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BACHELOR OF SCIENCE
CHEMICAL ENGINEERING (II)
SUBMITTED TO:
DEPARTMENT OF CHEMISTRY
SUPERVISED BY:
MR. KYAZZE PASCAL
Process Chemist, Works Department-Process Section (SCOUL)
30th May to 6th August 2016
DEDICATION
I dedicate this report to my beloved parents, Mr. Mafabi Patrick Gimei and Mrs. Nannozi Lucy,
for their encouragement, unconditional love and support that has made me the person I am today.
Thank you for believing in me and may the Almighty God reward you abundantly.
Also to my brothers, Mafabi Patrick and Gimei Peter, and my only beloved sister Nabisaawa
Christine whose love and company was very important to keep moving me forward. I wish you
the best in your future endeavors.
STUDENT DECLARATION
I, Gimei Benedict, humbly declare, that the work which is being presented in the Industrial
Training Report entitled THE PRODUCTION PROCESSES OF COMMERCIAL SUGAR
AT SUGAR CORPORATION OF UGANDA LIMITED (SCOUL), in partial fulfillment of
the requirements for the award of the Bachelor of Science in Chemical Engineering, and submitted
to the Department of Chemistry, Kyambogo University, is an authentic record of my own work
carried out during my industrial training period from 30th May 2016 to 6th August 2016 under the
supervision of Mr. Kyazze Pascal, Process Chemist Works Department (Process Section) at
SCOUL.
I also declare that, the matter presented in this Internship Report has not been submitted by me for
the award of any other degree elsewhere. It is only prepared for my academic requirement and not
for any other purpose. It should not be used with the interest of opposite party of the corporation.
Signature of Student
GIMEI BENEDICT
14/U/132/CHD/GV
B. Science in Chemical Engineering (Yr. 2)
Department Of Chemistry
Kyambogo University, Uganda.
0704649584 / gimibens@gmail.com
ii
APPROVAL
The undersigned certify that this Industrial Training Report has been submitted by Gimei
Benedict, Registration Number 14/U/132/CHD/GV, and to the department of Chemistry,
Kyambogo University, in partial fulfillment of the requirements for the award of the Bachelor of
Science in Chemical Engineering. We also certify that the above statement made by the student is
correct to the best of our knowledge. The training was carried out under special supervision and
within the time frame prescribed by the syllabus. We found the student to be hardworking, skilled,
bonafide and eager to undertake any commercial and industrial work related to his field of study
and hence we recommend the award of Bachelor of Science in Chemical Engineering.
Approved as to the style and content by:
Signature of Supervisor
MR. KYAZZE PASCAL
Process Chemist, Works Department-Process Section
Date: .
Signature & Stamp:
ACKNOWLEDGEMENTS
A great number of people have helped me in this internship training. First of all, I thank The
Almighty God, Who has enabled me produce this piece of work.
I would like to place on record my deep sense of gratitude to Mr. Obbo Vincent, Superintendent
Training, and the management of SCOUL, for the opportunity of the internship program.
I express my sincere gratitude to Mr. Kyazze Pascal, Industrial Chemist, Works Department
(Process Section), SCOUL, for his stimulating guidance, continuous encouragement and full
supervision throughout the course of present work, his support and effort to compile this report.
I am also indebted to Mr. Anwar Mubarak, Senior Deputy Manager, Works Department (Process
Section), SCOUL, for his generous guidance, help and constructive suggestions.
I would like to convey my thanks to the mechanical staff and electrical staff for giving me support
during maintenance work in the power house with mechanical and electrical engineering point of
views. In the Boiler house, I got support from Mr. Mugerwa Joseph (Boiler Engineer) and Mr.
Ssemwanga Siraj (Boiler Engineer), whose efforts provided me a valuable environment, in which
my practical growth occurred.
I also wish to extend my thanks to all the Process Chemists (Process House) especially Mr. Kirya
Keneth, Mr. Kizito Joel, Mr. Eyaru Francis, Mr. Iriso Richard and Laboratory Chemists, Mr.
Baryayefuza Frank, Mr. Woira Patrick and Mr. Alekuku Festos, and all my colleagues, for their
insightful comments and invaluable suggestions to improve the quality of this report work.
I am extremely thankful to my lovely niece, Miss Nambozo Winnie, Headmistress Mehta Central
Nursery, SCOUL, for providing me accommodation, meals and a valuable environment with
infrastructural facilities to work in, without which this work would not have been possible.
Finally, yet more importantly, I would like to express my deep appreciation to my parents, Mr.
Mafabi Patrick and Mrs. Nannozi Lucy, my sister and brothers for their perpetual support,
advice and encouragement that has enabled me reach this level as far as my Bachelors degree is
concerned. May the Almighty God reward them accordingly.
iv
ABSTRACT
Sugar Corporation of Uganda Limited, sugar factory with a distillery plant, is located at Lugazi
about 46 km west of Jinja along the main Kampala Jinja highway. SCOUL is one of the pioneers
of the sugar industry in Uganda. The main product of the company is commercial light-brown
and brown sugar. The working capacity of SCOUL sugar factory is 140 - 150 tons of crushing of
cane per hour. It has a maximum capacity of 160 tons of crushing of cane per hour.
The organization believes in strict adherence to commitment, discipline and fair business
principles. The operation activities of the factory revolve on its departments. There are different
types of employees who are hired at need basis, some employees are permanent who work for a
whole year and some are temporary (seasonal employees). The management is quite successful in
providing a congenital and co-operative atmosphere to its employees.
From the processing point of view, the production of cane sugar can be summarized in the
following way: Sugarcane is purchased from farmers (out-growers) or supplied from the company
estates and transported directly to the factory where it is weighed, conveyed, cutted, and fiberized.
Primary juice along-side juice from the second mill is then extracted by fiberized cane from the
milling operation and pumped for screening into a mixed juice tank for further processing. The
waste bagasse is used in the boilers as a fuel for the production of steam, in order to meet industrial
requirements. Excess bagasse is stored in the bagasse yard. The steam produced is supplied to
power house to run the turbines so as to generate electricity for the factory and also used to start
up motors that drive the milling operation. The sugar factory generates a total of 9.5MW of
electricity that it can also meet the energy requirements of Lugazi town if it is provided to them.
The mixed juice is then heated in different stages using exhaust steam supplied to process house.
Its then treated, clarified and evaporated to form concentrated solution (syrup). The syrup is then
sulphited and sent to vacuum pans for crystallization. Other by products are utilized for other
processes. The filter cake is utilized as fertilizer in the field, while final molasses that are separated
from the centrifugation process are supplied to ethyl alcohol production plant (distillery). The final
production of commercial light-brown sugar is about 2000 bags per shift. Each shift, is of 8 hours
and each bag is of 50kg. Therefore, final production is of about 250-300 tons/day.
