CEM Labwave 9000

Operation Manual
Moisture/Solids Analyzer
LabWave 9000
TM
Copyright 1999 by CEM Corporation

All Rights Reserved
This manual contains proprietary information
which shall not be disclosed or reproduced or transferred
to other documents without prior written permission
from CEM Corporation.
LabWave 9000 is a trademark of CEM Corporation.
CEM is a registered trademark of CEM Corporation.
U.S. patents 3,909,598, 4,291,775, 4,457,632, 4,466,804,
4,681,996, 4,753,889 and 4,438,500
Other U.S. and foreign patents pending
CEM Corporation
Matthews, North Carolina 28106
(704) 821-7015
FAX: (704) 821-7894
MANUFACTURED IN THE
UNITED STATES OF AMERICA
Part No. 600066
Rev. 1
NOTICE
The following precautions should be observed to avoid possible exposure
to excessive microwave energy:
Do not tamper with the safety interlocks. The LabWave 9000 is
equipped with three door safety interlock switches which prevent
the instrument from producing microwave power if the door is
open. Tampering with the safety interlocks will allow microwave
production when the door is open, which is very dangerous.
Do not place any object between the front of the microwave cavity
and the door or allow soil or cleaner residue to accumulate on seal
ing surfaces.
Do not operate the instrument if it is damaged. It is particularly
important that the instrument door close properly and that there
is no damage to the door (bent), hinges and latches (broken or
loosened), or door seals or sealing surfaces.
The instrument should be adjusted or repaired only by qualified
service personnel.
The following precautions should be observed to avoid instrumentinduced electromagnetic interference:
The possibility of instrument-induced electromagnetic interference (EMI) is minimal if precautions outlined above are
followed.
The instrument should not be placed close to any electrical device
susceptible to EMI. It is suggested that the user post a sign
warning pacemaker wearers that a microwave device is in
operation.
If the instrument is suspected of inducing EMI, the door and the
front of the cavity should be carefully inspected as outlined on
page 147. A microwave leakage measurement should be performed
as outlined on page 147. Leakage measured above the legal limit
of 5 mW/cm2 should be reported to the CEM Service Department.
This instrument utilizes high voltages and microwave radiation. Instrument service and repair should be performed only by those trained in
repair and maintenance of high voltage and microwave power systems.
This instrument complies with United States Code of Federal Regulations (CFR) Title 21, Part 1030 for microwave leakage. A verification
report is on file.
This instrument complies with United States Code of Federal Regulations (CFR) Title 47, Federal Communications Commission (FCC)
Part 18 Industrial, Scientific and Medical (ISM) Equipment
emissions requirements. A verification report is on file.
LabWave 9000
600066
Rev. 1
To the best of our knowledge, the information contained herein is

accurate. However, CEM Corporation cannot accept liability of any
kind for the accuracy or completeness of the information contained in
this manual. The final determination of the suitability and proper use
of the instrument described herein, the accuracy of the information
and data obtained from such use, and whether such use infringes any
patents or the legal safeguards of others are the sole responsibility of
the user.
Warnings, Cautions and Notes

Warnings, cautions and notes are included throughout this manual
and should be read thoroughly and strictly followed.
WARNING: A warning is inserted for essential information used to
emphasize dangerous or hazardous conditions to the operation, cleaning and maintenance of the instrument which may result in personal
injury.
CAUTION: A caution is inserted for essential information used to
emphasize procedures which, if not strictly followed, may result in
damage or destruction to the instrument or improper instrument
operation.
NOTE: A note is inserted for emphasis of procedures or conditions
which may otherwise be misinterpreted or overlooked and to clarify
possible confusing situations.
LabWave 9000
600066
Rev. 1
ii
Table of Contents
iii
Introduction
Principle of Operation
Additional Programs
1
1
2
II
Installation
Unpacking
Instrument Description
Instrument Location
Instrument Startup
Instrument Inspection
Printer Installation
Personal Computer or Serial Printer Setup (Port J2)
External Balance Setup (Port J1)
3
3
4
7
7
8
9
10
10
III
Setup
Date/Time
System Parameters
Calibrate Menu
Password
Standard Solution Test
11
12
13
20
22
25
IV
Operation
General Precautions
Sample Analysis
Sample Preparation
Sample Weight
Sample Holders
Thermapad
Sample Application
Drying Time and Microwave Power
Analysis Programs and Options
Bias Identification
Determining Ash/COH for Processed Meats
Ash Content of Meats
Methods Development
Applications
31
31
31
32
32
34
35
36
36
41
42
42
45
46
48
50
Quick Dry
Auto Time Sample Analysis
Constant Weight Sample Analysis
59
59
64
VI
Program/Edit/Run Method
Program/Edit Method
Moisture/Solids Analysis
Moisture/Fat Analysis
Moisture/Fat/Protein Analysis
Moisture/Fat/Protein Parameters
Program Deletion
Run Method
Moisture/Solids - Standard
Moisture/Solids - TSS (Total Suspended Solids)
69
69
70
72
73
74
75
76
76
80
LabWave 9000
600066
Rev. 1
Table of Contents (Continued)

