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1499
THE STAINLESS STEEL
INSPECTORS KIT
INSTRUCTIONS
TABLE OF CONTENTS
Kit Contains
1
8
400 pcs.
1
1
1
1
3
1
ElectroSpot II
Solutions #1, 2, 3, 4, 5, 6, 9 & 10
Test Papers - #0100
Aluminum Cathode
Alligator Clip
Metal Sample - Incoloy 825
Eye Dropper
Packing Foam
Kit Case
Introduction
Alloy identification by chemical color tests is a simple and versatile technique. Identification is
based on the level of various components in the alloy. Sensitive and interference-free chemical
color tests detect the alloying components. A color develops as a result of the chemical reaction
and, generally, the intensity of the color can be used to estimate the amount of alloying
component present.
Spot tests are easier, faster, and cheaper than chemical analysis. The results are not as exact,
but estimates of the concentrations can be made. This is usually sufficient for alloy identification,
differentiation and verification.
The KOSLOW 1499 Stainless Steel Inspectors Kit, is designed for the rapid identification of
steels and nickel alloys. It is comprised of individual tests for these common alloying components:
Chromium(Cr), Nickel(Ni), Molybdenum(Mo), Copper(Cu), Iron(Fe). Identification of most
stainless alloys is possible with only these tests. In cases where a group of alloys are of almost
identical composition, individual identification may not be possible, although the group to which
the alloy belongs can be determined.
Standard Coupon
The Inspectors Kit includes a metal sample to be used as a testing reference. Incoloy 825 was
selected as a standard because it contains each of the five distinctive elements that can be
identified using this kit. Working side by side with a known sample will show what a positive
result looks like before attempting tests on lesser known materials. It also assures that the
equipment, testing solutions and procedures are working as they should. P/N 1499 S.
Nickel
Iron
Moly
Copper
21%
42%
30%
3%
2%
ElectroSpot Sampling
Here is how a test is carried out: Attach the clip lead to the test metal, or press it against it if the
piece is too large for the clip to "bite." Add the solution to the test paper and place it on a cleaned,
sanded area of the metal surface. Select the appropriate current range and gently press the
aluminum rod into the test paper as described below holding for the prescribed time. Remove the
test paper, turn it over, and add the color developer solution.
Time in Seconds
10 Seconds
5 to 10 Seconds
5 to 10 Seconds
Comparison of the relative intensities of highly colored spots is difficult. Therefore, sampling time
and current should be as small as possible, yet long enough to result in a clearly recognizable
color. Experimentation with known alloys will make this clear. When testing an alloy of unknown
composition, use the high current range first so that traces will not be missed. Avoid
unnecessarily high currents because the tests are "cleaner" when not too much of the alloy
dissolves in the paper. When in doubt, use the medium current range and sample for 10 seconds.
The panel meter is used to visually check the current range! current fall, if any, and also to insure
that current is flowing. If no current flows, the instrument may be in the "off" position, or the clip is
not making good electrical contact. Alternatively, it may indicate that the battery is dead. Turn the
ElectroSpot apparatus off when not in use. Avoid shorting the leads together which is harmful to
the battery and the meter.
A clean, bare metal surface must be exposed for each test. Sand the surface with emery paper if
necessary, and wipe completely clean of filings. Select the current range of the ElectroSpot
apparatus for the amount of component expected. Use the high current range for low
concentrations (0.3-2%), the medium range for concentrations (1-10%), and the low current range
for high concentrations (10% or higher). Establish the best current range by trial-and-error, to give
a reasonably intense colored spot. If the spot is too intense, it will be difficult to estimate the
amount of the component by comparison. Weakly colored spots are easier to compare.
A file of properly labeled alloy standard should be maintained. The best spot testing results are
obtained by comparing test results of unknown and known metals. A Metal Standards Collection
#1900 is available from Koslow, consisting of coupons of common alloys.
Inquire about our Electronic Alloy Sorter - TE-3000, which is helpful in unknown identification.
