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Some
Method 1,
Analytes.
Analyte
CAS No.
Sensitivity
7732-18-5
N/A
1.2
Applicability.
Adherence to the
Summary of Method.
2.1
348
2.2
These
Definitions.
[Reserved]
349
4.0
Interferences.
4.1
Therefore, when
Attach a
Safety.
5.1
Disclaimer.
350
not address all of the safety problems associated with its
use.
Reference Method.
Probe.
Condenser.
6.1.3
Cooling System.
Metering System.
Other
351
rate to within 10 percent and determining sample gas volume
to within 2 percent, may be used, subject to the approval of
the Administrator.
6.1.5
Balance.
respectively.
6.2.
Approximation Method.
A schematic of the
Probe.
6.2.2
Condenser.
ml capacity, or equivalent.
6.2.3
Cooling System.
Drying Tube.
Valve.
Pump.
Volume Meter.
352
and calibrated over the range of flow rates and conditions
actually encountered during sampling.
6.2.8
Rate Meter.
Rotameter, or equivalent, to
Graduated Cylinder.
6.2.10
Barometer.
6.2.11
Vacuum Gauge.
25-ml.
[Reserved]
8.0
Storage.
8.1
Reference Method.
Preliminary Determinations.
Unless otherwise specified by the
353
0.61 m (24 in.), and a minimum of twelve traverse points
shall be used in all other cases.
Select a
Mark the
354
the silica gel to the nearest 0.5 g, and transfer the silica
gel to the fourth impinger; alternatively, the silica gel
may first be transferred to the impinger, and the weight of
the silica gel plus impinger recorded.
8.1.2.2
4-1.
It is recommended, but
Metering System.
8.4.1.
8.1.3.2
Sampling Train.
A lower
355
8.1.4
Take other
probe from the first impinger (or from the filter holder),
and conduct a leak check (mandatory) of the sampling train
as described in Section 8.1.3.2.
If
356
the leakage rate exceeds the allowable rate, either reject
the test results or correct the sample volume as in Section
12.3 of Method 5.
8.2
Approximation Method.
NOTE:
Temporarily
Then,
Record
357
358
9.0
Quality Control.
9.1
Section
Quality Control
Measure
Effect
Section 8.1.1.4
Ensures the
accuracy of the
volume of gas
sampled.
(Reference Method)
Section 8.2.1
Ensures the
accuracy of the
volume of gas
sampled.
(Approximation
Method)
9.2
Same as Method 5,
Section 9.2.
10.0
Approximation Method.
Analytical Procedure.
11.1
Reference Method.
359
ml.
Determine the
Approximation Method.
the two impingers, and measure the volume to the nearest 0.5
ml.
12.0
Reference Method
12.1.1
Nomenclature.
Bws
gas stream.
Mw
Pm
Pstd
360
(29.92 in. Hg).
R
Tm
Tstd
Vf
Vi
Vm
Vm(std)
Vwc(std)
Vwsg(std)
Wf
Wi
)Vm
361
meter at each traverse point, dcm (dcf).
Dw
12.1.2
Vwc(std) '
Eq. 4-1
' K1 (V f & V i)
where:
K1
12.1.3
Vwsg(std) '
(W f & W i) R Tstd
Pstd M w K2
' K3 (W f & W i)
where:
K2
K3
12.1.4
Eq. 4-2
362
Vm(std) '
V m Y P m Tstd
Pstd T m
Eq. 4-3
Vm Pm
' K4 Y
Tm
where:
= 0.3855 EK/mm Hg for metric units,
K4
Moisture Content.
Vwc(std) % Vwsg(std)
Bws '
Vwc(std) % Vwsg(std) % Vm(std)
12.1.6
Eq. 4-4
For
Calculate the
363
saturated conditions (see Section 4.1), and another based
upon the results of the impinger analysis.
The lower of
Approximation Method.
The
Nomenclature.
Bwm
Mw
Pm
Pstd
364
for metric units and
21.85 [(in. Hg)(ft3)]/[(lb-mole)(ER)] for
English units.
Tm
Tstd
Vf
Vi
Vm
Vm(std)
Vwc(std)
Dw
12.2.2
Vwc(std) '
' K5 (V f & V i)
where:
K5
Eq. 4-5
365
12.2.3
Vm(std) '
V m Y P m Tstd
Pstd T m
Eq. 4-6
Vm Pm
' K6 Y
Tm
where:
K6
12.2.4
Vwc(std)
% Bwm
Bws '
Vwc(std) % Vm(std)
Vwc(std)
'
% (0.025)
Vwc(std) % Vm(std)
13.0
Method Performance.
14.0
Pollution Prevention.
15.0
Waste Management.
16.0
Alternative Procedures.
Eq. 4-7
[Reserved]
[Reserved]
[Reserved]
References.
Air Pollution Engineering Manual (Second Edition).
366
Agency, Office of Air Quality Planning and Standards.
Research Triangle Park, NC.
2.
Testing Manual.
Angeles, CA.
3.
1973.
November 1963.
Bulletin WP-50.
1968.
18.0
367
Figure 4-1.
368
Figure 4-2.
Moisture
Method.
Sampling
Train
- Approximation
369
Plant
Location
Operator
Date
Run No.
Ambient temperature
Barometric pressure
Probe Length
SCHEMATIC OF STACK CROSS SECTION
Traverse
Pt. No.
Sampling
Time
(1), min
Stack
Temperature
EC (EF)
Pressure
differential
across orifice
meter )H
mm (in.) H2O
Meter
Reading gas
sample
volume
m3 (ft3)
)Vm
m3
(ft3)
Gas sample
temperature at
dry gas meter
Inlet
Tmin
EC(EF)
Outlet
Tmout
EC(EF)
Average
Figure 4-3.
Temperature
of gas
leaving
condenser
or last
impinger
EC(EF)
370
Location
Test
Date
Operator
Barometric pressure
Clock Time
Figure 4-4.
Gas volume
through
meter, (Vm),
m3 (ft3)
Comments:
Rate meter
setting
m3/min
(ft3/min)
Meter
temperature
E C (E F)
Impinger
volume, ml
Silica gel
weight, g
Final
Initial
Difference
Figure 4-5.