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ON
HIGHWAY ENGINEERING
PREPARED BY
M.L. RATHORE
LAB ENGINEER
DEPARTMENT OF CIVIL ENGINEERING
JAYPEE UNIVERSITY OF
ENGINEERING & TECHNOLOGY
A.B. ROAD RAGHOGARH-GUNA (M.P.)-473226 (INDIA)
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 0
PAGE NO
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Report writing
23
1.
46
2.
79
3.
10 12
4.
13 16
5.
17 19
6.
20 22
7.
23 25
8.
26 28
9.
29 30
10.
31 38
11.
39 43
12.
Viscosity of tar/bitumen
44 45
13.
46 47
14.
48 49
15.
50 52
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References
53
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 1
OBJECTIVES
It contains the aim of the experiment and how the author is going to achieve his aim.
EXPERIMENTAL SETUP WITH DIAGRAM
Write every experimental setup and instruments you used with their dimensions. Draw
a neat sketch of experimental setup.
EXPERIMENTAL METHOD
It should contain a brief description of experimental method, a neat sketch of
experimental setup.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 2
NB: Failure to submit the report and attend the viva voce will result in a zero mark.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 3
Experiment No-1
SET OF SIEVES
THEORY:
The aggregate used in surface course of the highway pavements are subjected to wearing due to
movement of traffic. When vehicles move on the road, the soil particles present between the
pneumatic tyres and road surface cause abrasion of road aggregates. The steel reamed wheels of
animal driven vehicles also cause considerable abrasion of the road surface. Therefore, the road
aggregates should be hard enough to resist abrasion. Resistance to abrasion of aggregate is
determined in laboratory by Los Angeles test machine. The principle of Los Angeles abrasion test is
to produce abrasive action by use of standard steel balls which when mixed with aggregates and
rotated in a drum for specific number of revolutions also causes impact on aggregates. The
percentage wear of the aggregates due to rubbing with steel balls is determined and is known as
Los Angeles Abrasion Value.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 4
PROCEDURE:
1. Aggregate sample weighing 5 kg (for Grade A, B, C & D) and 10 kg (for Grade E, F & G) is
put in the machine along with the abrasive charge as per given in table.
2. The machine is rotated at a speed of 30 to 33 R.P.M. for the specified number of
revolutions (500 for grade A, B, C, D and 1000 for E, F, G)
3. Now the sample is taken out of the machine and sieved through 1.7 mm I.S. Sieve and
the weight of aggregate passing through 1.7 mm sieve is determined.
12
11
8
6
12
12
12
500
500
500
500
1000
1000
1000
5000
5000
5000
5000
10000
10000
10000
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 5
Grading
Number of spheres used
Weight of charge
Number of revolution
S. No
=
=
=
=
Description
Sample 1
1.
2.
3.
4.
Percentage wear
Sample 2
W1 W2 100
W1
RESULT
Los Angeles Abrasion Value = %
PRECAUTIONS:
1. The cover should be fixed tightly before rotating the machine
2. All material should be discharged from the cylinder after the conduct of test.
INTERPRETATION OF RESULTS
Los Angeles abrasion test is commonly used to evaluate the hardness of the aggregates. The
test has more acceptability because the resistance to abrasion and impact is determined
simultaneously. Depending upon the numerical; value, the suitability of aggregates for different
road constructions can be judged as per the Indian Road Congress specifications given below;
Sr. No
1
2
3
4
5
6
Max Permissible
Abrasion Value in %
40
40
35
35
30
30
DISCUSSION:
Write the discussion/suitability of aggregate according to your result obtained.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 6
Experiment No-2
THEORY:
The property of a material to resist impact is known as toughness. Due to movement of
vehicles on the road the aggregates are subjected to impact resulting in their breaking down
into smaller pieces. The aggregates should therefore have sufficient toughness to resist their
disintegration due to impact. This characteristic is measured by impact value test. The
aggregate impact value is a measure of resistance to sudden impact or shock, which may
differ from its resistance to gradually applied compressive load.
In other words, Resistance of the aggregates to impact is termed as toughness. Aggregates used
in the pavement should be able to resist the effect caused by the jumping of the steel tyred
wheels from one particle to another at different levels causes severe impact on the aggregates.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 7
PROCEDURE:
1. Oven dried aggregate specimen passing 12.5 mm sieve and retained on 10 mm sieve is
filled in measuring cup in three equal layers by 25 blows with the help of tamping rod
and weighed.
2. The sample is now transferred to the cup of the impact test apparatus and compacted
by tamping rod 25 times again in 3 equal layers.
3. Now the hammer is raised to a height of 38 (0.5) cm above the surface of the
aggregate in the cup and is allowed to fall freely in the specimen. In this 15 blows are
given to the aggregate specimen at an interval of not less than one second between
successive falls.
4. Now the tested aggregate sample is sieved through 2.36 mm I.S. Sieve and the fraction
passing or retained through this sieve is weighed.
OBSERVATION & CALCULATIONS
S.No.
1.
2.
3.
4.
Determinations
5.
6.
Wa W3
100
Wa
RESULT
Aggregate Impact Mean Value = %
INTERPRETATION OF RESULTS
Aggregate impact value is used to classify the stones in respect of their toughness property as
indicated below;
S No
Aggregate impact value
Classification
1
< 10 %
Exceptionally Strong
2
10 20 %
Strong
3
20 30 %
Satisfactory for road surfacing
4
>35 %
Weak for road surfacing
The Indian Road Congress has recommended the following values for different types of road
construction.
S No
1
2
3
4
Type of pavement
WBM Sub base/base course
WBM wearing course
Dense Bituminous Macadam & SDBC
Bituminous Concrete (BC)
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 8
DISCUSSION:
Write the discussion/suitability of aggregate according to your result obtained.
PRECAUTIONS
1. Place the plunger centrally so that it falls directly on the aggregate sample and does not
touch the walls of the cylinder in order o ensure that the entire load is transmitted on o
the aggregates.
2. In the operation of sieving the aggregates through 2.36 mm sieve the sum of weights of
fractions retained and passing the sieve should not differ from the original weight of the
specimen by more than 1 gm.
