Uct Spe Catalog

UCT
E N V I R O F O R E N S I C S P H A R M A
SOLID PHASE
EXTRACTION CATALOG
800.541.0559 www.unitedchem.com
UCT is a respected leader in the drug testing,
pharmaceutical, clinical, environmental and
agricultural industries. Our wide range of
highly reproducible solid phase extraction
columns allow the chromatographer a
consistent extraction technique, and our
expertise in silane manufacturing allows a
greater control of the chemical processes
involved in producing our high quality
bonded phase. We manufacture our complete
product line of bonded phases. We manufacture
2
our complete product line of bonded silica
sorbents, packaged in a variety of formats,
w w w. u n i t e d c h e m . c o m
including SPE columns, 96 & 48 well plates,

universal cartridges and micro centrifuge tubes.
We also offer a variety of SPE accessories
including derivatizing reagents, GC liners,
and manifolds.
FORENSICS CLINICAL VETERINARY PHARMACEUTICAL
Since our beginnings in 1986, UCT has

evolved into a major competitor in the
field of silica based solid phase extraction
technology. Our commitment to ensuring
the satisfaction of our customers is accom-
plished by delivering on our promises:
top-quality, dependable solid phase
extraction products, and unmatched
technical support.
F O R E N S I C S
CUSTOMER SERVICE
PRICES AND TERMS RETURN POLICY
Our prices are subject to change without notice. The price Our Quality Manager will handle all returns. Before return-
in effect when we receive your order will apply. All prices ing merchandise, please call to obtain a return authorization
are in US Dollars and are F.O.B. Lewistown, PA 17044. number from your sales representative. We will need
Terms of payment are net 30 days. to know the reason for the return, date of purchase,
purchase order number and invoice number in order
MINIMUM ORDERS to issue a return authorization number. Returned mer-
We welcome all orders, therefore, we do not have a mini- chandise must be received before a credit can be issued.
mum order requirement. When ordering, please include Returns will not be accepted after 90 days. A restocking
your purchase order number, complete “Ship To” and fee of 25% of the price paid, or a minimum of $25.00
“Bill To” address, catalog number, quantity, and descrip- (whichever is greater) will be charged on all returns.
tion of product(s). Also include your name and a phone 3
number where you can be reached should we have any WARRANTY
questions concerning your order. All products manufactured by UCT are guaranteed against
Custom items will be evaluated on an individual basis; quantity defects in materials and workmanship for a period of 90
requirements may be necessary. days after shipment. UCT will replace any items that
prove to be defective during this time period.
SHIPMENTS
Normal processing is within 24-48 hours after receipt The exclusive remedy requires the end user to first ad-
of an order. Unless special shipping requests have vise UCT of the defective product by phone or in writing.
been made, our trained staff will send all orders by Secondly, the defective product must be returned within
UPS Ground service. The appropriate shipping charges 30 days after proper approval from our Quality Manager.
(freight & insurance costs) will be added to the invoice, All returns must indicate the purchase order number, the
unless otherwise instructed by the customer. lot number and the shipping date. UCT’s total liability is
limited to the replacement cost of UCT products.
SPECIAL PRICING
We offer special pricing for volume purchases and stand- This warranty does not apply to damage resulting
ing orders. Please call a sales representative for more from misuse.
information on special pricing qualifications.
Placing An Order Mail Technical Support
Phone: 717.247.0896 UCT, Inc. Phone: 215.781.9255

800.541.0559 2731 Bartram Rd. 800.385.3153
Fax: 717.247.0109 Bristol, PA 19007 Fax: 215.785.1226
Email: info@unitedchem.com
Forum: forums.unitedchem.com
Web: www.unitedchem.com
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4
A GREENER EARTH
Here at UCT, Inc. we are making an effort to keep the planet cleaner
and greener for everyone. It is our belief that we must act now to
preserve our environment for future generations to come.
Organizations we support:
Arbor Day Foundation
Audubon Society
Sierra Club

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TABLE OF CONTENTS
Solid Phase Extraction Phases .....................................................................................................................................................6-8
Reservoirs for Bonded Phase Extractions ...................................................................................................................................... 9
Use of Bonded Phases for Sample Preparation ........................................................................................................................... 10
CLEAN SCREEN® Sample Prep Products .................................................................................................................................11-19

Mechanism of CLEAN SCREEN® .................................................................................................................................... 12
Copolymeric Bonded Phases for Drug Abuse Testing ................................................................................................. 13
CLEAN SCREEN XCELTM .............................................................................................................................................14-15
CLEAN SCREEN® ETG / BNZ and CLEAN-THRU® TIPS................................................................................................. 16
CLEAN SCREEN® RSV ................................................................................................................................................17-19
XtrackT® HIGH-FLOW Bonded Phases .....................................................................................................................................20-21
CLEAN-UP® Solid Phase Extraction Phases.............................................................................................................................22-45

5
Hydrophobic Extraction Columns .............................................................................................................................23-26
Hydrophilic Extraction Columns ...............................................................................................................................27-31
Ion Exchange Extraction Columns ............................................................................................................................32-39
Copolymeric Extraction Columns ............................................................................................................................40-45
Covalent Extraction Columns ......................................................................................................................................... 46
STYRE SCREEN® Polymeric Resin Extraction Columns .........................................................................................................47-48

Benzenesulfonic Acid + C18, Polystyrene Divinylbenzene, Ion Exchange,
Reverse Phase, Carboxylic Acid and Quaternary Amine.............................................................................................. 48
Method Development Kits ........................................................................................................................................................49-50

Non-Polar Phases Endcapped, Polar Phases, Copolymeric Phases,
Ion Exchange Phases, Toxicology Phases and Pharmaceutical Phases .................................................................... 50
SELECTRASORBTM Bulk Sorbents ............................................................................................................................................51-53

Reservoirs...................................................................................................................................................................................54-55
Frits .................................................................................................................................................................................................. 56
Solid Phase Extraction Accessories .............................................................................................................................................. 57
Positive Pressure Manifold ......................................................................................................................................................58-59
Universal Vacuum Manifold and Accessories ........................................................................................................................60-61
Vacuum Manifold and Accessories ......................................................................................................................................... 62-63
SELECTRA-SIL® Derivatizing Reagents ....................................................................................................................................64-68
GC Liners ....................................................................................................................................................................................69-70
SELECTRA® HPLC Columns ........................................................................................................................................................... 71
96 Deep Well Plates ...................................................................................................................................................................72-74
48 Deep Well Plates ...................................................................................................................................................................75-77
Flash Chromatography Columns .............................................................................................................................................78-79

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UCT
SOLID PHASE EXTRACTION PHASES
6

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F UN C T I O N A LIZED S ILICA-BASED PHASES
REVERSE PHASE (HYDROPHOBIC)

SORBENT SORBENT CODE STRUCTURE
C2 ethyl C02 -SiCH2CH3
C3 propyl C03 -Si-(CH2)2CH3
C4 n-butyl Cn4 -Si-(CH2)3CH3
Ci4 isobutyl Ci4 -Si-CH2CH(CH3)2
Ct4 tertiary butyl Ct4 -Si-C(CH3)3
C5 pentyl C05 -Si-(CH2)4CH3
C6 hexyl C06 -Si-(CH2)5CH3
C7 heptyl C07 -Si-(CH2)6CH3
C8 octyl C08 -Si-(CH2)7CH3
C10 decyl C10 -Si-(CH2)9CH3
C12 dodecyl C12 -Si-(CH2)11CH3
C18 octadecyl C18 -Si-(CH2)17CH3
C20 eicosyl C20 -Si-(CH2)19CH3
C30 tricontyl C30 -Si-(CH2)29CH3
Cyclohexyl CYH1 -Si
Phenyl PHY1 -Si
NORMAL PHASE (HYDROPHILIC)

7
Silica SIL1 -SiOH
Diol DOL1 -Si-(CH2)3OCH2CHOHCH2OH
Cyanopropyl CNP1 -Si-(CH2)3CN
Florisil® FLS
Alumina, Acidic ALA
Alumina, Neutral ALN
Alumina, Basic ALB
Carbon CARB
ION EXCHANGE
Anion pka
Aminopropyl (1° amine) NAX1 -Si-(CH2)3NH2 9.8
N-2 Aminoethyl (1° & 2° amine) PSA1 -Si-(CH2)3NH(CH2)2NH2 10.1, 10.9
Diethylamino (3° amine) DAX1 -Si-(CH2)3N(CH2CH3)2 10.6
Quaternary Amine Chloride QAX1 -Si-(CH2)3N+(CH3)3 Cl- always charged
Quaternary Amine Hydroxide CHQAX1 -Si-(CH2)3N+(CH3)3 OH always charged
Quaternary Amine Acetate CAQAX1 -Si-(CH2)3N+(CH3)3 CH3COO always charged
Quaternary Amine Formate CFQAX1 -Si-(CH2)3N+(CH3)3 HCOO always charged
Polyimine PAX -Si-(CH2)3-R-[NHCH2CH2]X
Cation
Carboxylic Acid CCX1 -Si-CH2COOH 4.8
Propylsulfonic Acid PCX1 -Si-(CH2)3SO3H <1
Benzenesulfonic Acid BCX1 -Si-(CH2)2 SO3H always charged
Benzenesulfonic Acid High Load BCXHL1 -Si-(CH2)2 SO3H always charged
Triacetic Acid TAX -Si-(CH2)3NH-(CH2)2N(CH2COOH)2
CH2COOH
COPOLYMERIC (MULTIFUNCTIONAL PHASES)
Aminopropyl + C8 NAX2 -Si-(CH2)3NH2 & -Si-(CH2)7CH3

Quaternary Amine + C8 QAX2 -Si-(CH2)3N+(CH3)3 & -Si-(CH2)7CH3
Carboxylic Acid + C8 CCX2 -Si-CH2COOH & -Si-(CH2)7CH3
Propylsulfonic Acid + C8 PCX2 -Si-(CH2)3SO3H & -Si-(CH2)7CH3
Benzenesulfonic Acid + C8 BCX2 -Si-(CH2)2 SO3H & -Si-(CH2)7CH3
Cyanopropyl + C8 CNP2 -Si-(CH2)3CN & -Si-(CH2)7CH3
Cyclohexyl + C8 CYH2 -Si & -Si-(CH2)7CH3
COVALENT PHASES
Epoxy EPX -Si-(CH2)3 - O - CH2 - CH - CH2 - CH2

Aldehyde ALD -Si-(CH2)4CHO
Isocyanate ICN -Si-(CHUCT
) NCO O
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Thiopropyl THX -Si-(CH2P.)3800.385.3153
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F U N C TIONALIZED SILICA-BASED PHASES
SORBENT % ORGANIC EXCHANGE (meq/g)

C2 ethyl 6.60 N/A
C3 propyl 7.60 N/A
C4 n-butyl 8.50 N/A
Ci4 isobutyl 8.80 N/A
Ct4 tertiary butyl 8.50 N/A
C5 pentyl 9.50 N/A
C6 hexyl 11.00 N/A
C7 heptyl 11.00 N/A
C8 octyl 11.10 N/A
C10 decyl 15.70 N/A
C12 dodecyl not tested N/A
C18 octadecyl 21.70 N/A
C20 eicosyl 24.30 N/A
C30 tricontyl 26.00 N/A
Cyclohexyl 11.60 N/A
Phenyl 11.00 N/A
NORMAL PHASE (HYDROPHILIC)
Silica N/A N/A

8 Diol 8.00 N/A
Cyanopropyl 6.90 N/A
Florisil® N/A N/A
Alumina, Acidic N/A N/A

Alumina, Neutral N/A N/A
Alumina, Basic N/A N/A
Carbon N/A N/A
ION EXCHANGE
Anion
Aminopropyl (1° amine) 6.65 0.310
N-2 Aminoethyl (1° & 2° amine) 9.70 0.320
Diethylamino (3° amine) 8.40 0.280
Quaternary Amine Chloride 8.40 0.250
Quaternary Amine Hydroxide 8.40 0.250
Quaternary Amine Acetate 8.40 0.250
Quaternary Amine Formate 8.40 0.250
Polyimine 13.5 0.250
Cation
Carboxylic Acid 9.10 0.170
Propylsulfonic Acid 7.10 0.180
Benzenesulfonic Acid 11.00 0.320
Benzenesulfonic Acid High Load 15.00 0.650
Triacetic Acid 7.61 Anion 0.17 / Cation .06
COPOLYMERIC (MULTIFUNCTIONAL PHASES)
Aminopropyl + C8 12.3 0.163

Quaternary Amine + C8 13.60 0.160
Carboxylic Acid + C8 1 2.50 0.105
Propylsulfonic Acid + C8 14.62 0.114
Benzenesulfonic Acid + C8 12.30 0.072
Cyanopropyl + C8 14.60 0.163
Cyclohexyl + C8 N/A N/A
COVALENT PHASES
Epoxy N/A N/A

Aldehyde N/A N/A
Isocyanate 7.1 N/A
Thiopropyl 6.50 N/A

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RESERVOIRS FOR BONDED PHASE EXTRACTIONS
UCT 9
Chemistries are offered on these particles sizes...
Small Particle (5-20 µm)
Intermediate Particle (25-40 µm)
Standard Particle (40-60 µm)*
Large Particle (125-210 µm)
and are available in the following formats
Stated Volume (mL) Tube Configuration Bed Diameter (mm) Sorbent Mass (mg)
1 Cylindrical 5.5 50-200

10 Expanded 8.5 50-1000
15 Cylindrical 15.5 500-2000
25 Cylindrical 20 500-5000
75 Cylindrical 27.5 1000-10000
150 Cylindrical 38.0 10000-70000
*All phases are manufactured with 40-60 µm silica unless otherwise indicated.