ElectroSpot Maintenance
The ElectroSpot variable current source is virtually maintenance-free. The battery is good for over
one year or about 10,000 tests under normal use. It is tested by shorting the leads together. The
current reading should be about 20-25mA on the medium range and over 100mA on the high
scale. (Caution: do not leave the switch in the Hi setting for more than a few seconds to avoid
damaging the meter). In the Lo range, the current is about 510mA. When the battery needs
replacement, use an alkaline 9v battery only. Remove the battery gently to avoid loosening the
bracket from the plastic case. The timer has its own internal batteries. The aluminum cylinder
cathode probe should be cleaned with emery paper occasionally, especially when dull looking or
having a black deposit on the bottom.
Reagent Handling
Like the handling of any chemical reagent, good housekeeping practices are imperative.
Wear a lab coat or protective clothing. Some solutions can stain or damage clothing.
Eye protection or splash resistant goggles.
Gloves to prevent unnecessary exposure to skin.
Wash hands after kit use.
Wipe spills quickly.
Dispose of kit contents according to local regulations.
For complete information, consult the M.S.D.S. sheets inside kit.
Copper-in-Steel
Solutions required: 3 and 9; test papers
Add to test paper: 2 drops Solution 3
ElectroSpot: 10% copper and up, Lo current, 5 seconds
1-5% copper, Med current, 5-10 seconds,
Less than 1% copper, Hi current, 10 seconds.
Then add: 2-5 drops Solution 9, gradually, drop-by-drop
Observe: a pink color (violet at high copper levels) is a positive test for copper.
7
Iron
Solutions required: 6 and 10; test papers
Add to test paper: 1 drop Solution 6
ElectroSpot: 10% iron and up, LO current, 5 seconds
1-5% iron, LO current, 10 seconds; Less than 1% iron, Med current, 10 seconds
Then add: 5 drops Solution 10, gradually, drop-by-drop until the color persists.
Observe: a pink-red color is a positive test for iron.
Note: This test is used to identify nickel alloys, because of the low iron content, generally.
Refill Information
Qty.
30 mL
30 mL
30 mL
30 mL
30 mL
30 mL
30 mL
30 mL
1,000
1
Description
Solution 1
Solution 2
Solution 3
Solution 4
Solution 5
Solution 6
Solution 9
Solution 10
Test Papers
Metal Sample Incoloy 825
P/N
0001
0002
0003
0004
0005
0006
0009
0010
0100
1499S
For current prices and availability, call 201 541-9100. Website www.koslow/refill.com
Chrome Nickel Iron Moly Cobalt Copper Sulfur Carbon Other Elements TE Reading
202
18
Bal.
0.03
1.5
-3
303
18
Bal.
0.6
0.15
1.5
304
19
Bal.
0.03
0.08
316
17
12
Bal.
2.5
0.03
0.08
321
18
10.5
Bal.
0.03
0.08
Ti5XC Min.
410
12.5
Bal.
0.03
0.15
150
17-4 PH
16
75
72
17-7 PH
17
75
20Cb3
20
34
36
2.5
3.5
20
26-1
26
0.5
75
304L
19
10
Bal.
0.03
0.03
316L
17
12
Bal.
2.5
0.03
0.03
904L
20
25
50
4.5
1.5
Hastelloy B
64
28
2.5
135
Hastelloy D
92
1.5
Hastelloy X
22
50
18
1.5
0.6 Tung.
37
Hastelloy C276
15
60
16
2.5
4 Tung.
60
Haynes Stellite
20
10
52
15 Tung.
I-600
15
76
125
I-625
21
61
2.5
60
I-718
19
52
18
50
I-800
21
32
25
I-804
29
42
46
I-825
21
42
30
32
I-840
20
20
60
Invar
33-42
Bal.
I-X750
15
73
Kovar
29
Bal.
17
3 Ti
Monel 400
66
31
-225
Monel K500
66
29
3 Alum.
-275
Nichrome
20
80
The above data is a useful as a guide for the chemical spot test method.
10