Program/Edit/Run Method (Continued)
Moisture/Solids - TVSS (Total Volatile Suspended
Solids)
Moisture/Solids - TVSS (Total Volatile Suspended
Solids) - Alternate Mode
Moisture/Solids - Percent Ash/Volatile Solids
Moisture/Solids - Percent Ash - Alternate
Moisture/Solids - Syringe Weigh
Internal Balance Syringe Weigh
External Balance Syringe Weigh
Moisture/Solids - Dilution
Moisture/Fat or Moisture/Fat/Protein - Standard
Moisture/Fat or Moisture/Fat/Protein - Alternate
Moisture/Fat or Moisture/Fat/Protein - Dilutions
Moisture/Fat or Moisture/Fat/Protein - Modified Fat
VII
Maintenance, Troubleshooting and Service

Cleaning Recommendations
Routine Maintenance
Microwave Leakage Measurement
Microwave Power Measurement
Error Messages
Troubleshooting
Troubleshooting Guide
Service and Repair
85
90
96
101
107
108
112
116
121
126
133
139
147
147
147
147
148
151
153
154
155
VIII Ordering Information
161
IX
Specifications
Emission and Safety Approvals
163
163
Warranty
Customer Support Service Numbers
165
166
Appendix
LabWave 9000 Quick Selection Chart
LabWave 9000
600066
Rev. 1
iv
LabWave 9000
600066
Rev. 1
Introduction
The CEM LabWave 9000 Moisture/Solids Analyzer is an analytical

instrument designed to provide rapid moisture/solids analysis. The
LabWave 9000 consists of three major components:
the microwave drying system
an integrated analytical balance
a digital computer
The moisture or solids content of the sample is automatically calculated based on weight loss after drying. (The term moisture is
used throughout this manual when referring to any volatile substance
whose weight loss the LabWave 9000 can measure after drying.)
The LabWave 9000 utilizes microwave energy to dry samples. Microwave energy is transmitted at the speed of light. Polar compounds
such as water, polar organic solvents such as alcohols or ketones, and
ions in solution will absorb microwave energy and volatilize. Once
water and/or other solvents have been volatilized, the remaining solid
material does not usually absorb microwave energy and will remain
relatively cool. Thus, the weight loss is due only to the volatile solvents present in the sample.
The LabWave 9000 delivers approximately 630 watts of microwave
energy at a frequency of 2450 MHz when programmed for 100 percent
power. To control the rate of drying, percent of power may be programmed. The percent of power that is programmed into the Labwave
9000 establishes a percentage of each second of operation during
which the magnetron operates at 100 percent power. Thus, at 50 percent power, the instrument delivers 630 watts of power for one-half
second then turns off the microwaves for the next one-half second.
The LabWave 9000 is equipped with an exhaust system to remove
vapors, an analytical balance and a patented device to absorb excess
microwave energy. A microprocessor controls and monitors operations
and automatically calculates sample results.
LabWave 9000
600066
Rev. 1
Additional Programs
In addition to the standard features of moisture and solids analysis,
the LabWave 9000 also has the capability of performing the following
functions:
Fat Analysis For samples which require both moisture and fat
analyses. The sample is dried in the LabWave 9000, then transferred to the Fat Extraction System where the fat is removed.
The extracted sample is redried and reweighed in the LabWave
9000, and the percent moisture and fat content of the sample are
displayed. By using the alternate mode in the fat analysis program, the Fat Extraction System can extract one sample while
the LabWave 9000 is drying or redrying another, maximizing the
use of the two instruments to reduce sample analysis time. CEM
procedures for many products are AOAC approved.
Total Suspended Solids (TSS) For automatic calculation of TSS
after the filtrate is dried by the LabWave 9000. The nondissolved solids in a given volume of fluid are measured using
Initial Liquid Volume and the dried filtrate as the solids. The
results are calculated in units of mg/liter. This option is useful in
the wastewater industry.
Total Volatile Suspended Solids (TVSS) For automatic calculation of TSS after the filtrate is dried by the LabWave 9000 and
TVSS after the filtrate is ashed in a CEM MAS-7000 or other
ashing furnace. By using the alternate mode in the TVSS
program, one sample can be dried in the LabWave 9000 while a
second sample is being ashed in the MAS-7000, maximizing the
use of the two instruments to reduce sample analysis time.
Percent Ash/Volatile Solids Samples are first dried in the LabWave 9000, and percent moisture or solids is calculated. After
drying, the samples are ashed in a muffle furnace or a CEM
MAS-7000 and returned to the LabWave 9000 to be reweighed
and the percent ash/volatile solids calculated. By using the
alternate mode in the percent ash program, the ashing furnace
can ash one sample while the LabWave 9000 is drying or
reweighing another, maximizing the use of the two instruments
to reduce sample analysis time.
Syringe Weigh For samples that, due to rapid evaporation, cannot achieve a stable initial weight with the standard application.
This method is used with samples that contain ketones, alcohols
or aldehydes such as nail polishes or coatings. Initial weight of
the sample is measured in a tared syringe. Application of the
sample to a glass fiber pad from a syringe is the same as with
other analyses.
Dilution For the greatest accuracy and precision when analyzing viscous or heat sensitive samples or samples which dry
unevenly. The sample is diluted with water or a polar diluent,
which is miscible with the sample, and weighed on an external
balance connected to the LabWave 9000. The Labwave 9000
automatically calculates a dilution factor which is used to
calculate percent solids.
2
LabWave 9000
600066
Rev. 1
II
Installation
Unpacking
1. Carefully remove the LabWave 9000 from its shipping carton and
place it on a vibration-free workbench or laboratory table. Retain
all packing materials.
CAUTION
Do not lift the instrument by the door handle.
Damage to the door and lock mechanism may
result which could cause microwave leakage.
2. Verify that all accessories listed below and illustrated in figure 1
are included:
Starter Accessory Kit (P/N 302860), containing:
Balance Stem (2)
Standard Solution
Balance Pan (2)
Teflon Coated Spatula
Dispensing Bottle
Disposable Pipette
Weight
Glass Fiber Sample Pads
Fuse
Operation Manual
Pedestal Access Tool
3. Remove the cardboard and other packing materials from inside the
instrument cavity.
Balance
Stem
(003670)
Spatula
(302001)
Balance
Pan
(004120)
Dispensing
Bottle
(230230)
Standard
Solution
(302600)
Glass Fiber
Sample Pads
(200150)
Glass Fiber
Sample Pads
Weight
(260111)
Reorder part
Disposable
Pipette
(302150)
# 200150
CEM Corpo
ration
P.O. Box 200
Matthews,
NC 28106
1-800-334-6
(in NC: 1-704 317
-821-7
Telex: 80211 015)
8
FAX: 704-8
21-7015
n
o
ti
ra
o
rp
o
C
Fuse
(188320) (120V)
(188331) (240V)
rs
to
va
no
In
in
e
av
w
ro
ic
M
gy
lo
no
ch
Te
Pedestal
Access
Tool
(301710)
Operation
Manual (600066)
Figure 1. Accessories
LabWave 9000
600066
Rev. 1
Instrument Description
Display
LCD Board (304025)
Control Board (203170)
ABC
Keyboard (013310)
(See figure 3, pg. 5)
DEF
GHI
JKL
MNO
PQR
STU
VWX
YZ
SPACE
SYMBOL
START
STOP
ENTER
Serial Port J2
External
Balance
Port J1
Innovators in
Microwave Technology
Door
Seal
Balance
Air Shield
(500200)
Pedestal
Access
Balance
Pan & Stem
(See figure 12, pg. 160)
Parallel
Printer
Port
Figure 2. Front View