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U S E O F B O NDED PHASES FOR SAMPLE PREPARATION
CONDITIONING, SOLVATION (WETTING) WASHING THE SORBENT AND ELUTING
Columns are shipped dry, but those with hydrophobic Ideal washing removes as many interferences as possible
character need to be solvated in order to interact efficiently while retaining the analyte(s). Ideal elution recovers 100% of
and reproducibly with aqueous matrices. Sample capacity is the analyte while leaving behind interferences. Make certain
severely reduced on a dry column. your column is dry when changing between aqueous solu-
tions and organic solvents.
At low vacuum ( - 3 in. Hg) add 1.5 mL of methanol or aceto-
nitrile per 100 mg of sorbent to the sample preparation col- HYDROPHOBIC AND POLAR ANALYTES
umn. Release the vacuum or begin flushing immediately upon
completion. The more air which passes through the column The best approach towards using these types of sorbents is
before sample loading, the less solvated the sorbent will be. to search for a solvent mixture which will wash the most inter-
ferences from the sorbent without loss of analyte. Note that
Apply deionized or distilled water to remove excess solvent wash pH may greatly affect cleanup and/or recovery. Keep
which will interfere with hydrophobic binding. Use 1 mL H2O analyte and sorbent pKa in mind if applicable. Elute with the
per 100 mg sorbent. Momentary high vacuum (5 to 8 in. Hg) strongest organic solvent, or by raising the percentage of
10 may be necessary to restart flow. At - 2.5 in. Hg the column organic, possibly in combination with a pH change to disrupt
will resist air displacement (vacuum may be left on without binding.
drying the sorbent). If the sorbent is accidentally dried, resol-
vate and reflush.
When using ion exchange columns, apply 1mL of buffer to ION EXCHANGE
the column after flushing to ensure that the sorbent pH is
optimal for the sorbent analyte interaction desired. Where Ionic bonds are strong enough to allow the analyte to remain
ion exchange interactions are involved, follow guidelines bound while interferences are washed away with high per-
concerning pKa, pH and ionic binding. Use the same vacuum centages (up to 100%) of polar or nonpolar organic solvents.
guidelines as described for flushing. The pH will also affect sample cleanup. Remember to remain
2 pH units from the relevant pKa of your analyte and sorbent,
When doing work where a very clean baseline is required both of which need to remain charged for ionic retention.
washing the column with the elution solvent as part of the Elute with aqueous buffers containing a stronger counterion
conditioning step will improve the LOD and LOQ. than your analyte (classic ion exchange) or by changing pH to
disrupt the ionic attraction. Make sure the elution solvent has
enough organic character to overcome any adsorption due to
SAMPLE PREPARATION AND APPLICATION the packing material.
Mechanisms may be hydrophobic, polar, or ionic. Add internal
standard to the sample if quantitation is desired. Optimize COPOLYMERIC EXCHANGE
sample application by removing particulates if ecessary (cen-
trifugation or filtering) and/or diluting viscous matrices with For ionically bound analytes, use washes of high organic
water or buffer to ensure proper pH for desired interactions. strength to remove interferences retained by hydrophobic
The analyte and sorbent should be uncharged for optimum (solvent strength dependent) interactions. If your analyte is
hydrophobic retention. On ion exchange sorbents, analytes also capable of hydrophobic binding, remove polar interfer-
must be oppositely charged to the sorbent [anions (-) on ences ionically similar to your analyte by using aqueous or
anion exchange sorbents (+); cations (+) on cation exchange weak aqueous/organic washes while disrupting ionic (pH and
sorbents (-)]. During sample application, the analyte binds by ionic strength dependent) binding. Elute by simultaneously
displacing a counterion on the sorbent. disrupting ionic and hydrophobic interactions
Apply sample at a rate of 1mL/min. Again, a momentary

increase in vacuum may be needed to initiate
sample flow.

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CLEAN SCREEN ® SAMPLE PREP PRODUCTS
11

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MECHANISM OF CLEAN SCREEN ®
When a sample is loaded onto the column at pH 6, many carboxylic

Sample Application
acid functionalities present in the sample are ionized. This creates a
repulsion between the column and many sample borne interferences, NH +
thereby reducing the likelihood of their adsorbing onto the column.

SO 3 PCP
At this pH, ibuprofen & barbiturates are not ionized and are
hydrophobically adsorbed on to the column (figure 1). At the same
time, drugs with amine functionalities such as cocaine and
C nH 2n+1
phencyclidine adsorb on to the column via both hydrophobic and
ionic attraction (figure 1).
CH C OH
IBUP RO FEN CH 3 O
figure 1
The column can then be washed with water or weak aqueous Elution 1
buffers at or below pH 6 without risking loss of the analytes. After
NH +
drying the column, it is possible to elute the hydrophobically bound
analytes using solvents of minimal polarity such as methylene SO 3 PCP
12 chloride or a hexane/ethyl acetate mixture (figure 2). Cationic
analytes will remain bound to the column. Many compounds of
intermediate polarity and potential interferences will also remain C nH 2n+1

on the column. The majority of these potential interferences can
be removed by using a methanol wash.
CH C OH
IBUP RO FE N
CH 3 O
figure 2
Cationic analytes bound to the column can be eluted after another Dry Column
drying step. The drying steps are necessary to remove water which
would have prevented the water immiscible elution solvents from NH+
optimally interacting with the analytes (figure 3). SO3 PCP
CnH2n+1
H2O
figure 3
To elute the cationic analytes, an organic solution with a high pH Elution 2

should be used. A methylene chlorideisopropanol-ammonium
hydroxide mixture will simultaneously disrupt these ionic SO 3
interactions and successfully elute the desired compound (figure 4).

C nH 2n+1
NH +
PCP
figure 4

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CLEAN S C R E E N ®
COPOLYMERIC BONDED PHASES FOR DRUG ABUSE TESTING
Analytical demand for more efficient, robust and clean extraction of drugs from biological matrices led to the
development of CLEAN SCREEN® sorbents. Since 1986, CLEAN SCREEN® has led the industry with dependable
and reproducible Solid Phase Extraction products and applications. CLEAN SCREEN® phases are true copolymeric
sorbents that contain hydrophobic and ion exchange functional groups uniquely polymerized to a silica substrate.
The design and quality of CLEAN SCREEN® provides superior sample clean up, recovery and reproducibility.
Mixed mode separations allow maximum selectivity for extraction of acids, neutrals and bases. This selectivity
makes CLEAN SCREEN® ideal for both screening and confirmation analysis for virtually all drug categories.
CLEAN SCREEN® columns are used extensively by forensic and clinical chemists including:
• Post Mortem Investigations • Racing Laboratories

• Criminal Investigations • Therapeutic Drug Monitoring
• Urine Drug Testing • Medical Drug Screening
• Athletic Drug Testing
Note:
If performing extractions out of viscous matrices such as tissue or horse urine, turn to our XtrackT® section,
where high-flow/gravity flow columns are found. The DAU CLEAN SCREEN® sorbent as well as other phases
are available in this larger particle size.
DAU
13
Part Number without Part Number with Sorbent Amount/ Unit per CLEAN SCREEN DAU ®
Clean-Thru® Tips Clean-Thru® Tips Tube Volume Pack column is copolymerized on a
CSDAU131 CCDAU131 130mg/1mL 100 rigid, purified silica gel support.
CSDAU133 CCDAU133 130mg/3mL 50 The two functional groups
CSDAU203 CCDAU203 200mg/3mL 50 include a reverse phase, and an
CSDAU303 CCDAU303 300mg/3mL 50 ion exchanger, benzenesulfonic
CSDAU503 CCDAU503 500mg/3mL 50 acid. This column is commonly
CSDAU206 CCDAU206 200mg/6mL 50 used for analyzing a wide range
CSDAU506 CCDAU506 500mg/6mL 50 of drugs of abuse, including
CSDAU1M6 CCDAU1M6 1g/6mL 30 acidic, basic & neutral drugs.
ZSDAU005 ZCDAU005 50mg/10mL 50
ZSDAU013 ZCDAU013 130mg/10mL 50 Application: Dual functionality
ZSDAU020 ZCDAU020 200mg/10mL 50 for weak bases and hydrophobic
CSDAU515 CCDAU515 500mg/15mL 5 compounds.
% Organic Loading: 12.30 Exchange Capacity (meq/g): 0.072
THC
Part Number without Part Number with Sorbent Amount/ Unit per CLEAN SCREEN® THC
Clean-Thru® Tips Clean-Thru® Tips Tube Volume Pack column is copolymerized on a
CSTHC131 CCTHC131 130mg/1mL 100 rigid, purified silica gel support.
CSTHC203 CCTHC203 200mg/3mL 50 The two functional groups include
CSTHC303 CCTHC303 300mg/3mL 50 a reverse phase, and an ion
CSTHC503 CCTHC503 500mg/3mL 50 exchanger, primary amine.
CSTHC206 CCTHC206 200mg/6mL 50 This column is commonly
CSTHC506 CCTHC506 500mg/6mL 50 usedfor analyzing THC and
CSTHC1M6 CCTHC1M6 1g/6mL 30 its metabolites.
ZSTHC013 ZCTHC013 130mg/10mL 50
ZSTHC020 ZCTHC020 200mg/10mL 50 Application: Dual functionality for
acids and hydrophobic compounds.
% Organic Loading: 12.3 Exchange Capacity (meq/g): 0.163
GHB
Part Number without Part Number with Unit per

Clean-Thru® Tips Clean-Thru® Tips Pack
CSGHB203 200mg/3mL 50
ZSGHB020 200mg/10mL 50
ZCGHB020 200mg/10mL 50
The small polar nature of the molecule and the lack of a UV chromatophore complicate the chromatographic and
spectrophotometricanalysis of GHB. Chemically, GHB is unstable and readily
UCT | forms Gamma-butyrolactone
2731 Bartram Rd | Bristol, PA 19007when heated in
| USA
acid conditions. Most analytical methods are based upon the interconversion to the lactone
P. 800.385.3153 and chemical
| 215.781.9255 derivatization to
| F. 215.785.1226
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UCT
14
CLEAN SCREEN XCEL TM
UCT
2 STEP EXTRACTION COLUMN

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
T
CLEAN SCREEN XCE L ™
SOLID PHASE EXTRACTION COLUMNS
The Clean Screen Xcel solid phase extraction columns are a line of sample prep phases designed
to reduce the number of steps in the extraction, and therefore the amount of time and solvent
necessary to complete the sample cleanup. Further advantages include reduced sample size and
improved cleanliness and recovery.
CLEAN SCREEN XCEL I: CLEAN SCREEN XCEL I

The Xcel I column will extract a
wide array of basic drugs including Part Number Sorbent Amount/ Unit per
benzodiazepines and opiates. Endcapped Tube Volume Pack
CSXCE111 130mg/1mL 100
ZSXCE010 130mg/10mL 50
CLEAN SCREEN XCEL II 15

CLEAN SCREEN XCEL II:
The Xcel II column is designed solely for Part Number Sorbent Amount/ Unit per
the extraction of the THC metabolite. Endcapped Tube Volume Pack
ZSXCE2010 130mg/10mL 50
CLEAN SCREEN XCEL ™

SOLID PHASE EXTRACTION WELL PLATES
96 DEEP WELL PLATES
Part Number Sorbent Amount/ Unit per

Tube Volume Pack
WSH96XCE11 130mg 1
48 DEEP WELL PLATES

Tube Volume Pack
WSH48XCE11 130mg 1

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UCT
C L E A N SCREEN ®
ETHYL GLUCURONIDE SOLID PHASE EXTRACTION COLUMN
BENZODIAZEPINE SOLID PHASE EXTRACTION COLUMN
ETG
Part Number without Part Number with Sorbent Amount/ Unit per CLEAN SCREEN® ETG
Clean-Thru® Tips Clean-Thru® Tips Tube Volume Pack columns are available exclusively
CSETG203 CCETG203 200mg/3mL 50 from UCT for analysis by GC/MS &
ZSETG040 ZCETG040 400mg/10mL 50 LC/MS. This 3mL column contains a
proprietary carbon packing
material for the extraction and
concentration of ethyl glucuronide.
BNZ
Part Number without Part Number with Sorbent Amount/ Unit per CLEAN SCREEN® BNZ
Clean-Thru® Tips Clean-Thru® Tips Tube Volume Pack columns are available for
CSBNZ203 CCBNZ203 200mg/3mL 50 benzodiazepine extractions,
CSBNZ206 _______ 200mg/6mL 50 with specific focus on
ZSBNZ020 _______ 200mg/10mL 50 7-amino benzodiazepines.
ZSBNZ060 _______ 300mg/10mL 50
16
CLEAN-THRU ® T I P S
CLEAN-THRU ® tips provides the first solid phase extraction cartridge system that eliminates sample carry over
from the vacuum manifold lid. The technology was pioneered by our research scientists & consists of one of our
SPE columns with a disposable tip that attaches to the end of each column. Columns available in the CLEAN-THRU®
configuration are found in the CLEAN SCREEN ® sections. This system was designed in order to meet the strict
requirements that the Substance Abuse and Mental Health Services Administration certification has placed on labo-
ratories to address the problem of cross contamination between samples. CLEANTHRU® tips provide a completely
disposable system that eliminates any contact between the sample, wash solvents and the extraction apparatus.
The continuous passage of the sample through the system provides a direct, accurate route to waste or collection
vessels. As each extraction is completed, the column and tip are discarded as a unit. CLEAN-THRU® eliminates your
concerns about sample residue remaining in the extraction system.U CLEAN SCREEN® sorbent as well as other
phases are available in this larger particle size.
CLEAN-THRU® TIPS Standard UCT’s Column with

Configuration a CLEAN-THRU® Tip
Part Number Description Unit per bag
CLTTP050 TIP 50

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CLEAN SCREEN® RSV
UCT
REDUCED SOLVENT VOLUME EXTRACTION COLUMNS
Reduced Solvent Volume extraction columns are micro bed packed columns which
offer the advantages of disc technology yet maintain the proven track record of our
conventional SPE columns. Reduced Solvent Volume columns use 75% less solvent than
traditional packed columns. Less solvent means faster extractions, higher throughput
and less waste disposal, which translates into significant savings in both time and
money. Results demonstrate that therapeutic and abused drugs in urine and blood
matrices can be extracted with cleanliness, high recoveries and consistent reproducibility
by using the Reduced Solvent Volume extraction column.
17
Advantages of CLEAN SCREEN® RSV:
• 75% Reduction in total liquid volumes
• Lower cost per extraction
• Faster extraction times
• Less disposal cost
• Increased automated throughput
• 50% Reduction in eluate volume
• Faster dry down times
• Reduced exposure to organic solvents
• Superior flow characteristics
• Less flow restriction from matrix proteins
or particulates
• More reliable for automated processing
• High capacity
• Greater linear range

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UCT
C L E A N SCREEN ® RSV
CAPACITY
100
91% (n=4) for 1000 ng/mL
90
90% (n=2) for 3000 ng/mL
Absolute Recovery
80
70 91% (n=4) for 4000 ng/mL
60
50 No analyte breakthrough at 1000 ng/mL
40
and less than 0.2% analyte breakthrough
30
20 at 3000 and 4000 ng/mL levels.
10
0
1000 3000 4000
THC-COOH Standards (ng/mL) in spiked urine
18
RECOVERY
Concentration (ng/mL)
2000
Linear Ranges Exhibiting
1800
1600 Greater than
1400 85% Recoveries in Urine
1200
1000
800
600
25ng/mL 2ng/mL
400
Highest Concentration Tested
200
0 Lowest Concentration Tested
Butalbital
Amobarbital
Pentobarbital
Secobarbital
Phenobarbital
Benzoylecgonine
Phencyclidine
THC-COOH
Analyte
SOLVENT REDUCTION
Analyte Solvent Usage Solvent Usage % Solvent

Clean-Thru® Tips Reduced Solvent Traditional Packed Reduction
Volume SPE columns columns
Barbiturates 4.25 mL 18 mL 76%

Benzoylecgonine 4.65 mL 19 mL 76%
THC-COOH 4.85 mL 16.4 mL 73%
Phencyclidine 5.15 mL 19 mL 70%

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CLEAN SCREEN ® R S V
COPOLYMERIC EXTRACTION FOR ALL DRUG CLASSES
Part Number without Part Number with Sorbent Amount/ Unit per CLEAN SCREEN® DAU
Clean-Thru® Tips Clean-Thru® Tips Tube Volume Pack Column is copolymerized on a rigid,
CSDAUA83 CCDAUA83 80mg/3mL 50 purified silica gel support. The two
ZSDAUA08 ZCDAUA08 80mg/10mL 50 functional groups include a reverse phase,
and an ion exchanger, benzenesulfonic
acid. This column is commonly used for
analyzing a wide range of drugs of abuse,
including acidic, basic and neutral drugs.
SPECIFICALLY FOR THC & THCA EXTRACTION
Part Number without Part Number with Sorbent Amount/ Unit per CLEAN SCREEN® THC
CSTHCA83 CCTHCA83 80mg/3mL 50 purified silica gel support. The two
ZSTHCA08 ZCTHCA08 80mg/10mL 50 functional groups include a reverse
phase, and an ion exchanger, quaternary 19
amine. This column is commonly used
for analyzing THC and its metabolites.
CLE A N U P ® R SV
C18, OCTADECYL TRI-FUNCTIONAL
Part Number Part Number Sorbent Amount/ Unit per Pack % Organic Loading: 21.70
Endcapped Unendcapped Tube Volume Pack Application:
CEC18A083 CUC18A083 80mg/3mL 50 Removes hydrophobic impurities,
de-salting and purification
of hydrophobic compounds.

