3000

2900
2800
2700
2600
2500
2400
2300
2200
2100
2000
1900
1800
1700
1600
1500
1400
1300
1200
1100
1000
900
800
700
600
500
400
300
200
100
0
5

10

20

File: SAIFXR160630B-05 (C4P1).raw - Step: 0.020 - Step time: 2

Operations: Smooth 0.150 | Background 1.000,1.000 | Import

4000

2 ,d=3.33465

d value
Intensity Intensity %
Angstrom Count
%
17.50289
-10.89
-0.4
17.11595
14.8
0.5
16.65266
45
1.6
15.71402
22.5
0.8
15.50526
31.1
1.1
14.91155
44.8
1.6
14.73504
35
1.3
14.17192
57.2
2.1
13.93699
94.1
3.4
13.36343
13
0.5
13.24415
11
0.4
12.78695
22.8
0.8
12.69698
23.8
0.9
12.3273
-10.38
-0.4
12.12182
-3.02
-0.1
11.85607
8.86
0.3
11.61984
13.7
0.5
11.44398
15.7
0.6
11.35304
10.1
0.4
11.18203
-1.05
0
11.06313
4.23
0.2
10.75519
20.9
0.8
9.97648
458
16.5
9.2155
59
2.1
8.97922
164
5.9
8.69999
7.45
0.3
8.65198
5.1
0.2
8.51097
15.2
0.5
8.32924
669
24.1
8.12541
46.7
1.7
7.95173
14.1
0.5
7.91017
16.8
0.6
7.82629
10.1
0.4
7.73145
24.3
0.9
7.67828
26.1
0.9
7.5309
84.2
3
7.32572
25.5
0.9
7.06174
283
10.2
6.86163
23.1
0.8
6.70983
2.09
0.1
6.63439
0.3
0
6.59694
3.43
0.1
6.55277
0.88
0
6.51461
-0.28
0
6.4489
9.19
0.3
6.42341
16.9
0.6
6.35391
29.1
1
6.31864
27.7
1

Lin (Counts)

Angle
2-Theta
5.045
5.159
5.303
5.62
5.695
5.922
5.993
6.232
6.337
6.609
6.669
6.907
6.956
7.165
7.287
7.45
7.602
7.719
7.781
7.9
7.985
8.214
8.857
9.59
9.843
10.159
10.216
10.386
10.613
10.88
11.118
11.177
11.297
11.436
11.515
11.742
12.072
12.525
12.891
13.184
13.335
13.411
13.502
13.581
13.72
13.775
13.926
14.005

3000

2th=25.135 ,d=3.54014

2th=23.009 ,d=3.86226

2th=20.948 ,d=4.23723

1000

2th=19.752 ,d=4.49118

2000

2th=28.077 ,d=3.17553
2th=28.688 ,d=3.10927
2th=29.374 ,d=3.03823

2th=26.712 ,d=3.33465

4000

2th=18.153 ,d=4.88303

-0.2
0.3
0.1
0.4
0.5
0.3
0.3
0.7
0.7
0.7
0.6
0.6
0.7
1.1
0.9
0.7
0.8
0.7
0.5
0.2
0.7
0.6
0.4
0.5
0.7
1.3
1.1
0.5
6.3
2.7
3.2
3.3
0.9
0.8
0.8
0.7
4.1
0.8
0.7
0.4
0.6
0.6
1.2
21.1
10.9
2.5
1.5
1.6
2.6
2.5

2th=12.510 ,d=7.06977

-4.98
7.85
3.47
11.2
12.7
9.16
9.19
19.9
20.8
18.1
17.5
16.8
18
29.7
25.9
20
21.3
18.1
14.2
6.8
20.7
17.3
10.2
14.4
20
37.3
30.7
14.8
174
75.6
87.8
91.1
25.4
22.1
21.1
18.6
114
22.1
20.2
9.84
16.1
17.6
33
585
302
70.2
42.2
44.1
72.6
68.7

2th=8.840 ,d=9.99520
2th=9.813 ,d=9.00599
2th=10.620 ,d=8.32363

6.22803
6.1717
6.131
6.03352
6.01581
5.9487
5.92037
5.85274
5.828
5.76251
5.68006
5.65171
5.60822
5.56754
5.54005
5.50894
5.48587
5.46583
5.45078
5.38712
5.35472
5.32244
5.27325
5.22861
5.14405
5.05242
5.03686
4.96926
4.88235
4.75478
4.73382
4.71496
4.6038
4.56683
4.55299
4.53924
4.49038
4.44519
4.42351
4.37632
4.359
4.34332
4.29311
4.23948
4.20913
4.17299
4.11278
4.10266
4.04725
4.01182

Lin (Counts)

