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RFL,ISMAILA, ROHTAK
1.0 PURPOSE: To carryout Specification standard procedure for quality inspection of raw materials.
2.0 SCOPE: This Specification standard covers the Technical deliver condition for the supply of wire & rods (raw
materials) to RFL for manufacture of premium quality fasteners & auto parts.
3.0 RESPONSIBILITY: Met. Lab., Engineering & Design dpt. Person, Manufacturer & Supplier.
4.0 PROCEDURE:S.
NO.
1.
2.
3.
4.
5.
6.
REFERENCE
& RCORDS
ACTIVITIY
OUR SOURCES FOR STEEL MANUFATURERING :Mainly the following steel manufacturers are approved by our customers:1.1 M/S Mukand limited.
1.2 M/S Sun Flag Iron & steel Company limited.
1.3 M/S Usha Martin limited.
1.4 M/S Posco Phong works.
OUR APPROVED SOURCES FOR STEEL DRAWERS & SUPPLIERS:2.1 M/S Rohit steel (p) ltd.
2.2 M/S Juneja Bright steel (p) ltd.
2.3 M/S A.V. Wires (p) ltd.
2.4 M/S Shri Balaji Tech.
2.5 M/S Shri Mahavir Bright Steel ltd.
Suppliers of steel (for wire drawing) shall use the raw material of the approved steel manufacturers.
Note:- For using steel of any make other than the approved manufacturers, prior permission shall be
taken by the supplier from ROHTAS FASTNERS (P) LTD.
MANUFACTURING:Steel shall be made through Aluminum killed basic electric arc furnace using clean & classified scrap
& ferrous alloys. The raw material shall be totally free from tramp elements which are harmful for
cold forging operations. Secondary refining using idle furnace or vacuum designing might be
necessary to ensure close control over chemistry & cleanliness.
SURFACE COATING:The carbon steel wire rods shall be coated with heavy lubricant absorptive, Iron free chloride,
accelerated Zinc Phosphate coating (16gm/m2) or more with mixed lime soap which additionally
contain Molybdenum disulphide suitable for wire drawing as well as subsequent cold deformation.
As regards coating thickness - It shall be minimum 6 m.
DIMENSIONAL TOLERANCES:The wire rods shall be under tolerances as per standard IS:3739:1987 or B.S. 970:1991 part-III:SPECIFIED
TOLERANCE
3 to 25mm
-0.05mm
Above 25mm
-0.10mm
MACRO EXAMINATION OR CRACKS & SEAMS (ACID ETCHING):The steel shall be free from harmful surface defects during Visual inspection as per standard
IS:11371:1985, ASTM E 381 & WI/LAB/10. The surface shall be smooth & free from scale, scratch,
dent, pitting, rust, seams, Laps. The permissible level of seam shall not exceed the limits given
below:WIRE SIZE
PERMISSIBLE DEPTH OF SEAM
Up to 8mm
0.06mm
8~14mm
0.08mm
14~20mm
0.10mm
Over to 20mm
0.12mm
PREPARED BY
APPROVED BY
Raw
Material
inspection
report
F/LAB/01
&
Metallurgical
Test Report
F/LAB/02
RFL,ISMAILA, ROHTAK
S.
NO.
ACTIVITIY
7.
MACROETCH TESTING:It shall be done on wire rods as per standard IS:13015:1991, ASTM E 381 & WI/LAB/11 Method for
macro etch testing to inspect the Raw Material by matching standard photographs:7.1 Centre segregation- C (C-1, C-2, C-3, C-4 & C-5).
7.2 Random condition- R (R-1, R-2, R-3, R-4 & C-5)
7.3 Sub surface conditions- S (S-1, S-2, S-3, S-4 & S-5)
ACCEPTANCE CRITERIA:- C1R1S1 to C2R2S2
8.