Display displays instructional messages and analysis results on
a 30 character liquid crystal display which will display bit mapped
graphics or eight lines of text with thirty characters per line.
Keyboard controls operation of the LabWave 9000. Power level,
time, or other numeric data may be entered as requested on the
display.
F1 - F4 Press to perform functions as required on various display screens. In all editing functions, pressing F1 will clear the
variable to be edited; pressing F2 will change from upper to
lower case letters or vice versa.
0 - 9 Press to select values for parameters such as time and
power and to enter text items such as program name, etc. Pressing a numeric key one time will enter its numeric value. Pressing
the same numeric key two times will enter its first alpha (letter)
value. Pressing the same numeric key three times will enter its
second alpha value. Pressing the same numeric key four times
will enter its third alpha value. Pressing the same numeric key
five times will enter its numeric value, restarting the above
process. The 0 key multi functions with symbols. (Example: To
enter a program name of BEEF 1, press 1 three times; press 2
three times; press the right arrow key; press 2 three times;
press the right arrow key; press 2 four times; press the dot
key two times to enter a space; and press 1 one time.
. (dot) or Space Press to insert a space in a program name.
4
LabWave 9000
600066
Rev. 1
F1
F2
F3
F4
ABC
DEF
GHI
JKL
MNO
PQR
STU
VWX
YZ
SPACE
SYMBOL
START
STOP
TARE
ENTER
Figure 3. Keyboard
Enter Press to store entered parameters and data in computer
memory.
, , ,
Press to move the entry window (darkened or highlighted area of the display) to the selection to be programmed or
changed. The left arrow key is also the backspace key. When
entering method names, the right arrow key functions as
revert, to permit entry of consecutive letters using the same
number key.
Start/Stop Press to begin or stop sample analysis. Microwave

heating begins when the Start/Stop button is pressed unless the
instrument door is open. Percent power and time remaining for
the method will be displayed during operation. Operation will
continue through the analysis unless the Start/Stop button is
pressed to interrupt or stop an analysis. When the Start/Stop
button is pressed to stop operation, microwave energy and time
countdown are simultaneously suspended.
Tare Press to zero the weight of sample pads prior to sample
analysis.
Printer and Computer Ports allow communication with external devices for display and printout of analysis data.
Balance Air Shield prevents air flow within the microwave cavity from affecting weight measurements.
Balance Pan holds sample pads with sample during analysis.
Door Seal ensures tight fit between the door and interior cavity
to prevent microwave leakage.
LabWave 9000
600066
Rev. 1
Magnetron
Cooling
Fan
(184900)
Cavity Exhaust
Fan (184860)
Power
Switch
(142000)
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Power
Cord
Power Cord
Receptacle
(251460)
Fuses
15A - 120V (188320)
8A - 240V (188331)
Nameplate
Figure 4. Rear View
Exhaust Fan exhausts heat and moisture from instrument cavity during sample drying.
Magnetron Cooling Fan draws air through the magnetron.