14.209
14.34
14.435
14.67
14.713
14.88
14.952
15.126
15.19
15.364
15.588
15.667
15.789
15.905
15.985
16.076
16.144
16.203
16.248
16.442
16.542
16.643
16.799
16.944
17.224
17.539
17.594
17.835
18.155
18.647
18.73
18.806
19.264
19.421
19.481
19.541
19.755
19.958
20.057
20.275
20.357
20.431
20.673
20.937
21.09
21.275
21.59
21.644
21.944
22.14

0
5

10

20

File: SAIFXR160630B-05 (C4P1).raw - Step: 0.020 - Step time: 2

1) Obs. Max: 8.851 - FWHM: 0.257 - Raw Area: 4.771 Cps x d
2) Obs. Max: 10.607 - FWHM: 0.207 - Raw Area: 5.250 Cps x
3) Obs. Max: 20.931 - FWHM: 0.268 - Raw Area: 6.070 Cps x
4) Obs. Max: 26.729 - FWHM: 0.225 - Raw Area: 24.25 Cps x
5) Obs. Max: 28.085 - FWHM: 0.251 - Raw Area: 9.472 Cps x
6) Obs. Max: 39.587 - FWHM: 0.236 - Raw Area: 3.090 Cps x
7) Obs. Max: 50.235 - FWHM: 0.233 - Raw Area: 3.640 Cps x

22.5
22.636
22.75
22.988
23.215
23.455
23.533
23.613
23.747
24.056
24.309
24.439
24.6
24.884
25.015
25.067
25.281
25.617
25.917
26.022
26.235
26.314
26.73
27.029
27.228
27.296
27.616
27.883
27.983
28.097
28.519
28.659
29.118
29.214
29.388
29.612
29.691
29.938
30.075
30.444
30.565
31.039
31.168
31.221
31.34
31.491
31.558
31.624
31.975
32.06

3.94838
3.92501
3.90552
3.86577
3.82835
3.78983
3.77736
3.76476
3.7438
3.69644
3.65854
3.63935
3.61595
3.57529
3.5569
3.54957
3.52
3.47465
3.43509
3.42141
3.39419
3.38412
3.33246
3.29619
3.27259
3.26456
3.22746
3.19713
3.18601
3.17329
3.1273
3.11237
3.06435
3.05444
3.03677
3.01436
3.00647
2.98226
2.96894
2.93379
2.92246
2.87889
2.86731
2.86259
2.85196
2.83857
2.83271
2.82694
2.7967
2.78954

6.26
11.7
6.49
77.8
29.3
6.07
21
28.1
38.6
24.9
25.3
22.3
18.7
80.4
113
125
108
33.8
16.5
18
61.3
110
2771
21.1
73.7
86.6
283
358
732
986
159
267
61
85.8
212
55
35.6
22
12
144
118
20.3
27.3
24.9
7.44
9.09
15.2
17.6
32.4
44.7

0.2
0.4
0.2
2.8
1.1
0.2
0.8
1
1.4
0.9
0.9
0.8
0.7
2.9
4.1
4.5
3.9
1.2
0.6
0.6
2.2
4
100
0.8
2.7
3.1
10.2
12.9
26.4
35.6
5.7
9.6
2.2
3.1
7.7
2
1.3
0.8
0.4
5.2
4.2
0.7
1
0.9
0.3
0.3
0.5
0.6
1.2
1.6

32.189
32.273
32.511
32.576
32.757
32.877
33.048
33.176
33.604
33.969
34.101
34.22
34.458
34.598
34.715
34.995
35.154
35.233
35.362
35.444
35.575
35.649
35.889
36.004
36.174
36.658
36.763
37.061
37.135
37.378
37.458
37.6
37.808
37.895
38.054
38.213
38.371
38.561
38.746
38.958
39.129
39.265
39.586
39.975
40.115
40.411
40.698
40.815
40.875
40.954

2.77862
2.77156
2.75187
2.74648
2.73175
2.72201
2.70834
2.69821
2.66477
2.63703
2.62709
2.61822
2.60065
2.59051
2.58202
2.56201
2.55079
2.54522
2.53623
2.53055
2.52157
2.51648
2.5002
2.49247
2.48115
2.4495
2.44276
2.4238
2.41912
2.40392
2.399
2.39026
2.37757
2.37233
2.36279
2.35333
2.34397
2.3329
2.32215
2.31002
2.30029
2.29265
2.27478
2.25353
2.24601
2.23025
2.21516
2.2091
2.20601
2.2019

43.2
34.7
23.3
30.3
32.5
48.4
57.5
105
0.47
166
131
83.8
40.7
106
152
-3.71
32.8
45.6
63.6
68.2
52.4
48.7
7.55
12.6
39.3
213
158
41.6
37.8
24.5
24.7
27.6
37
40.7
30.3
15.4
33.5
104
62.5
26
16.5
31.2
308
32.1
17.5
88
6.35
10.4
12
17.5

