Академический Документы
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Культура Документы
1. Introduction
2. Stationary phases
3. Retention in Gas-Liquid Chromatography
4. Capillary gas-liquid chromatography
5. Sample preparation and injection
6. Detectors
(Chapter 2 and 3 in The essence of chromatography)
capillary
Dm
2 dp +
(1+p/e) u
k
+ qs
(1+k)2
df2
u + f(k)
Ds
dp2
Dm
2Dm
u
2k
3(1+k)2
df2
u +
Ds
Hmin = 2*(BC)1/2
uopt = (B/C)1/2
1+6k+11k2
96(1+k)2
d2
Dm
Cm =
1+6k+11k2
96(1+k)2
d2
Dm
C S + CM =
2k
3(1+k)2
df2
+
Ds
1+6k+11k2
96(1+k)2
d2
Dm
gas
H = B/u + (CS + CM)u
Hmin = 2*(BC)1/2
uopt = (B/C)1/2
DAB =
DAB = kT/(6BrA)
liquid
1
1
)
MWA MWB
2Dm
u
T
u
df
d
k
2k
3(1+k)2
df2
u +
Ds
1+6k+11k2
96(1+k)2
d2
Dm
b. fused silica
SiCl4 + O2
SiO2
Surface: SiOH,
Silanol
O--SiH-O
Siloxane
Polymer coating
Fused silica tube
Grob Test
Old column
New column