3. The tamping is to be done properly by gently dropping the tamping rod and not by
hammering action. Also the tamping should be uniform over the surface of the
aggregate taking care that the tamping rod does not frequently strike against the walls
of the mould.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 9
Experiment No-3
THEORY:
One of the model in which pavement material can fail is by crushing under compressive stress.
This test is used to determine the crushing strength of aggregates. The aggregate crushing value
provides a relative measure of resistance to crushing under gradually applied crushing load.
The principal mechanical properties required in road stones are (i) satisfactory resistance to
crushing under the roller during construction and (ii) adequate resistance to surface abrasion
under traffic. Also surface stresses under rigid tyre rims of heavily loaded and drawn vehicle are
high enough to consider the crushing strength of road aggregates as essential requirements in
India.
PROCEDURE:
1. Aggregate passing 12.5 mm I.S. sieve and retained on 10 mm sieve is taken and dried.
2. This aggregate filled in the cylindrical measure in three equal layers and each layer
tamped 25 times by the tamping rod.
3. Now the test sample is weighed and filled in the test cylinder in three equal layers and
tamped each layer 25 times. Let the weight of aggregate be W1 Kg.
4. Now the plunger is placed on the top of the test specimen and whole apparatus is put in
the compression testing machine.
5. Now the specimen is loaded to a total load of 40 tones at the rate of 4 tons per minute
i.e., the total load s reached in 10 minutes in the compression machine.
6. Now the test cylinder is removed from the compression machine and aggregate sieved
through 2.36 mm sieve. The material passed through the 2.36 mm sieve is weighed. Let
the weight be W2 Kg.
Details
Trial No.
1
2
1.
2.
3.
4.
5.
6.
W4
100
Wa
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 11
RESULT:
Aggregate Crushing Value = %
PRECAUTIONS:
1. The plunger should be placed centrally and rest directly on the aggregates. Care should
be taken that it does not touch the walls of the cylinder so as to ensure that the entire
load is transferred onto the aggregates.
2. In the operation of sieving the aggregates through 2.36 mm sieve and weighing care
should be taken to avoid loss of fines. The sum of weights of fractions retained and
passing the sieve should not differ from the original weight of the specimen by more
than 1 gm.
3. The tamping should be done properly by gently dropping the tamping rod and not by
hammering action. Also the tamping should be uniform over thy surface of the
aggregates taking care that the tamping rod does not frequently strike against the walls
of the mould.
INTERPRETATION OF RESULTS:
The suitability of aggregate is adjudged, dependent upon its proposed use in the pavement
layers. The table given below lays down specified limits of percent aggregate crushing value, for
different types of road construction.
S No
Type of Pavement
40
30
DBM/BC/SDBC
30
Cement Concrete
30
DISCUSSION:
Write the discussion/suitability of aggregate according to your result obtained.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 12
Experiment No-4
LENGTH GAUGE
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 13
THICKNESS GAUGE
SET OF SIEVES
THEORY:
The flakiness index of an aggregates is the percentage by weight of particles whose least
dimension (thickness) is less than three-fifths (0.6) of their mean dimension. The test is not
applicable to sizes smaller than 6.3 mm.
The elongation index of an aggregate is the percentage by weight of particles whose greatest
dimension (Length) is greater than 1.8 times of their mean dimension .The elongation index is
not applicable to sizes smaller than 6.3 mm
Thickness
gauge (0.6 Length gauge (1.8
times the mean sieve) times the mean sieve),
mm
mm
33.90
27.00
19.50
16.95
13.50
10.80
8.55
6.75
4.89
--81.0
58.5
--40.5
32.4
25.6
20.2
14.7
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 14
PROCEDURE:
Determination of Flakiness Index;
1. A sufficient quantity of aggregate is taken such that a minimum number of 200 pieces of
any fraction can be tested.
2. Each fraction is gauged in turn for thickness on the meal gauge.
3. The total amount passing in the gauge is weighed to an accuracy of 0.1 per cent of the
weight of the samples taken.
4. The flakiness index is taken as the total weight of the material passing the various
thickness gauges expressed as a percentage of the total weight of the sample taken.
Determination of elongation Index
1. This test is conducted by using metal length gauge of the description. A sufficient
quantity of aggregate is taken to provide minimum number of 200 pieces of any fraction
to be tested.
2. Each fraction shall be gauged individually for length on the metal gauge.
3. The total amount retained by the gauge length shall be weighed to an accuracy of at
least 0.1 per cent of the weight to the test samples taken.
4. The elongation index is the total eight of the material retained on the various length
gauges expressed as a percentage of the total weight of the sample gauged.
OBSERVATION SHEET
Passing
through
is sieve,
mm
Size of aggregate
Retained
on IS
sieve,
mm
Weight of the
fraction
consisting of at
least 200 pieces,
gm
Thickness
Weight of
gauge aggregates in each
size
fraction passing
thickness gauge,
mm
gm
Length
gauge
size
mm
Weight of
aggregates in each
fraction retained
on length gauge,
gm
63
50
W1 =
23.90
w1 =
--
--
50
40
W2 =
27.00
w2 =
81.0
x1 =
40
25
W3 =
19.50
w3 =
58.5
x2 =
31.5
25
W4 =
16.95
w4 =
--
--
25
20
W5 =
13.50
w5 =
40.5
x3 =
20
16
W6 =
10.80
w6 =
32.4
x4 =
16
12.5
W7 =
8.55
w7 =
25.6
x5 =
12.5
10.0
W8 =
6.75
w8 =
20.2
x6 =
10.0
6.3
W9 =
4.89
w9 =
14.7
x7 =
Total
W =
w =
x =
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 15
CALCULATIONS:
Flakiness Index =
w2 w 3 .........
W1 W2 W3 .......
Elongation Index =
x 2 x 3 .........
W1 W2 W3 .......
100
w
100 percent
W
100
x
100 percent
W
RESULT:
1. Flakiness Index = %
2. Elongation Index = ..%
PRECAUTIONS:
1.
2.
3.
4.
