2.20
5.3.2.300
78
Then enter the necessary data depending on the selected function. The same values may also be entered in menu 4.2 Relay
Contacts, p. 71
Range
Oxygen
Temperature
-30 to + 130 C
Sample flow
050 l/h
Saturation
0200 %
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5.3.2.400
5.3.2.50
5.3.2.1
5.3.2.22
5.3.2.32
Hysteresis: within the hysteresis range, the relay does not switch.
This prevents damage of relay contacts when the measured value
fluctuates around the alarm value.
Parameter
Range
Oxygen
Temperature
0100 C
Sample flow
050 l/h
Saturation
0200 %
5.3.2.32.20
5.3.2.32.30
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79
5.3.2.32.4
Control Parameters:
Range for each Parameter same as 5.2.1.43, p. 75
Actuator = Frequency
5.3.2.32.21
5.3.2.32.31
5.3.2.32.22
5.3.2.32.32
5.3.2.32.4
5.3.2.1
Control Parameters:
Range for each Parameter same as 5.2.1.43, p. 75
Function = Timer
5.3.2.24
5.3.2.24
Interval
5.3.2.340
5.3.2.44
5.3.2.54
80
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5.3.2.6
Off:
5.3.2.7
Hold:
Off:
5.3.2.24
5.3.2.341
daily
The relay contact can be closed daily, at any time of a day.
Start time: to set the start time proceed as follows:
1
5.3.2.44
5.3.2.54
5.3.2.6
5.3.2.7
Range: 00:00:0023:59:59
Run Time: see Interval
Delay: see Interval
Signal Outputs: see Interval
Output/Control: see Interval
5.3.2.24
weekly
] or [
] or [
] or [
] keys.
] keys.
] keys.
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81
5.3.2.342
5.3.2.342.1
5.3.2.342.2
5.3.2.342.8
5.3.2.44
5.3.2.54
5.3.2.6
5.3.2.7
5.3.2.1
Calendar:
Start time: The programmed start time is valid for each of the programmed days. To set the start time see 5.3.2.341, p. 81.
Range: 00:00:0023:59:59
Monday: Possible settings, on or off
to
Sunday: Possible settings, on or off
Run Time: see Interval
Delay: see Interval
Signal Outputs: see Interval
Output/Control: see Interval
Function = Fieldbus
The relay will be switched via the Profibus input. No further parameters are needed.
5.3.4
5.3.4.1
Input: The functions of the relays and signal outputs can be defined depending on the position of the input contact, i.e. no function,
closed or open.
Active: Define when the input should be active:
No:
When closed
When open:
5.3.4.2
Off:
82
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5.3.4.3
5.3.4.4
Fault:
No:
Yes:
5.3.4.5
Delay: Time which the instrument waits, after the input is deactivated, before returning to normal operation.
Range: 06000 Sec
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83
5.4 Miscellaneous
5.4.1
5.4.2
5.4.3
5.4.4
5.4.5
84
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5.5 Interface
Select one of the following communication protocols. Depending on
your selection, different parameters must be defined.
5.5.1
Protocol: Profibus
5.5.20
Device address:
Range: 0126
5.5.30
ID-Nr.:
5.5.40
Local operation:
5.5.1
5.5.21
5.5.31
Baud Rate:
5.5.41
Parity:
5.5.1
5.5.23
5.5.1
5.5.24
Protocol: Webserver:
Bereich: 0126
Device address:
see separate Webserver Manual.
5.5.1
Protocol: USB-Stick:
Only visible if an USB interface is installed. No further settings are
possible.
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85
10.
10.1. Reagents
Catalogue No.:
Product name:
Download
MSDS
86
102751.10
Filling solution 1ALK
Part of: A-87.290.060
The current Material Safety Data Sheets (MSDS) for the above listed Reagents are available for downloading at www.swan.ch.
A-96.250.531 / 241013
11.
Default Values
Operation:
Sensors:
Alarm Relay
Relay 1/2
Input
Logger:
Installation:
Sensors
Signal Output 1
Signal Output 2
Alarm Relay:
Miscellaneous:
Flow:.................................................................................. Q-Flow
O2 Offset:.......................................................................... 0.0 ppb
Quality Assurance:
Level:.................................................................................... 0: Off
Parameter:............................................................................Oxygen
Current loop:..................................................................... 4 20 mA
Function:.................................................................................. linear
Scaling: Range low:............................................................ 0.00 ppb
Scaling: Range high: ....................................................... 10.00 ppm
Parameter:.................................................................... Temperature
Current loop:..................................................................... 4 20 mA
Function:.................................................................................. linear
Scaling: Range low:................................................................ 0.0 C
Scaling: Range high: ............................................................ 50.0 C
Alarm oxygen; Alarm high: .............................................. 10.00 ppm
Alarm oxygen; Alarm low:................................................... 0.00 ppb
Alarm oxygen; Hysteresis:................................................... 100 ppb
Alarm oxygen; Delay: .............................................................. 5 Sec
Sample Flow, Flow Alarm: .......................................................... yes
Sample Flow, Alarm high:.....................................................25.0 l/h
Sample Flow, Alarm low: ........................................................8.0 l/h
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Relay 1
Relay 2
88
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Input:
Miscellaneous
Interface
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89
12.
A
Alarm Relay .
Index
......
75
12
32
.............
10
..
..
..
32
40
34
Sample Flow . . . . .
Sample requirements
Signal Outputs . . . .
Software . . . . . . . .
............
11
Electrodes, Installation of
Electrolyte exchange. . .
Establish Sample Flow .
Input . . . . . . . .
Instrument Setup .
Interface
RS232 . . . .
RS485 . . . .
USB . . . . . .
......
......
......
.
P-Band . . . .
Power Supply .
PROFIBUS . .
Relay.
. . . 10, 28
. . . . . . 52
90
........
........
........
87
21
........
Default Values
...
Mounting requirements
24
82
38
Fluidics
......
......
......
Cable thicknesses
Calendar . . . . . .
Changing values .
10, 28
32
32
33
55
. . . . 34
. . . . 12
. 10, 31
. . . . 37
Temperature compensation. . 8
Terminals 2526, 2829, 3132
USB Interface .
W
Wire
........
33
..............
24
.......
46
Z
Zero-Verification
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13.
Notes
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91
SWAN
is represented worldwide by subsidiary companies
and distributors.
cooperates with independent representatives
all over the world.
SWAN Products
Analytical Instruments for:
High Purity Water
Feedwater, Steam and Condensate
Potable Water
Pool and Sanitary Water
Cooling Water
Waster Water and Effluents
Made in Switzerland
92
A-96.250.531 / 241013