TABLE OF CONTENTS
DEDICATION................................................................................................................................ i
STUDENT DECLARATION....................................................................................................... ii
APPROVAL ................................................................................................................................. iii
ACKNOWLEDGEMENTS ........................................................................................................ iv
ABSTRACT ................................................................................................................................... v
TABLE OF CONTENTS ............................................................................................................ vi
BACKGROUND OF INDUSTRIAL TRAINING .................................................................. viii
CHAPTER ONE ........................................................................................................................... 1
1.0 INTRODUCTORY PAGE ..................................................................................................... 1
1.1 Company Profile: .................................................................................................................... 1
1.2 Objectives of the Company: ................................................................................................... 2
1.3 Management and Organizational Structure: ....................................................................... 2
CHAPTER TWO .......................................................................................................................... 4
2.0 INTRODUCTION................................................................................................................... 4
2.1 What is Sugar? ........................................................................................................................ 4
2.2 Properties of Sucrose (Sugar): ............................................................................................... 4
2.3 Uses of Sucrose: ....................................................................................................................... 5
2.4 Nutrition and Health Aspects of Sucrose: ............................................................................ 6
2.5 Constituents of Sugar Cane: .................................................................................................. 6
CHAPTER THREE ...................................................................................................................... 7
3.0 SUGAR FACTORY FEED SECTION AND MILL HOUSE SECTION DETAILS ....... 7
3.1 Block Flow Diagram ............................................................................................................... 7
3.2 Feed Section (Delivery, Weighing, Off-loading & Handling of Cane) ............................... 7
3.3 Cane Preparation .................................................................................................................... 8
3.4 Mills ........................................................................................................................................ 10
3.5 The Milling Process............................................................................................................... 10
3.5.1 Imbibition at the Mills ....................................................................................................... 11
CHAPTER FOUR ....................................................................................................................... 12
4.1 Boiler ...................................................................................................................................... 12
4.2 Boiler Feed Water Treatment (Water Chemistry) ............................................................ 13
vi
vii
To collectively appreciate and transform the basic knowledge as acquired in the lecture rooms,
to a more productive and practical bit by physically and mentally engaging to the best of my
ability in the real world.
To execute more information judgment at work place and accept the responsibility for it.
To recognize that financial and economic factors play important role in all science and
technology activities.
To develop own personality and communication skills for future roles as managers and leaders
in the scientific and technological world.
To appreciate that science and technology are expanding disciplines and that learning is a
continuous process
viii
CHAPTER ONE
1.0 INTRODUCTORY PAGE
1.1 Company Profile:
Sugar Corporation of Uganda Limited (SCOUL) was established in 1924 as Uganda Sugar
Factory. It was wholly owned by the Late Nanji Kalidas Mehta. The business was incorporated in
1934 as a limited liability company for the purpose of producing sugar for both local and
international markets. In 1972, the owners left the country due to political upheavals and the assets
of the Uganda Sugar Factory were expropriated by the then Government of Uganda. In 1980,
however, the new Government invited the Mehta family and handed them back their assets under
the joint venture agreement where all the assets were vested in a new company known as Sugar
Corporation of Uganda Limited (SCOUL).
The new company was incorporated on the 26th May 1980. (Government 51% shares, Mehta
family 49% share-holding) and set out to establish a new plant and rehabilitate the sugar cane
plantation and other infrastructure at a massive cost of US$86.645 million. The new Sugar factory
was inaugurated on 26th, January 1988. Currently SCOUL is 100% owned by the International
Investment Corporation ltd (Mehta family) after Government handed over all its shares on 10th
August 2009. Before this ceremony, government shares stood 24% (Ministry of Finance).
Presently, SCOUL, comprises of agricultural land of over 11,000 hectares, a sugar plant, a
distillery and a CO2 plant. In addition to the sugarcanes produced in its estate, SCOUL also buys
sugarcanes from out growers. The sugarcanes are processed in the factory to produce sugar and
molasses (by-product). Molasses is further processed in the distillery to produce Extra Neutral
Alcohol (ENA) and Technical Alcohol (TA). The raw CO2 gas produced from fermentation of
molasses is sent to CO2 plant for purification. The factory normally works continuously for 10
months with a scheduled stop (shut down) of two months period every year.
1.1.1 Location of the Organization:
The manufacturing center is situated at Lugazi Municipal council about 46km west of Jinja along
the main Kampala Jinja highway.
1
To ensure total satisfaction and to have the best supply of the sugar.
To provide fair work environment with job security and equal opportunity for all.
KEY
CHAPTER TWO
2.0 INTRODUCTION
2.1 What is Sugar?
Sucrose in common language is known as sugar (table sugar). Sucrose having a chemical
formula is also known by its structural name (D fructofuranosylD
glucopyranoside). Its molecular weight is 342.3 g/mole. It belongs to the family of disaccharides
composed of glucose and fructose joined by an - glycosidic bond (refer to Figure 1).
Figure 1
2.2 Properties of Sucrose (Sugar):
2.2.1 Physical Properties of Sucrose:
Its physical properties are shown in Table-1
Property
Value
1587.9
Density, kg/m3
Melting point, 0C
160~186
2.59
415.8
Amorphous at 220C
90.2
4.750.26
10.5
called inversion and the resulting glucose-fructose mixture is called invert. Sugar is destroyed by
Ph extremes, and inadequate Ph control can cause significant sucrose losses in the sugar factory.
c) Alkaline degradation
At high Ph, sucrose is relatively stable; however, prolonged exposure to strong alkali and
heat converts sucrose to a mixture of organic acids (mainly lactate), ketones, and cyclic
condensation products. In aqueous solutions, sucrose is most stable at Ph 9.0.
d) Thermal Degradation
At high temperatures (160-180C), sucrose decomposes with charring, emitting an odor
of caramel. Acid catalyzed thermo-lysis causes decomposition to glucose and fructofuranosyl
cation. The latter reacts with sucrose to form a complex mixture of products, including
fructoglucan and several ketoses. These substances are examples of fructo-oligosaccharides
(FOS) and are known to promote the growth of beneficial intestinal micro-organisms.
2.3 Uses of Sucrose:
a) Food Applications: Its principle contribution to food is sweetness. However it provides many
other functionalities, e.g. mouth feel and moisture retention. Cereals and backed goods are the
leading consumers of sucrose, followed closely by confectionary products. It is used as a
preservative in jam and jelly. It lowers the freezing point of ice cream and other frozen desserts
to improve product mouth feel and texture.
b) Feedstock for Chemical Synthesis: Sucrose reacts with fatty acids to produce esters with
degrees of esterification (DE) from 1 to 8.
c) Fermentation Feedstock: Sucrose, in the form of beet or cane molasses, is a fermentation
feedstock for production of a variety of organic compounds including lactic, glutamic, citric
5
acids, glycerol, and some antibiotics. Rum is made by fermentation of cane molasses. Beet and
cane molasses are used for production of bakers and brewers yeast. Ethanol is produced for
use in alcoholic beverages, and as a fuel, solvent, and feedstock for organic synthesis.
d) Pharmaceutical Applications: Sucralfate, an aluminum salt of sucrose octasulfate, is used as
an antacid and antiulcer medication. Bis- and tris-platinum complexes of sucrose show promise
as an anti-tumor agents. Sucrose monoesters are used in some pharmaceutical preparations. A
sucrose polyester is under evaluation as a contrast agent for magnetic resonance imaging
(MRI). Oral administration of this substance opacifies gastrointestinal tract and eliminates the
need for purging prior to MRI.
2.4 Nutrition and Health Aspects of Sucrose:
For many years, there has been concern by medical professionals and nutritionists over the
effects of dietary sugar on human health. Sucrose has been implicated as a cause of juvenile
hyperactivity, tooth decay, diabetes mellitus and obesity, atherosclerosis, hypoglycemia and
nutrient deficiencies. The sugar task forces select committee on Nutrition and Human Needs
recommended a daily consumption of sugars at 10% of total calories.
