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DISTILLATION HARDWARE
Note: The source of the technical material in this volume is the Professional
Engineering Development Program (PEDP) of Engineering Services.
Warning: The material contained in this document was developed for Saudi
Aramco and is intended for the exclusive use of Saudi Aramcos employees.
Any material contained in this document which is not already in the public
domain may not be copied, reproduced, sold, given, or disclosed to third
parties, or otherwise used in whole, or in part, without the written permission
of the Vice President, Engineering Services, Saudi Aramco.
Chapter : Chemical
File Reference: CHE-104.02
Engineering Encyclopedia
Section
Page
INFORMATION ............................................................................................................... 5
INTRODUCTION............................................................................................................. 5
SELECTING DISTILLATION TOWER CONTACTING DEVICES ................................... 6
Crossflow Devices ................................................................................................ 8
Sieve Trays........................................................................................................... 9
Valve Trays......................................................................................................... 10
Bubble-Cap Trays............................................................................................... 11
Summary ................................................................................................. 12
Downcomer Configurations...................................................................... 13
Countercurrent Devices ........................................................................... 14
Packing............................................................................................................... 15
Grids................................................................................................................... 18
Baffle Sections.................................................................................................... 19
Summary ............................................................................................................ 20
FACTORS AFFECTING TRAY PERFORMANCE......................................................... 21
Flow Regimes - Spray and Froth ........................................................................ 21
Entrainment ............................................................................................. 22
Jet Flooding ............................................................................................. 23
Downcomer Inlet Velocity ........................................................................ 24
Downcomer Residence Time................................................................... 25
Downcomer Filling ................................................................................... 25
Downcomer Sizing Criteria ...................................................................... 26
Weeping................................................................................................... 27
Dumping .................................................................................................. 28
Tray Turndown......................................................................................... 28
Entrainment-Weeping -- Tray Operating Window .................................... 29
Tray Efficiency ......................................................................................... 30
Tray Performance Diagram...................................................................... 31
Maximum Vapor Rate Considerations ................................................................ 32
Minimum Vapor Rate Considerations ................................................................. 32
Maximum Liquid Rate Considerations ................................................................ 33
Minimum Liquid Rate Considerations ................................................................. 33
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List of Figures
Figure 1. Crossflow Versus Countercurrent Devices...................................................... 6
Figure 2. Crossflow Contacting Devices......................................................................... 8
Figure 3. Sieve Tray Deck.............................................................................................. 9
Figure 4. Valve Trays ................................................................................................... 10
Figure 5. Bubble-Cap Trays ......................................................................................... 11
Figure 6. Stepped Versus Sloped Downcomers........................................................... 13
Figure 7. Straight, Modified Arc, and Arc-Type Downcomers....................................... 14
Figure 8. Countercurrent Devices-Random Packing .................................................... 16
Figure 9. Structured Packing by Koch Engineering ...................................................... 17
Figure 10. Various Types of Grids................................................................................ 18
Figure 11. Sheds/Disc and Donuts............................................................................... 19
Figure 12. Froth Regime Versus Spray Regime Operation .......................................... 21
Figure 13. Generating Entrainment .............................................................................. 23
Figure 14. Percent Jet Flood Versus Efficiency............................................................ 24
Figure 15. Downcomer Filling....................................................................................... 26
Figure 16. Effect of Weeping on Efficiency................................................................... 28
Figure 17. Effect of Liquid Rate on Sieve Tray Turndown ............................................ 29
Figure 18. Effect of Tower Loading on Tray Efficiency ................................................. 31
Figure 19. Typical Tray Performance Diagram............................................................. 32
Figure 20. Tray Layout Definitions................................................................................ 35
Figure 21. Downcomer Arrangements.......................................................................... 36
Figure 22. Tray Pass Arrangements............................................................................. 37
Figure 23. Pressure Balance For a Two-Pass Sieve Tray............................................ 40
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List of Tables
Table 1. Trays- A Summary of Characteristics............................................................. 12
Table 2. Counter Current Devices-A Summary of Characteristics ............................... 20
Table 3. Trays- A Summary of Characteristics............................................................. 53
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INFORMATION
INTRODUCTION
In distillation, vapor/liquid contacting devices are used to attain
equilibrium between the phases in contact. This module reviews
the most common contacting devices, their performance
characteristics, and the main tray design parameters.