COLD UPSET TEST:In order to assess the suitability of wire (coil) for cold forging, it shall be subjected to cold upsetting
test as per IS:11169:1984 part-1 or WI/LAB/25. This shall be carried out on representative samples of
length at least 1.5 times DIAMETER of wire, appropriate load shall be used to upset the sample to a
height 66% of the initial height for shown in the article 15.1, 15.2 & 80% of the initial height for
shown the 15.3 & 15.4 item. The upset samples shall be macro etched in Hydrochloric acid (HCL) &
inspected either visually or using magnifying glass.
ACCEPTANCE CRITERIA:-The inspection shall not reveal crack on the barrel surface.
9.
SURFACE DECARBURIZATION TEST:Using the appropriate measuring method IS:6396:2000, IS:11169:1984 & WI/LAB/21 or 22, a
transverse section shall be cut and polished of the wire and shall be examined under microscope to
determine whether decarb appearing in the zone of metal and the depth of the zone with
decarburization.
DECARBURIZATION:-Generally, loss of carbon at the surface of ferrous materials (steel).
9.1 COMPLETE (FULL) DECARBURIZATION:-Decarburization with sufficient carbon loss to
show clearly defined ferrite grains only under Microscopic examination.
A. In surface:-Only ferrite micro structure.
B. In core:-Uniform distribution of pearlite in ferrite matrix.
9.2 PARTIAL DECARBURIZATION:-Decarburization with loss of carbon sufficient to cause a
lighter shade of pearlite & significantly lower hardness observed on surface than the core.
ACCEPTANCE CRITERIA:WIRE SIZE
Up to 0.8mm
8.0 to 14.0mm
14.0 to 20mm
Over 20mm
PREPARED BY
COMPLITE DECARB
NIL
NIL
NIL
NIL
PARTIAL DECARB
0.10mm
0.11mm
0.12mm
0.13mm
APPROVED BY
Raw
Material
inspection
report
F/LAB/01
&
Metallurgical
Test Report
F/LAB/02
RFL,ISMAILA, ROHTAK
S.
NO.
10.
REFERENC
E&
RCORDS
ACTIVITIY
MICROSTRUCTURE:Using the appropriate measuring method as per IS:7739:1976-part-5, WI/LAB/16. A cross section shall
be cut polished and etched with natal (etching reagent) of the wire cut sample shall be examined on the
microscope as per following table.
ACCEPTANCE CHARECTERIA:PROCESS
PROCESS RETIO
STRUCTURE
AS ROLLED
..
AS ANNEALED
AS SPHROIDIZED ANNEALED
11.
GRAIN SIZE:Using the appropriate measuring method as per IS:4748-2009, ASTM E-112:1988 & WI/LAB/17, a
cross section shall be cut & after heating and cooling at sufficient temperature shall be polished &
shall be examined under microscope to determine average grain size of the material by matching
standard photographs.
Acceptable range of grain size:- 5~8 ASTM No.
12.
INCLUSION RATING:Using the appropriate measuring method as per IS:4163-2004 & WI/LAB/18, after full Hardening of
sample piece a transverse section shall be cut & polished sample shall be examined under microscope to
determine nonmetallic inclusion in the material by matching standard photographs & follow following
table.
ACCEPTANCE CRITERIA:SULPHIDE TYPE
ALUMINA TYPE
A
THIN
T
SILICATE TYPE
B
HEAVY
H
THIN
T
GLOBULAR OXIDE
TYPE
D
THIN
HEAVY
T
H
HEAVY
H
THIN
T
HEAVY
H
1.5
2.0
1.5
2.0
1.5
1.0
2.0
1.0
1.5
2.0
13.
1.0
2.0
1.0
2.0
MACHENICAL TEST:It shall be done on wire rods as per work instruction for Hardness test, Tensile test & Microstructure
examination:13.1 Hardness (As soft condition):- Using the appropriate Hardness testing method as per IS:1586-2000
& WI/LAB/13. A cross section shall be cut & face shall be smoothened of the wire cut sample &
shall be examined on the Hardness testing M/C. as per standard table.