DISCUSSIONS:
The presence of elongated particles in excess of 10 to 15 per cent is generally considered
undesirable, but no recognized limits are laid down. Indian standard explain only the method of
calculating both flakiness index and elongation index. But the specifications do not specify the
limits. British standard BS 882 of 1992 limits the flakiness index of the coarse aggregate to 50
for natural gravel and to 40 for rushed coarse aggregate. However, for wearing surfaces lower
values of flakiness index are required.
INTERPRETATION OF RESULTS:
Indian Road Congress (IRC: 111-2009), NRRDA (2007) and MORTH (2000) have recommended
the values of flakiness & elongation index as follows;
S No
Type of Pavement
Flakiness Index
Elongation Index
30
30
25
25
20
20
DBM/BC/SDBC
35
35
Cement Concrete
25
15
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 16
Experiment No-5
THEORY:
This test is done to determine the flash point and the fire point of asphaltic bitumen and fluxed
native asphalt, cutback bitumen and blown type bitumen as per IS: 1209 1978. The principle
behind this test is given below:
Flash Point The flash point of a material is the lowest temperature at which the application of
test flame causes the vapours from the material to momentarily catch fire in the form of a flash
under specified conditions of the test.
Fire Point The fire point is the lowest temperature at which the application of test flame
causes the material to ignite and burn at least for 5 seconds under specified conditions of the
test.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 17
PROCEDURE:
A) Flash Point
1. Soften the bitumen between 75 and 100oC. Stir it thoroughly to remove air bubbles and
water.
2. Fill the cup with the material to be tested upto the filling mark. Place it on the bath. Fix
the open clip. Insert the thermometer of high or low range as per requirement and also
the stirrer at a rate of approx 60 revolutions per minute, to stir it.
3. Light the test flame, adjust it. Supply heat at such a rate that the temperature increase,
recorded by the thermometer is neither less than 5oC nor more than 6oC per minute.
4. Open flash point is taken as that temperature when a flash first appears at any point on
the surface of the material in the cup.
5. Take care that the bluish halo that sometimes surrounds the test flame is not confused
with the true flash.
6. Discontinue the stirring during the application of the test flame.
7. Flash point should be taken as the temperature read on the thermometer at the time
the flash occurs.
B) Fire Point
1. After flash point, heating should be continued at such a rate that the increase in
temperature recorded by the thermometer is neither less than 5oC nor more than 6oC
per minute
2. The test flame should be lighted and adjusted so that it is of the size of a bead 4mm in
dia.
OBSERVATION
1.
2.
Rate of heating
Time in minutes
10
11
12
Temperature, C
Test property
1
Test Number
2
Mean value
3
1. Flash point
2. Fire point
3. Variations from mean value
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 18
RESULT
1. Flash Point = ..C
2. Fire Point = .C
PREACAUTIONS:
1. The test flame should neither be larger than stipulated nor be applied more frequently
than specified as the surface layer may get super heated.
2. The bluish halo that sometimes surrounds the test flame should not be confused with
the true flash.
INTERPRETATION OF RESULTS
The determination of flash point is helpful in assessing the safe limits of heating the bitumen.
The heating temperature of bitumen should be limited well below the flash point. IS: 73-1992 &
2006 have recommended the value of flash point as follows;
Reference: - IS: 73-1992
S-35
S-45
S-55
S-65
S-90
S-200
A-35
A-55
A-65
A-90
VG-10
VG-20
VG-30
VG-40
175
175
175
175
175
175
175
175
175
175
220
220
220
220
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 19
Experiment No-6
2.
3.
4.
5.
6.
7.
Briquette Mould
PROCEDURE:
1. The bitumen sample is heated at the temperature between 75 to 100 deg C to bring it in
fluid state.
2. In order to prevent the material under test from sticking, coat the surface of the plate
and interior surface of the sides of the mould with a mixture of glycerin and dextrin.
3. Pour the heated bitumen in the briquette assembly and placed on a brass plate.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 20
4. The whole assembly including bitumen briquette along with brass plate is allowed to
cool in air for about 30 to 40 minutes.
5. The excess bitumen is cut and surface is leveled with the help of a hot knife.
6. The whole assembly now is kept in a water bath maintained at 270.5C for about 85 to
95 minutes.
7. The side of the mould removed, the clips hooked on the machine and the pointer
adjusted to zero value or initial reading noted.
8. Now the clips are pulled apart horizontally at the rate of 50.0 2.5 mm per min. and the
distance up to the point of breaking of thread is noted. This distance in centimeter gives
the value of ductility of bitumen.
9. The ductility of bitumen may vary from 5 to 100 for different bitumen grades, but for
satisfactory performance it should not be less than 50.
OBSERVATION:
1.
2.
3.
4.
Ductility in cm
1
2
3
RESULT
Avg. ductility value of the given bitumen sample = ..cm
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 21
PRECAUTIONS:
1. The plate assembly upon which the mould is placed shall be perfectly flat and level so
that the bottom surface of the mould touches it throughout.
2. In filling the mould, care should be taken not to disarrange the parts and thus distort the
briquette and to see that no air pocket shall be within the mould.
INTERPRETATION OF RESULTS
A normal test is one in which the material between the two clips pulls out to a point or to a
thread and rupture occurs where the cross-sectional area is minimum. Report the average of
three normal tests as the ductility of the sample, provided the three determinations be within
0.5 percent of their mean value.
If the values of the three determinations do not lie within 0.5 percent of their mean, but the
two higher values are within 0.5 percent of their mean, then record the mean of the two
higher values as the test result.
Reference: - IS: 73-1992
S-35
S-45
S-55
S-65
S-90
S-200
A-35
A-55
A-65
A-90
VG-10
VG-20
VG-30
VG-40
50
75
75
75
75
---
10
15
15
15
75
50
40
25
DISCUSSION:
Write the discussion/suitability of bitumen according to your result obtained.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 22
Experiment No-7
2.
To determine the suitability of bitumen for its use under different climatic condition and
type of construction
APPARATUS/EQUIPMENTS REQUIRED:
1.
2.
3.
4.
5.
6.
THEORY:
This test is applied almost exclusive bitumen. For tars, cutback and emulsions other consistency
are used. This test determines the hardness or softness of bitumen by measuring the depth in
millimeter to which a standard loaded needle will penetrate vertically in 5 seconds while the
temperature of the bitumen sample is maintained at 25C.