2.5 Constituents of Sugar Cane:
CONSTITUENTS
% IN CANE
Dissolved
Sucrose
13%
Substances
Other
2%
Substances
Insolubles
Fiber
13%
Substances
Soil
2%
Water
100%
70%
Table 2
CHAPTER THREE
3.0 SUGAR FACTORY FEED SECTION AND MILL HOUSE SECTION DETAILS
3.1 Block Flow Diagram
The cane feed preparation, handling and juice extraction steps are shown in the diagram below:
Block Flow Diagram [Feed Section + Milling House]
Cane
Weigh-Bridge
Fibrizer
Equaliser
Cane carrier
Magnetic Separator
(70C)
Cane yard
Cane Kicker
Bagasse Elevator
Bagasse to
Boiler House
Mixed Juice
Tank
To Process House
Figure 2
3.2 Feed Section (Delivery, Weighing, Off-loading & Handling of Cane)
a) Delivery of Cane at the Factory:
The factory takes delivery of the raw material (sugar cane) directly at the factory
weighbridge. Cane transportation is done for 24 hours and is arranged by the factory by: Lorries,
trucks, tandems and trailers. All harvested canes, are transported to the factory within 36 hrs for
burnt cane and 48 hrs for green cane, from the time of harvesting, so as to avoid stale canes.
b) Weighing of Cane at the Weighbridge:
The weighing of cane is done at the factory weighbridge. There are two (2) inlets to the
7
weigh-bridges at the factory, one for out growers and the other for company contractors.
When the vehicles reach the weighbridge, the information and details of the farmer and cane are
entered and transferred onto a R.I.F.T. card. The first weighing is done after the removal of
trashes, and the second weighing is done after the removal of tops to get the gross weight of cane.
Upon off-loading, the empty vehicles are weighed again and their tare weight is taken. This finally
gives the net weight of which 5% of the cane is subtracted as tops and trashes and is allocated
to the particular grower by the weighbridge computer system.
c) Off-loading of Cane at The Cane Yard:
The factory cane yard is charged with receiving cane and offloading it safely for feeding to
feed tables, by use of several off-loading devices. The principal types of off-loading mechanisms
and equipment used at the factory cane yard are: Three (3) Sling bars (Lifting), Gantry crane
(Lifting), Hydraulic off-loaders and Mechanical off-loaders (Lifting).
3.3 Cane Preparation
Cane preparation involves three stages. Conveying of cane from feeder tables to cutters by
the Cane Carriers, Size reduction of the conveyed cane by the cane cutters and levelers to reduce
the cane to a length of about 10cm and finally Disintegration of cane by the Fibrizer to rapture
and expose sucrose cells for extraction by the mills.
a) Feed table:
The purpose of the feed table is to transfer the off-loaded sugar cane, onto the cane carrier.
There are four (4) Feed tables in the factory. Each feeder table is mounted with a Cane Kicker
that is used to even out the distribution of cane as it proceeds to the carrier. Conveyer belts and
impellers are also mounted on the feed table to transport the cane from feed point to cane carrier.
b) Cane Carrier:
The Cane Carrier is a moving apron that is generally supported by three chains and driven
independently, by an electric motor. It is a type of conveyer belt, consisting of both a drive and
non-drive shaft which carries cane from feed table and transports it towards the Cutters, Leveler,
Fiberizer, Equalisers, magnetic separator, mills, boilers, and finally to bagasse storage point. There
are three (3) cane carries at the factory namely: A, B1 and B2. They consist of a horizontal portion
and an inclined portion that conveys cane horizontally as well as vertically simultaneously.
8
3.4 Mills
A Mill is a machine which is used to extract the juice and separate the fiber from fiberized
cane. It consist of four (4) major components: Donnelly chute, Trash plate, Scrapers and Four (4)
rollers (top roller, underfeed roller, feed-roller & delivery/discharge roller)
3.4.1 Typical Layout of the Mills Configuration at SCOUL.
To Process
House
Rotary Screen
Bagasse to
Boiler
House
Fiberized
(70C)
Cane
Mill 1
Mill 2
Primary
Juice (Mill 1)
Mill 3
Mill 4
Mill 2 Juice
mill is collected in tanks as the bagasse is carried by Rake Elevators that are associated with each
mill. A biocide named Bussan is always added to the last mill juice tank to inhibit micro bio
activity that would lead to sugar losses.
3.5.1 Imbibition at the Mills
Imbibition is a general term which defines the process of adding water or thin juice to
bagasse in order to mix and dilute the juice concentration and maximize extraction. Bagasse, even
when subjected to high and repeated pressures never gives up all the juice it contains. It approaches
to a minimum moisture in the most favorable cases and retains a high proportion of juice,
amounting roughly to half its weight. In order to extract as much as possible of the sugar which it
retains, Simple and Compound Imbibition is carried out.
Primary Bagasse from Mill 1 mixed with juice from Mill 3 while Bagasse from Mill 2 is
mixed with juice from Mill 4. This is termed as Compound Imbibition. Since the Bagasse moisture
content at Mill 3 cannot be reduced, the juice it comprises is replaced with water. In this process,
the bagasse is sprayed with water at 70C. This water spreads in the bagasse and dilutes the juice
which it contains. Mill 4 then recovers bagasse at limiting moisture (less than 49%). This moisture
will consist no longer of absolute juice but of diluted juice. Hence the sugar will have been
extracted and the operation is continuous.
a) A Rotary Screen filter:
It is used for separation of suspended bagasse particles from extracted juice.
b) Mixed Juice Tank:
It is a tank which stores extracted juice for further processing in process house.
c) Bagasse Elevator:
It is a type of inclined carrier which transports the bagasse (moisture of about less than 49%)
from last mill outlet to all boilers inlet and towards the bagasse storage point.
11
CHAPTER FOUR
4.0 BOILER HOUSE
4.1 Boiler
A Boiler is an equipment which is used to convert water into steam. The main type of boilers
installed at the factory are water tube boilers which use bagasse as a fuel. There are four (4) water
tube boilers installed at the factory, so further discussion will be related to water tube boilers only.
Steam Generation:
The furnace material is made of cast iron, furnace inside layer is made of refractory bricks,
middle is of insulating bricks and outer is cast iron. Furnace tube material is Mild Steel. Bagasse
from the last mill (Mill 4) is sent to the boilers by a bagasse elevator and is used as the fuel for
boiler furnaces. Bagasse having less than 49% moisture is burned. Air is supplied to furnace by
Forced Draft Fan, Secondary Fan, and Induced Draft Fan. The furnace is operated under negative
draft produced by maintaining a Speed Ratio of (F.D. Fan): (I.D. Fan) to 1:1.2. A steam super
heater is integrated with boiler and in this, saturated steam is converted to superheated steam by
exchanging heat with flue gases. An air pre-heater is also integrated with boiler. Flue gases enter
the air preheater at 220C and leave at 210C. 2 tons of steam is produced per ton of bagasse
combusted.
Superheated steam from all the four boilers combines in the common steam header at 400C
temperature and 34 kg/cm2 pressure, and then this steam is transferred to power house to run
turbines. When steam reaches the power house its temperature becomes 370 ~ 390C due to heat
losses to environment, while the pressure of the steam reduces to 30 kg/cm2 due to pressure drop
in pipes and valves. After steam turbines its temperature becomes near about 160C - 180C and
then it goes to steam desuperheater, where its temperature is reduced to 125C which is the
requirement of process house.
The boilers are installed to generate steam from water working with the following specifications.
Boiler(1,2,3,4) Specifications
Capacity Inlet
Water T
35
95C
tons/hr
Inlet
Water P
40
kg/cm2
Outlet
Steam T
360C
Outlet
Steam P
34
Furnace
T
780C
Outlet T
Outlet
Flue
Preheater
gases T
inlet T
390C
220C
Boiler
Bank
Air
210C
kg/cm2
Steam
Drum
De-aerator
FEED WATER
STORAGE TANK
Make-up water from
pre-boiler station
Mud
Drum
Booster
Pump
c) De-aeration:
In order to prevent corrosion in boilers and feed pipes, both dissolved oxygen and carbon
dioxide are eliminated from the boiler water. Oxygen is usually removed from boiler water by
thermal de-aeration. This is done by a pressure vessel known as a de-aerator.