Fuses prevent electrical power overload.
Power Cord Receptacle receives the female end of the power
cord.
Power Cord conducts electrical power from the AC outlet to the
instrument. It is detachable.
Power Switch turns electrical power to the instrument on and
off.
Nameplate lists model and serial number.
LabWave 9000
600066
Rev. 1
Instrument Location
Place the LabWave 9000 in a location that:
1. provides at least 8 in. (20 cm) open space on each side and 6 in. (15
cm) open space in the rear of the instrument for ventilation.
2. is free from vibration of large equipment and/or excessive walkthrough traffic.
3. provides a temperature range of 41F (5C) to 104F (40C) and a
humidity range of 10-85 percent relative humidity.
4. provides adequate bench space for sample handling and printer
placement (if applicable).
5. allows instrument to be connected to a dedicated, grounded 120
VAC (108-122 VAC), 60 Hz outlet (240 VAC, 216-244 VAC, 50 Hz
outlet, where appropriate) supplying 20A @ 120 VAC (10A @ 240
VAC). The LabWave 9000 should be operated on a stabilized, constant voltage AC power supply, and the voltage must be within 10%
of the specified level.
CAUTION
Line voltage fluctuations greater than 10% will
affect instrument performance.
6. provides access to a fume hood or other means of fume disposal for
an instrument equipped with an accessory exhaust hose.
Instrument Startup
1. Plug the female end of the power cord into the power cord receptacle on the power panel in the rear of the instrument. Plug the
male end of the power cord into a grounded, dedicated electrical
outlet.
2. Position the power switch located on the power panel in the rear of
the instrument in the on position.
CAUTION
Permit the Labwave 9000 to warm up (power
switch on, microwaves not being produced) for at
least 45 minutes prior to operation. If the instrument is switched off for an extended period of
time (weekend, holidays, etc.), ensure that warmup time is permitted prior to use.
Note: CEM Corporation recommends that the power cord be connected to an AC power receptacle and the power switch remain in the
on position at all times.
LabWave 9000
600066
Rev. 1
Instrument Inspection
1. Inspect the instrument cover and door for cracks, dents, or warping.
2. Inspect the rubber door seal for damage.
3. Inspect the door for proper alignment. When closed, the door and
seal should seat firmly against the front of the microwave cavity.
The door must open and close freely with no binding or restriction
of movement.
WARNING
If damage is noted, do not attempt instrument
operation.
4. Open the instrument door and inspect the balance stem that protrudes from the interior floor to ensure that:
a. it is free to move vertically a short distance. Carefully move the
stem up and down with your fingers.
b. it is centered within the floor opening. If the stem is not properly centered, contact the CEM Service Department or your distributor for instructions.
If the instrument has been damaged in shipping, contact the freight
carrier to report damage and to file a damage report. Contact the CEM
Service Department or your distributor to report damage and to
request service information.
CEM Corporation
Service Department
P.O. Box 200
3100 Smith Farm Road
Matthews, NC 28106-0200 USA
Within the continental United States
(800) 726-5551
Outside the United States
Telephone: (704) 821-7015
FAX: (704) 821-7894
CEM Ltd.
2 Middle Slade
Buckingham Ind. Park
Buckingham MK18 1WA
United Kingdom
Tel: (44) 1-280-822873
Fax: (44) 1-280-822342
CEM GmbH
Carl-Friedrich-Gauss-Str. 9
47475 Kamp-Lintfort
Germany
Tel: (49) 2842-96440
Fax: (49) 2842-964411
CEM S.r.l.
Via DellArtigianato, 6/8
24055 Cologno al Serio
Italy
Tel: (39) 35-896224
Fax: (39) 35-891661
LabWave 9000
600066
Rev. 1
Printer Installation
The LabWave 9000 supports a variety of different printer standards
IBM, Epson Compatible Graphics, Citizens, HP DeskJet, HP
LaserJet and Canon BubbleJet. The Canon BJC-4300 is available from CEM Corporation. This printer is factory set and
requires no setup.
To install the Canon BJC-4300, follow the procedures outlined below.
Refer to the manual shipped with the printer for illustrations and
explanation of the terminology used.
1. Press the LabWave 9000 power switch to the off position.
2. Remove the printer and its accessories from the shipping carton.
Place the printer on a vibration-free printer stand or a solid,
sturdy laboratory workbench or table. Save all packing material.
3. Plug the LabWave 9000 power cord into a grounded AC electrical
outlet. Plug one connector of the cord shipped with the printer into
the socket on the printer. Plug the other connector into the parallel
port of the LabWave 9000 (figure 2, page 4).
4. Press the power switch of the printer to on.
6. Press the Labwave 9000 power switch to on.
LabWave 9000
600066
Rev. 1
Personal Computer or Serial Printer Setup (Port J2)

Outlined below are default values for a personal computer or serial
printer to be connected to Port J2.
2400 Baud
No Parity
8 Data Bits
1 Stop Bit
Pin
2
3
5
Out
RX
TX
GRD
External Balance Installation