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UCT
XtrackT ® HIGH-FLOW SOLID PHASE EXTRACTION COLUMNS
20

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Xtr a c k T ®
HIGH-FLOW BONDED PHASES
Viscous sample matrices are frequently resistant to flow through standard solid phase columns. Increased particle
size enhances flow characteristics allowing ease of sample application and analysis. XtrackT® columns are designed
to give uniform flow for even the most viscous samples including equine urine, post mortem blood and tissues,
meconium, amniotic fluid, milk, etc.
XtrackT® also functions as a gravity flow column for most blood and urine samples. A single column provides
extraction for a broad spectrum of compounds with selective elution of acid neutrals, steroids and bases XtrackT®
yields very clean extractions and excellent recoveries without need for additional liquid clean up steps. XtrackT®
is available in hydrophobic, hydrophilic, ion exchange, and copolymeric phases, including the CLEAN SCREEN®
DAU sorbent. XtrackT® is recommended for any chemist challenged by viscous sample matrices, or those desiring
gravity flow capacity.
Upon request, we can also provide any of our CLEAN-UP® sorbents in this large particle size.
Advantages of XtrackT®
• Resists plugging • Broad spectrum extractions
• Improved flow of all sample types • Very clean extractions
• Gravity flow of most samples • High recoveries
• Reproducibility
21
GRAVITY-FLOW CLEAN SCREEN® DAU COLUMNS
Part Number with Part Number without Sorbent Amount/ Unit per CLEAN SCREEN® DAU
XRDAH203 XCDAH203 200mg/3mL 50 purified silica gel support. The two
XRDAH303 XCDAH303 300mg/3mL 50 functional groups include a reverse
XRDAH503 XCDAH503 500mg/3mL 50 p h a s e , a n d a n i o n e x c h a n g e r,
XRDAH206 XCDAH206 200g/6mL 50 benzenesulfonic acid. This column is
XRDAH506 XCDAH506 500g/6mL 50 commonly used for analyzing a wide
XRDAH20Z XCDAH20Z 200mg/10mL 50 range of drugs of abuse, including
XRDAH50Z XCDAH50Z 500mg/10mL 50 acidic, basic & neutral drugs.
XRDAH515 XCDAH515 500mg/15mL 50
XRDAHM15 XCDAHM15 1g/15mL 30
HIGH-FLOW CLEAN-UP® ENDCAPPED C18 COLUMNS
Part Number with Part Number without Sorbent Amount/ Unit % Organic Loading: 21.70
per
Clean-Thru® Tips Clean-Thru® Tips Tube Volume Pack Application:
XRODHM06 XCODHM06 1g/6mL 30 Removes hydrophobic impurities,
XRODH515 XCODH515 500mg/15mL 50 de-salting and purification of
hydrophobic compounds.
HIGH-FLOW CLEAN-UP® PROPYLSULFONIC ACID COLUMNS
Part Number with Part Number without Sorbent Amount/ Unit per % Organic Loading: 9.70
Clean-Thru® Tips Clean-Thru® Tips Tube Volume Pack
XRPCH50Z XCPCH50Z 500mg/10mL 50 Application:
Scavenger for amines,
alcohols and other nucleophiles
High-Flow also available in:

Carboxylic Acid, Aminoethyl, Benzenesulfonic Acid and Quaternary Amine

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CLEAN-UP ® SOLID PHASE EXTRACTION COLUMNS
22
HYDROPHOBIC HYDROPHILIC ION EXCHANGE

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CLEAN- UP ®
HYDROPHOBIC EXTRACTION COLUMNS
This sorbent is composed of a silica backbone bonded

Example of a Hydrophobic Phase
with hydrocarbon chains. It is used to extract compounds
which exhibit non-polar or neutral characteristics out of
Si
complex matrices. The C18 phase is the most widely used
O OSi(CH3 )3
for non-polar interactions because of its nonselective nature;
C18 will extract a large number of compounds with differing Si O Si (CH2)17 CH3
chemical properties. To enchance selectivity, UCT offers a
O OSi(CH3 )3
wide range of hydrophobic sorbents. Multiple chain configu-
rations are available for some Endcapped or unendcapped Si
sorbents are available for all chain lengths. O OSi(CH3 )3
Si O Si (CH2)17 CH 3
O OSi(CH3 )3 23
Silica Backbone
Hydrocarbon Chain
Analytes* Washes Elutions

alkanes aqueous, non-polar
alkenes usually with to
aromatics some polar polar organic
neutral compounds organic solvent
*typical compounds which can be extracted using hydrophobic columns

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UCT
CL E A N - U P ®
MECHANISM OF HYDROPHOBIC BONDING

Hydrophobic Sorbents & Structures
Compounds are retained by non-polar interactions
from polar solvents or matrix environments. They are Sorbent Structure
bound by dispersion forces / van der Waals forces. C2 ethyl -SiCH2CH3
Elution, or disruption of the non-polar interactions
is achieved by solvents or solvent mixtures with suf- C3 propyl -Si-(CH2)2CH3
ficient non-polar character. Some polar solvents, such
C4 n-butyl -Si-(CH2)3CH3
as acetonitrile have enough non-polar characteristics
to disrupt nonpolar binding to cause elution of a Ci4 isobutyl -Si-CH2CH(CH3)2
compound from the sorbent. Methanol can be used
as well, although it should be noted that it will take Ct4 tertiary butyl -Si-C(CH3)3
off both polar and nonpolar analytes of interest and C5 pentyl -Si-(CH2)4CH3
interferences.
C6 hexyl -Si-(CH2)5CH3
C7 heptyl -Si-(CH2)6CH3
Example of a Hydrophobic Bonding C8 octyl -Si-(CH2)7CH3
24 H C10 decyl -Si-(CH2)9CH3

H H
C12 dodecyl -Si-(CH2)11CH3
C
C C C18 octadecyl -Si-(CH2)17CH3
H
H H C20 eicosyl -Si-(CH2)19CH3
H
Sorbent H C H C30 tricontyl -Si-(CH2)29CH3
C C
Cyclohexyl -Si
H Compound Phenyl -Si
H H
UNENDCAPPED VS. ENDCAPPED
Bonded phases are manufactured by the reaction In order to decrease this slight polarity, these
of organosilanes with activated silica. During the hydroxyl sites are deactivated. Proprietary bonding
polymerization reaction of carbon chains to the silica techniques ensure that these sites are 100% reacted,
backbone, a very stable silyl ether linkage forms. Our leading to a complete endcapping. Because there
unendcapped columns allow hydroxyl sites to remain, are no hydroxyl sites left, our endcapped columns
thus making these columns slightly hydrophilic. are more hydrophobic than our unendcapped columns.
OH OSi(CH3)3
O O
Si O Si Si O Si
O O
OH OSi(CH3)3
Si Si
Unendcapped Structure Endcapped Structure

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CLEAN - UP ®
C8, OCTYL
Part Number Part Number Sorbent Amount/ Unit per % Organic Loading: 11.10
Endcapped Unendcapped Tube Volume Pack
CEC081L1 CUC081L1 50mg/1mL 100 Application:
CEC08111 CUC08111 100mg/1mL 100 Removes large or more
CEC08113 CUC08113 100mg/3mL 50 hydrophobic compounds.
CEC08123 CUC08123 200mg/3mL 50
CEC08153 CUC08153 500mg/3mL 50
CEC08156 CUC08156 500mg/6mL 50
CEC081M6 CUC081M6 1g/6mL 30
CEC0811Z CUC0811Z 100mg/10mL 50
CEC0812Z CUC0812Z 200mg/10mL 50
CEC0812M15 CUC0812M15 2g/15mL 20
CEC0815M25 CUC0815M25 5g/25mL 20
C18, OCTADECYL 25
CEC181L1 CUC181L1 50mg/1ml 100 Application:
CEC18111 CUC18111 100mg/1ml 100 Removes large or more
CEC18113 CUC18113 100mg/3ml 50 hydrophobic compounds.
CEC18123 CUC18123 200mg/3ml 50
CEC18153 CUC18153 500mg/3ml 50
CEC18156 CUC18156 500mg/6ml 50
CEC181M6 CUC181M6 1g/6ml 30
CEC1811Z CUC1811Z 100mg/10ml 50
CEC1812Z CUC1812Z 200mg/10ml 50
CEC1815Z CUC1815Z 500mg/10ml 50
CEC1812M15 CUC1812M15 2g/15ml 20
CEC1815M25 CUC1815M25 5g/25ml 20
CEC18110M375 CUC18110M75 10g/75ml 10
C30, TRICONTYL
CEC30111 CUC30111 100mg/1mL 100 Application:
CEC30123 CUC30123 200mg/3mL 50 Removes large or more
CEC30156 CUC30156 500mg/6mL 50 hydrophobic compounds.
CEC301M6 CUC301M6 1g/6mL 30

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UCT
U
CL E A N - U P ®
CYCLOHEXYL
CECYH123 CUCYH123 200mg/3mL 50 Application:
CECYH153 CUCYH153 500mg/3mL 50 Scavenger for phenolic compounds.
CECYH1M6 CUCYH1M6 1g/6mL 30
CECYH12M15 CUCYH12M15 2g/15mL 20
PHENYL
26 CEPHY1L1 CUPHY1L1 50mg/1mL 100 Application:
CEPHY111 CUPHY111 100mg/1mL 100 Scavenger for polar compounds.
CEPHY123 CUPHY123 200mg/3mL 50

CEPHY1M6 CUPHY1M6 1g/6mL 30
CEPHY12Z CUPHY12Z 200mg/10mL 50
OTHER REVERSE PHASES AVAILABLE:
C2 ethyl Ct4 tertiary butyl C10 decyl

C3 propyl C5 pentyl C12 dodecyl
C4 n-butyl C6 hexyl C20 eicosyl
Ci4 isobutyl C7 heptyl

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U CLEAN-UP®
This sorbent is composed of a

silica backbone bonded with
carbon chains containing polar
functional groups. Groups which
will possess such polarity include
amines, hydroxyls and carbonyls.
HYDROPHILIC NORMAL PHASE EXTRACTION COLUMNS
Si
Example of a Hydrophilic Phase
O OH
Si O Si (CH2)3 O CH2
OH OH
CH CH2
27
O OH
Si
O OH OH OH
Si O Si (CH2)3 O CH2 CH CH2
O OH
Silica Backbone
Hydrophilic Chain
Analytes* Washes Elutions

R-OH, R-SH non-polar organic polar organic
R-NH2, solvents solvent
R2-NH, ie: hexane/ethyl acetate (80:20) usually with
R3-N methylene chloride some aqueous

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UCT
CLEAN-UP® HYDROPHILIC NORMAL PHASE EXTRACTION COLUMNS
Mechanism of
Hydrophilic Bonding Hydrophilic
Sorbents & Structures
Compounds are retained on hydrophilic
sorbents through polar interactions including Sorbent Structure
hydrogen bonding, pi-pi or dipole-dipole Silica -SiOH
interaction. These types of interactions
Diol -Si-(CH2)3OCH3CHOHCH2OH
occur when a distribution of electrons
Cyanopropyl -Si-(CH2)3CN
28
between individual atoms in functional
groups is unequal, causing negative and
positive polarity. Compounds typically

extracted on a hydrophilic column include Note: If un-ionized, ion exchange sorbents can
be used as hydrophilic (polar) sorbents.
analytes which have polar groups,
including amines, hydroxyls and carbonyls.
Elution is performed by strong polar solvents.
Example of Hydrophilic Bonding
O
+
H -
O C CH2 CH2
OH Compound
O-
H+
CH CH2
Sorbent

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CLEAN-UP ®
HYDROPHILIC EXTRACTION COLUMNS
UNBONDED SILICA (ACID WASHED)
Part Number Sorbent Amount/ Unit per 40-63 µm Particle Size

Endcapped Tube Volume Pack 60A Pore Size
CUSIL111 100mg/1mL 100 500m2/g Surface Area
CUSIL123 200mg/3mL 50
CUSIL153 500mg/3mL 50 Application:
CUSIL156 500mg/6mL 50 Removes hydrophilic (polar)
CUSIL1M6 1g/6mL 30 impurities, purification of
CUSIL11Z 100mg/10mL 50 hydrophilic (polar) compounds.
CUSIL12M15 2g/15mL 20
CUSIL15M25 5g/25mL 20
CUSIL110M75 10g/75mL 10
PHARMA-SIL®
Part Number Sorbent Amount/ Unit per 40-63 µm Particle Size 29
PHSIL1L1 50mg/1mL 100 525m2/g Surface Area
PHSIL123 200mg/3mL 50
PHSIL156 500mg/6mL 50 Application:
PHSIL1M6 1g/6mL 30 Removes hydrophilic (polar)
PHSIL12M15 2g/15mL 20 impurities, purification of
PHSIL15M25 5g/25mL 20 hydrophilic (polar) compounds.
HIGH SURFACE ACTIVITY SILICA
Part Number Sorbent Amount/ Unit per 40-63 µm Particle Size

HSSIL153 500mg/3mL 50 547m2/g Surface Area
HSSIL156 500mg/6mL 50
Application:
Removes hydrophilic (polar)
impurities, purification of
hydrophilic (polar) compounds.
FLORISIL®
Part Number Sorbent Amount/ Unit per % Organic Loading: N/A

Endcapped Tube Volume Pack
CUFLS111 100mg/1mL 100 Application:
CUFLS123 200mg/3mL 50 Removes polar-type compounds.
CUFLS153 500mg/3mL 50
CUFLS156 500mg/6mL 50 Florisil® products are
CUFLS1M6 1g/6mL 30 manufactured by
CUFLS11Z 100mg/10mL 50 U.S. Silica, Co.
CUFLS12Z 200mg/10mL 50
CUFLS15Z 500mg/10mL 50
CUFLS12M15 2g/15mL 20
CUFLS15M25 5g/25mL 20
CUFLS110M75 10g/75mL 10

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UCT
CL E A N - UP ®
ALUMINA, ACIDIC

CUALA111 100mg/1mL 100 Application:
CUALA123 200mg/3mL 50 Removes polar-type compounds.
CUALA153 500mg/3mL 50
CUALA156 500mg/6mL 50
CUALA1M6 1g/6mL 30
CUALA12M15 2g/15mL 20
30
ALUMINA, BASIC

CUALB123 200mg/3mL 50 Application:
CUALB153 500mg/3mL 50 Removes polar-type compounds.
CUALB156 500mg/6mL 50
CUALB1M6 1g/6mL 30
CUALB12Z 200mg/10mL 50
CUALB15Z 500mg/10mL 50
CUALB12M15 2g/15mL 20
CUALB15M25 5g/25mL 20
CUALB110M75 10g/75mL 10
ALUMINA, NEUTRAL

CUALN1L1 50mg/1mL 100 Application:
CUALN111 100mg/1mL 100 Removes polar-type compounds.
CUALN123 200mg/3mL 50
CUALN1M6 1g/6mL 30
CUALN12Z 200mg/10mL 50
CUALN15Z 500mg/10mL 50
CUALN12M15 2g/15mL 20
CUALN15M25 5g/25mL 20

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CLEAN- UP ®
CN, CYANOPROPYL
CECNP1L1 CUCNP1L1 50mg/1mL 100 Application:
CECNP111 CUCNP111 100mg/1mL 100 Removes steroid-type compounds.
CECNP123 CUCNP123 200mg/3mL 50
CECNP1M6 CUCNP1M6 1g/6mL 30
DIOL 31
% Organic Loading: 8.00
Endcapped Tube Volume Pack Application:
CUDOL111 100mg/1mL 100 Removes hydrophilic (polar)
CUDOL123 200mg/3mL 50 impurities, purification of
CUDOL153 500mg/3mL 50 hydrophilic (polar) compounds.
CUDOL156 500mg/6mL 50
CUDOL15Z 500mg/10mL 50
CUDOL12M15 2g/15mL 20
CARBON-GRAPHITIZED NON-POROUS, 120/400 MESH
Part Number Sorbent Amount/ Unit per CLEAN-UP Carbon

CUCARB1L1 50mg/1mL 100 Application:
CUCARB111 100mg/1mL 100 Carbon supports have been used to
CUCARB123 200mg/3mL 50 isolate extremely polar organic com-
CUCARB153 500mg/3mL 50 pounds. They work by a hydrophobic
CUCARB156 500mg/6mL 50 mechanism with a high surface area
CUCARB1M6 1g/6mL 30 and ion exchange. This interaction can
happen in a wide range of polar and
non-polar solvents.