This test is widely used world over for classifying the bitumen into different grades. 80/100
bitumen denotes that the penetration value ranges between 80 and 100.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 23
PROCEDURE:
1. The bitumen is softening to a pouring consistency at a temperature not more than
60C for tars and 90C for bitumen and Stir it thoroughly to remove air bubbles and
water.
2. Pour it into a container to a depth of at least 15mm in excess of the expected
penetration.
3. Cool it at an atmospheric temperature of 15 to 30C for 1 to 1.5 hours for 35 mm
depth container and 1.5 to 2 hrs for 45 mm deep container. Then place it in a
transfer dish in the water bath at 25.0 + 0.1C and allow it to remain for 1 to 1.5
hours for 35 mm deep container and 1.5 to 2 hrs for 45 mm deep container.
4. At the end of one hour, the sample is taken out of water bath and needle is brought
in contact with the surface of bitumen sample and the reading of dial is set at zero
or the reading of dial noted, when the needle is in contact with the surface of the
sample.
5. Now the needle is released and allowed to penetrate for 5 seconds and the final
reading is recorded on the same sample at least three penetration observations
should be taken at distances at least 10 mm apart. After each test, the sample
needle is disengaged, wiped wit benzene or petrol and dried.
6. The mean value of three measurements is reported as penetration test.
7. The accuracy of the test depends upon pouring temperature, size of needle, weight
placed on needle, and test temperature.
OBSERVATION:
1. Pouring temperature, C
= .
3. Room temperature, C
= ..
= ..
= ..
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 24
Trial Numbers
Readings
1
PRECAUTIONS:
1. There should be no movement of the container while needle is penetrating into the
sample.
2. The sample should be free from any extraneous matter.
3. The needle should be cleaned with benzene or petrol and dried before each
penetration.
INTERPRETATION OF RESULT
The grade of bitumen is specified in terms of penetration value. 30/40 grade bitumen indicates
the penetration value of the bitumen in the range of 30 to 40 at standard test conditions.
Penetration test is applied exclusively to bitumen. Tars being soft, penetration test on these
materials cannot be carried out.
Reference: - IS: 73-1992
S-45
S-55
S-65
S-90
S-200
A-55
A-65
A-90
50-60
60-70 80-100
VG-20
VG-30
VG-40
80-100
60-80
50-70
40-60
DISCUSSION:
Write the discussion/suitability of bitumen according to your result obtained.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 25
Experiment No-8
2.
3.
4.
5.
6.
PROCEDURE:
1. Sample material is heated to a temperature between 75 and 100C above the
approximate softening point until it is completely fluid.
2. Place the rings on a metal plate and coat its surface with mixture of glycerin and dextrin.
3. Fill the molten bitumen in the rings in sufficient quantity to give an excess above the
level of the ring.
4. Cool the specimen in air for about 30 minutes.
5. After cooling in air level the material in the ring by removing the excess with a warmed
sharp knife.
6. The bitumen test sample placed in the brass ring is suspended in distilled water at a
given temperature.
7. A steel ball is put on the bitumen and the water bath is heated such that the
temperature of water bath rises by 5C per minute.
8. The temperature at which the softened bitumen touches the metal plate placed at a
specified distance (25 mm) below the ring is noted. This temperature is called the
softening point of the bitumen. Higher the softening point, harder the grade of the
bitumen.
OBSERVATION:
1. Bitumen grade: .
2. Approximate softening point: ...
3. Liquid used in the bath: ..
4. Period of air cooling, minutes: ..
5. Period of cooling in water bath, minutes = ..
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 27
RATE OF HEATING:
Time ( minutes)
1
2
3
4
5
6
7
8
Temperature (C)
Time (minutes)
9
10
11
12
13
14
15
16
Temperature (C)
OBSERVATION TABLE:
Test property
Trial-1
Ball Number
(i)
(ii)
Trial-2
Ball Number
(i)
(ii)
Mean value
softening point
Temperature(C) at which
sample touches bottom plate
RESULTS:
Avg. Value of Softening point = .Deg C
PRECAUTIONS:
1. Distilled water should be used as the heating medium
2. During the conduct of test the apparatus should not be subjected to vibrations.
3. The bulb of the thermometer should be at about the same level as the rings.
INTERPRETATION OF RESULTS:
Softening point indicates the temperature at which binders possess the same viscosity.
Bituminous materials do not have a definite melting point. Rather the change of state from
solid to liquid is gradual and over a wide range of temperature. Softening point has particular
significance for materials that are to be used as joint and crack fillers. Higher softening point
ensures that they will not flow during service. In general, the higher the softening the lesser the
temperature susceptibility. Bitumen with higher softening point may be preferred in warmer
places.
S-35
S-45
S-55
S-65
S-90
S-200
A-35
A-55
A-65
A-90
VG-10
VG-20
55-65
50-60
50-60
45-55
40-55
30-45
55-70
45-60
45-60
35-50
40
45
VG-30 VG-40
47
50
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 28
Experiment No-9
3.
4.
5.
6.
Filter paper,
Balance
Commercial benzene or petrol
A sample of 500 gm.
10. Repeat the procedure (not less than 3 washings) until the extract is no longer cloudy and
is fairly light in color.
11. Remove the filter paper from the bowl and dry in air.
12. Brush the loose particles from the filter into the bowl
13. Dry the filter to constant weight in an oven at 980 C to 105o C.
14. Obtain the weight of the filter and bowl with dry aggregates
OBSERVATIONS & CALCULATIONS:
S.No
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
Particulars
Trial-1
Trial-2
Trial-3
BEFORE TEST
Weight of bowl + sample (W1), g
Weight of bowl (W2) g
Weight of filter (W3), g
AFTER TEST
Weight of bowl + sample (W4),g
Weight of filter (W5), g
Weight of sample (W1-W2), g
Weight of aggregates in bowl (W4-W2), g
Weight of aggregates in filter (W5-W3), g
Weight of aggregates WA = (W4-W2) + (W5-W3)
Weight of bitumen, WB = (W1-W2) - WA
W
Bitumen content = B 100%
WA
REPORTING OF RESULTS:
Bitumen Content in given sample = . %
PRECAUTIONS
1. Separate the particles of the mixture as uniformly as possible taking care not to fracture
the mineral particles.