4.2.1 Boiler Feed Water Specifications:
The following specifications are met in order to minimize scaling and maximize Boiler efficiency.
Property
Value
100-200 mg/l
Hardness
0%
PH
8.5 ~ 10
14
CHAPTER FIVE
5.0 POWER HOUSE
5.1 Turbines
A Turbine is a device which converts internal energy of a fluid to mechanical or useful work.
There are two fundamental types of turbines:
1) Hydraulic Turbine (Turbine driven by incompressible fluid)
a) Water Turbine (Turbine driven by water)
2) Pneumatic Turbine (Turbine driven by compressible fluid)
a) Steam Turbine (Turbine driven by superheated steam)
b) Gas Turbine (Turbine driven by any other dry gas)
In the power house at SCOUL, sugar factory, steam turbines are used, so major focus of
attention will be the steam turbine. A figure of a typical steam turbine is shown below:
()
=
()
()
Where: = () and = ( )
There are two (2) turbines used in power house. One of them generates 6MW of work power, and
the other generates 3.5MW of work power. Their specifications are given below;
16
Turbine Specifications
Turbines Steam
Power
Used
Inlet
Outlet Inlet
Temp Temp
Pressure
Outlet
No. of
No. of
Pressure
Rotations Rotations
before
after
reduction reduction
3.5 MW
1500 rpm
6 MW
38tons/hr 6MW
1500 rpm
390C 160C
Drive shaft
Steam
Turbines
Boilers
1,2,3,4
COMMON STEAM
HEADER
Alternator
A. C
Process House
CHAPTER SIX
6.0 PROCESS HOUSE
6.1 Block Flow Diagram (Process House)
()2
Juice
3 4
Mud Recirculation
Tank
Field as Fertilizer
Filter Cake
Clear
Juice
Heater
Evaporator
s
Sugar Drying
Mud-Bagacilo Mixer
Sugar Bagging
Storage
Treated Juice
Tank
Clarifier
Vapour Cell
Reaction tank
Syrup Sulphitation
Pan Boiling
Centrifugation
Cooling Crystallisers
To Market
18
40C
45C to 50C
Ph of juice
5 to 5.5
Heating Medium
19
45C to 50C
70C to 74C
Ph of juice
5 to 5.5
Heating Medium
it
swirls
around
the
tubes
Four
meter
long
tubes
depending
on
the
air
Equation of reaction:
()
Liming is then carried out after raw juice from the raw juice heaters has obtained a
temperature of 70C. At this temperature, the necessary activation energy is provided for the
reaction to take place. The reaction takes place in a reaction vessel. The vessel is mounted with a
stirrer, rotating to make the mixture homogeneous. The action of lime and heat neutralizes the
natural acidity of the raw juice and also yields insoluble precipitates from the calcium present in
the lime added and phosphates which are naturally present in cane juice. Calcium Phosphate is
the resultant precipitate formed upon liming.
Holding time is given as retention time in the reaction vessel to maintain the PH value at
specified point. This process is also good for enzymatic action on starch. The juice is kept at 70C
for about 10 minutes to allow enzymes in the juice to reduce starch content to an acceptable level.
Raw juice is limed to a PH value of 7.8 8.0, to reduce turbidity problems. Also, at this PH value,
sucrose is relatively stable. Inversion that would occur as a result low Ph and high temperature
would have been eliminated. Further heating to about 103C-105C is also applied for the reaction
to go to completion and also coagulate the albumin, waxes and gums.
b) Addition of Phosphoric Acid:
The success of flocculation is always dependent upon the extent of the calcium phosphate
precipitation and, therefore, on the concentration of the calcium and phosphate ions. Phosphoric
acid ( ) is always added to the juice as it leaves the reaction vessel to increase the
concentration of phosphate content in the juice in and guarantee enough time to form a floc of
good quality for proper clarification, and also give a slightly alkaline PH (7.3-7.6) prior to heating.
The addition of this acid, forms a coagulant known as Tri-Calcium Phosphate (complex).
The + ions adsorbed at the juice particle surfaces act as nuclei for this precipitation and the
impurities become incorporated into the coagulum with the calcium phosphate acting as bridges
between the impurity particles.
Equation of reaction:
+ +
( )
Tri-Calcium Phosphate
22
70C to 75C
103C to 105C
Ph of juice
7.3 to 7.6
Heating Medium
23
a) Flashing to 100C:
Flashing is the removal of all the dissolved air, non-condensable gases and vapors from
the treated juice and also air bubbles attached to the suspended particles to avoid undesirable
effects like flocs floatation during settling. This flashing is effected in a Flash tank. It is a simple
cylindrical tank located just above and ahead of the clarifier, with a flue open to the atmosphere.
Treated juice from the secondary / treated juice heaters discharges tangentially into this
tank. Since the treated juice that has been brought to about 103-105C, it partially flashes into
vapour when discharged into this vessel at atmospheric pressure, and in doing so, the flashing
causes a temperature drop to 100C. Likewise the juice entering at a high velocity is reduced to a
laminar flow (low and uniform speed) as it flashes and swirls in a tangential manner. Therefore
the juice going to the clarifier will be constantly at 100C to avoid formation of any convectional
currents and get rid of air or gas bubbles.
b) Addition of Magna flocculant:
The flocculant is added to the treated juice from the flash tank as it enters tangentially at the
top, into the feed compartment of the clarifier. This flocculant is a high molecular weight
polymer which attaches all suspended particles and impurities with it (it is sticky) and forms a
strong bond with them which causes the formation of mud. Addition of this flocculant improves
clarification and reduces the necessary settling time. The mud formed, having high density starts
to fall under the action of gravity to the bottom of the clarifier, which is known as Subsidation.
c) The Clarifier (Subsidation):
A clarifier is a vessel into which the treated juice to be settled is fed uniformly and
continuously, and which is large enough to reduce the velocity of flow and of circulation of the
treated juice to such a low value that it does not prevent settling from taking place. Its main purpose
is to clarify the treated juice by removing impurities in the form of mud. The time necessary for
settling always depends mainly on the difference in density between the treated juice and the
particles of the precipitate. There are two (2) clarifiers used at the factory and only one clarifier
operates in the season during production. The clarifiers used at SCOUL are Rapidor 444 type.
They consist of four (4) superimposed compartments, each fed separately by a rotating central
24
shaft by means of openings situated in the upper part of the compartment as shown in figure 13
below:
Bridge Support
Foam Chamber
Overflow
Box
Mud
Withdraw
Line
Feed
Compartment
Baffle
plate
Central shaft
Scrapper
Mud boot
Tray
Liquidating
Pump
Vertical tubes through the roof of the clarifier allow escape of gas from each compartment to
atmosphere.
6.2.4 Typical Layout of the Clarification Process at SCOUL.
Clear juice to vapour cell
Juice Heating
Defecation /Treatment
50C
Subsidation
Flash Tank
Mixed
()
Juice
70C
Floc
103C
Vapour Line
Juice Heater
Raw Juice Heater
Magna
Clarifier
100C
Treated Juice Tank
Reaction
Vessel
Treated Juice
Heater
The main factor controlling settling is the difference in density between the material to be
settled and the liquid in which it is mixed. This is effected by use of a high molecular weight
flocculant to increase on the settling rate of mud.