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UCT
UCT
32
CLEAN-UP® ION EXCHANGE EXTRACTION COLUMNS
This sorbent is composed of a silica back-

bone bonded with a carbon chain terminated
by a negatively or positively charged functional
group. Ion exchange interactions occur be-
tween a sorbent that carries a charge and
a compound of opposite charge.
Si
Example of a Cation Exchange Phase
Si
Si
Example of a Anion Exhange Phase
O OH
Si O Si (CH 2) 3
O OH
NH 3 +
O OH O OH
Si O Si (CH 2)2 SO3- Si O Si (CH 2) 3 NH 3+
O OH O OH
Si
Silica Backbone
O OH
Anion Exchanger
Si O Si (CH 2)2 SO3-
O OH
This electrostatic interaction is reversible
by neutralizing the sorbent and /or analyte.
Silica Backbone Ion exchange bonds can also be disrupted
by introduction of a “counter ion” to com-
Anion Exchanger
pete with the analyte for binding sites on
the sorbent.
Anions Cations
Organic solvent or aqueous Organic solvent or aqueous

buffer at pH that allows the ion buffer at pH that would neutralize
to remain charged AND/OR at the ion AND/OR at a high
a low ionic strength AND/OR ionic strength AND/OR at a
at a weak concentration. strong concentration.

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MECHANISM OF ION EXCHANGE BON D I NG
Compounds are retained on the sorbent through ionic bonds. Therefore, it is essential that the sorbent and the
analyte to be extracted are charged. Generally, the number of molecules with charged cationic groups increases
at pH values below the molecules pKa value. The number of molecules with charged anionic groups decreases at
pH values below the molecule’s pKa value. To ensure 99% or more ionization, the pH should be at least two pH
units below the pKa of the cation and two pH units above the pKa of the anion. Elution occurs by using a solvent
to raise the pH above the pKa of the cationic group or to lower the pH below the pKa of the anion to disrupt
retention. At this point, the sorbent or compound will be neutralized.
ION EXCHANGE SORBENTS & STRUCTURE
Sorbent Structure pKa
Anion Exchangers
Aminopropyl (1º amine) -Si-(CH2)3NH3+ 9.8
N-2 Aminoethyl (1º & 2º amine) -Si-(CH2)3NH2+(CH2)2NH3+ 10.1, 10.9
Diethylamino (3º amine) -Si-(CH2)3NH+(CH2CH3)2 10.6
Quaternary Amine Chloride -Si-(CH2)3N+(CH3)3 Cl- always charged
Quaternary Amine Hydroxide -Si-(CH2)3N+(CH3)3 OH always charged
Quaternary Amine Acetate -Si-(CH2)3N+(CH3)3 CH3COO always charged
Quaternary Amine Formate -Si-(CH2)3N+(CH3)3 HCOO always charged 33
Polyimine -Si-(CH2)3R-[NHCH2CH2]X
Cation Exchangers
Carboxylic Acid -Si-CH2COOH 4.8
Propylsulfonic Acid -Si-(CH2)3SO3H <1
Benzenesulfonic Acid -Si-(CH2)2 SO3H always charged
Benzenesulfonic Acid High-Load -Si-(CH2)2 SO3H always charged
Triacetic Acid -Si-(CH2)3NH-(CH2)-N(CH2COOH)2
CH2COOH
NOTE: In an un-ionized state, these sorbents are hydrophilic (polar) sorbents.

NOTE: Neutralization can occur on either the sorbent or the analyte of
interest. Either will disrupt the bond of the desired compound.
Example of Anion Exchange Binding

O
-
CH2 NH3+ O C
Sorbent Compound
Example of Cation Exchange Binding
- +
SO3 H3 N
Sorbent Compound

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UCT
A MAP TO OPTIMIZING SAMPLE CLEAN UP
SAMPLE
NATURE
OF SAMPLE
GAS LIQUID SOLID
ANALYTE
CONFIGURATION
MOLECULAR
NATURE HYDROPHOBIC, LOG P > 2.5 HYDROPHILIC, LOG P < 2.5

OF ANALYTE
MATRIX AQUEOUS, BIOLOGICAL FLUIDS, BUFFERS NON POLAR ORGANIC
TYPE
34 NON POLAR, REVERSE PHASE EXTRACTION POLAR OR NORMAL PHASE EXTRACTION
OF EXTRACTION
INVOLVES VANDERWALLS/DISPERSION FORCES

BONDING INVOLVES HYDROGEN BONDING
INTERACTION BETWEEN SORBENT CH BONDS AND
MECHANISM
ANALYTE CH BONDS
π−π AND DIPOLE/DIPOLE INTERACTIONS
AMINES, HYDROXYLS, CARBONYLS,

TYPES PROTONATED/NEUTRAL STATE,
OF FUNCTIONAL AROMATIC RINGS, HETERO ATOMS (O, S,
AROMATICS, ALKYLCHAINS
GROUPS N, P)
ANALYTE
POLARITY LOG P > 3 LOG P < 2 ANALYTE CHARGE δ+ LOG P < 1 δ-
SORBENT C8 - C30 C2 - C7 CN, NH2, CARBON ALUMINA SILICA GEL

TYPE PS/DVD CYCLOHEXYL PSA, FLUOROSIL
PHENYL, DIOL
PI
ELUTION SOLVENT:
NON POLAR TO MODERATELY POLAR SOLVENTS MEDIUM TO HIGH POLARITY SOLVENTS
WATER/ACETONITRILE/METHANOL MIXES METHANOL/ETHYL ACETATE/ACETONE/THF
MIXES
TYPICAL APPLICATIONS:
LIPIDS, OIL ADDITIVES, CARBOHYDRATES, DRUGS OF ABUSE, PHARMACEUTICALS,
PHENOLS, OIL SOLUBLE VITAMINS, TDM, PESTICIDES
PESTICIDES, HERBICIDES
PARTITION COEFFICIENT
Po/w = (Coil /Cwater) EQUILIBRIUM. OIL IS USUALLY OCTANOL
LOG P SCALE
HYDROPHILIC (POLAR) < 1
UCT | MODERATELY
2731 Bartram Rd |POLAR 1-219007 | USA
Bristol, PA
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UCT HYDROPHOBIC
www.unitedchem.com
(NONPOLAR) >2
USING SOLID PHASE EXTRACTION
NATURE
OF SAMPLE
ANALYTE
IONIC CONFIGURATION
NATURE
MUST BE ABLE TO BE CHARGED OF ANALYTE
AQUEOUS OR ORGANIC MATRIX
TYPE
ION EXCHANGE OF EXTRACTION 35
BONDING
INVOLVES IONIC EXCHANGE
MECHANISM
ACIDS AND BASES TYPES

ANIONS: PHOSPHATES, CARBOXYLIC ACIDS,
OF FUNCTIONAL
SULFONIC ACIDS
GROUPS
CATIONS: AMINES, PURINES, PYRIMIDINES
ANIONS CATIONS ANALYTE

POLARITY
WEAK STRONG STRONG WEAK
QAX & NH 2, DEAE, CCX, TAX, & BCX, PCX & SORBENT
COPOLYMERS PSA, PI, & COPOLYMERS COPOLYMERS TYPE
COPOLYMERS
ELUTION SOLVENT:
ACIDIC ELUTION BASIC ELUTION
SOLVENT SOLVENT
TYPICAL APPLICATIONS:
ANY CHARGED COMPOUNDS
UCT, Inc.
2731 BARTRAM ROAD
BRISTOL, PA 19007
800-385-3153
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UCT
C L E A N - UP ®
ANION EXTRACTION COLUMNS
AMINOPROPYL
Part Number Sorbent Amount/ Unit per % Organic Loading: 6.65

Tube Volume Pack
CUNAX1L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.310
CUNAX111 100mg/1mL 100
CUNAX123 200mg/3mL 50 Application:
CUNAX153 500mg/3mL 50 Scavenger for acids, cyclic
CUNAX156 500mg/6mL 50 compounds, cholesterols, and other
CUNAX1M6 1g/6mL 30 lipid-type and compounds.
CUNAX11Z 100mg/10mL 50
CUNAX12M15 2g/15mL 20
CUNAX110M75 10g/75mL 10
36
PSA ( N-2 AMINOETHYL )

Tube Volume Pack

CUPSA1L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.320
CUPSA111 100mg/1mL 100
CUPSA123 200mg/3mL 50 Application:
CUPSA153 500mg/3mL 50 Scavenger for acids, cyclic
CUPSA156 500mg/6mL 50 compounds, cholesterols, and other
CUPSA1M6 1g/6mL 30 lipid-type and compounds.
CUPSA11Z 100mg/10mL 50
CUPSA110M75 10g/75mL 10
DIETHYLAMINO

Tube Volume Pack
CUDAX111 100mg/1mL 100 Exchange Capacity (meq/g): 0.320
CUDAX123 200mg/3mL 50
CUDAX153 500mg/3mL 50 Application:
CUDAX156 500mg/6mL 50 Scavenger for acids, cyclic
CUDAX12M15 2g/15mL 20 compounds, cholesterols, and other
CUDAX15M25 5g/25mL 20 lipid-type and compounds.

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CLEAN - UP ®
ANION EXTRACTION COLUMNS
QUATERNARY AMINE WITH CHLORIDE COUNTER ION

Tube Volume Pack
CUQAX1L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.250
CUQAX111 100mg/1mL 100
CUQAX123 200mg/3mL 50 Application:
CUQAX153 500mg/3mL 50 Scavenger for acids and sulfonyl
CUQAX156 500mg/6mL 50 chlorides, isocyanates and weak
CUQAX1M6 1g/6mL 30 electrophiles.
CUQAX12Z 200mg/10mL 50
CUQAX12M15 2g/15mL 20
QUATERNARY AMINE WITH ACETATE COUNTER ION
Part Number Sorbent Amount/ Unit per % Organic Loading: 8.40 37

Tube Volume Pack
CAQAX111 100mg/1mL 100 Exchange Capacity (meq/g): 0.250
CAQAX123 200mg/3mL 50
CAQAX1M6 1g/6mL 30 Application:
CAQAX15M25 5g/25mL 20 Scavenger for acids and sulfonyl
chlorides, isocyanates and weak
electrophiles. Useful when charge
on ion being removed is weaker than
the acetate counter ion.
QUATERNARY AMINE WITH HYDROXIDE COUNTER ION

Tube Volume Pack % Organic Loading: 8.40
CHQAX1L1 50mg/1mL 100
CHQAX111 100mg/1mL 100 Exchange Capacity (meq/g): 0.250
CHQAX123 200mg/3mL 50
CHQAX153 500mg/3mL 50 Application:
CHQAX156 500mg/6mL 50 Scavenger for acids and sulfonyl
CHQAX1M6 1g/6mL 30 chlorides, isocyanates and weak
CHQAX12Z 200mg/10mL 50 electrophiles. Useful when charge
CHQAX12M15 2g/15mL 20 on ion being removed is weaker than
CHQAX15M25 5g/25mL 20 the hydroxide counter ion.
POLYIMINE
% Organic Loading: 13.5
Tube Volume Pack
Exchange Capacity (meq/g): 0.88
CUPAX123 200mg/3mL 50
CUPAX153 500mg/3mL 50
Application:
CUPAX1M6 1g/6mL 30
Scavenger for acids and sulfonyl
chlorides, isocyanates and other
electrophiles.

