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2. Referenced Documents
1. Scope
1.1 This test method covers the testing of large single- and
double-walled tanks, pressure and vacuum vessels, laminated,
lined- or double-walled parts, complex piping systems, flexible
containers (such as aircraft fuel tanks), glass-to-metal seals in
hybrid packages, and systems that inherently contain or will
contain ammonia (such as large tonnage refrigeration systems
and fertilizer storage systems).
1.2 This method can be used on piping, valves and containers with welded, fitted, or laminated sections that can be sealed
at their ends or between their outer and inner walls and that are
designed for internal pressures of 34.5 kPa [5 psig] or greater.
3. Terminology
4. Summary of Practice
1
This test method is under the jurisdiction of ASTM Committee E07 on
Nondestructive Testing and is the direct responsibility of Subcommittee E07.08 on
Leak Testing Method.
Current edition approved June 15, 2012. Published July 2012. Originally
approved in 1985. Last previous edition approved in 2006 as E1066 - 95(2006).
DOI: 10.1520/E1066-12.
2
The gas temperature is referenced to 0C. To convert to another gas reference
temperature, Tref, multiply the leak rate by (Tref + 273)/273.
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standards Document Summary page on
the ASTM website.
4
Available from American Society for Nondestructive Testing (ASNT), P.O. Box
28518, 1711 Arlingate Ln., Columbus, OH 43228-0518, http://www.asnt.org.
Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E1066/E1066M 12
8.3 Apparatus for Injecting Ammonia Gas:
8.3.1 Pressure GageThe gage must be able to withstand
normal test pressures. The gage must be accurate to within 1 %
of full scale. The gage must read at least 1.5 but not more than
4 the maximum test pressure to be used. The gage must be in
current calibration.
8.3.2 Pressure-Relief Valve, if high pressures are to be used.
8.3.3 Pressure-Reducing, -Control, and -Mixing Valves, for
the ammonia and nitrogen circuits if not already mixed.
8.3.4 High-Conductance Injection Line and Exhaust Line.
7. Interferences
7.1 The interior and exterior welds and joints where leaks
are often found must be free of oil, grease, flux, slag, paint, or
other contaminants that might temporarily block or mask
leakage. New containers should not be painted prior to test.
Smoking during the test may cause false indications.
9.1 Openings:
9.1.1 Seal all openings using plugs or covers that can
withstand the test pressure and can be completely removed
after the test.
9.1.2 Locate the test gas inlet on the bottom of the test
object with the trapped air vent at the highest point.
9.1.3 Components rated at pressures below the test pressure
must be isolated.
8. Apparatus
8.1 Apparatus for Precleaning:
8.1.1 Gloves.
8.1.2 Vacuum Pump or Heat Gun, if necessary to dry
container.
8.1.3 Spray Gun, if aerosol cleaner not used.
8.1.4 Ammonia-Sensitive Monitor, to test area contamination.
8.2 Safety Apparatus:
8.2.1 Mask, covering mouth and nose.
8.2.2 Ammonia Monitors.
8.2.3 Gas Mask, if personnel work inside the tank or with
high concentrations of ammonia during a test.
E1066/E1066M 12
11. Color-Change Method
11.1 Sensitivity:
11.1.1 By varying the ammonia concentration, the test
pressure and the development time, any leakage rate from
4.5 10 11 to 4.5 1012 mol/s [1 to 1 107 Std cm3/s]2 can
be detected. The equation in 11.1.2 is usually applied by
specifying the smallest leakage rate required (MDLR), as well
as the maximum test pressure allowable. Depending on which
is the more important remaining variable, test time or ammonia
concentration, the less critical variable is solved for.
11.1.2 Leakage Rate CalculationThe following equation
allows precise calculation of the test time in seconds (t),
percentage of ammonia tracer (c), and absolute pressure in
pounds per square inch (psia) within the test vessel (p) for any
minimum detectable leakage rate (MDLR). This equation is
based on laboratory data using the time in seconds required to
generate a 1-mm reaction spot as the diameter of the minimum
development area. Leakage rates are expressed in atmcm3/s.
MDLR 5
where:
t
c
p
MDLR
=
=
=
=
2.534
(1)
time in seconds,
% ammonia,
psia, and
atmcm3/s.
t5
2.534p
(2)
or
t5
2.534 ~ 50!
~ 15 3 502 2 3241!~ 50 2/3 !~ 1 3 1026 !
(3)
11.1.4 It has been determined experimentally for wall thicknesses of 1 to 50 mm that for any given pressure differential,
the observed leakage rate varies inversely with the thickness of
the wall being tested. Although the relationship is not linear,
the decrease in observed leakage can be approximated by
adding the following numbers to the exponents of the theoretical MDLR you wish to detect.
11.1.4.1 For wall thicknesses of 2 to 10 mm [0.08 to 0.4 in.]
add nothing.
11.1.4.2 For wall thicknesses between 10 and 25 mm [0.4 to
1 in.] add 1.
11.1.4.3 For wall thicknesses between 25 and 50 mm [1 to
2 in.] add 2.
10.4 Process:
10.4.1 If the test object does not contain ammonia, it should
be pressurized slowly to between 6.9 and 69 kPa [1 and 10
psig] with pure ammonia. If leak location rather than the
leakage rate is desired, a cloth saturated with ammonium
hydroxide can be placed in the pressurized space. Move the
developer vapor slowly over areas of possible leaks. A white
cloud will be produced at the leak location.
10.4.2 Mark and seal leak locations with tape whenever
possible.
E1066/E1066M 12
(2) Fill with ammonia to a gage pressure of 96.5 kPa [14
psig].
(3) Pressurize with nitrogen up to a gage pressure of 289.6
kPa [42 psig].
(b) 1 % Ammonia-99 % Nitrogen Mixture:
(1) Fill with nitrogen to atmosphere.
(2) Fill with ammonia to a gage pressure of 4.14 kPa [0.6
psig].
(3) Pressurize with nitrogen up to a gage pressure of 289.6
kPa [42 psig].
11.3.3.4 If the container being tested is a pressure vessel that
will not be under steady pressure when in use, three successive
increases and decreases in pressure during the test may be more
successful in finding intermittent small leaks than severe
over-pressurization.
11.3.3.5 If the container or part is double-walled or lined,
ammonia can be introduced between the walls and the outside
of both walls developed.
11.3.4 Inspect:
11.3.4.1 After the appropriate development time, all color
indications 1 mm or larger indicate unacceptable leaks. In case
of doubt, circle suspected areas and allow 1 to 2 min additional
development time.
11.3.4.2 As leaks develop, dust off developer and cover leak
with adhesive tape. The tape not only marks the point for
repair, but prevents tracer leakage from contaminating the
atmosphere.
11.3.5 Repair and ReinspectIf extensive welding is
required, it may be necessary to exhaust the tracer and rinse the
container with nitrogen before beginning repairs.
11.3.6 Post Clean:
11.3.6.1 Flush mixture to the outside or into water and purge
with nitrogen or compressed air to remove all traces of
ammonia.
11.3.6.2 The developer can be brushed, vacuumed, or
washed off.
E1066/E1066M 12
13.1.1
13.1.2
ity).
13.1.3
13.1.4
13.1.5
13.1.6
13.1.7
13.1.8
Date tested.
Conditions (temperature, pressure, relative humidTest gas mixture.
Test pressure.
Test time.
Leak locations.
Leakage rate.
Signature of tester.
14. Keywords
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