2. The cover plate should be fixed tightly on the bowl.
INTERPRETATION OF RESULTS:
The results of the test are an indication regarding the quantity of bitumen that has been used in
bituminous mix. By performing this field test a substantial saving in the cost of bitumen can be
had by ensuring that the optimum quantity of bitumen has been provided. Also the
performance of the road will be affected if lesser or more quantity of bitumen is used.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 30
Experiment No-10
OBJECTIVES
1. To determine the strength (Marshall Stability Value) and flexibility (flow value)
for the given bitumen mixture.
2. To determine the density-voids analysis for the given bituminous mixture;
3. To determine the suitability of bituminous mixture to meet the specified criteria
for the surface course.
INTRODUCTION
Bruce Marshall, formerly bituminous engineer with Mississippi State Highway
Department, USA formulated Marshall Method for designing bituminous mixes.
This test is done to determine the Marshall stability of bituminous mixture. The
principle of this test is that Marshall Stability is the resistance to plastic flow of
cylindrical specimens of a bituminous mixture loaded on the lateral surface at 5 cm per
minute. It is the load carrying capacity of the mix at 60oC and is measured in kg.
The sample needed is From Marshall stability graph, select proportions of coarse
aggregates, fine aggregates and filler in such a way, so as to fulfill the required
specification. The total weight of the mix should be 1200 gm for one specimen.
EQUIPMENT/APPARATUS
The apparatus for the Marshall Stability test consists of the following:
1. Specimen Mould Assembly comprising mould cylinders 10 cm diameter x 7.5 cm
height, base plate and extension collars. They are designed to be interchanged with
either end of cylindrical mould. Three mould cylinders are recommended.
2. Specimen extractor for extracting the compacted specimen from the mould. A
suitable bar is required to transfer load from the extension collar to the upper
proving ring attachment while extracting the specimen
3. Compaction Rammers having a flat circular tamping face 4.5kg sliding weight
constructed to provide a free fall of 45.7cm. Two compaction rammers are
recommended.
4. Compaction pedestal consisting of a 20 x 20 x 45 cm wooden block capped with a 30
x 30 x 2.5 cm MS plate to hold the mould assembly in position during compaction.
Mould holder is provided consisting of spring tension device designed to hold
compaction mould in place on the compaction pedestal.
5. Breaking head. The Breaking head consist of upper and lower cylindrical segments
or test heads having an inside radius curvature of 5 cm. The lower segment is
mounted on a base having two perpendicular guide rods which facilitate insertion in
the holes of upper test segments. assembly with provision to fix flow meter
6. Loading Machine motorized, loading machine is provided with a gear system to lift
the upward direction. Recalibrated proving ring of 5 tone capacity is fixed on the
upper end of the machine, specimen contained in the test head is placed in between
the base and the proving ring. The loading jack produces uniform vertical movement
of 5 cm/ min. Machine is capable of reversing its movement downward also. This
facilitates adequate space for placing test head system. After one specimen has
been tested.
7. Flow Meter. The flow meter consists of guide sieve and a gauge. The activating pin
of the gauge slides inside the guide sleeve with a slide amount f fractional
resistance. Least count of 0.025mm is adequate. The flow value refer top the total
vertical upward movement form the initial position at zero load to value at
maximum load. The dial; gauge at the flow meter should be able to measure
accurately the total vertical movement upward.
In addition to the above the following general equipments are also required
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 32
Bitumen Mixer, Digital & Manual Compactor, Moulds and Marshall Stability Test Apparatus
NOTES:
1. At least 2 specimens (but preferably 3 or 4 specimen) for each combination of
aggregate and bitumen should be prepared.
2. For surface course with 12 mm aggregate, the expected optimum bitumen
content may be about 6.5 %. Therefore specimen should be made at 5.5 %, 6.0
%, 6.5 %, 7.0 % and 7.5 % bitumen content.
-----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
D.B.M.
Grading
B.C.
2
Layer thickness
S.No
S.D.B.C.
75-100
IS Sieve Size
50-75
40
25
19 mm
13.2 mm
50
25/40
45 mm
100
37.5 mm
95-100
100
26.5 mm
63-93
90-100
19 mm
--
71-95
100
13.2 mm
55-75
56-80
90-100
9.5 mm
--
--
4.75 mm
38-54
2.36 mm
100
90-100
100
100
59-79
90-100
70-90
90-100
52-72
70-88
38-54
35-51
35-51
35-55
53-71
28-42
28-42
24-39
24-39
28-44
42-58
1.18 mm
--
--
15-30
15-30
20-34
34-48
10
600 microns
--
--
--
--
15-27
26-38
11
300 microns
7-21
7-21
9-19
9-19
10-20
18-28
12
150 microns
--
--
--
--
5-13
12-20
13
75 microns
2-8
2-8
3-8
3-8
2-8
4-10
14
4.0 %
4.5 %
4.5 %
5.0 %
5.2 %
5.4 %
IS Sieve
600 microns
300 microns
75 microns
TEST PROCEDURE
1. In conducting the stability test, the specimen are heated at a temperature of 60
10 C (37.8 10C for specimens in which tar has been used in place bitumen),
either in a water bath for 30-40 minutes or in an oven for a minimum of 2 hours.
2. Remove the specimens from the water bath (or oven) and place the lower
segment of the breaking head. Then place the upper segment of the breaking
head on the specimen and place the complete assembly in position of the
Marshall testing machine.
3. Place the flow meter (dial gauge) over one of the post and adjust into read zero.
4. Apply a load at a rate of 50 mm per minute until the maximum load reading is
obtained.
5. Record the maximum load in Newton (N). At the same instant obtain the flow as
recorded on the flow meter in unit of mm.
6. The total time between removing the specimen from the bath and completion of
the test should not exceed 30 seconds.
RECORD OF OBSERVATIONS
1.
2.
3.
4.