13.2 Hardness (As Quenched):- The wire/rods shall be subjected to appropriate Heat treatment to ensure
the as quenched hardness as per IS:5517:1993 & WI/LAB/28.
13.3 Tensile strength test:- (As soft condition):-The tensile test shall be performed as per standard
IS:1608:2005 & WI/LAB/23.
PREPARED BY
APPROVED BY
Raw
Material
inspection
report
F/LAB/01
&
Metallurgic
al Test
Report
F/LAB/02
RFL,ISMAILA, ROHTAK
S.
NO.
14.
REFERENCE
& RCORDS
ACTIVITIY
The Mechanical test value as per Standard IS:5517:1993 & IS:1586:2000, IS:1608:2005, and follow
this table:Tensile
Strength
Kg/mm2
% of
Elonga
tion
% of
Reduc
tion
Hardness
as black
bar
S
No.
Material
Grade
Standard
SAE1010
SAE:1976
38~45
22
60
60~73
2
3
4
5
6
7
8
9
10
11
12
13
SAE1015
SAE1018
SAE1020
SAE1035
SAE1040
AISI 1541
SAE10B21
SAE15B25
SAE15B41
AISI4135
AISI4140
SAE 8620
38~45
38~45
40~45
45~50
45~55
45~55
45~60
50~60
50~60
45~60
45~60
45~60
22
22
22
22
20
20
20
20
20
20
20
20
60
60
60
50
50
50
55
55
50
50
50
60
60~73
60~73
60~73
70~79
70~79
70~79
70~83
75~83
75~83
70~79
70~79
70~79
14
En1A(P)
38~45
10
....
70~79
15
16
17
18
19
20
21
22
23
24
En1A(L)
En8D
En8M
En43B
En9
En19
EN 24
EN 31
En32B
En353
.....
50
50
50
50
50
50
....
40
50
70~79
70~79
70~79
70~79
70~79
70~79
80~85
85~95
70~79
70~79
SCM415H
38~45
50~60
45~60
50~60
50~60
50~60
60~80
....
45~55
42~55
45~60
10
20
20
20
18
22
22
.....
20
20
25
20
50
70~79
26
27
28
29
30
31
32
33
34
35
36
37
38
SCM415H
SCM420H
SCM435H
S10C
S20C
S30C
S35C
S38C
S40C
S45C
S48C
S50C
S55C
45~60
45~60
45~60
38~45
38~45
40~45
45~60
45~60
45~60
50~60
50~60
50~60
50~60
20
20
20
20
20
20
20
20
20
20
20
18
18
50
50
50
60
60
60
50
50
50
50
50
50
60
70~79
70~79
70~79
60~73
60~73
60~73
70~79
70~79
70~79
70~79
70~79
70~79
75~85
39
16MnCr5
42~55
22
50
75~85
40
41
42
43
44
45
46
47
20MnCr5
C 10
C 15
C 35
CK 35
C 45
CK 45
41Cr4
CEW-1
ERW-1
do
do
do
do
do
do
do
do
do
do
do
do
BS:970:
1955
do
do
do
do
do
do
do
do
do
do
JIS G:4051:
1981
do
do
do
do
do
do
do
do
do
do
do
do
do
DIN:17210:
1969
42~55
38~45
38~45
45~60
45~60
50~60
50~60
45~60
22
22
22
20
20
20
20
20
50
60
60
50
50
50
50
50
32~45
22
60
48
....
Hardness
(HRB Max.)
As
As
Anne
Drawn
aled
Max
85M
90
ax.
90
90
90
90
90
90
92
92
90
90
90
90
90
Hardness as Quenched
(HRC Min.)
Surface
Micro
structure
core
25Max.WQ
do
do
do
42
45
45
34
37
45
45
45
35
do
do
do
45
48
48
38
42
48
48
48
38
IP
Martensite
LCM
25Max.WQ
IP
Martensite
.....