Treated juice, at the entry to the clarifier, should have a laminar flow (low and uniform
velocity). Higher rates of juice flow creates eddies which are detrimental to the settling.
Treated juice going to the clarifier should be constantly at about 100C. This is so to avoid
formation of convectional currents and get rid of air or gas bubbles attached to the suspended
particles which would prevent proper settling during the clarification process.
Holding time is given as retention time in the clarifier (about 2 to 2 hrs) for proper settling
in order to obtain a good quality of clear juice.
26
Mode of Operation:
The thick mud from the mud mixer goes into the vacuum filter where the juice is extracted
from the mud by suction with the help of vacuum pump. As the drum rotates, suction is applied
successively by vacuum in spider coils to three different segments / zones, forming a thin cake
on the filtering surface. There are three (3) vacuum zones in the vacuum filter:
by the sweet water tanks onto the cake. This is the beginning of the washing. After the last
drip pipe, vacuum is highest as drying of the cake commences. A light filtrate is obtained and
is sent to a light filtrate receiver bottle. This filtrate is pumped back to the reaction tank.
3) No vacuum zone: Just before the filter drum re-enters the liquid in the tank, it arrives at a
scraper formed by a rigid strip of rubber belting which bears lightly on the perforated screen.
When the filter section is about to reach the scraper, the distributor valve breaks the vacuum
which has held the cake against the filter surface. Then the slightest contact of the scraper
detaches the cake and it drops onto a belt conveyor which removes it outside the building.
6.3.1 Typical Layout of the Filtration Process at SCOUL.
Vacuum into rotary filter spider coils
Bagacillo
Cyclone Separator
Heavy
Filtrate
Mud-Mixer
Mud Trough
Light
Filtrate
Filter Cake
Damacide
Filtrate
Tank
Mud
Recirculation
Tank
Vacuum Pump
Pump
To reaction Tank
To field as fertilizer
29
6.4 Evaporation
Evaporation is a process of concentrating the solution by eliminating the solvent (water),
due to a high latent heat of vaporization of water. During this process, the brix (Bx) concentration
of the clear juice increases from around 13Bx to syrup of around 60Bx in order to promote the
growth of sugar crystals. Over 80% of water is eliminated in the clear juice by boiling it off. The
water is removed by boiling the juice in two (2) stages. Using a single effect evaporator vessel
(vapor cell) and using a series of multiple effect evaporator vessels. The evaporators are designed
and operated in such a way that the brix of the syrup lies between 60-64brix.
6.4.1 The Evaporator vessel and Heat Transfer Mechanism
The evaporators consist of a vertical cylinder, built onto a tubular calandria across which
heat exchange takes place. Exhaust steam and bled vapours are used as the heating medium for
concentrating the juice. The heating steam surrounds the outside of the calandria tubes and the
juice to be evaporated circulates inside the tubes. Vapour to metal tube (conduction) and from
metal tube to juice (convection). The heat transfer coefficients from vapour to metal and across
the metal surface are very high compared with that from metal to juice.
The vessel terminates vapour at the top in a save-all, which separates the liquid droplets that
may be entrained with the vapour from the juice. All the steam used for heating is transformed
into condensate in the calandria. Non-condensable gases are vented off by a small gas pipes
leading from the calandria to atmosphere for only vessels under atmospheric pressure and into the
vapour space of the vessel, to the exterior of the vessel for all vessels under vacuum.
a) Vapour Cell (Single Effect Evaporator)
Evaporation by heating with exhaust steam in a single vessel is called evaporation in single
effect. Clear Juice from the clear juice receiving tank is pumped to a clear juice heater, to raise
the temperature of the clear juice to boiling point (100C) and then admitted to the vapour cell.
The vapour cell is a separate single effect used to heat and evaporate almost 70% of the water
from clear juice, using low pressure steam (exhaust steam) at atmospheric pressure of about
0.5kg/cm2 at temperatures of about 120-125C. The vapours generated from heating the juice are
bled to pans and juice heaters. There are three (3) vapour cells installed at the factory.
30
120C
Body 1
Atm. p
Clear
Body 2
Vacuum
Entrainment Trapper
80C
Body 3
Vacuum
To Vapour
Line Juice
Heater
55C
Body 4
Vacuum
Juice
Juice
Exhaust steam
Gate - Valve
Siphon (U-tube)
To Syrup Sulphitor
Syrup
60Brix
Syrup Pump
Figure 17: Quadruple effect principle with Vapour Bleeding- Layout Diagram
During the evaporation process a certain amount of vapours drawn off the vessels is used
for heating and pan boiling. This practice is called vapour bleeding and results in steam saving /
steam economy. Exhaust steam at atmospheric pressure of 0 - 0.2 in Hg and temperature of 120125C is used for boiling clear juice in body 1. The vapors produced by evaporation of solution
are bled off and used in next effect as heating media. The vessels following the first body are put
31
under vacuum. Body 2 is at a higher vacuum than body 1, thus juices moves from body 1 to
body 2 by opening a gate-valve on a pipe connecting both bodies. Bled vapours from body 1 are
used to heat and evaporate the same solution at pressure of 5 8 in Hg and temperatures of 90100C. Body 3 is at a higher vacuum than body 2, juice will likewise move from body 2 to body
3 by opening a gate-valve on a pipe connecting both bodies. Bled vapours from body 2 are used to
heat and evaporate the same solution at pressure of 1218 in Hg and temperatures of 70-80C.
Body 4 is at the highest vacuum than all bodies, juice will likewise move from body 3 to
body 4 by opening a gate-valve on a pipe connecting both bodies. Bled vapours from body 3 are
used to heat and evaporate the same solution at pressure of 22 25 in Hg and temperatures of 5560C. The juice is boiled at a maximum level of two sight glasses in all evaporator bodies to
prevent entrainment. The vapour from the 4th body first passes through an entrainment
separator, to a vapour line juice heater, before its condensed in a condenser by spraying cold
water from the spray pond onto it to establish the vacuum in the evaporator set.
6.4.3 Creation of Vacuum for the Evaporator Set and Vacuum Pans
Water
Vapour
Hot water
Multi - jet
Condenser
10 meters
wind
Condensate
Pumps
Figure 18: Creation of vacuum and cooling effect of hot water condensate-diagram
32
Cold water from the spray pond is fed to the multi-jet condensers which is sprayed through jet
nozzles onto the vapours leaving the evaporator set and vacuum pans. The vapours condense to
form hot water condensate. In doing so, the necessary vacuum at atmospheric pressure of 101,325
K.pa is then created at a water leg of height 10 meters. The hot condensate is pumped back to the
spray pond for cooling by evaporation and the process is continuous.
6.4.4 Condensates
All the steam used for heating is transformed into condensate in the calandria. Condensate
from each vessel is extracted from a calandria under any vacuum to a condensate bottle attached
to a condensate pump, due to the pressure ruling in the calandria. The types of pumps used are
Centrifugal pumps. These pumps are provided with a small pressure-equalisation line to put
the admission valve of the body of the pump in communication with the top of the calandria so
that the condensate can easily flow. Condensate from the 1st vessel is sent directly for Boiler feed,
2nd vessel is first sent to Condensate tanks to Make-up for boiler feed, and 3rd and 4th vessels
are sent to sweet water tank and used for Imbibition, filter-cake washing and dilution of molasses.
Precautions:
1) Shut down condition: In shut down condition, water is circulated in the evaporator tubes to
avoid the risk of the tubes collapsing since the tubes are the heart of the evaporator.
2) Scale formation: Sodium hydroxide is circulated during heat exchanger cleaning to remove
the scaling. This is the salting out of materials that are deposited on the walls of heating tubes.
