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forExternalPipelineCoating
TABLEOFCONTENTS
1.0
2.0
3.0
4.0
5.0
6.0
7.0
SCOPE........................................................................................................................................................................................2
MATERIALS.............................................................................................................................................................................2
APPLICATION .........................................................................................................................................................................2
INSPECTION ............................................................................................................................................................................5
COATING REPAIR..................................................................................................................................................................7
QUALITY CONTROL TESTS................................................................................................................................................8
HANDLING AND STORAGE PROCEDURES.....................................................................................................................9
APPENDICES
I
II
BendTestProcedure
FoamStructureTestProcedure
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
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1.0
SCOPE
1.1
General
1.2
ConflictingRequirements
1.3
IndustryStandards
1.3.1
Pipingshallbesuppliedwithoutvarnish
ormilllacquers.
2.2
Coating
Shopappliedexternalcoatingmaterial
shallbeoneofthefollowingfusion
bondedepoxypowders:
2.2.1
Forlinesoperatingattemperaturesup
to150F
3MScotchkote206N
InternationalInterponHD3005
NapGuardMarkX
LillyPipeclad
ValsparD1003LD
2.2.2
Forlinesoperatingattemperatureupto
230F
3MScotchkote226Norequivalent
2.3
BatchInformation
2.3.1
SteelStructuresPaintingCouncil(SSPC)
SSPCSP1 SurfacePreparation
SSPCSP10NearWhiteMetalBlast
SSPCVIS1Pictorial Surface Preparation Standards
forPaintingSteel
Surfaces
1.3.2
2.0
MATERIALS
2.1
Piping
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
2.3.2
Themanufacturer'sname
Thematerialidentificationnumber
Thebatchnumber
Dateofmanufacture
Theshelflifeandstorage
temperaturelimits
Infraredscanofpowderandtypical
powderscansforcomparison.
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Geltimeatrecommended
applicationtemperature.
Particlesizedistribution.
2.3.3
2.3.4
2.4
RepairMaterials
2.4.1
2.4.2
3.0
APPLICATION
3.1
General
3.1.1
3.1.2
ItshallbetheApplicator'sresponsibility
tostopthecoatingprocessatanytime
when conditions may exist that might
adverselyaffectthecoatingquality.The
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
3.1.3
3.1.4
3.2
SurfacePreparation
3.2.1
Priortoabrasivecleaning,alloil,grease,
salts, and other deleterious materials
shallberemovedbysolventcleaningin
accordance with SSPC SP1 or by
detergent washing or steam cleaning.
No residue that will affect adhesion
shallbeleftonthesurface.
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3.2.2
3.2.3
3.2.4
Forconsistentsurfacefinish,astabilized
working mix shall be maintained by
frequent small additions of new
abrasive
commensurate
with
consumption;infrequentlargeadditions
shallbeavoided.
3.2.5
3.2.6
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
3.2.8
Surfacepreparationshallnotreducethe
pipewallthicknessbelowtheminimum
requiredbythepipeSpecification.
3.2.9
3.2.10
3.3
Heating
3.3.1
Beforecoating,thepipeshallbeheated
so that its temperature is within the
application
temperature
range
recommended
by
the
coating
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3.3.3
3.3.4
3.3.5
3.4
SurfaceConditioning
Unlessotherwisespecificallydeletedin
thepurchaseorderorrequestfor
quotation,aftertheappropriatesurface
cleanlinesshasbeenachieved,SSPC
SP10,thepipeshallbetreatedas
follows:
3.4.1
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
3.4.3
Treatmentshallbeforaminimumof20
seconds with the pipe surface
temperature between 110F (66C).
With approval of Company, treatment
time can be extended at the rate of 1
second for each degree below 110F
(2secondsforeachdegreebelow43C).
3.4.4
3.4.5
Thewashsolutionandrinsewillresultin
a weak concentration of approximately
1.5%orlessphosphoricacid.Itshallbe
the responsibility of the Applicator in
the proper handling and disposing of
this waste including neutralizing if
required,inamannerrecommendedby
themanufacturer.