NOTE:
1. The measured stability of a specimen multiplied by the ration for the thickness of
specimen is equal to the corrected stability for a 63.5 mm specimen.
2. Volume-thickness relationship is based on a specimen diameter of 10 cm.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 35
COMPUTATION OF RESULTS
S. No. Determinations
1
Weight of Compacted Specimen , Wm in gm
2
Volume of Compacted Specimen, Vm .r 2 .h in cm3
Trial-1
Trial-2
Wm
, g/cm3
Vm
0.99
0.99
2.70
2.70
Gt
W1 W 2 W 3 W 4 W b
Or , G t
W1
W2
W3
W4
Wb
G1
G2
G3
G4
Gb
W
W
G
agr
agr
agr
Wm
Wm Ww
Wb
Gb
Percent Volume of Bitumen V
b
W1 W 2 W 3 W 4 W b
Gm
11
12
13
14
Wb
Gb
Gt
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 36
CORRECTION FACTOR
It is possible while making the specimen the thickness slightly vary from the standard
specification of 63.5 mm. Therefore, measured stability values need to be corrected to those
which would have been obtained if the specimens had been exactly 63.5 mm. This is done by
multiplying each measured stability value by an appropriated correlation factors as given in
Table below.
Volume of Specimen in Cubic
Centimeter
457 470
471 482
483 495
496 508
509 522
523 535
536 546
547 559
560 573
Approximate Thickness of
Specimen In mm
57.1
58.7
60.3
61.9
63.5
65.1
66.7
68.3
69.9
Correction Factors
1.19
1.14
1.09
1.04
1.00
0.96
0.93
0.89
0.86
Viscosity
Modified Bitumen
Graded (VG) Hot Climate
Cold Climate
Bitumen
75 blows on each face of the specimen
9.0 (900 Kg) 12.0 (1200 Kg) 10.0 (1000 Kg) AASHTO T245
24
2.5 4
3.5 5
25
35
2.5 5
35
2.5 5
35
65 75
65 75
65 75
80 % Minimum
95 %
Minimum
95 %
Minimum
Test Method
AASHTO T245
MS-2 & ASTM
D2041
MS 2
AASHTO T283
IS: 6241
4
15
14
13
12
11
5
16
15
14
13
12
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 37
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 38
Experiment No-11
DEFLECTION:
Pavement surface deflection measurements are the primary means of evaluating a flexible pavement
structure and rigid pavement load transfer. Although other measurements can be made that reflect (to
some degree) a pavement's structural condition, surface deflection is an important pavement
evaluation method because the magnitude and shape of pavement deflection is a function of traffic
(type and volume), pavement structural section, temperature affecting the pavement structure and
moisture affecting the pavement structure.
Deflection measurements can be used in back calculation methods to determine pavement structural
layer stiffness and the sub grade resilient modulus. Thus, many characteristics of a flexible pavement
can be determined by measuring its deflection in response to load. Furthermore, pavement deflection
measurements are non-destructive.
EQUIPMENT/AAPARATUS:
Benkelman Beam consists of a slender beam 3.66 mtr long pivoted at a distance of 2.440 mtr
from the tip as shown in fig below and a loaded truck (8 to 10 tons).
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 39
The equipment is light weight and made of aluminium for easy portability and
use at any test location.
The apparatus is compact, unique and possess a telescopic design for quick set up
and storage during transport to the test location.
The equipment is supplied in two parts for assembling on site with easy hand
tools.
One end of the beam rests at a point under investigation while the beam is
pivoted in the centre.
The free end carries a dial gauge to record the deflections. The other end is kept
on a stable platform.
The beam is put in contact with the pavement under test between the tires of
the vehicles.
The measurement of the deflection is carried out when the vehicle passes over
the test area.
UTILITY
Direct reading of deflection dial indicators eliminates the need for conversions or
calculations during measurement.
It is used to measure the deflection of the road surface when loaded by the
wheels of vehicles.
ACCESSORIES
APPLICATIONS
PROCEDURE
Deflections shall be measured as follows:
1. The test point shall be pre-selected and marked. For highway pavements, test point
shall be located at the distances from the edge of the lane given in table below;
Lane width
(meters)
2.8 or less
0.5
3.0
0.6
3.2
0.7
3.4
0.8
3.6 or more
0.9
2. The tyre pressure should be checked before the first test and then at intervals not
exceeding three hours.
3. The truck shall initially be positioned with the test wheel between 100 and 150 mm to
the rear of the test spot, i.e. Position A.
4. The probe of the beam shall be inserted between the dual tyres of the test wheel with
the toe located on the test spot.
5. The locking device shall be released and the rear of the beam adjusted so that the
plunger is in contact with the dial gauge.
6. The dial gauge shall be set to road between 9 and 11 mm (the actual reading need not
be recorded) and the vibrator set in operation.
7. The truck shall be moved forward at creep speed so that the test wheel passes over the
test spot and continues advancing to position B which is 2.7+0.1 meters beyond the test
spot.
8. The START READING, S is the maximum dial gauge reading occurring during this
movement of the truck from position A to position B, and will normally occur as the
wheel passes over the test spot. This reading shall be recorded.
9. The INTERMIDIATE READING, I is that figure indicated by the dial gauge at the
movement the truck stops with the test wheel in the position B. This reading shall be
recorded.
10. The truck shall be moved forward until the test wheel is in position C which is not less
than 10 meters from position B.
11. The FINAL READING, F is that figure indicated by the dial gauge when the truck has
stopped in position C. this figure shall be recorded.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 41
Temperature measurements must be made when the top layer of the pavement consists of 40
mm or more of bitumen bound material .The following procedure should be followed:
1. A hole should be made with the mandrel to a depth of 40mm or to such a depth that it
does not break through the bitumen bound material.
2. The hole should be filled with glycerol or oil and the thermometer inserted.
3. The temperature should be recorded at least hourly, or at decreasing time intervals
down to 15 minutes when successive temperatures differ by more than 3 C.
No beam readings should be made outside the pavement temperature range of 5C to 30C
when the top layer of the pavement consists of 40 mm or more of bitumen bound material.