1. Press the LabWave 9000 power switch to the off position and
remove the power cord from the electrical outlet.
2. Place the external balance on a sturdy laboratory workbench or
table.
3. Plug one connector of the cord shipped with the external balance
into the socket on the balance and the other connector into the
external balance port of the LabWave 9000 (figure 2, page 4). Plug
the balance power cord into a grounded AC electrical outlet.
4. Based on the type external balance used, refer to the
manufacturers manual and/or CEM instructions for specific
procedures for setup and configuration of the balance and
instrument.
External Balance Setup (Port J1)

Outlined below are default values for available external balances.
Cables for Denver and Sartorius balances are available from CEM
Corporation.
10
Denver Instrument:
Cable No. 500665
300 Baud
No Parity
8 Data Bits
2 Stop Bits
Sartorius:
Cable No. 500660
1200 Baud
Odd Parity
7 Data Bits
1 Stop Bit
Mettler:
2400 Baud
Even Parity
7 Data Bits
1 Stop Bit
Scientech:
2400 Baud
Even Parity
7 Data Bits
1 Stop Bit
LabWave 9000
600066
Rev. 1
III Setup
Prior to system operation and sample analysis, perform the following
procedures to set system parameters such as date/time, printer functions, utilities, calibration, system password, etc.
1. Ensure that the power switch is in the on position. Press the
Start/Stop key to activate the system to the Main Menu.
LabWave 9000
Moisture and Solids Analyzer
MAIN MENU
F1: QUICK DRY
F2: PGM/EDIT/RUN METHOD
F3: SYSTEM SETUP
2. Press F3 to activate the System Setup screen.
SYSTEM SETUP
F
F
F
F
1
2
3
4
:
:
:
:
S
S
C
S
e
e
a
e
t D a t e / T i m e
t S y s t e m P a r a m e t e r s
l i b r a t e
t P a s s w o r d
ANY KEY - MAIN MENU
3. Press F1 to set date/time format.
LabWave 9000
600066
Rev. 1
11
SET FORMAT
12/24 Hour Format = XX Hr
Date Fmt = XX/XX/XXXX xx:xx
XX/XX/XXXX xx:xx
F1 - 12/24
F2 - Date Fmt
F3 - Set Clk
F4 - Esc
4. Hour Format can be set for either 12 hour or 24 hour format.

Change format by pressing F1. Date format can be set for either
year/month/date, month/date/year or date/month/year. Change
date format by pressing F2.
5. Press F3 to set clock (date/time).
SET DATE/TIME
Year
Month
Day
Hour
Min
XXXX
XX
XX
XX XX
XX
Arr - Up/Dn
F2 - AM/PM
F4 - Exit
Ent - Save
6. Using the numeric keys, enter the four-digit year. Press the down
arrow key to move the entry window to month. Using the numeric
keys, enter the month. Continue using the down arrow key and
numeric keys to enter the day of the month, the hour and minutes.
If necessary, press F2 to change AM to PM or vice versa. If an
error is detected in entered data, use the up and down arrow
keys to move the entry window to the desired position, and using
the numeric keys, enter the correct information.
7. Press Enter to save data in the instrument computer.
Note: If correct date and time settings have been previously set, press
F4 to exit back to System Setup screen.
SYSTEM SETUP
F
F
F
F
1
2
3
4
:
:
:
:
S
S
C
S
e
e
a
e
t D a t e / T i m e
t S y s t e m P a r a m e t e r s
l i b r a t e
t P a s s w o r d
ANY KEY - MAIN MENU
8. Press F2 to activate the Set System Parameters screen.
12
LabWave 9000
600066
Rev. 1
SET SYSTEM PARAMETERS

F1:
Sel Printer/Balance
F2:
Utilities
F3:
System Info
Any Key - Exit
9.
Press F1 to activate the Select Printer/Balance screen.

SELECT PRINTER/BALANCE
F1: Select Printer
F2: Select Print Style
F3: Select Print Form
F4: Select Ext Balance
Any Key - Exit
10. Press F1 to activate the Select Printer screen.

SELECT PRINTER
1>
2>
3>
4>
5>
6>
IBM
EPSON
CITIZENS
HP DESK JET
HP LASER JET
CANON BUBBLE
Up/Dn Arr - Sel
Ent - Exit
11. Use the up and down arrow keys to choose the type printer
installed with the instrument. Refer to Printer Installation,
page 9 for printer information. Press Enter to exit.
F1: Select Printer
Any Key - Exit
12. Press F2 to activate the Select Print Style screen.
LabWave 9000
600066
Rev. 1
13
CANON BUBBLE
Quality
Pitch
XXXXX
XX cpi
F1 - Quality
F2 - Pitch
Ent - Exit
13. Printer quality can be set for Draft Quality or Near Letter
Quality. If required, change printer quality by pressing F1.
Printer pitch can be set for 10, 12 or 17. If required, change
printer pitch by pressing F2.
14. Press Enter to accept selection and exit.
F1: Select Printer
Any Key - Exit
15. Press F3 to activate the Select Print Form screen.