The first section, Selecting Tower Contacting Devices, covers:
Vapor-handling limitations.
Liquid-handling limitations.
Other limitations.
Tray performance.
Hardware definitions.
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Crossflow Devices
Figure 2 illustrates a typical arrangement and key components
for a one-pass tray and a two-pass tray.
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Sieve Trays
The contacting area consists of flat plates containing
perforations, usually 1/2 in. (13 mm) in diameter (Figure 3).
They are the simplest trays to fabricate and are therefore the
cheapest. They also exhibit good capacity, excellent efficiency,
and good turndown characteristics (about 3/1). Their flat surface
facilitates maintenance. Thus, they may be used in fouling
services, provided the hole size is large enough.
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Valve Trays
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Bubble-Cap Trays
Figure 5 illustrates bubble cap trays, which were the first type of
tray developed for continuous distillation. Although they provide
excellent vapor-liquid contact over a wide range of throughputs,
they are relatively expensive to fabricate, install, and maintain.
As distillation hardware evolved, bubble-cap trays were largely
displaced first by sieve trays and later by valve trays. Despite
their expense, bubble cap trays are sometimes specified in
fouling, low pressure drop, and high turndown services.
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Summary
Tray
Type
Capacity
Efficiency
High.
Equal to or
better than
other tray
types.
Cost per
Unit Area
Flexibility
Remarks
Lowest of all
trays with
downcomers.
Medium. 3/1
can usually
be achieved.
Alternative to
valve trays
when high
turndown is not
required.
First choice for
most
applications.
Not
recommended
for moderate to
severe fouling
services.
Sieve
Medium to
high.
Valve
Medium to
High.
Medium.
high; as good As good as About 10%
as sieve
sieve trays. greater than
trays.
Sieve Trays.
High.
Possibly up
to 5/1.
Bubble
Cap
Medium to
high, except
low to
medium at
high liquid
rate.
High.
Use for high
5/1 or slightly flexibility where
higher.
fouling of valve
trays may be a
problem.
Medium to
high.
High.
At least twice
the cost of
sieve trays.
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Downcomer
Configurations
The standard type of downcomer is the straight, or chordal,
downcomer shown in Figure 6 and Figure 7. For a given tower
diameter, a certain amount of the available tray cross-sectional
area, the downcomer area, is needed for liquid handling with the
remainder, the bubble area, available for vapor flow. Therefore,
any changes that reduce the tray area used by downcomers,
increases the area available for vapor flow. Such a goal can be
achieved by using stepped or sloped downcomers as shown in
Figure 6. The process performance characteristics of sloped
and stepped downcomers containing the same inlet and outlet
areas are identical. They can therefore be used
interchangeably.
The required downcomer cross-sectional area is greater at the
top of the downcomer where most of the vapor disengagement
takes place. Sloped or stepped downcomers provide the
required area at the top of the downcomer, and at the same
time, they reduce the tray area taken by the downcomers at the
bottom. As a result, the tray area available for vapor-liquid
contact and vapor disengagement with stepped or sloped
downcomers is higher than for straight downcomers.
Sloped or stepped downcomers are most effective when used in
trays with moderate-to-high liquid rates to increase their vapor
capacity (existing units) or to reduce the required tray diameter
(new units).