LCM
90
95
90
90
90
90
90
90
90
90
90
do
45
48
45
48
45
48
45
48
45
48
48
52
60
62
25Max.WQ
30
35
90
90
90
90
90
90
90
90
90
90
90
90
90
90
28
32
28
32
48
50
25Max.WQ
do
do
30
34
42
45
42
45
42
45
45
48
45
50
45
50
52
55
75~85
60~73
60~73
70~79
70~79
70~79
70~79
70~79
90
90
90
90
90
90
90
85
28
32
25Max.WQ
42
45
42
45
45
48
45
48
45
50
IP
Martensite
40~60
....
.....
25Max.WQ
30
28
35
Martensite
IP
Martensite
32
LCM
NOTE:- Spheroidized Annealed Hardness should be 85HRB max. in all type of material grades.
PREPARED BY
APPROVED BY
Raw
Material
inspection
report
F/LAB/01
&
Metallurgica
l Test Report
F/LAB/02
RFL,ISMAILA, ROHTAK
S.
NO.
15.
REFERENCE
& RCORDS
ACTIVITIY
The Chemical Composition as per IS:228 Raw Material Grade - Check & match the Mill T.C. &
Spectro test report as per following table:S.
No.
Material
Grade
Standard
SAE1010
SAE:1976
SAE1015
do
SAE1018
do
SAE1020
do
SAE1035
do
SAE1040
do
AISI 1541
ASTM A 29
ASTM A 576
SAE10B21
do
SAE 15B23
do
10
SAE15B25
do
11
SAE15B41
do
12
AISI 4135
SAE J 403
13
AISI 4140
do
14
SAE 8620
ASTM J 29
SAE A 32-90
14
En1A(P)
BS:970: 1955
16
En8D
do
17
En8M
do
18
En43B
do
19
En9
do
20
En 18
do
21
En18D
do
22
En19
do
23
EN24
do
24
EN31
do
25
En32B
do
26
En353
do
27
C-20
IS:2073:1970
28
C-40
29
C-45
PREPARED BY
C
0.08
0.13
0.13
0.18
0.15
0.20
0.18
0.23
0.32
0.38
0.37
0.44
0.36
0.44
0.18
0.23
0.20
0.25
0.23
0.28
0.36
0.44
0.33
0.38
0.38
0.43
0.17
0.23
0.07
0.15
0.40
0.45
0.35
0.45
0.45
0.50
0.50
0.60
0.35
0.45
0.38
0.43
0.35
0.45
0.35
0.45
0.90
1.20
0.10
0.18
0.20
Max.
0.15
0.25
0.35
0.45
0.40
0.50
Mn
0.30
0.60
0.30
0.60
0.60
0.90
0.30
0.60
0.60
0.90
0.60
0.90
1.35
1.65
0.80
1.10
0.80
1.20
0.90
1.20
1.35
1.65
0.70
0.90
0.75
1.00
0.60
0.95
0.80
1.20
0.70
0.90
1.00
1.30
0.70
1.00
0.50
0.80
0.10
0.35
0.65
0.80
0.50
0.80
0.45
0.70
0.30
0.75
0.60
1.00
0.50
1.00
0.60
0.90
0.60
0.90
0.60
0.90
0.35
Max.
Max.
1.15
0.10
0.05
0.05
0.90
0.20
0.35
Max.
Max.
1.50
0.40
0.10
0.05
0.05
0.90
0.20
0.35
Max.
Max.
1.40
0.35
0.10
0.05
0.05
1.00
....
0.35
Max.
Max.
1.60
0.05
0.07
0.05
.....
....
0.35
Max,
Max.
0.35
0.05
0.05
0.75
0.08
Max.
Max.
Max.
1.25
015
0.05
0.055
0.055
....
....
0.35
Max.
Max.
0.05
0.055
0.055
....
....
0.35
Max.
Max.
0.05
0.055
0.055
....
....
0.35
Max.
Max.
APPROVED BY
Ni
Other
....
....
....
....
....
....
....
....
....
....
....
....
....
....
.....