Select Print Form
F 1 - Print Data in Rows
F1 - Form
Ent - Exit
16. Print form can be set to print data in rows or columns. If

required, change print form by pressing F1. (Examples of print
form are provided on page 15.)
14
LabWave 9000
600066
Rev. 1
Example: Rows
Program Name
Sample ID
Percent Moisture
Percent Solids
1
12345678
91.92%
08.08%
Example: Columns
ID Num
%Moisture
12345678
91.93%
23456789
91.94%
34567890
91.91%
%Solids
08.07%
08.06%
08.09%
Diff Time
15
15
15
Diff Wt.
0.2
0.2
0.2
Dry Time
02:07
01:48
02:11
Example: Data Results Screen

DATA RESULTS
MOISTURE BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
F1-WEIGHTS
X.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F2-GRAPH
SAMPLE ID
F3 - PRN GRAPH
F4 - EXIT
Note: Press F2 for display of graph.

Note: F3 - PRN GRAPH is not available if using an HP Laser Jet or
HP Desk Jet.
Example: Data Results in display graph form
TIME 3.5 MINS.
XX.XXXX
XX.XXXX
XX:XX
LabWave 9000
600066
Rev. 1
W
E
I
G
H
T
15
17. Press Enter to exit to the Select Printer/Balance screen.

F1: Select Printer
Any Key - Exit
18. Press F4 to activate Select External Balance screen.

SELECT BALANCE
1>
2>
3>
4>
Denver Instrument
Sartorius
Mettler
Scientech
Up/Dn Arr - Sel
Ent - Exit
19. Available external balances include Denver Instrument,

Sartorius, Mettler and Scientech. External balances are utilized
only for select methods of operation. If an external balance is to be
utilized, select the proper balance by pressing the Up or Down
key. Refer to External Balance Setup, page 10 for proper
settings of external balances. Press Enter to exit.
F1: Select Printer
Any Key - Exit
20. Press any numeric key to exit the Select Printer/Balance program
and return to the Set System Parameters screen.
F1: Sel Printer/Balance
F2: Utilities
F3: System Info
Any Key - Exit
21. Press F2 to activate the Utilities screen.
16
LabWave 9000
600066
Rev. 1
Utilities
F1:
Set Display Contrast
Any Key - Exit
22. Press F1 to activate the Set Display Contrast screen.
USE UP and DOWN ARROWS

TO ADJUST CONTRAST
F4 to exit
23. Use the up and down arrow keys to adjust screen contrast to
desired level.
24. Press F4 to exit.
Utilities
F1:
Set Display Contrast
Any Key - Exit
25. Press any numeric key to exit.

F1: Sel Printer/Balance
F2: Utilities
F3: System Info
Any Key - Exit
26. Press F3 to activate System Info screen.
LabWave 9000
600066
Rev. 1
17
System Info
F1: System Data
F2: Print Profile Data
F3: Sftw Version
Any Key - Exit
27. Press F1 to activate System Data screen.

System Data
Line Freq
XXHz
S1 = XXXXXXXX
F4 - Exit

System Info
F1: System Data
F3: Sftw Version
Any Key - Exit
29. Press F2 to activate Print Profile Data screen.

Print Profile Data
F1
F2
F3
F4
Profile Data to Prn

Profile Data to PC
Data Results to PC
Select PC Terminator
OFF
OFF
OFF
Any Key - Exit
Note: Profile data is time and weight readings transmitted through

external ports at a rate of once per second. Data can be transmitted
either to a personal computer (serial port) or printer (parallel port).
Based on PC software, select appropriate line terminator.
30. If profile data is desired, choose the method of printing by pressing F1 for printer (on or off) or F2 for a PC (on or off). Press
F3 to transmit all data or % solids results to a PC or to turn this
function off. Press F4 to select PC terminator.
18
LabWave 9000
600066
Rev. 1
Select PC Terminator
F1: Line Feed
F4 - Exit
31. PC line termination is based on the PC software. Press F1 to

toggle to the appropriate method for data line transmission to the
PC Line Feed, Carriage Return, or Carriage Return/Line
Feed. Press F4 to exit.
System Info
F1: System Data
F3: Sftw Version
Any Key - Exit
32. Press F3 to activate Software Version screen.
LabWave 9000
Software Version XXXXXX
Copyright XXXX, XX XX
Any Key - Exit
Note: The software version is used for service purposes only to assist
the technician in determining instrument functions and capabilities.
System Info
F1: System Data
F3: Sftw Version
Any Key - Exit
34. Press any numeric key to exit System Info screen.
LabWave 9000
600066
Rev. 1
19

F1:
F2:
F3:
Sel Printer/Balance
Utilities
System Info
Any Key - Exit
35. Press any numeric key to exit Set System Parameters screen.
SYSTEM SETUP
F1: Set Date/Time
F2: Set System Parameters
F3: Calibrate
F4: Set Password
Any Key - Main Menu
36. Press F3 to activate the Calibrate screen.

CALIBRATE MENU
F1:
F4:
Calibrate Balance
Exit
Wt. 0.0000g
Note: The instrument door must be closed prior to pressing F1 to

activate the Calibrate Balance screen. If the door is open when F1 is
pressed, the following screen will appear for three (3) seconds and
three (3) audible beeps will sound.
CALIBRATE MENU
F1:
F4:
Calibrate Balance
Exit
Door Must be Closed.