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For uniform liquid flow distribution onto a tray, the chord at the
bottom of the downcomer must have certain minimum length,
often expressed as a percentage of the tower diameter. In some
services where very low liquid rates must be handled, this
minimum chord length provides a downcomer whose area is too
large for the liquid flow rate being handled (that is, the chord is
about 6.8% of the tower cross-sectional area). A modified arc
(also known as segmental) downcomer can be specified (Figure
7) to overcome this limitation while still meeting the minimum
requirement. The modified arc downcomer has an area less
than the 6.8% provided by the minimum (65% of tower
diameter) chordal downcomer, but has a projected weir length
at least equal to the minimum. Some older towers may contain
a full arc-type downcomer. This style of downcomer functions in
the same manner as a modified arc but is more expensive to
build and thus is no longer used in new towers.
Countercurrent
Devices
Packing, grids, and baffle sections are the three types of
countercurrent devices reviewed in this section. Table 2 at the
end of the section, summarizes their characteristics.
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Packing
Although a packed tower design may result in a smaller tower
diameter, the total cost of the installation with packing, packing
supports, distributors, and redistributors are generally higher
than that of a trayed tower.
The most common uses of packing in distillation services are:
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Grids
Grids are similar to structured packing in that they are fabricated
in panels and installed in an ordered manner. However, their
efficiency characteristics are much poorer due to their high open
area and low surface area per unit of volume. The first grid to
appear on the market, circa 1961, was the Glitsch grid. It was
intended for use in services where entrainment removal was
critical but where fouling was too severe to use crinkled wire
mesh screens.
In recent years, several new grids have come on the market.
They are Flexigrid by Koch Engineering and Snapgrid by Nutter
Engineering. Pictures of these major grids are shown in Figure
10.
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Baffle Sections
There are two basic types of baffle sections. The first type is
sheds; the second type is disc and donuts (Figure 11). These
devices operate differently from grids or packing. In baffle
sections, the liquid cascades from baffle to baffle in the form of
liquid curtains. As the vapor flows through these curtains, the
liquid is broken up into droplets and mass transfer occurs.
However, this is a very inefficient liquid/vapor contacting
mechanism.
For severe fouling services, baffle sections are about the only
internal available if long run lengths are required. Because of
their high open area, they have high capacity but very poor
efficiency. Thus, baffle sections require a disproportionate
amount of tower height for the functions they perform.
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Summary
Device
Capacity
Efficiency
Medium to
High.
Cost per
Unit Area
Medium to low,
depending on
material of
construction.
Flexibility
Remarks
> 3/1.
Good for DP
service. Mainly
used in vacuum
pipestills and in
various high
liquid rate
absorbers
> 3/1.
Best efficiency
per unit of DP.
Structured
Packing
Flexipac;
Montz
Gempak;
Mellapak
IntaloxStructured
Medium to
very high
depending
on size
used.
Glitsch Grid
Flexigrid
Very high.
Poor as
fractionation
device. Good
for entrainment
removal and
heat transfer.
Medium to
high.
Low
less than
2/1.
Very high.
Poor as
fractionation
device.
Medium.
Low.
< 1.5/1
Used in severe
fouling service;
e.g., slurry
pumparound in
cat fractionator.
Snapgrid
Sheds and
Disc and
Donuts
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Downcomer
Residence Time
The difference between the liquid and vapor densities, (L-V) is
one measure of the difficulty of separation in the downcomer.
Thus, based on buoyancy considerations, as the difference of
L-V gets smaller, disengaging becomes more difficult. For this
reason, the downcomer sizing criteria allow lower velocities
(higher residence time) for high-pressure systems, where L-V
is low.
Downcomer Filling
The liquid height in the downcomer is called downcomer filling,
expressed in inches of clear liquid or as a percent of the tray
spacing. Since the liquid enters the downcomer as froth, the
actual fluid level in the downcomer will be higher than the filling
calculated as clear liquid (Figure 15). The exact height depends
on the average froth density in the downcomer. As the liquid
travels downward in the downcomer, the vapor disengages and
escapes from the top of the downcomer. If the downcomer is
sized properly, the liquid leaving should be essentially clear
liquid. Thus, there is a froth density gradient down the
downcomer that ranges from the froth density on the tray (at the
top) to clear liquid at the bottom.