B 0.0005
0.003
do
.....
do
....
do
...
.....
...
.....
0.35
0.75
....
.....
....
....
....
.....
....
.....
....
....
...
.....
....
.....
....
1.30
1.80
....
....
....
....
...
1.00
1.50
.....
....
...
....
...
....
...
Raw
Material
inspection
report
F/LAB/01
&
Metallurgical
Test Report
F/LAB/02
RFL,ISMAILA, ROHTAK
S.
NO.
REFERENCE
& RCORDS
ACTIVITIY
The Chemical Composition as per IS:228 Raw Material Grade Check & match the Mill T.C. & Spectro
test report as per following table:S.
No.
Material
Grade
Standard
30
SCM415H
JIS G 4105:2003
31
SCM420H
do
32
SCM435H
do
33
SCM440H
do
34
S10C
35
S20C
do
36
S30C
do
37
S35C
do
38
S38C
do
39
S40C
do
40
S45C
do
41
S48C
do
42
S50C
do
43
S55C
do
44
16MnCr5
DIN:17210:1969
45
20MnCr5
do
46
C 10
do
47
C 15
do
48
C 35
do
49
CK 35
do
50
C 45
do
51
CK 45
do
52
41Cr4
53
530M40
BS:970: 1955
54
SS 304
.....
55
CEW-1
BS:970: 1955
56
ERW-1
IS:3074:2013
57
MS
IS:226:1975
PREPARED BY
Mn
0.55
0.90
0.55
0.90
0.55
0.90
0.55
0.90
0.30
0.60
0.30
0.60
0.60
0.90
0.60
0.90
0.60
0.90
0.60
0.90
0.60
0.90
0.60
0.90
0.60
0.90
0.60
0.90
1.00
1.30
1.10
1.40
0.30
0.60
0.30
0.60
0.50
0.80
0.50
0.80
0.50
0.80
0.50
0.80
0.60
0.90
0.60
0.90
2.00
Max.
0.30
0.60
0.60
Max.
Si
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.40
0.15
0.40
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.35
0.15
0.40
0.10
0.35
1.0
Max.
..
..
.....
..
S
0.03
Max.
0.03
Max.
0.03
Max.
0.030
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.035
Max.
0.045
Max.
0.045
Max.
0.045
Max.
0.035
Max.
0.045
Max.
0.035
Max.
0.035
Max.
0.040
Max.
0.03
Max.
0.040
Max.
0.040
Max.
0.055
Max.
P
0.03
Max.
0.03
Max.
0.03
Max.
0.030
Max.
0.03
Max.
0.03
Max.
0.030
Max.
0.03
Max.
0.03
Max.
0.03
Max.
0.03
Max.
0.03
Max.
0.03
Max.
0.03
Max.
0.035
Max.
0.035
Max.
0.045
Max
0.045
Max
0.045
Max.
0.035
Max.
0.045
Max.
0.035
Max.
0.030
Max.
0.035
Max.
0.045
Max.
0.040
Max.
0.040
Max.
0.055
Max.
Cr
0.85
1.25
0.85
1.25
0.85
1.25
0.85
1.25
Mo
0.15
0.25
0.15
0.2 5
0.15
0.35
0.15
0.35
Ni
Other
....
....
....
....
....
....
....
....
....
.....
....
....
....
.....
....
....
....
....
....
....
....
.....
....
....
....
.....
....
....
....
.....
....
....
....
.....
....
....
....
.....
....
....
....
.....
....
....
....
.....
....
....
.....
.....
....
....
.....
....
.....
.....
.....
....
....
.....
....
...
...
....
....
...
...
....
....
...
...
....
....
...
...
....
....
....
.....
0.80
1.10
1.00
1.30
0.90
1.20
0.90
1.20
18.0
20.0
...
8.00
10.0
....
.....
.....
....
.....
..
..
..
..
..
..
APPROVED BY
Raw
Material
inspection
report
F/LAB/01
&
Metallurgical
Test Report
F/LAB/02
RFL,ISMAILA, ROHTAK
S.
