FACULTY OF CHEMICAL ENGINEERING

Universiti Teknologi MARA (UiTM) Terengganu

Kampus Bukit Besi,
Bukit Besi, Dungun, TERENGGANU

TECHNICAL/EXECUTIVE REPORT : CHEMICAL ENGINEERING

Lab No. :
Topic :

Module :

Titration of Acids and Bases

Mark :
Date :

Participant
*Please cancel which
is not necessary.

Instructor

Course : Chemical Engineering

No.

Semester : 1

Name

Ezzanie Balqhis bt Basir

Nurul Nazirah Bt Abdul Rahman

3/8/2016
Group

10

:
Matrix No.

Signatu

201680069
4
201680062
6

Sir Rafie

Objective :
1
2

To determine molarity of standard sodium hydroxide (NaOH)

To calculate percentage of potassium hydrogen phthalate (KHP) in an unknown
acidic sample.

Demonstrate effective team role and responsibility in the task execution.

Abstract :

re

The experiment is briefly about titration of acids and bases.There are two acids
that were used in this experiment which is potassium hydrogen phthalate (KHP)
and unknown acid.The base that was used in this experiment is sodium
hydroxide solution (NaOH).

The standardization of sodium hydroxide solution (NaOH) are carried out first by
measuring the weight of weighing paper and potassium hydrogen phthalate
(KHP) separately.Once the weighing paper and the potassium hydrogen
phthalate (KHP) are measured,record the reading of mass of both weighing paper
and hydrogen phthalate (KHP).After that,pour the sodium hydroxide solution
(NaOH) into the burette until it is full.Mix the potassium hydrogen phthalate
(KHP) with distilled water in the conical flask until it is dilute.Add 3 drops of
phenolphthalein into the conical flask.Slowly,add the sodium hydroxide solution
(NaOH) drop by drop into the conical flask containing dilute potassium hydrogen
phthalate solution (KHP).

Observe the changes colour of phenolphthalein from pink colour turns to

colourless once the sodium hydroxide solution (NaOH) are added into the conical
flask.

When the phenolphthalein in the conical flask show changes in colour from pink
to colourless once the sodium hydroxide solution (NaOH) are added drop by
drop,it shows that the end point of neutralization between sodium hydroxide
solution (NaOH) and potassium hydrogen phthalate (KHP).

Part 1:Standardization of NaOH solution

Data/Results
/Calculation:

No
1
2
3
4
5
6
7

Measureme
nts
Mass of
weighing
paper+KHP
Mass of
weighing
paper
Mass of KHP
used
Final burette
reading
Initial
burette
reading
mL of NaOH
used
Molarity of
NaOH

0.7140g

0.6670g

0.5580g

0.1440g

0.1440g

0.1440g

0.5700g

0.5230g

0.4140g

37.0mL

33.0mL

22.0mL

0.0mL

0.0mL

0.0Ml

20.0mL

20.0mL

20.0mL

1.0 mol

1.0 mol

1.0 mol

0.7144g

0.6370g

0.5170g

0.1440g

0.1440g

0.1440g

0.5704g

0.4930g

0.3730g

37.5mL

32.5mL

25.5mL

0.0mL

0.0mL

0.0mL

20.0mL

20.0mL

20.0Ml

1.1535

1.1323

0.8327

52.75%

46.60%

49.90%

Part 2:Analysis of unknown acidic solution

No
1

2
3
4
5
6
7
8
Discussion:

Measureme
nts
Mass of
weighing
paper+unkn
own
Mass of
weighing
paper
Mass of
unknown
used
Final burette
reading
Initial
burette
reading
mL of NaOH
used
Mass of KHP
in unknown
Percent of
KHP in
unknown
The percentage of KHP

in the sample is 52.75%,46.60% and

49.90%
2

Compute the standard deviation (SD) of the results

Compute the average deviation from the mean to the test the
result.Explain the test result.

There is no effects of NaOH molarity to percentage of KHP in

unknown sample

The effects of wrong titration techniques to the experiment results

is no consistency in the reading of the experiment.

Conclusion:

The molarity of the standard sodium hydroxide solution (NaOH) is

1.0 mol

The percentage of potassium hydrogen phthalate (KHP) in an

unknown acidic sample is 52.75%,46.60% and 49.90%

References:

Approval

https://www.coursehero.com

Chemistry textbook

Example report at http://ichemey.org

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