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Weeping
At low vapor velocities, the dry-tray pressure drop of the tray is
insufficient to support the liquid head on the tray; as a result,
some liquid begins to flow intermittently through the vapor
openings. This liquid bypassing begins at the "weep point." As
the vapor rate decreases further, more liquid pours through the
holes and weeping becomes continuous.
Although the total quantity of liquid that weeps is constant at a
given vapor rate, the weep rate per hole fluctuates. That is,
some holes are weeping while others are in the vapor bubbling
mode. At any instant, a given hole may be bubbling, weeping, or
doing neither, in a random distribution across the contacting
area of the tray.
Although weeping can occur on all tray types, it is less of a
problem in valve trays, which are the most widely used tray in
Saudi Aramco plants. Since weeping occurs only at reduced
rates, it is the major factor in determining tray turndown, the
range of vapor loadings over which acceptable fractionation is
achieved. (See Tray Turndown discussion.) For sieve trays,
turndown ratio is usually between 2/1 to 3/1; for valve trays, 3/1
to 5/1.
As Figure 16 shows, when vapor rate decreases, weeping
increases very rapidly and tray efficiency begins to decrease
sharply. Weepage up to 20% of the liquid rate has small effect
on efficiency and is acceptable.
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Dumping
When all the liquid flows through the holes on a tray, that is, no
liquid flows over the weir, dumping is said to occur.
When dumping takes place, tray efficiency is extremely poor
and the products will be off-spec. Trays should not be operated
in the dumping region.
Tray Turndown
Turndown is a measure of the hydraulic flexibility of the tray. It
is defined as the ratio of maximum to minimum loadings in a
range over which acceptable tray performance is achieved. This
usually is the range over which the tray efficiency stays at or
above the design value (Figure 16).
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Tray Efficiency
The vapor and liquid phases must be dispersed thoroughly and
remain in contact long enough for mass transfer to occur and to
achieve good efficiency. The vapor residence time is the time
for the vapor to flow through the volume of froth on the tray.
Likewise, the liquid residence time is the time for the liquid to
flow through the volume of froth on the tray. Both of these
variables depend on liquid and gas rates as well as the weir
height and bubble area on the tray.
The efficiency is also affected by the vapor and liquid
diffusivities. Since these values are fixed for a given system,
there is no way to change them through tray hardware changes.
To achieve good efficiency, a designer must optimize the weir
height, open area, bubble area, number of liquid passes, and
other variables. Excessive weeping, entrainment, and operation
in the spray regime must be avoided.
Figure 18 illustrates the effect of tower loading on valve and
sieve tray efficiencies. The operating range for the valve tray is
wider, reaching to very low turndown. Sieve tray efficiency may
be somewhat higher near design loadings.
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Weeping or dumping.
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2.
3.
4.
Evaluate flexibility.
5.
Hardware definitions.
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Hardware Definitions
Figure 18 and Figure 19 are typical layouts of single-pass trays,
illustrating the tray characteristics discussed in the following
sections.
Tower Diameter and
Tray Spacing
These two parameters set the capacity of the tower. As the
distance between trays (the tray spacing, H) increases, tower
capacity increases. For most services, the most economical
spacing falls between 18-24 in. Spacings above 36 in. provide
little capacity advantage and are not usually recommended.
Likewise, tray spacings as low as 12 in. can be used, but this
increases the tower diameter (DT) required to handle a given
set of vapor and liquid loadings. In addition, low spacings make
maintenance much more difficult. The Saudi Aramco
Engineering Standards specify minimum tray spacing
requirement at various tower diameters.