3.5
CoatingApplication
3.5.1
coating
manufacturer's
requirements/recommendations. The
pipe shall be coated while its surface
temperature
is
within
the
manufacturer's
recommended
temperaturelimits.
3.5.2
Thecoatingshallbeappliedtoproduce
auniformdrycoatingthicknessof:
12milsminimumforlinesoperatingat
temperatures up to 230F coated with
3M Scothkote 226N. (Minimum
required thickness on equivalent high
temperaturecoatingsshallbeaccording
tomanufacturersrecommendation.)
3.5.3
at
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
3.5.4
3.5.5
3.5.6
3.5.7
4.0
INSPECTION
4.1
General
4.1.1
4.1.2
TheApplicatorshallnotifytheCompany
notlessthanfivedaysinadvanceofthe
start of each production run and shall
provide him with a detailed time
schedule to permit him to witness all
processingandtestingphases.
4.1.3
4.1.4
4.1.5
TheCompanyshallhavetherighttohalt
the coating of pipe pending alterations
orcorrectionstotheprocesstocorrect
allfaultsfoundintheworkthatresultin
failureoftheworktoconformtothese
Specifications.
PreheatTemperatures
Optical
pyrometers
and/or
thermometers shall be used to assure
correct pipe temperature (see Section
3.3).Tempilstiksmaybeusedtocheck
accuracy of the pyrometers and/or
thermometers, but their use must be
minimized(see3.3.4).
4.4
Thickness
4.4.1
4.4.2
4.4.3
4.5
HolidayDetection
4.5.1
Allcoatedpipeshallbe100%inspected
for holidays. Either a pulsating or a
nonpulsating spiral coil or wet sponge
detector is acceptable, provided it
meetsandisoperatedaccordingtothe
requirements in NACE Recommended
TableI
RequiredRecords
Coating/Inspecti
onStep
1.SurfaceProfile
RequiredFrequency
Checkthreelocationsperjoint:
a. At beginning of each eighthour shift
and every two hours throughout the
shift.
b.Wheneveranychangeinabrasivetype
or blast pressure is made (see Section
4.2).
2.Thickness
Fivemeasurementsperjointofpipe(see
Section4.4).
3.
Repaired 100% inspected. Record number of
Holidays
repaired holidays per joint (see
Section4.5.5).
4.2
SurfacePreparation
4.2.1
4.2.2
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
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4.5.3
4.5.4
4.5.5
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
5.0
COATINGREPAIR
Each length of coated pipe leaving the
Applicator's premises shall be
completely free of holidays and visual
coatingdefects.
5.1
RejectedCoatings
5.2
HolidayRepair
Allcoatingdefectsdisclosedbyvisualor
holiday detector inspection shall be
repaired at no additional expense to
Company.Forallholidayrepairswhere
repairs are approved by Company, the
followingprocedureshallbefollowed:
5.2.1
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5.2.2
5.2.3
Thematerialforpatchingrepairsinthe
millshallbethoselistedinSection2.4of
this Specification. No thermoplastic
patchsticksshallbeused.
5.2.4
5.2.5
6.0
Aftercuring,allpatchesshallbevisually
inspected and jeeped with a wand
electrode of fine brass whiskers at a
voltage of not less than 100 volts/mil
andtestedforadhesionbyknifelifting.
Theuseofawetspongedetectorsetat
the manufacturer's recommended
parameters is also acceptable. The
patchshallbeholidayfreeandshallnot
disbondwhenliftedwithaknife.
QUALITYCONTROLTESTS
The Applicator shall perform the tests
listedinthissection.TheCompanymay
bepresentduringthetests.Testresults
mustbemadeavailablewithin72hours
of taking the sample. No pipe lot shall
beacceptedbeforethetestresultsfrom
the representative samples are known.
If any test results do not meet the
Specification, the Company will specify
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
SampleFrequency
FromJointNo.