Wt. 0.0000g
37. Press F1 to activate the Calibrate Balance screen.
20
LabWave 9000
600066
Rev. 1
CALIBRATE BALANCE
Clear Pan and Press TARE
F4 - Exit
38. Open the instrument door, lift the air shield, and clear the balance pan. Close the instrument door.
39. Press the Tare key.
TARE
<* * *W A I T* * *>
Sending Calibrate Command
Any Key - Abort
Place Calibration weight on

Balance, then press ENTER
50.000g
Any Key - Abort
40. Open the instrument door, lift the air shield, and place the calibration weight supplied with the instrument in the starter
accessory kit on the balance pan. Close the instrument door.
<* * *W A I T* * *>
+50.000g
Any Key - Abort

LabWave 9000
600066
Rev. 1
21
Calibration Complete
Remove Calibration Weight
+50.000g
Press Any Key

Note: CEM Corporation recommends that the balance be calibrated
during initial system setup, if the instrument is relocated, if the balance pan is replaced, and as part of a monthly routine maintenance
program.
CALIBRATE MENU
F1:
F4:
Calibrate Balance
Exit
Any Key - Exit

SYSTEM SETUP
F1: Set Date/Time
F3: Calibrate
F4: Set Password
ANY KEY - MAIN MENU
43. Press F4 to activate Set Password screen.
F1:
F2:
F4:
Activate Password
Deactivate Password
Esc
Note: Activation of a password prevents unauthorized entry of programs into the instrument or unauthorized alteration of program
parameters. Once a password is entered and activated, new programs
cannot be entered and program parameters cannot be altered without
entry of the proper password.
22
LabWave 9000
600066
Rev. 1
CAUTION
To avoid being unable to enter new programs or
to alter program parameters, ensure that any
activated password is recorded or documented for
later retrieval.
44. If a password is not desired, press F4 to exit and return to the
System Setup screen. If a password is to be entered, press F1 to
activate the Activate Password screen.
Password Activated
ENT: Accept
F1: Menu
45. Press Enter.
Enter New Password
L/R - Arrow
ENT - Accept
46. Using the numeric keys and the right arrow key, enter the
selected password (8 letters and/or numbers maximum). (Exam
ple: For the password CEM, press 1 four times; press 2 three
times; and press 5 two times.) If an error is made during entry,
use the left and right arrow keys to move cursor to letter or
number to be corrected. Press the applicable numeric key the
appropriate number of times to select the correct letter or num
ber. Note: A space is not permitted as part of a password.
47. Press Enter.
Enter New Password

New Password
F1 - ReEnter
CEM
CEM
ENT - Accept
Note: If password is entered incorrectly or if the password is to be

altered or changed, press F1 to clear the existing password and enter
the selected (new) password.
LabWave 9000
600066
Rev. 1
23
48. Press Enter to accept the password and return to the System
Setup screen.
SYSTEM SETUP
F1: Set Date/Time
F3: Calibrate
F4: Set Password
ANY KEY - MAIN MENU
Note: When the password is entered and accepted, it will be required

prior to system operation.
49. If the password is to be deactivated, press F4 to activate the
Password screen.
Enter Password
L/R - ARROW
F4 - ESC
ENT - ACCEPT
50. Using the numeric keys and the right arrow key (for double letter entry), enter the accepted password.
51. Press Enter.
F1:
F2:
F4:
Activate Password
Deactivate Password
Esc
52. Press F2 to deactivate the password.

Password Deactivated
ENT: Accept
F1: Menu
53. Press Enter to accept deactivation of password.
24
LabWave 9000
600066
Rev. 1
SYSTEM SETUP
F1: Set Date/Time
F3: Calibrate
F4: Set Password
ANY KEY - MAIN MENU
54. Press any numeric key to return to the Main Menu.

MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
55. To verify proper operation of the LabWave 9000, perform the

Standard Solution Test as outlined below.
Standard Solution Test

Note: CEM Corporation recommends that the Standard Solution Test
be performed during system setup and monthly as part of a routine
maintenance program.
CAUTION
Permit the LabWave 9000 to warm up (power
switch on, microwaves not being produced) for at
least 45 minutes prior to operation. If the instrument is switched off for an extended period of
time (weekend, holidays, etc.), ensure that warmup time is permitted prior to use.
56. Press F1 to activate the Quick Dry screen.
NAME
POWER
TIME
F2 - Case
Up/Dn - Arr
000
00:00
F4 - Quit
Ent - Run
F3 - End (Const. Wt)
CAUTION
If the LabWave has not been operated for a
period of one hour, preheat the instrument by
operating it empty for 5 minutes at 100% power
in the Quick Dry program.
LabWave 9000
600066
Rev. 1
25
57. Press the down arrow key to move the cursor to power. Using
the numeric keys, enter 100% power by pressing 1, 0, 0. Press
the down arrow key to move the selector to time. Enter 5
minutes of time by pressing 5, 0, 0.
58. Press Enter.
TIME
XX:XX xx
DRY TIME
05:00
ID POWER
100%
UNDER
-
MOISTURE
F1 - EDIT F2 - DATA
F3 - M/S F4 - EXIT
0 - ID
5 - BAL SP
Wt. X.XXXX g
Note: The flat straight line in the microwave indicator box indicates
that microwaves are not being produced.
59. Press Tare.
TARE
<***WAIT***>
60. Wait for the instrument to zero the weight of the balance pan.
The Quick Dry screen will reappear with a T beside the micro
wave indicator to indicate that the weight has been tared.
T
ID POWER
100%
F1 - EDIT F2 - DATA
F3 - M/S F4 - EXIT
MOISTURE
UNDER
TIME
XX:XX xx
DRY TIME
05:00
0 - ID
5 - BAL SP
Wt. X.XXXXg
61. Press Start.