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Downcomer Area
This is the area in Figure 18 and Figure 19 (Sdi, Sdo) that
handles liquid as it flows from a given tray to the tray below. The
edge of the downcomer is usually chordal in shape, and its
maximum width is called the downcomer rise (r).
Downcomer
Clearance
This is the vertical clearance (c) between the tray floor and the
bottom edge of the downcomer apron (Figure 20).
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Multipass Trays
As the liquid rate on a tray increases, the capacity of the tower
can usually be increased if the liquid flow is split into more than
one path (Figure 22). Such split-flow trays are called multipass
trays. On multipass trays, the downcomers nearest the tower
centerline are inboard downcomers, while those farthest away
are called outboard downcomers.
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Contacting Area
Definitions
During tray design, such terms as active area, hole area, waste
area, and free area are used. They are explained below (see
also Figure 18 and Figure 19).
Active or Bubble Area (At) - This is the area between the
through and leaves the active area (At) it expands over the
downcomer(s) and its velocity drops. Thus, an area greater than
the bubble area is available for vapor flow. This larger area is
known as the free area (Af). The free area is what determines
the trays capacity. When multipass trays are designed, the tray
(either inboard or outboard) that has the smallest free is used to
set the trays capacity. For trays with sloped or stepped
downcomers, the average free area is used.
Flow Path Length (lfp) - The length of the contacting area in the
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D = hd + P + L + La
d
a
Pressure balance for outboard downcomer filling:
D = hd + Pd + La + L
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Tray diameter
Tray spacing
Downcomer area
Downcomer type
Weir height
Downcomer clearance
Jet flooding.
Key Performance
Parameters
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Tray diameter and tray spacing are the two most important
variables in tray design because they determine the diameter
and height of the tower. They affect two important performance
parameters: jet flooding and downcomer filling (downcomer
flooding). The tray diameter is the main variable in determining
the velocity of vapor between trays and, as a result, jet flooding.
Tray spacing also affects jet flooding. Higher tray spacing
between trays allows more liquid droplets to settle before they
reach the tray above; thus it helps reduce entrainment and the
percent jet flood. Improvement for tray spacings above 36 in. is
marginal. Because of the trade-off between tower diameter (tray
diameter) and height (tray spacing), finding the most economical
design may require the evaluation of alternative tray spacings.
Tray diameter and tray spacing also affect downcomer filling.
Vapor velocities determined by the tray diameter affect the tray
pressure drop of a tray and as a result the downcomer filling.
Tray spacing sets the height available for vapor disengagement
in the downcomers. Liquid height is the numerator and tray
spacing the denominator in determining the percent downcomer
filling.
The Saudi Aramco Engineering Standards, SAES-C-001, 5.1.3,
specify minimum tray spacing requirements for tower access
and service.
Towers with high liquid rates use more than one tray pass. The
upper acceptable limit of liquid rate per tray pass is about 15
gpm/in. of weir or according to the SADP criteria, 5000 gph/ft of
diameter. Tray hydraulics at higher liquid rates become
unpredictable.
The downcomer area determines the inlet velocity in the
downcomer and along with the tray spacing, the residence time
of liquid in the downcomer. SADP specify maximum inlet
velocity and minimum residence time requirements. Vendors
(see Glitsch valve tray design manual) have similar criteria.
When the downcomer inlet velocity sets the size of the
downcomer (usually at high liquid rates), it may be possible to
increase the cross sectional space available for vapor flow by
using sloped downcomers. The liquid leaving the downcomer is
relatively clear of vapor; thus, higher velocities (on clear liquid
basis) at the bottom of the downcomer are acceptable.
The active or bubble area of a tray normally is the area left after
the downcomer area is determined. Very small residence time
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and small flow path lengths along the bubble area may result in
low tray efficiencies.