Scale formation causes clogging of tubes and thus reduce the heat transfer coefficient.
3) Corrosion: Many solutions attack ferrous metals thus causing damage to evaporators and
contamination of products. It is therefore important to use evaporators whose material of
construction is compatible with the solution being evaporated.
Calculation of Amount of Vapors Generated
Amount of vapors generated in the multiple effect evaporators is given by the following formula:
= (
) %
33
() + ()
()
The excess air is provided by an air compressor that supplies compressed air through nozzles.
The Sulphur-dioxide gas is then cooled by a tower of cooling pipes to about 70C. Syrup enters
the sulphitor at the top, while Sulphur dioxide enters the sulphitor via a perforated pipe located
near the bottom of the vessel and is bubbled through a mass of syrup. The process is countercurrent to expose all the syrup to the gas and enable even mixing since Sulphur dioxide is a light
gas and settles easily at the bottom. The final acidity or pH sought after Sulphitation is 5.5-6.0.
Precaution: In the presence of water, sulphur burns to give sulphuric anhydride (() ), instead
of sulphurous anhydride (() ). On reacting with water, (() ) immediately forms sulphuric
acid ( () ) that can easily corrode the pipes. Care is always taken to avoid the introduction
of water or moisture into the furnace. Accordingly, the air for combustion should always be dried.
34
Raw Syrup
300-350C
Sulphited Syrup to
70C
Pump
Syrup
Sulphitor
Cooling tank
Compressed air
Drain
Compressor
() gas
To Syrup
Tank
35
Syrup
A-Light
B-Heavy
A-Heavy
C-Light
60 (Bx)
A-Massecuite 94 (Bx)
A-Horizontal crystallizer
B-Massecuite 96 (Bx)
C-Massecuite 98 (Bx)
B-Horizontal crystallizer
C-Horizontal crystallizer
B-Vertical crystallizer
A-Centrifugals
A Sugar
A-Molasses
C-Vertical crystallizer
B-Centrifugals
B-Sugar
C-FW Centrifugals
B-Molasses
Melt
C-Melter
C-Sugar
C-AFW Centrifugals
2) Continuous Pans: This consists of a horizontal cylindrical vessel in which a heat exchanger
is arranged along its length. Vertical baffles longitudinally and transversely divide the vessel
into several compartments. There is only 1 Continuous pan (B-pan) at the factory.
6.6.2 Different Grades of Sugar boiling
Spontaneous formation n of new crystals occurs at Very High Super-Saturation Coefficients (SSC)
There are 3 zones or areas of super-saturation for pure sucrose; they are defined as:
Metastable zone: The SSC is high enough for added crystals to grow while no new crystals will
form. Sugar boiling is generally carried out here.
Intermediate zone: The SSC is high, where added crystals will grow and new crystals will form,
but only in the presence of existing crystals.
Labile zone: The SSC is very high; new crystals form spontaneously and crystals growth is rapid.
A Pan-boiling:
Depending on the raw materials available, A-light, B-seed, syrup/melt or even water is used
as the footing for A-strikes. The sugar boiler introduces into the A-pan a certain quantity (about
600cft) of syrup of about 80-83 purity with Sufficient B-seed (about 200cft), so that the calandria
is completely covered to improve the rate of nucleation. This is done after the vacuum in the pan
has reached 23-25Hg. Steam is then turned on into the calandria and the mixture is supersaturated
to a metastable zone. When the super-saturation has attained the required value, graining is carried
out by sudden introduction of small drinks of syrup. Hot water is usually added after every drink,
in case of any false grains and also make sure that the concentration does not fall too far. Graining
is continued with the addition of syrup or water until the level of the massecuite in the pan has
reached to about 4 glasses (about 1000cft) and to the required crystal size of about 0.8mm. This is
referred to as footing, i.e. when the pan is almost full. At this point, the massecuite is cut into half
to make two pans of A-grain (each about 500cft) and each pan is developed using syrup to about
3.5-4 glasses and tightened to the required brix of about 92-94 and required crystal size of
0.8mm. A-massecuite is then dropped to the A-horizontal crystallizers for further crystallization.
B Pan-boiling:
B massecuite is achieved using two types of pans. (Batch pan and a Continuous pan)
37
i)
B-Batch Pans: The raw materials used as the footing for B-strikes are: A-heavy and slurry.
Slurry: Is a mixture of icing sugar and rectified spirit. The purpose of slurry is to enable crystals
to grow faster or to enable seed graining to the pan where the super-saturation coefficient (SSC)
of the syrup is just short of the spontaneous crystal formation.
The sugar boiler introduces into the B-pan a certain quantity of sufficient A-heavy molasses
for making two pans after the vacuum in the pan has reached 23-25Hg. The massecuite is
supersaturated to a metastable zone. When the super-saturation has attained the required value,
graining is carried out by addition of a suitable amount of slurry. Hot water is usually added to
harden the grain and dissolve any false grains. Graining is continued with the addition of
conditioned A-heavy molasses regularly, until the crystals become visible to the naked eye. The
level of the massecuite in the pan reaches to about 4 glasses to the required crystal size of about
0.6mm and is cut into half which is sent to a B-vacuum crystallizer for storage of B-grain.
ii)
B-Continuous Pan:
This is an automated pan equipped with automated systems of control designed to maintain
at a constant level of: Steam pressure in the tubes, Vacuum in the pan, Pressure of agitating steam
and massecuite level in the pan. It possesses vertical baffles which divide the pan into a number of
10 compartments. These compartments communicate with each other by an opening located at
the base of the partitions. The first compartment delivers into the second compartment, the second
delivers into the third, which delivers into the fourth, and so on.
The pan is fed directly with B-grain pumped from the B-vacuum crystallizer into the first
compartment. Each compartment is set to boil the massecuite to a specified brix read from a Brix
meter. Automatic opening and closing of valves is set to allow either feeding of water or
conditioned A-heavy molasses to develop B-grain and obtain the required Brix. When the
required Brix of about 94-96 is obtained in the last compartment, the B-massecuite automatically
discharges into a B-horizontal crystallizer for further crystallization.
C Pan-boiling:
C-light molasses and B-heavy molasses are used as footing of C-massecuite. The sugar boiler
introduces into the C pan a certain quantity of sufficient C-light molasses (about 2 glasses) into a
40 ton capacity pan after the vacuum in the pan has reached 23-25Hg. The massecuite is
supersaturated to a metastable zone. When the super-saturation has attained the required value,
38
graining is carried out by addition of a suitable amount of slurry. When the grains start to appear,
hot water is usually added to harden the grain and dissolve any false grains. Graining is continued
with the addition of conditioned C-light and B-heavy molasses regularly, until the crystals
become visible to the naked eye. The level of the massecuite in the pan reaches to about 4 glasses
and is cut into half, of which is sent to a C-vacuum crystallizer for storage of C-grain. C-grain
is then pumped from the C-vacuum crystallizer into a 60 ton capacity C pan after the pan has
attained a vacuum of 23-25Hg. Steam (vapour) is then opened into the calandria of the pan to
start boiling of the C-grain. When saturation starts in the pan, small drinks of conditioned B heavy
molasses is fed into the pan till its full. When the pan is filled up to capacity and has become tight,
the steam is stopped and the pan is kept under vacuum for half an hour. C-massecuite is then
dropped into the C-crystallizer at 960 to 980 Brix.