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UCT
CLEAN-UP®
CATION EXTRACTION COLUMNS
CARBOXYLIC ACID

Tube Volume Pack
CUCCX1L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.170
CUCCX111 100mg/1mL 100
CUCCX123 200mg/3mL 50 Application:
CUCCX153 500mg/3mL 50 Scavenger for strong anions
CUCCX156 500mg/6mL 50 (Quaternary amines or metals)
CUCCX1M6 1g/6mL 30
CUCCX12Z 200mg/10mL 50
CUCCX12M15 2g/15mL 20
CUCCX15M25 5g/25mL 20
38 PROPYLSULFONIC ACID

Tube Volume Pack
CUPCX111 100mg/1mL 100 Exchange Capacity (meq/g): 0.180
CUPCX123 200mg/3mL 50
CUPCX153 500mg/3mL 50 Application:
CUPCX156 500mg/6mL 50 Scavenger for amines, alcohols and
CUPCX12Z 200mg/10mL 50 other nucleophiles.
CUPCX15Z 500mg/10mL 50
TRIACETIC ACID

Tube Volume Pack
CUTAX111 100mg/1mL 100 Exchange Capacity: Anion: 0.17
CUTAX123 200mg/3mL 50 Cation: 0.06
CUTAX153 500mg/3mL 50 Application:
CUTAX156 500mg/6mL 50 Chelator for metal ions.
CUTAX1M6 1g/6mL 30 i.e. tin
CUTAX110M75 10g/75mL 10 palladium
copper
ruthinium
chromium
nickel

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CLEAN - UP ®
CATION EXTRACTION COLUMNS
BENZENESULFONIC ACID

Tube Volume Pack
CUBCX1L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.320
CUBCX111 100mg/1mL 100
CUBCX123 200mg/3mL 50 Application:
CUBCX153 500mg/3mL 50 Scavenger for amines, alcohols and
CUBCX156 500mg/6mL 50 other nucleophiles.
CUBCX1M6 1g/6mL 30
CUBCX11Z 100mg/10mL 50
CUBCX12M15 2g/15mL 20
CUBCX110M75 10g/75mL 10
BENZENESULFONIC ACID - HIGH LOAD 39
Tube Volume Pack
CUBCX1HL1L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.320
CUBCX1HL11 100mg/1mL 100
CUBCX1HL23 200mg/3mL 50 Application:
CUBCX1HL53 500mg/3mL 50 Scavenger for amines, alcohols and
CUBCX1HL56 500mg/6mL 50 other nucleophiles.
CUBCX1HLM6 1g/6mL 30
CUBCX1HL1Z 100mg/10mL 50
CUBCX1HL2M15 2g/15mL 20

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UCT
UCT
40
CLEAN-UP® COPOLYMERIC EXTRACTION COLUMNS
This sorbent is composed of a silica back-

bone with two types of functional chains
attached - an ion exchanger or polar chain
and a hydrophobic carbon chain. Our
copolymeric phases are produced in a way
to allow for equal parts of each functional
group to attach to the silica backbone. This
Si
Example of a Copolymeric Phase
O OH
Si O Si (CH2)3 NH3+
copolymerization technique yields reproducible

bonded phases and unique copolymeric O OH
chemistries which allow the controlled use
of mixed mode separation mechanisms.This Si
type of dual chemistry is beneficial especially
when one is looking for both a neutral & O OH
charged compound. This is common when a Si O Si CnH2n+1
neutral parent drug metabolizes & becomes
a charged compound. O OH
Silica Backbone
Hydrophobic Chain
Ion Exchanger
Analytes Washes Elutions
Cations/Anions 1) Aqueous to disrupt 1) Organic, possibly with some

hydrophilic interactions. aqueous to elute hydrophobically
Alkanes bound analytes.
Alkenes 2) Methanol to disrupt residual
hydrophobic and hydrophilic 2) Aqueous buffer with a pH that
Aromatics interferences. would neutralize ionically bound
analytes or an aqueous with high
ionic strength or a solvent with a
counter ion that would bind
to sorbent.

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CLEAN - UP ®
COPOLYMERIC EXTRACTION COLUMNS
COPOLYMERIC SORBENTS & STRUCTURES
Sorbent Structure* pKa
Benzenesulfonic Acid (BCX2) -Si-(CH2)2 SO3H always charged

Strong Cation Exchange Column
Propylsulfonic Acid (PCX2) -Si-(CH2)3 SO3H <1

Strong Cation Exchange Column
Carboxylic Acid (CCX2) -Si-(CH2)2 COOH 4.8

Weak Cation Exchange Column
Quaternary amine (QAX2) -Si-(CH2)3 N+(CH3)3 always charged

Strong Anion Exchange Column
Aminopropyl (NAX2) -Si-(CH2)3 NH3 + 9.8

Weak Anion Exchange Column
41
Cyanopropyl (CNP2) -Si-(CH2)3CN
Hydrophilic Exchange Column
Cyclohexyl (CYH2) -Si-(CH2)

Hydrophobic Exchange Column
*Each copolymeric sorbent also contains a carbon chain approximately equal to a C8 chain
MECHANISM OF COPOLYMERIC BONDING
Using a sample composed of a theoretical neutral parent

drug and its charged (acidic) metabolite, it is applied
at a pH of 6 (figure 1). At this pH, many amine groups are Example of Copolymeric Bonding
positively charged. Since the column is also positively
charged, compounds with this chemistry (cations)
are repelled. Depending on the pKa of the metabolite, O
carboxylic acid groups may be negatively charged, allowing -
the metabolite to bond to the positively charged sorbent. (CH 2 )n NH 3+ O C
Since the column also possesses a hydrophobic chain,
the neutral parent drug also bonds to the column.
Water or a weak aqueous buffer (pH6) washes away

hydrophilically bound interferences (figure 2). The column
is then dried, careful to free the column of any residual
aqueous phase that would interfere with elution. Compounds
Sorbent

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UCT
Sample Application
-
O C
Sorbent
NH3+ Metabolite
figure 1
Sorbent
O
Parent Drug NH +
Sorbent
NH3+ NH +
Aqueous Buffer
O
-
Sorbent O C
Column Wash NH3 + Metabolite
42
figure 2
Sorbent
Hydrophilically
Bound
O Compounds
Parent Drug
OH
Sorbent
NH3 + HO
SH
Aqueous Buffer
O
-
Elution 1 Sorbent
NH3+
O C
figure 3
Sorbent
The hydrophobically bound neutral

Hexane / Ethyl
parent drug is eluted with a solvent of Acetate
80:20
minimal polarity, such as hexane/ethyl
Sorbent
acetate - 80:20. NH3+
Parent Drug
Sorbent
NH3+
Elution 2
figure 4
Sorbent
The final elution employs an acid to

neutralize the charge of acidic analytes.
O Strong Acidic
Ionic interaction is released, and analytes HO C Solution
Sorbent pH 2-3
are eluted in an appropriate solvent mixture. NH3+

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Metabolite
Anion Exchange Sorbent Cation Exchange Sorbent 43
Goal pH Goal pH
WASH To promote > analyte pKa To promote > analyte pKa

bonding between or bonding between or
sorbent and analyte < sorbent pKa sorbent and analyte < sorbent pKa
Elution To disrupt > analyte pKa To promote > analyte pKa

bonding between or bonding between or
sorbent and analyte < sorbent pKa sorbent and analyte < sorbent pKa
Percent of Compound in Ionic State
Functionality Ionization pH units away from pKa

2 < pKa 1 < pKa at pKa 1 > pKa 2 > pKa
Acid Anionic (-) 1 9 50 91 99
Base Cationic (+) 99 91 50 9 1

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UCT
CLEAN-UP®
HYDROPHOBIC PLUS CYCLOHEXYL

Tube Volume Pack
CUCYH256 500mg/6mL 50 Exchange Capacity (meq/g): N/A
CUCYH2M6 1g/6mL 30
Application:
Dual functionality for phenols and
HYDROPHOBIC PLUS PROPYLSULFONIC ACID

Tube Volume Pack
CUPCX2L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.114
CUPCX211 100mg/1mL 100
CUPCX223 200mg/3mL 50 Application:
CUPCX256 500mg/6mL 50 Dual functionality for weak bases
CUPCX22Z 200mg/10mL 50 and hydrophobic compounds.
44
HYDROPHOBIC PLUS CARBOXYLIC ACID

Tube Volume Pack
CUCCX2L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.105
CUCCX211 100mg/1mL 100
CUCCX223 200mg/3mL 50 Application:
CUCCX256 500mg/6mL 50 Dual functionality for strong base and
HYDROPHOBIC PLUS BENZENESULFONIC ACID

Tube Volume Pack
CUBCX2L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.072
CUBCX211 100mg/1mL 100
CUBCX223 200mg/3mL 50 Application:
CUBCX253 500mg/3mL 50 Dual functionality for strong base and
CUBCX256 500mg/6mL 50 hydrophobic compounds.
CUBCX2M6 1g/6mL 30
OCTADECYL PLUS BENZENESULFONIC ACID

Tube Volume Pack
CUBCX35Z 500mg/10mL 50 Exchange Capacity (meq/g): 0.072
CUBCX32M15 2g/15mL 20
Application:
Dual functionality for strong base and

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CLEAN - UP ®
HYDROPHOBIC PLUS QUATERNARY AMINE

Tube Volume Pack
CUQAX2L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.160
CUQAX211 100mg/1mL 100
CUQAX223 200mg/3mL 50 Application:
CUQAX253 500mg/3mL 50 Dual functionality for weak acids and
CUQAX256 500mg/6mL 50 hydrophobic compounds.
CUQAX2M6 1g/6mL 30
HYDROPHOBIC PLUS AMINOPROPYL 45
Tube Volume Pack
CUNAX2L1 50mg/1mL 100 Exchange Capacity (meq/g): 0.163
CUNAX211 100mg/1mL 100
CUNAX223 200mg/3mL 50 Application:
CUNAX253 500mg/3mL 50 Dual functionality for strong acids
CUNAX256 500mg/6mL 50 and hydrophobic compounds.
CUNAX2M6 1g/6mL 30
CUNAX210M75 10g/75mL 10

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UCT
C L E A N - UP ®
COVALENT EXTRACTION COLUMNS
COVALENT
Covalent sorbent has aldehyde functional groups that are bound to the silica
backbone by a hydrocarbon chain. The aldehyde group will react selectively
with compounds containing a primary amine. A formal bond is created
between the stationary support and the primary amine containing material.
MECHANISM OF COVALENT BONDING
The primary amine in the sample performs a nucleophilic attack on the aldehyde
functional group attached to the support. This results in a Schiff base, with the
amine immobilized on the stationary support. This chemistry can be utilized to
bind proteins, such as antibodies, to the support, allowing highly specific extractions.
THIOPROPYL
46

Tube Volume Pack

CUTHX1L1 50mg/1mL 100 Application:
CUTHX111 100mg/1mL 100 Scavenger for alkylating agents,
CUTHX123 200mg/3mL 50 alcohols and amines.
CUTHX153 500mg/3mL 50
CUTHX156 500mg/6mL 50
CUTHX1M6 1g/6mL 30
CUTHX11Z 100mg/10mL 50
CUTHX12M15 2g/15mL 20
CUTHX15M25 5g/25mL 20
CUTHX110M75 10g/75mL 10

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STYRE SCREEN ® POLYMERIC RESIN EXTRACTION COLUMNS
47

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UCT
S T Y R E S CR EEN ®
POLYMERIC RESIN EXTRACTION COLUMNS
Styre Screen® extraction columns contain an ultra clean, highly cross-linked styrene and divinylbenzene copolymer
sorbent that is functionalized with both a reverse phase, hydrophobic component and a strong cation exchanger.
High and reproducible recoveries for acidic, neutral and basic compounds are achievable with a single column. The
Styre Screen® particles have an average particle size of 30 microns and a very high analyte capacity making them ideal
for standard solid phase extraction applications. The increased analyte capacity means that less sorbent bed mass is
needed which results in faster flow rates and less solvent use. Higher throughput and less solvent waste disposal
translate into significant savings in both time and money. In addition, no conditioning steps are required for most
drugs of abuse applications.
DBX - BENZENESULFONIC ACID + C18
Part Number Sorbent Amount/ Unit per Application:

Tube Volume Pack Dual functionality for weak acids
SSDBX031 30mg/1mL 100 and hydrophobic compounds.
SSDBX033 30mg/3mL 50
SSDBX056 50mg/6mL 50
DVB - POLYSTYRENE DIVINYLBENZENE

48
Tube Volume Pack N/A
SSDVX031 30mg/1mL 100

BCX - ION EXCHANGE

Tube Volume Pack Scavenger for amines, alcohols
SSBCX031 30mg/1mL 100 and other nucleophiles.
SSBCX033 30mg/3mL 50
SSBCX056 50mg/6mL 50
C18 - REVERSE PHASE

Tube Volume Pack Removes hydrophobic impurities,
SSC18031 30mg/1mL 100 de-salting and purification of
SSC18033 30mg/3mL 50 hydrophobic compounds.
SSC18056 50mg/6mL 50
CCX - CARBOXYLIC ACID

Tube Volume Pack Scavenger for strong anions.
SSCCX031 30mg/1mL 100 (Quaternary amines or metals)
SSCCX033 30mg/3mL 50
SSCCX056 50mg/6mL 50
QAX - QUATERNARY AMINE

Tube Volume Pack Removes large or more
SSQAX031 30mg/1mL 100 hydrophobic compounds.
SSQAX033 30mg/3mL 50
SSQAX056 50mg/6mL 50

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
UCT understands that the optimum
sorbent for any given separation
cannot always be chosen empirically
and that the cost of purchasing
individual sorbents for screening
purposes can be prohibitive. We offer
UCT
SOLID PHASE EXTRACTION COLUMN METHOD DEVELOPMENT KITS
49
the following kits at prices designed
to reduce the cost of assay development:
• Non-Polar Phases
• Polar Phases
• Ion Exchange Phases
• Copolymeric Phases
• Pharmaceutical Phases
• Toxicology Phases

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UCT
S O L I D P H AS E EXTRACTION COLUMN
METHOD DEVELOPMENT KITS
NON-POLAR PHASES, ENDCAPPED
Part Number: MDK-NPE-I Total Number of Tubes: 140 7 packages / 10 each
CEC18111 CECn4111 CEC08111 This kit contains ten 100 mg/1 ml tubes of each of seven non-polar phases
CECYH111 CEPHY111 which include the endcapped hydrophobic phases, for C2, C4, C8, C18 and C30
CEC02111 CEC30111 along with cyclohexyl (CYH), and phenyl (PHY) phases.
POLAR PHASES
Part Number: MDK-PU-I Total Number of Tubes: 80 8 packages / 10 each
CEC02111 CUDOL111 CUPSA111 This kit contains ten 100 mg/1 ml tubes of each of eight phases with polar
CUCNP111 CUSIL111 CUDAX111 characteristics, including C2, cyanopropyl (CNP), diol (DOL), silica (SIL),
CECNP111 CUNAX111 primary amine (aminopropyl; NAX), secondary amine (aminoethyl; PSA),
tertiary amine (diethylamino; DAX).
50
COPOLYMERIC
Part Number: MDK-PU/1EX-11 Total Number of Tubes: 60 6 packages / 10 each
CUCNP211 CUCCX211 This kit contains ten 100 mg/1 ml tubes of each of six mixed mode phases containing a
CUNAX211 CUPCX211 non-polar and polar or ion exchange functionality. The non-polar functionality in each case
CUQAX211 CUBCX211 has an effective chain length of a C8. The polar or ion exchange functionality of each phase
consists of one of the following: cyanopropyl (CNP2), primary amine (aminopropyl; NAX2),
quaternary amine (QAX2), carboxylic acid (CCX2), propylsulfonic acid (PCX2), and
benzenesulfonic acid (BCX2).
ION EXCHANGE PHASES
Part Number: MDK-IEX-I Total Number of Tubes: 70 7 packages / 10 each
CUNAX111 CUCCX111 This kit contains ten 100 mg/1 mL tubes of each of seven ion exchange phases including
CUPSA111 CUPCX111 primary amine (aminopropyl; NAX), secondary amine (aminoethyl; PSA), tertiary amine
CUDAX111 CUBCX111 (diethylamino; DAX), quaternary amine (QAX), carboxylic acid (CCX), propylsulfonic acid
CUQAX111 (PCX), and benzenesulfonic acid (BCX) phases.
TOXICOLOGY PHASES
Part Number: MDK-TOX-111 Total Number of Tubes: 40 8 packages / 5 each
CSDAU203 CEC02123 This kit contains five 200 mg/3 ml tubes of each of eight phases. The two standard phases
CSTHC203 CEC08123 used for drugs of abuse testing are CSDAU and CSTHC. Other phases commonly used in
CUSIL123 CEC18123 toxicology are the polar and non-polar phases. The polar phases are unbonded silica and
CECNP123 CUC18123 cyanopropyl (CNP); the non-polar phases are endcapped, C2, C8, and both endcapped and
unendcapped C18.
PHARMACEUTICAL PHASES
Part Number: MDK-PHM-111 Total Number of Tubes: 40 8 packages / 5 each
CEC08123 CEC18123 This kit contains five 200 mg/3 ml tubes of each of eight phases that are most often selected
CUBCX223 CUCCX123 for pharmaceutical applications. Two copolymeric phases having the dual functionalities of
CUNAX223 CUQAX123 non-polar C8 and either benzenesulfonic acid (BCX) or aminopropyl (NAX). The remaining
CEC02123 CUCNP123 columns are phases which include three endcapped, hydrophobic phases (C2, C8, C18), two
ion exchange phases (CCX, QAX), and one polar phase (CNP).