3. 60 M
0.90
15.00M
11.75M
HIGHWAY
2.75 M
0.0 M A
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 42
OBSERVATIONS
All reports shall include the following;
(a)
(b)
(c)
(d)
(e)
(f)
(g)
Name of Road
Section/Location
Lanes
Distance from lane edge.
The actual axle load used.
The rebound deflection of the pavement (to 0.01mm).
The date and time of readings.
Location of Pavement
Type of
test point Temperature soil &PI
Moisture
content
Final
(F)
Rebound
deflection
(mm)
1
2
CALCULATIONS
The rebound deflection of the pavement shall be calculated in the following manner.* *
1. Two pavement rebound indicators shall be established by subtracting the intermediate
and final readings from the start reading, i.e. (S I) and (S F)
2. If the indicators so obtained agree within 0.03 mm the true rebound deflection at
temperature T shall be calculated as: XT = 2(S F)
3. If the indicators (S I) and (S F) differ by more than 0.03 mm* * * the initial shape of
the bowl has been such as to influence the front support legs of the instrument and the
calculations shall be adjusted as follows: XT = 2 (S F ) + 5.82 (I F)
4. The pavement rebound deflection at a standard temperature of 20C shall be
20 t
calculated from the above figure by applying the formula: X 20 X T
110
Where,
X20 = temperature corrected rebound deflection in millimeters and
t = temperature in degrees Celsius 40 mm below the surface of the pavement.
Note:
** If the dial gauge has been modified to road pavement deflection directly, the questions in 4.1 (b) and
(c) must be divided by 2.If the dial gauge is graduated in an anticlockwise direction the terms within
which the brackets will have to be reversed to give a positive value.
***A larger difference can be tolerated if it is confirmed while testing that the legs of the beam are not
sitting in the bowl.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 43
Experiment No-12
VISCOSITY TEST
(REFERENCE: - IS: 1206-1978)
OBJECTIVE:
To determine the viscosity of road tar/bitumen.
APPARATUS/EQUIPMENTS REQUIRED:
Ten millimeter orifice viscometer is specified for testing road tar and is called tar
viscometer, 4.0 mm orifice is used to test cutback grades, 0 and 1 and 10 mm orifice to
test all other grades. The apparatus consists of main part like cup, valve, water bath,
sleeves, stirrer, receiver and thermometers, etc.
THEORY:
Viscosity is the measure of resistance to flow. It is measured by recording the time in
seconds taken by 50 c.c. of the material to flow through a specified orifice of standard
dimension into a receiver at specified temperature.
PROCEDURE:
1. The tar cup is properly leveled and water in the bath is heated to the
temperature specified for the test and is maintained throughout the test. Stirring
is also continued.
2. The sample material is heated at the temperature 20C above the specified test
temperature, and the material is allowed to cool.
3. During this the material is continuously, stirred.
4. When material reaches slightly above test temperature, the same is poured in tar
cup, until the leveling peg on the valve rod is just immersed.
5. In the graduated receiver (cylinder), 20 ml of mineral oil or one percent by weight
solution of soft soap is poured.
6. The receiver is placed under the orifice.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 44
7. When the sample material reaches the specified testing temperature within
0.1C and is maintained for 5 minutes, the valve I opened.
8. The stop watch is started, when cylinder records 25ml.
9. The time is recorded for flow up to a mark of 75ml. (i.e., 50ml of test sample to
flow through the orifice).
The viscosity test on road tar is carried out using 10 mm orifice and the standard test
temperature for road tar grades RT1, RT2, RT3, and RT4 are 35, 40, 45, and 55C respectively. In
case the viscosity test is being carried out to classify a given sample of road tar of to find its
grade, then the test should be first conducted at the lowest temperature of testing road tar, i.e.
35C; if the time taken for 50ml of the tar sample to flow through the 10 mm orifice is more
than 55 sec, of if the sample does not flow freely test may be repeated at the next higher
temperature, till the viscosity value falls in the specified range.
The viscosity test on cutback bitumen is carried out using 4.0 mm orifice for grades 0 and 1 (SC
0, MC 0, RC 0, SC 1, MC 1, RC 1, at 25C). The test for cutback grades 2 and 3 are
carried out at 25C using 10 mm orifice and those for grades 4 and 5 are carried out at 40C
using 10 mm orifice. For details of requirements of cutbacks see Tables 23.1 a, b & c. if the
viscosity of an unknown grade of cutbacks, is to be determined, the orifice size and the trial test
temperature may be chosen using judgment. If the viscosity value of the trial test does not fall
within the specified range, test should be repeated by altering the test temperature or orifice
size of both suitably.
OBSERVATION:
1.
2.
3.
4.
5.
Material: .
Grade: .
Specified temperature, C =
Size of orifice, mm = .
Actual test temperature, C
Test Property
1
Test run
2
Mean value
3
Viscosity in seconds
Repeatability, percent
RESULTS
For test sample =
Standard value = .
%age error =.
PRECAUTIONS:
REMARKS:
DISCUSSION:
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 45
Experiment No-13
PROCEDURE
1. Clean, dry and weigh the specific gravity bottle along with the stopper (Weight
A).
2. Fill the specific gravity bottle with freshly boiled distilled water and insert the
stopper firmly. Keep it in the water bath having a temperature of 27.0 + 1oC for
not less than half an hour and weigh it (Weight B).
3. Weigh the specific gravity bottle about half-filled with the material (Weight C).
4. Weigh the specific gravity bottle about half-filled with the material and the other
OR,
i) Specific gravity (Solids and semi-solids) = (C-A)/ [(B-A) - (D-C)]
ii) Specific gravity (Liquids) = (E-A)/ (B-A)
RESULT:
Specific Gravity of bitumen =
The average of the two results should be reported.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 47
Experiment No-14
3 . The aggregate and binder are mixed thoroughly till they are completely
coated and mixture is transferred to a 500 ml beaker and a l l o w e d t o
cool at room temperature for about two hours.
4. D i s t i l l e d water is then added to immerse the coated aggregates.
5 . The beaker is covered and kept in a water-bath maintained at 40 0C
taking care that t h e l e v e l o f w a t e r i n t h e w a t e r - b a t h i s a t l e a s t
half the height of the b e a k e r .