Melt
Sulphited syrup
Conditioned
B - heavy
Conditioned
C - light
Conditioned
A - heavy
Slurry
Conditioned
B - seed
Syrup
Tank
B Continuous
C
PANS
B
PANS
1&2
Water
Steam
Water
C-Massecuite
A
PANS
Pan (4)
5, 6, 7
Steam
Water
B-Massecuite
Agitator
Steam
A-Massecuite
Horizontal
Crystallisers
39
Water
Steam
inner circumference and a back-liner screen sandwiched between them to allow molasses to
escape.
Suspension
Head
Spindle
Massecuite
Feeder
Casing
Charge
regulator
Basket
Wash Spray
Discharge Plough
Sugar
discharger
The massecuite falls onto a distributor, spreading it evenly over the surface of the cover
screen. The spindle is driven by an electric motor and rotates at a maximum speed of about 1,350
rpm inside a housing. As the machine accelerates to a high speed, the molasses is separated from
the crystals by centrifugal force developed giving rise to A-heavy molasses. The centrifugal force
of the spinning, forces molasses to separate from the crystals, and pass through the perforations
while the crystals remain inside the basket. The basket wall is constructed in such a ways so as to
withstand the centrifugal force developed during the operation. Hot water and steam is sprayed to
42
the inside of the sugar wall to remove residual molasses sticking to the crystals. This gives rise to
A-light molasses. Then an electric brake engages followed by a mechanical brake that slows the
basket down to 50 rpm. A discharge valves opens and the sugar crystals are removed/scrapped
off the walls of the basket at the end of a cycle operation by means of a plough which is lowered
into the basket. The sugar falls through the centre of the basket and is discharged onto a carrier
below (hopper), while the basket rotates.
Batch cycle of Operation: The capacity of the process is measured in cycle time. A cycle is
defined as the sequence of operations from charging A-massecuite into the basket to the
discharging of sugar and is typically denoted by the following steps:
1) Charging and accelerating 65s
3) Drying 36s
6) Discharging 20s
Total Time = 2minutes, 34 seconds. At this rate there should be between 17-22 cycles per hour.
2) Continuous Centrifugals (B and C-Centrifugal Machines)
The Continuous Centrifugals are used for curing B and C-massecuites. The continuous
centrifugals are designed with a cone-shaped basket, which is usually belt-driven from below
along-side the machine. The inner surface of the basket is fitted with a screen with a backing screen
within them. The basket rotates at a maximum speed of 1,730 rpm depending on the size and duty
of the machine. Massecuite is continuously fed into the cone. Sugar crystals rise up the inclined
screen whilst molasses is forced through the perforations and exits the process. The crystals are
flung off the top edge of the cone and strike the wall of the stationary outer housing.
43
B-Massecuite curing:
B-massecuite from the B-pug-mills is fed into the middle of a cone and is then eventually
distributed in the basket. The centrifugal force causes the massecuite to climb up the cover screen
forcing the molasses to escape through the cover screen and backing screen. The molasses then
climb up the basket wall behind the backing screen and goes through openings in the basket wall
and finally into the molasses chamber. B-heavy is thus obtained. The sugar left on the cover screen
goes up and is thrown out over the rim into the magma mixers. Steam is used at the entrance of
the massecuite to facilitate curing. The steam enters a jacket outside the central tube and heats the
entering massecuite. Steam inside the jacket finally goes out through holes in the central tube at
the bottom of the jacket and mixes with the incoming massecuite. B sugar obtained is mixed with
water to form seed used as A-pan footing.
C-Massecuite curing:
C-massecuite is double cured giving rise to Final Molasses, C-light molasses and C-sugar.
C-massecuite from C-For-Worker-pug-mills is fed into the first set of Centrifugals (C-For-Worker
Centrifugals). The massecuite is then sunned dry without washing and steaming is done giving rise
to Final Molasses which is weighed and sent to distillery. The cured sugar from the for-workers
is discharged into a C-After-Worker-magma mixer, where its mixed with water, forming a magma
of high purity then pumped into a second set of Centrifugals (C-After-Worker Centrifugals) for
second curing giving rise to C-light molasses and C-sugar. C-Sugar is mixed with water and
pumped to the C-melter. In the C-melter, the C-Sugar is melted with water and the C-melt formed
is conditioned for A-boiling. The C-melter melts all sugars and makes a homogeneous mixture.
6.8.2 Hopper:
Hopper is used to supply the final commercial sugar obtained from A-fugals to a belt
conveyor that conveys the sugar to the fluidised bed drier. A magnetic separator is placed at the
end of the hopper in order to trap any magnetic particles that come along hopping with the sugar.
6.9 Sugar Drying (Fluidised Bed Drier)
A Fluidised Bed-Drier is used to dry the final product sugar crystals with the help of steam.
The drier is divided into two compartments: hot air and cool air chamber. Drying is generally done
by blowing heated air from a heat exchanger (radiator) by use of a Forced Draft fan, through
perforated screens into the hot air chamber, fluidising the sugar, swirling the grains thus drying
44
them. The air passes around the sugar crystals in co-current flows within the dryer. As the heated
air makes contact with the moist sugar, moisture is driven off from the liquor covering the crystals.
Once the moisture has been evaporated off, cold air is blown into the cooler section where the
sugar is cooled. An Induced Draft Fan is then used to suck out dust, vapours to a scrapper tank.
6.10 Packaging and Storage:
After drying, sugar goes into a sugar beam as a temporary storage where weightment machines
are connected. Sugar is then packed into 50 kg bags and stored. Manual packaging is used and it
is closed by a sewing machine. In an 8 hrs shift of regular crushing of cane, approximately 2000
bags of sugar are produced. The final production of sugar is 250 tons of cane per day.
6.6.3 Typical Layout of the Centrifugation / Separation Process at SCOUL.
C Melter
Melt
C - Vertical Crystalliser
B Massecuite
A- Heavy
C Massecuite
A- Light
C- Light
B- Heavy
A Massecuite
A Pug Mill
B Pug Mill
A fugals
B fugals
1,2,3,4
1,2,3,4
C-FW fugals
1,2,3,4
C-AFW
fugals 1 & 2
Water
Water
Water
Commercial Sugar
B Magma
Mixer
B-seed
C-AFW Magma
Mixer
C-sugar
C-FW
Magma
C-FW Sugar
Hopper
To A-Pan boiling
CHAPTER SEVEN
7.0 ACTIVITIES CARRIED OUT, SKILLS AQUIRED AND CHALLENGES FACED
7.1 CHEMICAL LABORATORY
The laboratory is responsible for quality control and assurance by sampling and analysis of
critical control parameters in the sugar manufacturing process and also advises the process on
performance of particular unit operations. This chapter contains the activities I carried out during
my training period. They are listed below;
1) Brix, Pol and PH Test.
46
known
as
PH
and
alkaline.
for
determining
the
Ph,
47
1) Analysis Carried Out: Determination of Pol, Brix and Purity for Juices
Sample
Brix (Bx)
Pol
Purity (%)
Primary Juice
16.64
13.89
83.47
Mixed Juice
10.84
8.97
82.75
2.30
1.81
78.70
Clear Juice
11.61
9.63
82.95
Filtrate
7.78
6.06
77.89
PH
6.78
2) Analysis Carried Out: Determination of Pol, Brix and Purity for Syrup and Massecuites
Samples from Syrup to Molasses are diluted (Dilution Factor of 10) before testing for brix and pol.
Sample
Brix (Bx)
Pol
Purity (%)
Syrup
54.80
45.23
82.54
A-massecuite
93.80
78.69
83.89
B-massecuite
96.70
65.36
67.59
C-massecuite
98.55
51.52
52.25
3) Analysis Carried Out: Determination of Pol, Brix and Purity for Sugars and Molasses.