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SELECTRASORB ™
BULK SORBENTS PACKING MATERIAL
51
COPOLYMERIC BONDED PHASES
FOR DRUG ABUSE TESTING
Description Part Number Sizes
CSDAU
CSDAU00X 10g
CSDAU00C 100g
CSDAU00K 1kg
CSTHC
CSTHC00X 10g
CSTHC00C 100g
CSTHC00K 1kg

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UCT
S E L E C T R A S ORB ™
BULK SORBENTS
HYDROPHOBIC HYDROPHILIC
Description Part Number Part Number Sizes Description Part Number Part Number Sizes
Endcapped Unendcapped Endcapped Unendcapped
C8, OCTYL CN,CYANOPROPYL

CEC0800X CUC0800X 10g CECNP00X CUCNP00X 10g
CEC0800C CUC0800C 100g CECNP00C CUCNP00C 100g
CEC0800K CUC0800K 1kg CECNP00K CUCNP00K 1kg
C18, OCTADECYL UNBONDED SILICA

40-63 µm CUSIL00X 10g
Tri-Functional CUSIL00C 100g
CEC1800X CUC1800X 10g CUSIL00K 1kg
CEC1800C CUC1800C 100g
CEC1800K CUC1800K 1kg PHARMA-SIL™
40-63 µm PHSIL00X 10g
PHSIL00C 100g
PHSIL00K 1kg
52 High Surface Activity Silica
40-63 µm HSSIL00X 10g
HSSIL00C 100g
COPOLYMERIC HSSIL00K 1kg
Description Part Number Part Number Sizes DIOL

Endcapped Unendcapped CUDOL00X 10g
CUDOL00C 100g
BENZENESULFONIC CUDOL00K 1kg
ACID + C8
CUBCX20X 10g FLORISIL
CUBCX20C 100g CUFLS00X 10g
CUBCX20K 1kg CUFLS00C 100g
CUFLS00K 1kg
CARBOXYLIC
ACID + C8 ALUMINA, ACIDIC
CUCCX20X 10g CUALA00X 10g
CUCCX20C 100g CUALA00C 100g
CUCCX20K 1kg CUALA00K 1kg
QUATERNARY ALUMINA, BASIC

ACID + C8 CUALB00X 10g
CUQAX20X 10g CUALB00C 100g
CUQAX20C 100g CUALB00K 1kg
CUQAX20K 1kg
ALUMINA, NEUTRAL
AMINOPROPYL CUALN00X 10g
+ C8 CUALN00C 100g
CUNAX20X 10g CUALN00K 1kg
CUNAX20C 100g
CUNAX20K 1kg

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SELECTRASOR B ™
BULK SORBENTS
ION EXCHANGE ( ANION ) ION EXCHANGE ( CATION )
Description Part Number Sizes Description Part Number Sizes
N-2 AMINOETHYL CARBOXYLIC ACID

CUPSA00X 10g CUCCX00X 10g
CUPSA00C 100g CUCCX00C 100g
CUPSA00K 1kg CUCCX00K 1kg
AMINOPROPYL PROPYLSULFONIC ACID

CUNAX00X 10g CUPCX00X 10g
CUNAX00C 100g CUPCX00C 100g
CUNAX00K 1kg CUPCX00K 1kg
DIETHYLAMINO BENZENESULFONIC ACID

CUDAX00X 10g CUBCX00X 10g
CUDAX00C 100g CUBCX00C 100g
CUDAX00K 1kg CUBCX00K 1kg
QUATERNARY AMINE BENZENESULFONIC ACID ( HIGH LOAD ) 53

with CHLORIDE CUBCX1HL00X 10g
COUNTER ION CUBCX1HL00C 100g
CUQAX00X 10g CUBCX1HL00K 1kg
CUQAX00C 100g
CUQAX00K 1kg TRI-ACETIC ACID
CUTAX00X 10g
QUATERNARY AMINE CUTAX00C 100g
with ACETATE CUTAX00K 1kg
COUNTER ION
CAQAX00X 10g
CAQAX00C 100g STYRE SCREEN®
CAQAX00K 1kg
Description Part Number Sizes
QUATERNARY AMINE
with HYDROXIDE
COUNTER ION DBX-BENZENESULFONIC ACID + C8
CHQAX00X 10g SSDBX00X 10g
CHQAX00C 100g SSDBX00C 100g
CHQAX00K 1kg
POLYIMINE DVB POLSTYRENE DIVINYLBENZENE

CUPAX00X 10g SSDVB00X 10g
CUPAX00C 100g SSDVB00C 100g
CUPAX00K 1kg
C18 REVEERSE PHASE OCTADECYL

SSC1800X 10g
SSC1800C 100g
BCX-BENZENESULFONIC ACID
SSBCX00X 10g
SSBCX00C 100g
QAX QUATERNARY AMINE

SSQAX00X 10g
SSQAX00C 100g

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UCT
R E S E R V OIRS
EMPTY POLYPROPYLENE RESERVIORS
Part Number Description

Empty Reservoirs Standard Configuration Units
RFV0001P 1 mL capacity 50
FLANGELESS RESERVOIRS
Part Number Description Units

54 RFT00R3P Empty Flangeless Tube, 50
4 mL capacity
RFT01FR3P Empty Flangeless Tube, 50

1 Frit (Filter Tube)
4 mL capacity
GLASS RESERVOIRS
Part Tube Frit Tube

Number Volume Description Description Units
RFV0008G 6 mL No Frits Empty Glass Tube 30
RFV01F8G 6 mL 1 Tefton Frit Inserted Glass Tube 30
FR10081T 6 mL Tefton Frit Only None 60
CARTRIDGES

Empty Reservoirs Standard Configuration Units
RFTO2FLC Large cartridges w/cap, 1 Frit Loose, 1 Frit Inserted 50
RFTO2FMC Medium cartridges w/cap, 1 Frit Loose, 1 Frit Inserted 50
RFTO2FSC Small cartridges w/cap, 1 Frit Loose, 1 Frit Inserted 50

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RESERVOI R S
55
FRITTED POLYPROPYLENE RESERVIORS
Part Number Part Number
Fritted Reservoirs Fritted Reservoirs Description
1 Frit, 10 Micron Porosity 2 Frits, 10 Micron Porosity Standard Configuration Units
RFV01F1P RFV02F1P 1 mL capacity 50
Part Number Part Number

Fritted Reservoirs Fritted Reservoirs Description
1 Frit, 20 Micron Porosity 2 Frits, 20 Micron Porosity Standard Configuration Units
RFT01F1P RFT02F1P 1 mL capacity 50

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UCT
FRITS
56
POROUS POLYPROPYLENE FRITS

10 Micron Porosity (1/16” thickness) Standard Configuration Units
FR10011P 1 mL capacity 100


FT20011P 1 mL capacity 100
TEFLON FRITS
Part Number Description Units

FR10081T 6 mL capacity 60
FR10041T 3 mL capacity 60

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
S OLID PHASE EXTRACTION ACCESSORIE S
STOPCOCK VALVES
Quantity Part Number

16 VMF02116
24 VMF02024
Solvent resistant, reusable luer fitted valves to be used in conjunction with

a vacuum manifold. Provides individual flow control to each SPE reservoir.
ADAPTERS

15 AD0000AS
Adapter cap has a tapered fit for 1, 3 and 6mL size reservoirs with a standard luer
fitting on top. These adapters are ideal when a sample volume exceeds the
capacity of the SPE column or when sequential extractions are desired.
57
FLANGE CAPS
Part Number Cap Volume Quantity

CR00011P 1 mL 50
CR00013P 3 mL 50
CR00018P 6 mL 50
CR00015P 15 mL 50
CR00025P 25 mL 50
Inlet caps plug the top of SPE tubes.
MALE LUER CAPS

50 LUER50
Fits a standard luer, for all reservoir sizes.
CLEAN-THRU® TIPS

50 CLTTP050
Eliminates sample carry over from the vacuum manifold lid. Tips connect to
the luer tip on the SPE reservoir and are passed through the manifold, directly
into the waste or collection vessel. They provide a completely disposable system
that eliminates any contact between the sample, or wash solvents and the
extraction apparatus.

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UCT
UCT
58
POSITIVE PRESSURE MANIFOLD
Features:
• All 48 positions are individually regulated to provide
even pressure to each column
• 4 banks of 12 positions. Individual flow indicator on

each bank. Pressure always provided to bank 1.
Pressure supply to banks 2-4 individually controlled
• Capacity 1 to 48 columns of either 1mL, 3mL , 6mL,

10mL or 15mL
• Air supply: N2 or compressed air 75psi (must be

filtered to 10 µm)
• Dual pressure regulators allow users to set 2 different

pressures for extraction and column drying
• Includes waste reservoir that can be emptied between

each waste step if desired
• Single switch raises and lowers the sample racks and

creates an airtight seal
POSITIVE PRESSURE MANIFOLD ACCESSORIES
Part Number Description Unit

VMFPPMRK10 10 mL & 15 mL SPE rack. 1
VMFPPMRKA1 Adapter extraction plates for 1 mL columns. 1
VMFPPMIK Installation kit (contains 25 ft ¼” O.D. tubing, in line air filter, 1
2 - ¼” compression fittings, one (1) set of gaskets.)
VMFPPMCRKG13 Collection rack for 13 x 10 mm test tubes 1

VMFPPMCRKG16 Collection rack for 16 x 10 mm test tubes 1
VMFPPMWRK Waste rack 1
VMFPPMWBN Waste container (pre-drilled for optional tubing attachment.) 1
VMFPPRAF Replacement in line air filter. 1
VMFPPMGSKBL Brown PPM Gasket 1
VMFPPMGSKOR Orange PPM Gasket 1
VMFPPMLPLT Lift Plate 1

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
Collection rack for Collection rack for Pre-drilled waste PPM Waste tray draining
13 x 100mm test tubes 16 x 100mm test tubes container kit; 10 ft tube and stopcock
Part#: VMFPPMCRKG13 Part#: VMFPPMCRKG16 Part#: VMFPPMWBN Part#: VMFPPMWTDK
59
Adaptor extraction Adaptor extraction Adaptor extraction plates 10mL /15mL
plates for 1mL columns plates for 3mL columns for 6mL columns extraction plates
Part#: VMFPPMRKA1 Part#: VMFPPMRKA3 Part#: VMFPPMRKA6 Part#: VMFPPMRK10
Brown PPM Gasket Orange PPM Gasket Restrictor Plate

Part#: VMFPPMGSKBL Part#: VMFPPMGSKOR Part#: VMFPPMFRPLT
UCT Installation kit (contains

25’1/4” O.D. tubing,
in line air filter, 2-1/4”
compression fittings,
one (1) set of gaskets
Part#:
UCT | 2731VMFPPMIK
In-line air filter
Part#: VMFPPMRAF
Bartram Rd | Bristol, PA 19007 | USA

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UCT
U N I V E R S A L VAC UUM MANIFOLD
UNIVERSAL VACUUM MANIFOLD

COMPLETE SYSTEM
Part Number: VMFUVWP

• A manifold system that accommodates a 24, 48 and
96 well plate configuration.
• System includes collection plate, extraction plate, manifold
and vacuum gauge waste base.
• Extraction and collection plates for 24 well and 48 well
configurations are included.
• Erlenmeyer flask and tubing are included.
60
24 WELL PLATE MANIFOLD SYSTEM
Part Number: VMF24WP

• System includes 24 well collection plate, extraction plate, manifold and
vacuum gauge waste base.
• Extraction plate can accomodate (24) 6 mL SPE columns.
• UCT SPE columns can be packed in 500 mg,1 and 2 gram formats.
• Collection plate will accomodate 16x100mm and 16x125mm test tubes.
48 WELL PLATE MANIFOLD SYSTEM

• System includes 48 well collection plate, extraction plate, manifold and vacuum
gauge waste base.
• Extraction plate can accomodate (48) 4.5 mL SPE columns in a staggered array.
• Elute samples directly into 12 x 75 mm test tube or 2 mL analytical vials.
96 DEEP WELL PLATE MANIFOLD SYSTEM

• System includes manifold and vacuum gauge waste base.
• Well plates are separate and not included with system.
• Accomodates most standard 96 well plates.
• Collect directly into microplate.

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
UNIVERSAL MANIFOLD ACCESSOR I E S
Description: 24 Well Extraction Plate Description: 24 Well Collection Plate

Part Number: VMF24EP Part Number: VMF24CP
Unit: 1 Unit: 1
Description: 48 Well Extraction Plate Description: 48 Well Collection Plate

Part Number: VMF48EP Part Number: VMF48CP
Unit: 1 Unit: 1
Description: Manifold Top Description: Neoprene Gasket

Part Number: VMFUVMT Part Number: VMFUVNG
Unit: 1 Unit: 1
61
Description: Manifold Base Description: EPDM Gasket
Part Number: VMFUVMB Part Number: VMFUVEG
Unit: 1 Unit: 1
Description: Spacer 1/2’’ Description: Spacer 1’’

Part Number: VMFUV05SP Part Number: VMFUV10SP
Unit: 1 Unit: 1
Description: Collection Plate Riser Description: Spigot

Part Number: VMFUVR1 Part Number: VMFUVST
Unit: 1 Unit: 1
Description: Description:
Vacuum Base & Waste Gauge Vacuum Pump
Part Number: VMFUVVGWB Part Number: ECROCKER400
Unit: 1 Unit: 1

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
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UCT
VACUUM MANIFOLD 16 POSITION SYSTEM
62

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
VACUUM MANIFOLD
Our vacuum Manifold System consists of a rigid

Corian ® lid which resists warping with extended
use. The lid is outfitted with bulkhead luer fit-
tings to allow for sample to elute directly into
disposable test tubes. The lid is available with 16
or 24 positions, consisting of two parallel rows
and corner leg supports to prevent damage
to the luers and tips when the lid is not be-
ing used. The vacuum chamber is a glass block
designed to allow for visible inspection of the
extraction process and ease when cleaning. The
block is equipped with a vacuum control valve
for optimizing sample flow rate during the ex-
traction process.
A vacuum gauge and bleed valve allows for easy

monitoring of the vacuum process. Polypropylene
racks are provided according to the number of These manifold systems are durable and chemi-
positions on the manifold lid and are highly cally resistant units designed to provide years of 63
resistant to chemical degradation and abuse. trouble-free extractions. A safety tray comes as
The test tube racks provided allow the use of part of the complete manifold system, so as to
12-13 mm or 16 mm disposable test tubes. prevent the glass block from cracking or chipping.
VACUUM MANIFOLD ACCESSORIES
Description Units Part Number 16 Position System Part Number 24 Position System
Glass Block 1 VMF06123 VMF04123
Manifold Lid 1 VMF06120 VMF04120
Gasket 2 VMF06121 VMF04121
Collection Rack 1 VMF06125 VMF04125
Description Units Part Number for 16 or 24 Position

Vacuum Gauge & Valve Assembly 1 VMF02122
Retaining Clips for Collection Rack 12 VMF02129
Bulkhead Luer Fittings 12 VMF21BFN
Manifold Lid Legs 4 VMF02120-1
Luer Plugs 12 VMF21PLN
Luer Caps 50 LUER50
Clean-Thru® Tips 50 CLTTP050
Teflon Luer Tips 12 VMF020TT
Manifold Safety Tray 1 VMF02072
Stopcocks 16 VMF02116
24 VMF02024
Vacuum Pump 1 ECROCKER400

- 1/8 hp, 115 volts, 4.2 amps, 60 Hz
NOTE: A Complete Vacuum Manifold System includes a glass block, Corian® manifold lid, a cover gasket, a vacuum gauge and valve
assembly, teflon tips (16 or 24), an adjustable collection rack, bulkhead luer fittings, plugs (16 or 24), and a glass block safety tray.
P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
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UCT
S E L E C T R A -S IL ®
DERIVATIZING REAGENTS
64
BENEFITS OF DERIVATIZATION
• Improved chromatographic resolution - increased volatility - reduced intermolecular hydrogen bonding - separation of structurally
similar compounds.
• Improved mass spectral characteristics - higher mass fragments - greater S/N (signal to noise ratio) - more unique masses-
increased abundance/sensitivity of molecular ions.
• Improved thermal stability of some compounds - reduced thermal degradation - higher temperatures to speed analysis.
• Increased instrument and lab productivity - fewer reinjections or repeats due to peak tailing - high confidence in analyte identification
and quantitation - easy to perform - inert by-products of derivatization will not degrade capillary column performance.
PRODUCT RECOMMENDATIONS
Derivatizing reagents are sold bottled in airtight septum vials blanketed with nitrogen to maintain their activity. Contact with
moisture can greatly reduce reactivity. Protect from air and moisture. Keep bottle tightly sealed when not in use.
It is critical that pipettes, glassware, vials, etc. be free of water or alcohol before derivatization.