NO.
ACTIVITIY
S.
No.
Material
Grade
Standard
58
STKM-11
JIS:3345
Mn
Si
Cr
Mo
Ni
Other
0.12
Max.
0.45
Max.
..
0.040
Max.
0.040
Max.
..
..
..
Note:- Maximum Impurities & Gaseous Element are as follows:Cr-0.20~0.25%, Ni-0.20max., Cu-0.25%max., Mo-0.055max., N-80ppm max., O-20ppm max. & H-2ppm max.
16.
17.
SUPPLY CONDITION:Material supply as per our requirements & as per standard IS:11169:1984 for cold extrusion & cold
headed process:17.1 HR
:-Hot Rolled.
17.2 HRPPD:- Hot Rolled Pickled Phosphated & Drawn.
17.3 SA
:- Spheroidized Annealed.
17.4 SAPPD:- Spheroidized Annealed, Pickled, Phosphated & Drawn
18.
SUPPLY IDENTIFICATION :The supplier shall inspect every lot as per standard IS:1387:1993 for conformance to the
specifications & shall issue a test certificate to this effect. Following points shall be included in test
certificate:18.1 Identification tag (Manufacturer & Supplier).
18.2 RFL P. O. & Date.
18.3 Delivery Invoice No. & date.
18.4 Grade of Steel.
18.5 Quantity (Coil No. & Weight).
18.6 Heat No.
18.7 Test certificate (Chemical & Mechanical).
Note:- RFL reserves the right to inspect the Raw Material at the steel mill & prior to dispatch.
In such cases RFL will send prior information to the steel mills.
PREPARED BY
APPROVED BY
Raw
Material
inspection
report
F/LAB/01
&
Metallurgical
Test Report
F/LAB/02
RFL,ISMAILA, ROHTAK
S.
NO.
19.
20.
21.
ACTIVITIY
COLOUR CODING:When supplied by steel supplier each coil shall be identified with color coding for showing material
grade as per IS:2049:1978. The following color coding to be done at one line in bundle or end of
rods:S. No. Material Grade Color Coding
19.1
SAE 15B25
Yellow
19.2
SAE 10B21
Sky blue
19.3
EN8D
Green
19.4
S45C
Blue
19.5
SAE 1010
White
19.6
SAE 1018
Pink
19.7
SAE 1040
White Yellow
19.8
SAE 4140
Orange
19.9
SAE 1541
White green
19.10 SCM 415
Silver Dark
19.11 SCM 420
Golden
19.12 41Cr4
Brown
19.13 New Grade
Black
19.14 Rejected
Red
DAVIATION:20.1 Accepted
:- If accepted, Material taking to under processing.
20.2 Under Deviation :- If any deviation desired from the requirements of this specification
Written approval of Raw Material authority, Dept. HOD,
Quality HOD, Plant HEAD & MD before taking in process.
20.3 Rejected
:- If Rejected, Raw Material shall be sent back to Supplier immediately.
PREPEARATION OF THE TEST REPORT:21.1 Experience:- 1 year min.
21.2 Post.:Minimum Executive Engineer.
21.3 Education:- B. Sc. (PCM), Diploma/Degree in Metallurgy or Mechanical stream.
21.4 Area:Metallurgical laboratory.
21.5 Knowledge:- Well handling of Metallurgical testing instruments all important testing
Parameters and its procedure.
22.
23
PRESERVED TEST SAMPLE & DOCUMENTS:23.1 Retention Period of test samples:- 6 Month.
23.2 Retention Period of Documents:- 1 Year.
PREPARED BY
APPROVED BY
Raw
Material
inspection
report
F/LAB/01
&
Metallurgical
Test Report
F/LAB/02
REV. No.
EFFECTIVE DATE
AMENDMENT
Page No.
01
20.07.15
ALL PAGE
02
28.10.15
PREPARED BY:-
APPROVED BY:-