Sample
Brix (Bx)
Pol
Purity (%)
A-heavy molasses
81.10
56.21
69.31
A-light molasses
61.00
50.10
82.13
B-heavy molasses
80.20
35.76
44.59
B-seed (sugar)
92.10
80.76
87.69
C-light molasses
85.30
54.55
63.95
Melt (C-sugar)
41.20
37.00
89.81
Final Molasses
86.30
30.33
35.14
48
extraction
of
pol
and
for
the
50
I have learnt the essence of safety and the precautions to be taken, in any engineering work
environment. Overcoats, a helmet and safety shoes must strictly be worn at all times before
setting a foot into the factory.
I have also learnt the importance of building a collaborative relationship and friendship with
different and various categories of people (staff and workers) in the field, for future
employment opportunities.
I have also learnt the benefits associated with team work by practically being part of it, at the
best of my ability, through partaking safety practices of the factory and laboratory standards.
I have also learnt the essence of building confidence and develop a personality, based on
effective communication skills through collective and interactive avenues for future roles.
I have also been able to understand that some problems encountered in the industry rarely
have unique solutions, and there is no need to gain experience necessary for selecting the
optimal solutions from the many options.
Finally, I have been able to learn all the chemical and physical processes of sugar production,
the design, construction and operation of all the equipments used for production and I have
appreciated all the knowledge acquired during my studies in a more practical bit.
Safety skills: My Overcoat, helmet and safety shoes have strictly been worn at all times.
Time Management: I have kept a good profile on attendance and punctuality without any
unscheduled absences and I have always completed my work before leaving for the day.
Confidence: I have also developed an outstanding ability and confidence to explain all the
details learnt about sugar processing and technology.
Work product: The quality of my research work from various assignments given to me and
experiments carried out in the laboratory has been excellent according to my supervisor. I have
always completed my work on time with minimal errors and without constant supervision.
51
Operational skills: How to start and operate a Rapi-pol extractor using a Spanner as well as a
Tumbler. Likewise, how to operate a Refractometer and Polarimeter and take readings.
Communication skills: The factory employees comprises of people from different parts of the
country. I was challenged at times to speak using Luganda with some of the operators which
has also improved my communication skills to a certain level.
Dust and flue gas: The factory boilers operate using bagasse as fuel. Some flue gas and dust
escapes and circulates inside the factory which was so dangerous when inhaled.
Uncontained Bagacillo: Fine particles of bagasse escape when conveyed to the cyclone
separator at the filter station and were dangerous to my eye-sight and also when inhaled.
Noise impingements: The factory does not provide hearing impingements to its workers or
trainees. At times, it became so hard to listen to my supervisors explanations when training or
for him to listen to my questions and thus I had to strain my voice.
Sampling in Dirty Areas: Some factory areas are extremely dirty with sticky molasses. The
factory does not provide hand gloves in such cases where we had to get our hands and coats
very dirty and sticky with molasses. On the other hand, no soap or detergents were provided
for washing our hands. I believe this extremely has an effect on the health of workers.
Cost of Living: No form of allowances or accommodation were given to trainees. The current
cost of living in Lugazi has been higher than what I expected. All transport, food, research,
and safety working equipment costs, were catered for by my pocket.
Language Barrier: This was one of the major challenges faced especially when interacting
with the operators. In most cases, when my supervisor was a little busy, he could hand me over
to the operators for a while. Some of them could not explain in English and preferred using
Luganda. It was a struggle for me to understand some unit operations in a different-language.
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The factory should provide hearing impingements to its workers or trainees that are just
sufficient to block any excessive noise. A lot of noise in the factory causes hearing side-effects.
The factory should provide hand gloves to its workers and trainees to enable those who work
in extremely dirty areas maintain a good-hygiene and health. Most of them use bare hands, and
of which, no soap or detergents are provided to them for washing hands.
The management of SCOUL should put into consideration, the importance of their trainees to
the organisations. Despite trainees benefiting from the knowledge acquired, their research can
also benefit the organization as well or would be motivated to come back and work as
permanent employees. Therefore, I advise the company, to consider some little allowances for
trainees as they strive to survive during their internship training.
The management of SCOUL should also start giving incentives or benefits to its employees to
improve the production.
The packaging is manually controlled causing more men power. From my observation, the
hygiene of men power employed has not been so proper. If the packaging process can be
automated, it could save costs, time and the risk of contaminating the sugar to be bagged.
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The factory should also devise ways of studying and setting up a short retention time clarifier
purposely for the filtrate to avoid recirculation of non-sugars and sugars in the reaction tank.
The excess bagasse produced by the factory should be sold or exported to paper and board
making industries as it is a raw material for making paper bags, card-boards, etc.
Not all the power produced is used by the factory and therefore the factory should start up a
power project, which can meet the energy requirements of the whole Lugazi town.
The Operation of the plant is often at times, below its capacity and other times, abrupt
stoppages of the mill (No crushing). This is a strong weakness to the factory since the demand
of sugar is increasing with the passage of time and therefore the importance of this sugar plant
has to be much increased.
The university should also play a role of connecting students to organisations for a placement
of internship training. Students do struggle on their own to get placements of which some are
lucky and some just fail to get and yet all do pay a fixed ITCSP fee for industrial training. It
could only take a recommendation for one to easily get a place.
The university should at-least organize one or two sessions with students to brief them on what
is expected to be done during training and guidance on how to make industrial training reports.
Providing a log book is not quite be enough to fully provide the guidance needed.
Internship allowances should be provided to students in time, preferably two weeks prior to
training so that students can easily plan for their accommodation especially in urban areas
where costs of living are high.
Organization of study trips to such organisations especially for those doing engineering
sciences, should be put into consideration as this will benefit many students who wouldnt have
gotten a chance to train from such a valuable organization for their practical growth.
Likewise, organization of public meetings and exhibitions at the University should be put into
consideration, inviting experienced personnel form SCOUL, to share with students more about
cane sugar engineering and technology.
7.2.4 References
1) E. Hugot Handbook of Cane Sugar Engineering, 3rd, completely revised, Edition, 1986.
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APPENDIX A
Bagasse: The residue after extraction of juice from the cane that has passed through the mills
Bagacillo: Very small/fine particles of bagasse separated from the mass of final bagasse
Entrainment: The process by which vapours escape with juice droplets in cases due to a very
high vacuum.
Filter Cake: The dry and porous material formed and scrapped off onto the screens of filters
and has undergone different vacuum zones. Its later sent to the field as fertilizer.
Final Molasses: Heavy molasses obtained from curing the last grade of the massecuite (Cmassecuite).
Imbibition: The general term which applies to the process of adding water or thin juice to
bagasse to mix and dilute the juice concentrate therein.
Inversion: The process that takes place when sucrose is exposed to high temperatures and low
PHs, and breaks down into equal parts of glucose and fructose referred to as invert sugar.
Molasses: The product obtained from curing of massecuite that contains sucrose, invert sugar,
ash and other insoluble matter.
Purity: The mass of pol (or sucrose) expressed as a percentage of the brix of a sugar solution
Seed: Sugar or magma obtained from curing massecuite that is mixed with water and used as
a footing for further boiling of massecuite.
Syrup: The concentrated clarified juice leaving the last evaporator vessel.
Sulphited Syrup: Syrup that has been bubbled through a mass of Sulphur dioxide gas.
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APPENDIX B
Reaction vessel
Flash Tank
Lime Preparation
Cyclone Separator
Quadruple-effect evaporators
Entrainment trapper
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Sulphitation vessel
Centrifugal Machines
Pug-mill and
transient heater
Trainee
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