The open or hole area of a tray affects tray performance
parameters such as dry tray pressure drop, weeping and tray
flexibility, and the transition between the froth and spray
regimes on the tray. Lowering the open area increases the
vapor velocity through the holes, the dry tray pressure drop, and
as a result, the downcomer filling. High vapor velocities through
the holes, especially when the liquid rates are low, may result in
a spray rather than froth vapor-liquid contact on the tray. High
open area reduces the flexibility of the tray and may result in
weeping and dumping at turndown conditions.
The weir height is a key factor in determining the liquid height
on the tray. As such, it affects tray performance parameters
such as pressure drop, weeping, and tray flexibility. It also
affects the spray-froth transition and the tray efficiency. Along
with the downcomer clearance, it determines the downcomer
sealing. The downcomer clearance also affects the pressure
loss under the downcomer (or downcomer contraction pressure
loss hd) and therefore, downcomer filling. For trays with high
liquid rates, shaped lip downcomers help reduce pressure drop.
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(b)
(c)
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Tower Internals
The following is a list of common tower internals. The design of
most of these internals is covered in SADP-C-001. In addition to
SADP, vendors can provide designs and design criteria.
Tray support.
Downcomer seal.
Antijump baffle.
Tower inlets.
Tower drawoffs.
Reboiler drawoffs.
Tray Transitions
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Downcomer Seal
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Seal Pan
Seal pans provide seal for the bottom tray. A typical seal pan
arrangement is shown in Figure 27.
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Summary
Valve and sieve trays are the trays most commonly used in
the petroleum industry. Valve trays are the first choice for
most Saudi Aramco applications.
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WORKAIDS
WORK AID 1:
Tray
Type
Capacity
Efficiency
Cost per
Unit Area
Sieve
Medium to
high.
Valve
Medium.
High.
Medium to
high; as good As good as About 10%
sieve trays. greater than
as sieve
Sieve Trays.
trays.
Bubble
Cap
Medium to
high, except
low to
medium at
high liquid
rate.
Medium to
high.
High.
At least twice
the cost of
sieve trays.
Flexibility
Remarks
Medium.
3/1 can
usually be
achieved.
Alternative to
valve trays
when high
turndown is not
required.
High.
Possibly up
to 5/1.
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WORK AID 2:
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GLOSSARY
Nomenclature
Ad
A1
Af
Ap
At
Aw
Co
CSB
DT
Fh
Aeration factor
FP
hd
he
ho
hon
hr
ht
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hv
hw
hwi
hwo
K1
La
lfp
lud
lw
lwi
LLH
LLL
Np
Pd
Pw
Sd
Sdi
Sdo
St
TT
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Ui
Uo
Va
VL
VN
Vapor velocity based on the net tray area available for liquid
disengagement, ft/s, m/s
Definitions
Active Area
Antijump Baffle
Arc Downcomer
Baffle Sections
Blank Tray
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Cartridge Tray
Chimney Tray
Choking
Chordal Downcomer
Column
Cross-Flow Devices
Debottlenecking
Demisting
Downcomer Area
Downcomer Clearance
Downcomer Contraction
Pressure Drop
Downcomer Filling
Downcomer Fooding
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Downcomer Rise
Downcomer Seal
Downcomers
Dumped Packing
Dumping
Entrainment
Flexibility
Flooding
Flow Regimes
Free Area
Froth
Grids
Hole Area
Inboard Downcomer
Jet Flooding
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Outboard Downcomer
Packing
Percent Jet Flood (% flood) The ratio, expressed as a percent, of the vapor velocity
between the trays, V, divided by the maximum vapor
velocity that will not cause flooding.
Plates
Pumparound
Random Packing
Seal Pan
Sheds
Sieve Tray
Sloped Downcomer
Spray
Stages
Stepped Downcomer
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Straight Downcomer
Structured Packing
Superficial Velocity
Support Ring
Tower
See column.
Tray Loadings
Tray Spacing
Tray Turndown
Truss
Turndown
Ultimate Capacity
Valve Tray
Waste Area
Any area in the active area that is farther than 3 in. from
the edge of a contacting device.
