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[11]
[45]
Boehme et al.
[54] METHOD OF PREPARING PERACETIC
ACID
[30]
[56]
[51]
[52]
[58]
Patent Number:
Date of Patent:
4,904,821
Feb. 27, 1990
References Cited
FOREIGN PATENT DOCUMENTS
260/502 R
[57]
ABSTRACT
lower-boiling solvent.
9 Claims, 1 Drawing Sheet
US. Patent
lvEm:
E0532
KW-25 HI
IILJI
4,904,821
4,904,821
gen peroxide to carboxylic acid used was set at certain 65 peracetic acid, 14-17% by wt. acetic acid, remainder
Water.
values before the reaction was started. It also turned out
Suitable organic phosphates for purposes of the in
that the safety of the system did not, as assumed, remain
vention are those with 3-30 carbon atoms such as trisub
continuously constant after a certain value but rather
4,904,821
25-30% by wt.
This bottom mixture placed in a receiver before the
start of the reaction is maintained constant during the
condensed.
4,904,821
0.43 and 0.54, and the reactants are placed in the bottom
of said distillation zone before the start of said reaction,
tributyl phosphate.
55
60
65
1k
=1