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
SELECTRA - S I L ®
SILYLATION REAGENTS
Silyl derivatives are the most widely used chemical derivatization reagents, especially for
gas chromatography. Silyl derivatization requires an “Active” hydrogen as seen in acids,
alcohols, thiols, amines, amides, enolizable ketones and aldehydes to be replaced by a
trimethysilyl group or tertiary butyl dimethylsilyl.
BSTFA N,O-bis(Trimethylsilyl)trifluoroacetamide
Part Number Quantity Units per pack

SBSTFA-0-1 1 gm vial 10 • Trimethylsilyl donor strength equal to BSA.
SBSTFA-0-10 10 gm vial 1 • Reacts with the same classes of compounds as BSA
SBSTFA-0-25 25 gm vial 1 producing the same derivatives.
SBSTFA-0-100 100 gm vial 1 • Increased volatility of the reaction by-products over the
non-fluorinated derivatives of BSA.
BSTFA W/1% TMCS N,O-bis(Trimethylsilyl)trifluoroacetamide w/1% Trimethylchlorosilane 65
SBSTFA-1-1 1 gm vial 10 • Trimethylsilyl donor strength equal to BSA.
SBSTFA-1-10 10 gm vial 1 • Reacts with the same classes of compounds as BSA. producing
SBSTFA-1-25 25 gm vial 1 the same derivatives.
SBSTFA-1-100 100 gm vial 1 • TMCS (Trimethylchlorosilane) added to derivatize amides, many
secondary amines and hindered hydroxyls that are not reactive to
BSTFA alone.
• Increased volatility of the reaction by-products over the
BSTFA W/10% TMCS N,O-bis(Trimethylsilyl)trifluoroacetamide w/10% Trimethylchlorosilane
Part Number Quantity Units per pack • Trimethylsilyl donor strength equal to BSA.
SBSTFA-10-1 1 gm vial 10 • Reacts with the same classes of compounds as BSA. producing
SBSTFA-10-10 10 gm vial 1 the same derivatives.
SBSTFA-10-25 25 gm vial 1 • TMCS (Trimethylchlorosilane) added to derivatize amides, many
SBSTFA-10-100 100 gm vial 1 secondary amines and hindered hydroxyls that are not reactive to
BSTFA alone.
• Increased volatility of the reaction by-products over the
MSTFA N-Methyl-N-trimethylsilyltrifluoroacetamide

SMSTFA-0-1 1 gm vial 10 • A trimethylsilyl adduct with donor strength equal to BSA and BSTFA.
SMSTFA-0-10 10 gm vial 1 • Most volatile of the TMS derivatives.
SMSTFA-0-25 25 gm vial 1 • Often elutes at the solvent front of the GC.
SMSTFA-0-100 100 gm vial 1
MSTFA W/1% TMCS N-Methyl-N-trimethylsilyltrifluoroacetamide w/1% trimethylchlorosilane

SMSTFA-1-1 1 gm vial 10 • A trimethylsilyl adduct with donor strength equal to BSA and BSTFA.
SMSTFA-1-10 10 gm vial 1 • Most volatile of the TMS derivatives.
SMSTFA-1-25 25 gm vial 1 • Often elutes at the solvent front of the GC.
SMSTFA-1-100 100 gm vial 1 • Addition of TMCS aids in the derivatization of amides,
secondary amines and hindered Hydroxy groups.

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UCT
SEL E C T R A -S IL ®
SILYLATION REAGENTS
MTBSTFA N-Methyl-N-(tert-butyldimethylsilyl) trifluoroacetamide

SMTBSTFA-0-1 1 gm vial 10 • Derivatizes hydroxyl, carboxyl, thiol and primary and secondary amines.
SMTBSTFA-0-10 10 gm vial 1 • Derivatives are more stable than TMS derivatives to hydrolysis.
SMTBSTFA-0-25 25 gm vial 1 • Reaction by-products are neutral and volatile.
SMTBSTFA-0-100 100 gm vial 1
MTBSTFA W/1% TBDMCS N-Methyl-N-(tert-butyldimethylsilyl) trifluoroacetamide w/ 1% tert-butyldimethylchlorosilane

SMTBSTFA-1-10 10 gm vial 1 • Addition of TBDMCS (tertiary butyl-dimethylchlorosilane) increases the
SMTBSTFA-1-25 25 gm vial 1 silylation ability of this reagent to derivatize hindered alcohols and amines.
SMTBSTFA-1-100 100 gm vial 1 • Derivatives are more stable than TMS derivatives to hydrolysis.
• Reaction by-products are neutral and volatile.
66
MTBSTFA W/10% TBDMCS N-Methyl-N-(tert-butyldimethylsilyl) trifluoroacetamide

SMTBSTFA-10-1 1 gm vial 10
SMTBSTFA-10-25 25 gm vial 1 • Addition of TBDMCS (tertiary butyl-dimethylchlorosilane) increases the
SMTBSTFA-10-100 100 gm vial 1 silylation ability of this reagent to derivatize hindered alcohols and amines.
• Derivatives are more stable than TMS derivatives to hydrolysis.
• Reaction by-products are neutral and volatile.
MTBSTFA W/10% TBDMCS Trimethylchlorosilane

STMCS-0-1 1 gm vial 10 • Catalysts used to increase the reactivity of other silylation reagents.
STMCS-0-10 10 gm vial 1 • Used to form trimethysilyl esters of organic acids.
STMCS-0-25 25 gm vial 1
STMCS-0-100 100 gm vial 1
SELECTRA-SIL® SOLVENTS FOR DERIVATIZING REAGENTS

Solvent Part Number Size Units
Acetonitrile (ACN) SACN-0-50 50 mL vial 1
Pyridine SPYR-0-50 50 mL vial 1

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
SELECTRA - S I L ®
ALKYLATION REAGENTS
Silyl derivatives are the most widely used chemical derivatization reagents, especially for
gas chromatography. Silyl derivatization requires an “Active” hydrogen as seen in acids,
alcohols, thiols, amines, amides, enolizable ketones and aldehydes to be replaced by a
trimethysilyl group or tertiary butyl dimethylsilyl.
TMPAH 0.2M Trimethylanilium hydroxide in Methanol

STMPAH-0-1 1 gm vial 10 • Used for the methylation of barbiturates, sedatives,
STMPAH-0-10 10 gm vial 1 xanthines,and alkaloids by GC.
STMPAH-0-25 25 gm vial 1 • The derivatization of these compounds often can
STMPAH-0-100 100 gm vial 1 be done in the injector of the GC.
4 CB 4-Carbethoxyhexafluorobutyrl Chloride 67
S4CB-0-1 1 gm vial 10 • Peptides + Propionic anhydride converts N-termini and Lysines
S4CB-0-10 10 gm vial 1 to propyl amides. This results in a decrease in net charge of the
S4CB-0-25 25 gm vial 1 peptides and increased hydrophobicity.
SELECTRA-SIL® SPECIALIZED REAGENTS
PFPOH Pentafluoropropanol
Part Number Quantity Units per pack • Used in combination with the acid anhydrides to add more
SPFPOH-0-1 1 gm vial 10 fluorine atoms to the parent molecule.
SPFPOH-0-10 10 gm vial 1 • This reaction is especially used for carboxylic acids.
SPFPOH-0-25 25 gm vial 1 • The addition of fluorine atoms into the molecule greatly
SPFPOH-0-100 100 gm vial 1 adds to the sensitivity of certain detectors (i. e. ECD, MS).
HFIP Hexafluoro-2-propanol

SHFIP-0-1 1 gm vial 10 • Used in combination with the acid anhydrides to add
SHFIP-0-10 10 gm vial 1 more fluorine atoms to the parent molecule.
SHFIP-0-25 25 gm vial 1 • This reaction is especially used for carboxylic acids.
SHFIP-0-100 100 gm vial 1 • The addition of fluorine atoms into the molecule greatly
adds to the sensitivity of certain detectors (i. e. ECD, MS)

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UCT
SEL E C T R A -S IL ®
ACYLATION REAGENTS
MBTFA N-methyl-bis-trifluoroacetamide

SMBTFA-0-1 1 gm vial 10 • This reacts with primary and secondary amines,
SMBTFA-0-10 10 gm vial 1 hydroxyl and thiol groups under mild, nonacidic conditions.
SMBTFA-0-25 25 gm vial 1 • Produces very volatile derivatives of carbohydrates.
SMBTFA-0-100 100 gm vial 1 • Can be used to selectively acylate amines in the presence of hydroxyl
and carboxyl groups that have been protected by silylation.
TFAA Trifluoroacetic acid anhydride

STFAA-0-1 1 gm vial 10 • Reacts readily with alcohols, phenols and amines producing
STFAA-0-10 10 gm vial 1 stable volatile derivatives for TCD, FID, ECD and other
STFAA-0-25 25 gm vial 1 detectors. Most reactive of all the perfluoroacid anhydrides
STFAA-0-100 1 00 gm vial 1 and frequently used to identify methamphetamine.
68
PFAA Pentafluoropropionic acid anhydride

SPFAA-0-1 1 gm vial 10 • Reacts readily with alcohols, phenols and amines producing
SPFAA-0-10 10 gm vial 1 stable volatile derivatives for TCD, FID. Commonly used in
SPFAA-0-25 25 gm vial 1 the determination of Benzoylecgonine and Opiates.
SPFAA-0-100 100 gm vial 1 • Acidic by-products of this reaction must be removed before
the derivative can be injected onto the GC.
HFAA Heptafluorobutyric acid anhydride

SHFAA-0-1 1 gm vial 10 • Reacts readily with alcohols, phenols and amines producing
SHFAA-0-10 10 gm vial 1 stable volatile derivatives for TCD, FID,ECD and other detectors.
SHFAA-0-25 25 gm vial 1 • Used in the determination of Amphetamines and Phencyclidine.
SHFAA-0-100 100 gm vial 1 • It is suggested that amine bases (such as triethylamine) be used to
react with the acidic by-products of these to drive the reaction
to completion.
TFAI - N-Trifluoroacetylimidazole

STFAI-0-1 1 gm vial 10 • Reacts readily with alcohols, phenols and amines producing stable
STFAI-0-5 5 gm vial 1 volatile derivatives for TCD, FID, ECD and other detectors.
• Offer considerable advantages over the anhydrides for the
preparation of perfluoroacyl derivatives; the reactions are
smooth, quantitative and produce no acid byproducts.
• Principal byproduct is imidazole (relatively inert).
PIA Propionic Anhydride

SPIA-0-1 1 gm vial 10

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GC LINERS
69

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UCT
G C L I N E RS
Description Instrument / Liner Part Number Part Number Quantity
GCL2MM 1 Pack
2mm Straight Splitless
Agilent GCL2MM-5 5 Pack
2.0mm ID x 6.5mm OD x 78.5mm 5181-8818 GCL2MM-25 25 Pack
GCL2MMGW 1 Pack
Agilent GCL2MMGW-5 5 Pack
2mm Straight Splitless with Deactivated Glass Wool 5181-8818 GCL2MMGW-25 25 Pack
2.0mm ID x 6.5mm OD x 78.5mm
GCLGN2MM 1 Pack
Agilent GCLGN2MM-5 5 Pack
2mm Splitless Gooseneck
2.0mm ID x 6.5mm OD x 78.5mm GCLGN2MM-25 25 Pack
GCLGN2MMGW 1 Pack
Agilent GCLGN2MMGW-5 5 Pack
2mm Splitless Gooseneck with Deactived Glass Wool
2.0mm ID x 6.5mm OD x 78.5mm GCLGN2MMGW-25 25 Pack
70
GCL4MM 1 Pack
Agilent GCL4MM-5 5 Pack

4mm Straight Splitless
4.0mm ID x 6.5mm OD x 78.5mm 210-3003 GCL4MM-25 25 Pack
GCL4MMGW 1 Pack
4mm Straight Splitless with Deactivated Glass Wool Agilent GCL4MMGW-5 5 Pack
4.0mm ID x 6.5mm OD x 78.5mm 19251-60540 GCL4MMGW-25 25 Pack
GCLRG4MM 1 Pack
4mm Splitless Recessed Gooseneck Agilent GCLRG4MM-5 5 Pack
4.0mm ID x 6.5mm OD x 78.5mm GCLRG4MM-25 25 Pack
GCLRG4MMGW 1 Pack
4mm Splitless Recessed Gooseneck with Deactived Glass Wool Agilent GCLRG4MMGW-5 5 Pack
4.0mm ID x 6.5mm OD x 78.5mm GCLRG4MMGW-25 5 Pack
GCLGN4MM 1 Pack
4mm Splitless Gooseneck Agilent GCLGN4MM-5 5 Pack
4.0mm ID x 6.5mm OD x 78.5mm 5181-3316 GCLGN4MM-25 25 Pack
GCLGN4MMGW 1 Pack
4mm Splitless Gooseneck with Deactived Glass Wool
Agilent GCLGN4MMGW-5 5 Pack
4.0mm ID x 6.5mm OD x 78.5mm 5062-3587 GCLGN4MMGW-25 25 Pack
GCLUN4MM 1 Pack
4mm Straight Splitless Open Top Uniliner Perkin-Elmer GCLUN4MM-5 5 Pack
4.0mm ID x 6.2mm OD x 92.1mm GCLUN4MM-25 25 Pack
GCLUN4MMGW 1 Pack
Perkin-Elmer GCLUN4MMGW-5 5 Pack
4mm Straight Splitless Open Top Uniliner
with Deactived Glass Wool GCLUN4MMGW-25 25 Pack
4.0mm ID x 6.2mm OD x 92.1mm