1.6
1.3
0.8
1.1
1.2
1.7
2.1
3.8
0
6
4.7
3
1.5
3.8
5.5
-0.1
1.2
1.6
2.3
2.5
1.9
1.8
0.3
0.5
1.4
7.7
5.7
1.5
1.4
0.9
0.9
1
1.3
1.5
1.1
0.6
1.2
3.7
2.3
0.9
0.6
1.1
11.1
1.2
0.6
3.2
0.2
0.4
0.4
0.6

41.243
41.39
41.476
41.646
41.881
42.384
42.525
42.662
42.821
42.952
43.006
43.082
43.514
43.814
43.914
43.962
44.237
44.291
44.466
44.549
44.656
45.014
45.343
45.543
45.761
45.884
46.194
46.311
46.433
46.626
46.715
46.923
46.988
47.237
47.569
47.648
47.742
47.847
48.035
48.155
48.373
48.542
48.701
48.999
49.302
49.436
49.607
49.714
49.896
50.244

2.18714
2.17974
2.17541
2.16689
2.15528
2.13087
2.12413
2.11762
2.11013
2.10402
2.1015
2.09796
2.07812
2.06457
2.06013
2.05799
2.04581
2.04344
2.03583
2.0322
2.0276
2.0123
1.99847
1.99016
1.98117
1.97613
1.96362
1.95892
1.95406
1.94641
1.94293
1.93477
1.93225
1.92265
1.91001
1.90701
1.90349
1.89956
1.89256
1.88813
1.88012
1.87396
1.86822
1.85754
1.84684
1.84215
1.83619
1.8325
1.82623
1.81441

32.5
47.6
45.4
28.7
143
91.9
161
111
19.7
15.9
15.3
12.9
25.6
5.01
9.88
14.8
30.1
31.3
30.4
32.4
44.4
138
52.5
34.2
98
158
1.38
-1.45
6.19
-2.32
-2.03
25.9
20
70
5.54
8.53
15.6
9.82
13
11.2
35.3
20.3
12.3
58.9
6.62
4.95
14.3
16.1
25
398

1.2
1.7
1.6
1
5.2
3.3
5.8
4
0.7
0.6
0.6
0.5
0.9
0.2
0.4
0.5
1.1
1.1
1.1
1.2
1.6
5
1.9
1.2
3.5
5.7
0
-0.1
0.2
-0.1
-0.1
0.9
0.7
2.5
0.2
0.3
0.6
0.4
0.5
0.4
1.3
0.7
0.4
2.1
0.2
0.2
0.5
0.6
0.9
14.4

50.409
50.559
50.628
50.692
50.795
51.144
51.258
51.424
51.658
51.761
51.859
52.131
52.385
52.714
52.824
52.932
52.991
53.111
53.19
53.362
53.508
53.708
53.831
53.982
54.064
54.159
54.283
54.372
54.546
54.7
54.957
55.345
55.471
55.58
55.75
55.847
56.224
56.388
56.668
56.924
57.224
57.401
57.521
57.833
58.019
58.122
58.406
58.573
58.757
58.812

1.80884
1.80383
1.80154
1.79942
1.79602
1.78456
1.78086
1.77552
1.76802
1.76473
1.76162
1.75307
1.74518
1.73507
1.7317
1.72843
1.72662
1.72302
1.72064
1.71549
1.71116
1.70526
1.70167
1.69725
1.69486
1.69212
1.68856
1.686
1.68103
1.67666
1.66942
1.65864
1.65516
1.65219
1.64754
1.64491
1.63478
1.6304
1.62302
1.61631
1.60855
1.60401
1.60096
1.59306
1.58839
1.58582
1.57878
1.57467
1.57019
1.56887

155
33.4
37.6
42.3
51.3
32.4
39.6
32.9
28.7
32.4
21.7
12.8
27.5
-0.73
5.44
10.2
7.36
8.16
4.23
18.4
11
5.55
4.56
9.58
5.2
2.6
13
20.1
34
22.2
107
21.3
29.1
32.7
36.4
34.2
25.4
12.5
11.7
15.7
3.78
-0.36
8.47
3.7
11.4
16.1
215
96.7
17.7
18.9

5.6
1.2
1.4
1.5
1.9
1.2
1.4
1.2
1
1.2
0.8
0.5
1
0
0.2
0.4
0.3
0.3
0.2
0.7
0.4
0.2
0.2
0.3
0.2
0.1
0.5
0.7
1.2
0.8
3.9
0.8
1.1
1.2
1.3
1.2
0.9
0.5
0.4
0.6
0.1
0
0.3
0.1
0.4
0.6
7.8
3.5
0.6
0.7