1
200
500
Every500jointshereafter
Thelastjoint.
Onerandom,fromeachday's
production
6.2
BendTest
TheApplicatorshallperformbendtests
perAppendixIoneachsamplelistedin
Section1.
6.3
DifferentialScanningCalorimeter
Analysis
6.4
AdhesionTest
Atproductionstartup,afterproduction
interruptions,atthestartofusinganew
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thesteel.A3inchdiameterPVCcellis
centered over the intentional holiday
and fixed to the coated surface with
silicone. The cell is filled with 3% NaCl
electrolyteandaplatinumwireanodeis
inserted below the electrolyte level. A
3.5 DC voltage (reference saturated
calomel) is impressed and the entire
testplateandapparatusaremaintained
at150Ffor24hours.
6.4.2
AttheintersectionoftheX,anattempt
shallbemadetoforcethecoatingfrom
thesteelsubstratewiththeknifepoint.
Refusal of the coating to peel
constitutes a pass. Partial or complete
adhesion failure between the coating
and the metal substrate constitutes a
failure.
6.5
FoamStructureTest
6.6
CathodicDisbondmentTest
Thefollowingcathodicdisbondment
test,shallbeconductedonthesamples
listedinSection6.1.
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
Attestcompletion,a30degree"V"cut
ismadethroughthecoatingoriginating
at the intentional holiday.Theamount
of coating disbonded in the "V" is
evaluated and expressed in millimeters
radius (mmr), as measured from the
holiday edge to where well bonded
coatingexists.
Themaximumdisbondmentallowedis8
mmr.
7.0
HANDLINGANDSTORAGE
PROCEDURES
7.1
7.2
7.3
7.4
TheCompanywillhaveauthoritytostop
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SpecificationforFusionBondedEpoxyforExternalPipelineCoating
applicable APIStandardsatApplicator's
expense. Pipe damaged beyond
permissible repair shall become the
property of Applicator. The actual
Company invoiced cost of scrapped
pipe, including pipe, coating, and
transportation, shall be deducted from
theamountduetheApplicator.
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APPENDIXI
BENDTESTPROCEDURE
Scope
ThisprocedurechecksdegreeofcureandadhesionofFBEcoatedpipe.
Equipment
Fourpointbendapparatus
Procedure
1. Cutaminimumoffour8in(longitudinal)x1in(circumferential)xthickness(pipe+coating)strapsoutof
thecoatedpipe.Filealledgessmooth.
2. Usingafourpointbendapparatus,bendeachstrapuntilfailure,whichisthepointwherecracksbeginto
bevisibleinthecoatingwhenviewedwithnomagnification.
3. Measurethestrapthickness(pipe+coating),t,andthedeflectedangle,A,asshowninFigure:
4. Calculatetheamountofbendindegrees/pipediameter.
degrees/pipediameter=(A.t)/d(Eq.1)
whereA
= deflectionangleindegrees
d
= distancebetweentwocenterpointsinbendtestrig(where
strainisconstant),usually2inches.
t
= pipewall+coatingthickness.
5. Topass,theaverageofthevaluesfromEquation1forthefour(ormore)samplesmustbegreaterthan2.9
degrees/pipediameter.Anysinglevaluemustbeatleast2.3degrees/pipediameter.Also,thecoating
shallshowfulladhesiontothesteelinthebend,withnosplitting,cracking,orflakingoccurringbeforea
bendof2.9degrees/pipediameterisobtained.
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
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APPENDIXII
FOAMSTRUCTURETESTPROCEDURE
Scope
Thisprocedurecoversthetestmethodtodeterminethedegreeoffoamingexperiencedbythecoatingduring
application.
Equipment
Sharpknife.
40powermagnifier(ormicroscope).
Procedure
Use the knife to "snap" off coating from surface and examine crosssections under magnification. Ratethe
presenceofvoidsaccordingtotheexamplesinFigure:
SpecificationforFusionBondedEpoxyforExternalPipelineCoating
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