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
SELECTRA® HPLC COLUMNS
HPLC COLUMN

SLPHY100ID21 Phenyl HPLC Column - 100 x 2.1 1
SLPHY50ID21 Phenyl HPLC Column - 2.1mm x 50mm 1
GUARD COLUMN

SLPHYGDC Phenyl HPLC Guard Column 1
9 6 D E E P WELL P LATES
IDEAL FOR ALL SPE APPLICATIONS AND HIGH THROUGHPUT SCREENING
Our 96 Deep Well Plates are made from solvent resistant,

low extractable polypropylene. Standard frits are polyethyl-
ene with 20µ pores.
96 DEEP WELL FILTER PLATES

Description Part Number Units
72 Empty 96 deep well plate with one frits inserted WSH961FR 1
Loose 96 deep well plate square frits FRSH2096P 96
96 well collection plate WSH96CP 1
96 well plate sealable lid WSH96PS 1
Sorbent Part Numbers Sorbent Amount Sorbent Part Numbers Sorbent Amount
per Well, mg per Well, mg
Endcapped C18 Endcapped C2
WSHCEC18105 50 WSHCEC02105 50
Endcapped C8 Cyclohexyl
WSHCEC08105 50 WSHCYH105 50
Endcapped C4 Phenyl
WSHCEC04105 50 WSHPHY105 50

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
96 DEEP WELL PL AT E S
NORMAL PHASE (HYDROPHILIC) ION EXCHANGE (ANION)
Silica Aminopropyl
WSHSIL105 50 WSHNAX105 50
Pharma-Sil® PSA ( N-2 Aminoethyl )
WSHPHSIL105 50 WSHPSA105 50
High Surface Activity Silica Diethylamino
WSHHSSIL105 50 WSHDAX105 50
73
Diol Quaternary Amine
WSHDOL105 50 WSHQAX105 50
Cyanopropyl Polyimine
WSHCNP105 50 WSHPAX105 50
Florisil® 60-100 mesh
WSHFLS05 50 ION EXCHANGE (CATION)
WSHFLS11 100
WSHFLS12 200 Sorbent Part Numbers Sorbent Amount
WSHFLS13 300 per Well, mg
Florisil® 100-200 mesh, Grade A Benzenesulfonic Acid
WSHFLSA05 50 WSHBCX105 50
Alumina, Acidic Benzenesulfonic Acid High Load
WSHALA05 50 WSHBCX1HL105 50
Alumina, Neutral Carboxylic Acid
WSHALN05 50 WSHCCX105 50
Alumina, Basic Propylsulfonic Acid
WSHALB05 50 WSHPCX105 50
Tri-Acetic Acid
WSHTAX105 50
WSHTAX11 100
WSHTAX12 200
WSHTAX13 300

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UCT
9 6 D E E P WELL PLATES
COPOLYMERIC (MULTIFUNCTIONAL PHASES) POLYMERIC RESIN
Aminopropyl DBX Benzenesulfonic
+ C8 Acid + C8
WSHNAX205 50 WSHDBX403 30
WSHNAX21 100 WSHDBX406 60
WSHNAX22 200
WSHNAX23 300 DVB Polystyrene
Quaternary Divinylbenzene
Amine + C8 WSHDVB403 30
WSHQAX205 50 WSHDVB406 60
WSHQAX21 100
WSHQAX22 200 C18 Reverse
WSHQAX23 300 Phase C18
Carboxylic WSHC18403 30
Acid + C8 WSHC18406 60
WSHCCX205 50
74
WSHCCX21 100 BCX Benzenesulfonic
WSHCCX22 200 Acid
WSHCCX23 300 WSHBCX403 30

Propylsulfonic WSHBCX406 60
Acid + C8
WSHPCX205 50 QAX Quaternary
WSHPCX21 100 Amine
WSHPCX22 200 WSHQAX403 30
WSHPCX23 300 WSHQAX406 60
Benzenesulfonic
Acid + C8 CCX Carboxlic
WSHBCX205 50 Acid
WSHBCX21 100 WORCCX403 30
WSHBCX22 200 WSHCCX406 60
WSHBCX23 300
Cyanopropyl
+ C8
WSHCNP205 50
WSHCNP21 100
WSHCNP22 200
WSHCNP23 300
Cyclohexyl
+ C8
WSHCYH205 50
WSHCYH21 100
WSHCYH22 200
WSHCYH23 300
Diol + C18
WSHDOL305 50
WSHDOL31 100
WSHDOL32 200
WSHDOL33 300

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
• Over 40 different sorbent chemistries

• Method development formats
• Custom packing and manufacturing
• Competitive pricing
• Full service technical support
• Satisfaction guaranteed
• Up to a 5mL sample volume per well
• Compatible with Robotic and Liquid Handling Systems Including:
Advanced Chemtech, Beckman, Bohdan, Gilson, Hamilton,
Packard, Sagian, Tecan, Tomtec, Zinser, Zymark
48 DEEP WELL FILTER PLATES

Description Part Number Units
Empty 48 deep well plate with one frit inserted WIM481F 1 75
Loose 48 deep well plate frits FR10481P 48
48 deep well collection plate WIM48CP 1
Endcapped C18 Endcapped C2
WIMCEC1811 100 WIMCEC0211 100
WIMCEC181M 1000 WIMCEC021M 1000
Endcapped C8 Cyclohexyl
WIMCEC0811 100 WIMCYH11 100
WIMCEC081M 1000 WIMCYH1M 1000
Endcapped C4 Phenyl
WIMCEC0411 100 WIMPHY11 100
WIMCEC041M 1000 WIMPHY1M 1000

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
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UCT
4 8 D E E P WELL P LATES
NORMAL PHASE (HYDROPHILIC) ION EXCHANGE (ANION)
Silica Aminopropyl
WIMSIL11 100 WIMNAX11 100
WIMSIL1M 1000 WIMNAX1M 1000
Pharma-Sil™ PSA ( N-2 Aminoethyl )
WIMPHSIL11 100 WIMPSA11 100
WIMPHSIL1M 1000 WIMPSA1M 1000
High Surface Diethylamino
Activity Silica WIMDAX11 100
WIMHSSIL11 100 WIMDAX13 300
WIMHSSIL13 300 WIMDAX15 500
WIMHSSIL15 500 WIMDAX1M 1000
76
WIMHSSIL1M 1000 Quaternary Amine
Diol WIMQAX11 100
WIMDOL11 100 WIMQAX13 300

WIMDOL13 300 WIMQAX15 500
WIMDOL15 500 WIMQAX1M 1000
WIMDOL1M 1000 Polyimine
Cyanopropyl WIMPAX11 100
WIMCYN11 100 WIMPAX13 300
WIMCYN13 300 WIMPAX15 500
WIMCYN15 500 WIMPAX1M 1000
WIMCYN1M 1000
Florisil® 60-100 ION EXCHANGE (CATION)
mesh
WIMFLS11 100 Sorbent Part Numbers Sorbent Amount
WIMFLS13 300 per Well, mg
WIMFLS15 500 Benzenesulfonic Acid
WIMFLS1M 1000 WIMBCX11 100
Florisil® 100-200 WIMBCX13 300
mesh, Grade A WIMBCX15 500
WIMFLSA1 100 WIMBCX1M 1000
WIMFLSA3 300 Benzenesulfonic
WIMFLSA5 500 Acid High Load
WIMFLSAM 1000 WIMBCXH1L11 100
Alumina, Acidic WIMBCXH1L13 300
WIMALA1 100 WIMBCXH1L15 500
WIMALA3 300 WIMBCXH1L1M 1000
WIMALA5 500 Carboxylic Acid
WIMALAM 1000 WIMCCX11 100
Alumina, Neutral WIMCCX13 300
WIMALN1 100 WIMCCX15 500
WIMALN3 300 WIMCCX1M 1000
WIMALN5 500 Propylsulfonic Acid
WIMALNM 1000
Alumina, Basic WIMPCX11 100
WIMALB1 100 WIMPCX13 300
WIMALB3 300 WIMPCX15 500
WIMALB5 500 WIMPCX1M 1000
WIMALBM 1000 Tri-Acetic Acid
WIMTAX11 100
WIMTAX13 300
WIMTAX15 500

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
COPOLYMERIC (MULTIFUNCTIONAL PHASES) POLYMERIC RESIN
Aminopropyl + C8 DBX Benzenesulfonic Acid + C8
WIMNAX21 100 WIMDBX41 100
WIMNAX2M 1000 WIMDBX4M 1000
Quaternary Amine + C8
WIMQAX21 100 DVB Polystyrene Divinylbenzene
WIMQAX23 300 WIMDVB41 100
WIMQAX25 500 WIMDVB43 300
WIMQAX2M 1000 WIMDVB45 500
Carboxylic Acid + C8 WIMDVB4M 1000
WIMCCX21 100
WIMCCX23 300 C18 Reverse Phase C18
WIMCCX25 500 WIMC1841 100
WIMCCX2M 1000 WIMC1843 300
77
Propylsulfonic Acid + C8 WIMC1845 500
WIMPCX21 100 WIMC184M 1000
WIMPCX23 300
WIMPCX25 500 BCX Benzenesulfonic Acid
WIMPCX2M 1000 WIMBCX41 100
Benzenesulfonic Acid + C8 WIMBCX43 300
WIMBCX21 100 WIMBCX45 500
WIMBCX23 300 WIMBCX4M 1000
WIMBCX25 500
WIMBCX2M 1000 QAX Quaternary Amine
Cyanopropyl + C8 WIMQAX41 100
WIMCNP21 100 WIMQAX43 300
WIMCNP23 300 WIMQAX45 500
WIMCNP25 500 WIMQAX4M 1000
WIMCNP2M 1000
Cyclohexyl + C8
WIMCYH21 100
WIMCYH23 300
WIMCYH25 500
WIMCYH2M 1000
Diol + C18
WIMDOL31 100
WIMDOL33 300
WIMDOL35 500
WIMDOL3M 1000

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
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UCT
U
78
FLASH CHROMATOGRAPHY COLUMNS
Compatible with common Flash Systems including Biotage®*
• Ensures high yield separations

• Observe reproducible results
• Guaranteed not to leak
• Optimized performance
* Biotage is a trademark of Dyax Corporation

P. 800.385.3153 | 215.781.9255 | F. 215.785.1226
FLASH CHROMATOGRAPHY COL U M NS
ULTRA FLASH® I
COMPATIBLE WITH BIOTAGE®
SILICA C18
Silica Quantity Silica Quantity

Part Number Size Bed Weight per package Part Number Size Bed Weight per package
FUSIL12S-20 12S 4g 20 FEC1812S-100 12S 4g 100
FUSIL12S-100 12S 4g 100 FEC1812M-20 12M 8g 20 79
FUSIL12M-20 12M 8g 20 FEC1812M-100 12M 8g 100
FUSIL12M-100 12M 8g 100 FEC1840S-12 40S 40g 12
FUSIL40S-12 40S 40g 12 FEC1840S-100 40S 40g 144
FUSIL40S-100 40S 40g 144 FEC1840M-12 40M 90g 12
FUSIL40M-12 40M 90g 12 FEC1840M-100 40M 90g 144
FUSIL40M-100 40M 90g 144 FEC1840L-12 40L 120g 12
FUSIL40L-12 40L 120g 12 FEC1865M-6 65M 300g 6
FUSIL65M-6 65M 300g 6
ULTRA FLASH® II
COMPATIBLE WITH BIOTAGE
FLASHMASTER®
SILICA C18
Silica Quantity Silica Quantity

Part Number Size Bed Weight per package Part Number Size Bed Weight per package
MUSIL12M15 15mL 2g 20 MEC1812M15 15mL 2g 20

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UCT
DCN-013204-186
Annual Excellence
in Solid Phase
Extraction Award
UCT
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Uct Spe Catalog

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Uct Spe Catalog

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UCT

including SPE columns, 96 & 48 well plates,

FORENSICS CLINICAL VETERINARY PHARMACEUTICAL

Since our beginnings in 1986, UCT has

Placing An Order Mail Technical Support

Phone: 717.247.0896 UCT, Inc. Phone: 215.781.9255

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

CLEAN SCREEN® Sample Prep Products .................................................................................................................................11-19

XtrackT® HIGH-FLOW Bonded Phases .....................................................................................................................................20-21

CLEAN-UP® Solid Phase Extraction Phases.............................................................................................................................22-45

STYRE SCREEN® Polymeric Resin Extraction Columns .........................................................................................................47-48

Method Development Kits ........................................................................................................................................................49-50

SELECTRASORBTM Bulk Sorbents ............................................................................................................................................51-53

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

REVERSE PHASE (HYDROPHOBIC)

NORMAL PHASE (HYDROPHILIC)

COPOLYMERIC (MULTIFUNCTIONAL PHASES)

Aminopropyl + C8 NAX2 -Si-(CH2)3NH2 & -Si-(CH2)7CH3

Epoxy EPX -Si-(CH2)3 - O - CH2 - CH - CH2 - CH2

SORBENT % ORGANIC EXCHANGE (meq/g)

NORMAL PHASE (HYDROPHILIC)

Silica N/A N/A

Alumina, Acidic N/A N/A

COPOLYMERIC (MULTIFUNCTIONAL PHASES)

Aminopropyl + C8 12.3 0.163

Epoxy N/A N/A

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

and are available in the following formats

1 Cylindrical 5.5 50-200

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

CONDITIONING, SOLVATION (WETTING) WASHING THE SORBENT AND ELUTING

vate and reflush.

Apply sample at a rate of 1mL/min. Again, a momentary

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

When a sample is loaded onto the column at pH 6, many carboxylic

thereby reducing the likelihood of their adsorbing onto the column.

intermediate polarity and potential interferences will also remain C nH 2n+1

optimally interacting with the analytes (figure 3). SO3 PCP

To elute the cationic analytes, an organic solution with a high pH Elution 2

interactions and successfully elute the desired compound (figure 4).

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

• Post Mortem Investigations • Racing Laboratories

% Organic Loading: 12.30 Exchange Capacity (meq/g): 0.072

% Organic Loading: 12.3 Exchange Capacity (meq/g): 0.163

Part Number without Part Number with Unit per

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

CLEAN SCREEN XCEL I: CLEAN SCREEN XCEL I

CLEAN SCREEN XCEL II 15

CLEAN SCREEN XCEL ™

96 DEEP WELL PLATES

Part Number Sorbent Amount/ Unit per

48 DEEP WELL PLATES

Part Number Sorbent Amount/ Unit per

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

CLEAN-THRU® TIPS Standard UCT’s Column with

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

UCT | 2731 Bartram Rd | Bristol, PA 19007 | USA

THC-COOH Standards (ng/mL) in spiked urine

Analyte Solvent Usage Solvent Usage % Solvent

Barbiturates 4.25 mL 18 mL 76%