6. A f t e r 2 4 h o u r s t h e b e a k e r i s t a k e n o u t c o o l e d a t
r o o m temperature and the extent of stripping is estimated visually while the
specimen is still under water.
7. The stripping value is the ratio of the uncovered area observed visually to the
total area of aggregates in each test, expressed as percentage.
8. The mean of three results is reported as stripping value of the t ested
aggregates and is expressed as the nearest whole number.
OBSERVATIONS
CALCULATION
Road aggregate stripping value = percent fines =
W2
100
W1
RESULT:
The result is reported as the percentage of stone surface that remains c o a t e d a f t e r
t h e s p e c i f i e d p e r i o d s , t h e m e a n v a l u e o f a t l e a s t t h r e e visually
estimated values, being rounded off to the nearest 5 percent.
PRECAUTION:
Care shall be taken while mixing aggregates with bitumen.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 49
Experiment No-15
THEORY
Soundness is the property of aggregate to resist disintegration when subjected to freezing and
thawing. The test is intended to study the resistance of Aggregates to weathering condition in
concrete or other applications. It is carried out to judge the durability of soundness of the
Aggregate.
In order to quicken the effect of weathering due to alternate set-dry and or freeze-thaw
cycles in the laboratory, the resistance to disintegration of aggregate is determined by soaking
the aggregate specimen in saturated solution of sodium sulphate or magnesium sulphate.
PREPARATION OF REAGENT.
1. Saturated solution of sodium sulphate (the anhydrous Na2SO4 or the crystalline
Na2SO4.10 H2O) is prepared in water at a temperature of 250 to 300C. It should be
ensured that the solution is saturated and excess salt is present.
2. The solution is maintained at a temperature of 27 2 C and stirred at frequent
intervals until it is used. At the time of using the solution should have a specific gravity
of not less than 1.151 and not greater than 1.171 and discolored solution should not be
used.
3. It may be necessary to use not less than 420 gm of anhydrous salt or 1300 gm of the
crystalline decahydrate salt per liter of water.
4. Alternatively saturated solution of magnesium sulphate may be prepared by dissolving
either anhydrous (Mg SO4) or crystalline (Mg SO4. 7H2O) magnesium sulphate. At the
time of using, the solution should have a specific gravity of not less than 1.295 and not
more than 1.308. Not less than 400 gm of the anhydrous salt or 1600 gm of the
crystalline hepta hydrate may be used per liter of water.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 50
PREPARATION OF SPECIMEN
Coarse Aggregate:
The specimen of coarse aggregate for the test may be prepared after removing the fraction
finer than 4.75 mm is sieve. The sample should be of such a size that it will yield not less than
the following amounts of the different size which should be available in amounts of 5 % or
more
Sieve size of square hole
Weight of specimen
10 mm to 4.75 mm
20 mm to 10 mm
Consisting of 12.5 to 10 mm -33%
20 to 12.5 mm -67%
40 mm to 20 mm
Consisting of 25 to 20 mm - 33%
40 to 25 mm 67%
63 mm to 40 mm
Consisting of 50 to 40 mm -50%
63 to 50 mm -50%
300 gm
1000 gm
3000 gm
1500 gm
3000 gm
Fine Aggregate
Fine aggregate for the test shall be passed through a 10 mm IS Sieve. The sample shall be of
such a size that it will yield not less than 100 gm of each of the following sizes which shall be
available in amount of 5 % or more, expressed in terms of the following sieves;
Passing IS Sieve
600 mic
1.18 mm
2.36 mm
4.75 mm
10 mm
Retained on IS Sieve
300 mic
600 mic
1.18 mm
2.36 mm
4.75 mm
PROCEDURE
1. The sample of coarse aggregate should be thoroughly washed and dried to a constant
weight at 105 to 110C and is separated to different size ranges.
2. The proper weight of the sample for each fraction is weighed and placed in separate
containers for the test. In the case of fraction coarser than 20 mm, the particles are also
counted.
3. The samples are immersed in the prepared solution of sodium suplhate or magnesium
sulphate for 16 to 18 hours in such a manner that the solution covers them to a depth
of at least 15 mm.
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 51
4. The containers are kept covered to reduce evaporation and during the period of
immersion, the temperature of the solution is maintained at 27 1C.
5. After the immersion period, the aggregates are removed from the solution, drained for
about 15 minutes and placed in the drying oven at 105 to 110C.
6. The samples are dried to a constant weight at this temperature by checking the weights
after 4 hours upto 18 hours.
7. When the successive weights differ by less than 1 g, it may be considered that constant
weight has been attained and then it may be allowed to cool to room temperature.
Then the aggregates are again immersed in the prepared solution, for the next cycle of
immersion and drying. The number of cycles of alternate immersion and drying are
minimum five (5) for road aggregates.
8. After completion of the final cycle, the sample is cooled washed free from the sulphate.
This may be determined when there is no more reaction of the wash water with barium
chloride (i.e. when there is no white precipitation when barium chloride is added to
wash water it can be said that there is no sulphate with wash water).
9. Each fraction of the sample is then dried to constant temperature of 105 to 110C and
weighed. Coarse aggregate fractions are sieved by IS sieves of sizes indicated below:
Size of aggregate
63 to 40 mm
31.5 mm
40 to 20 mm
16.0 mm
20 to 10 mm
8.0 mm
10 to 4.75 mm
4.0 mm
10. Each fraction of aggregate is examined visually to see if there is any evidence of
excessive splitting crumbling or disintegration of the grains. A combined sieve analysis of
all the material subjected to the above test cycles may also be carried out to note the
variation from the original grain size distribution of the sample.
OBSERVATIONS & CALCULATIONS
Sieve size
mm
Passing Retained
63
40
20
10
Total
40
20
10
4.75
Grading
original
sample
percent
%age passing
fine sieve
after test
(actual % loss)
Weighted
average
(corrected
percent loss)
3000
1500
1000
300
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 52
REFERENCES
Prepared By: M.L. Rathore (Lab Engineer), Civil Engg Dept, JUET Guna (M.P.): 53