59.169
59.27
59.453
59.56
59.745
60.018
60.222
60.435
60.655
60.739
60.974
61.185
61.295
61.448
61.624
61.752
61.907
62.03
62.169
62.248
62.441
62.559
62.633
62.745
62.922
63.063
63.285
63.347
63.456
63.647
63.857
64.009
64.146
64.26
64.672
64.729
65.008
65.129
65.288
65.455
65.579
65.665
65.755
65.9
66.023
66.16
66.31
66.522
66.605
66.821

1.56025
1.55782
1.55345
1.55093
1.54655
1.54019
1.53545
1.53055
1.52552
1.52362
1.51831
1.51358
1.51112
1.50773
1.50384
1.50103
1.49764
1.49497
1.49196
1.49025
1.48611
1.48358
1.48202
1.47964
1.47591
1.47295
1.46832
1.46702
1.46477
1.46083
1.45652
1.45344
1.45066
1.44836
1.44013
1.439
1.43349
1.43113
1.42803
1.42478
1.42239
1.42073
1.41902
1.41624
1.4139
1.4113
1.40846
1.4045
1.40295
1.39894

7.64
10.1
17.7
14.9
74.8
380
185
32.9
5.03
5.44
13.3
15.8
13.9
17.9
26.5
15
21
21
16.2
15.7
6.48
15.9
20
18
16.2
8.89
16.4
20.4
21.9
5.16
27.4
51.2
64.6
57.2
25.9
33.3
77.7
66.4
35
19.2
12.9
7.92
3.45
19.5
18
10.6
-3.28
3.34
4.99
7.07

0.3
0.4
0.6
0.5
2.7
13.7
6.7
1.2
0.2
0.2
0.5
0.6
0.5
0.6
1
0.5
0.8
0.8
0.6
0.6
0.2
0.6
0.7
0.6
0.6
0.3
0.6
0.7
0.8
0.2
1
1.8
2.3
2.1
0.9
1.2
2.8
2.4
1.3
0.7
0.5
0.3
0.1
0.7
0.6
0.4
-0.1
0.1
0.2
0.3

66.914
66.996
67.043
67.195
67.359
67.453
67.532
67.806
68.069
68.168
68.333
68.446
68.803
68.888
69.082
69.182
69.493
69.718

1.39721
1.39571
1.39483
1.39205
1.38906
1.38736
1.38592
1.38099
1.3763
1.37454
1.37161
1.36963
1.36338
1.36192
1.35857
1.35685
1.35153
1.34772

30.3
33.6
35.8
7.79
18.1
9
4.34
152
109
164
223
175
34.4
32
11.5
13.8
16
21.6

1.1
1.2
1.3
0.3
0.7
0.3
0.2
5.5
3.9
5.9
8.1
6.3
1.2
1.2
0.4
0.5
0.6
0.8

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30

40

50

60

2-Theta - Scale

w - Step: 0.020 - Step time: 29.1 s - WL1: 1.5406 - kA2 Ratio: 0.5 - Generator kV: 40 kV - Generator mA: 35 mA - Type: 2Th/Th locked
und 1.000,1.000 | Import

2 ,d=3.33465

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30

40

50

60

2-Theta - Scale

w - Step: 0.020 - Step time: 29.1 s - WL1: 1.54

7 - Raw Area: 4.771 Cps x deg.
07 - Raw Area: 5.250 Cps x deg.
68 - Raw Area: 6.070 Cps x deg.
25 - Raw Area: 24.25 Cps x deg.
51 - Raw Area: 9.472 Cps x deg.
36 - Raw Area: 3.090 Cps x deg.
33 - Raw Area: 3.640 Cps x deg.

8) Obs. Max: 60.029 - FWHM: 0.306 - Raw Area: 4.643 Cps x deg.
9) Obs. Max: 12.524 - FWHM: 0.318 - Raw Area: 3.576 Cps x deg.
Operations: Smooth 0.150 | Background 1.000,1.000 | Import

2th=68.316 ,d=1.37191

2th=60.038 ,d=1.53972

2th=58.403 ,d=1.57886

2th=50.229 ,d=1.81490

2th=44.995 ,d=2.01309
2th=45.882 ,d=1.97621

2th=41.877 ,d=2.15549
2th=42.524 ,d=2.12417

2th=38.597 ,d=2.33080
2th=39.602 ,d=2.27390

2th=36.666 ,d=2.44900

2th=34.019 ,d=2.63322
2th=34.699 ,d=2.58317

2th=28.077 ,d=3.17553
2th=28.688 ,d=3.10927
2th=29.374 ,d=3.03823
2th=30.452 ,d=2.93308

2th=25.135 ,d=3.54014

2th=23.009 ,d=3.86226

2th=20.948 ,d=4.23723

2th=19.752 ,d=4.49118

2th=26.712 ,d=3.33465

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2th=68.316 ,d=1.37191