Weeping
Weir
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ADDENDUM:
TABLE OF CONTENTS
TOWER INTERNALS.................................................................................................... 63
Drawoffs ............................................................................................................. 63
Partial Drawoffs at Tray Inlet.................................................................... 63
Total Drawoffs at Tray Inlet...................................................................... 63
Details of Column Drawoffs ..................................................................... 64
Drawoff Nozzle Sizing.............................................................................. 65
Potential Hydraulic Problems at Drawoff Locations ............................................ 66
Reboiler Drawoffs .................................................................................... 67
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TOWER INTERNALS
Drawoffs
The liquid flowing down a column may be withdrawn partially or totally. A partial drawoff
normally does not exceed 60% of the internal reflux product at the drawoff tray.
Withdrawal should be from the inlet of a fractionating tray, from a blank tray, or from a
pan extending across the column. A complete pan should be used when appreciable
liquid holdup is required, as for product surge or water settling (SADP-C-001 3.1.4).
The following general principles should be used in designing drawoffs.
Partial Drawoffs at
Tray Inlet
A recessed box should be used under the downcomer with the drawoff nozzle on the
bottom or on the side of the box. The downward liquid velocity should not exceed 0.06
m/s (0.2 ft/s) based on the horizontal cross section. The depth of the box should be 1.5
times the drawoff nozzle diameter with a minimum of 152 mm (6 in.). If the length to
depth ratio of the box exceeds 1.5, a flat, antivortex baffle should be provided at tray
level. The drawoff box should not restrict the downcomer entrance on the tray below.
Total Drawoffs at
Tray Inlet
For a total liquid drawoff, a high overflow weir should be provided that will prevent the
liquid from flowing onto the next tray.
The tray spacing should be adequate to allow overflowing this weir without filling the
downcomer at a maximum tray pressure drop. A drawoff nozzle behind the downcomer
should be high enough to ensure that the downcomer will be sealed at the maximum
anticipated tray pressure drop. Locate the bottom of the drawoff nozzle not less than 1.5
times the maximum anticipated tray pressure drop above the bottom of the downcomer.
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Details of Column
Drawoffs
Vapor risers should be provided in a blank tray. The risers are sized based on a
pressure drop of 13 to 51 mm (0.5 to 2 in.) of liquid. The risers should be 152 mm (6 in.)
higher than the high liquid level. Flat baffles of the riser diameter should be placed
above and below the risers to improve the vapor distribution over the blank tray. The
annular area between baffles and riser should not be less than the riser cross section.
For a partial drawoff, the overflow weir should be notched to a depth of 200 to 250 mm
(8 to 10 in.) to minimize changes in overflow rate with fluctuations of liquid level. The
flow rate through the notches should be calculated from the following equations:
Q = 5.21 10 -5 b h on 1.5
where:
Q
b
hon
=
=
=
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Normal tray spacing is usually provided below a blank tray and above the high liquid
level on the blank tray.
velocity through the nozzle of 0.9 m/s (3 ft/s). For this velocity, the required nozzle
diameter should be determined from the following equations:
D = 37.3 Q
where:
0.5
If the calculated nozzle size is less than the line size, the line size is used.
Total Drawoffs - The theoretical nozzle size should be calculated by the formula:
D = 54.8 Q
0.4
The actual nozzle size should have at least a 20% greater area than the calculated
theoretical size.
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Vapor Drawoffs, Bottom Drawoffs, and Blank Tray Drawoffs - These drawoffs should
have the same size as the connected line in cases where a liquid head of 0.3 m (1 ft) or
greater is available. When the available liquid head is less than 0.3 m (1 ft), the Total
Drawoffs formula should be used.
Coke Strainers - In vacuum pipestills and fractionators for cracked products, coke
strainers should be used to keep large pieces of coke out of the pump suction lines
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Reboiler Drawoffs
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