TIME
XX :XX xx
DRY TIME
0 5 : 0 0
ID POWER
1 0 0 %
MOISTURE
XXX.X X
F3 - M/S
26
STOP
Wt.
X.XXXXg
LabWave 9000
600066
Rev. 1
Note: The flashing wavy line in the microwave indicator box indicates
that microwaves are being produced.
62. Permit the instrument to operate empty with microwaves being
produced for the full 5 minutes to preheat the instrument prior to
operation. At the end of the 5-minute period, five short beeps will
sound, and the Data Results screen will appear.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
* *I N V A L I D* *
SAMPLE ID
F3 - PRN GRAPH
F4 - EXIT

TIME
XX:XX xx
DRY TIME
05:00
ID POWER
100%
MOISTURE
UNDER
F1 - EDIT F2 - DATA
F3 - M/S F4 - EXIT
0 - ID
5 - BAL SP
Wt. X.XXXXg
64. Press F1 to edit parameters for the Saline Solution Test.

NAME
POWER
TIME
F2 - Case
Up/Dn - Arr
000
00:00
F4 - Quit
Ent - Run
65. Using the up and down arrow keys, position the cursor for
entering a program name.
66. Using the numeric keys, enter a procedure name. (Example: For
the name test, press 7 three times; press 2 three times; press
7 two times, press the right arrow key; press 7 three times.
If editing of the name is necessary, press F1 to clear the existing
name or use the left and right arrow keys to position the cur
sor in the proper position and re-enter the desired letter or num
ber or enter a new program name. If desired, upper and lower
case letters can be utilized in the name by pressing F2.)
LabWave 9000
600066
Rev. 1
27
67. When the procedure name has been entered, press the down
arrow key to move the selector to power. Enter 100% power by
pressing 1, 0, 0.
68. Press the down arrow key to move the selector to time. Enter 3
minutes, 30 seconds of time by pressing 3, 3, 0.
69. Press Enter to perform the test procedure.
TIME
XX:XX xx
DRY TIME
03:30
TEST
ID POWER
100%
MOISTURE
UNDER
F1 - EDIT F2 - DATA 0 - ID
F3 - M/S F4 - EXIT 5 - BAL SP
Wt. X.XXXXg
70. Open the instrument door, lift the air shield, and place two glass
fiber sample pads on the balance pan. Close the instrument door.
Press the Tare key.
TARE
<***WAIT***>
71. Wait for the instrument to zero the weight of the balance pan and
sample pads. The Quick Dry screen will reappear with a T
displayed beside the microwave indicator when the tare function
is complete.
TEST
ID POWER
100%
UNDER
T
MOISTURE
TIME
XX:XX xx
DRY TIME
03:30
Wt. X.XXXXg
72. Remove the sample pads from the balance pan. Using a pipette,
apply approximately 3 mL of Standard Solution to the sample
pads. Quickly place the sample pads on the balance pan and position the air shield. Close the instrument door. Press Start.
28
LabWave 9000
600066
Rev. 1
TEST
TIME
XX:XX xx
DRY TIME
03:30
ID POWER
100%
MOISTURE
XX.XX%
F3 - M/S
STOP
Wt. X.XXXXg
Note: The wavy line in the microwave indicator box indicates that
microwaves are being produced.
73. The instrument will record the initial weight of the sample prior
to beginning analysis. As analysis begins, sample weight
decreases as the moisture is removed. During the drying time, the
F3 key may be pressed to alternate between displaying % moisture, % solids or % dry weight. The dry time displayed will begin
counting down. When the drying time of 3 minutes, 30 seconds is
complete, five short beeps will be heard, and the Data Results
screen will appear.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID
F3 - PRN GRAPH
F4 - EXIT
74. Record the moisture and solids data. (If a printer is installed,
data will be printed.) Press F2 to activate a visual graph of data
results on the display. Press F3 to print a graph of data results.
(To print a graph of data results, print graph, Select Print Form,
page 14, must be in the on position.) Press F4 to exit and
return to the Quick Dry screen. Remove the sample pads from the
balance pan.
TIME
XX:XX xx
DRY TIME
03:30
TEST
ID POWER
100%
MOISTURE
UNDER
LabWave 9000
600066
Rev. 1
Wt. X.XXXXg
29
75. Repeat the Standard Solution Test four (4) times beginning with
step 71. Compare the results of the five Standard Solution Tests.
The five solids test results should not vary more than 0.10%. If
results fall outside the required range, repeat the tests to verify
that the proper procedures have been followed. If results are
unsatisfactory, call the CEM Service Department or your local
distributor for assistance.
76. Press F4 to end saline solution test and exit the Quick Dry program.
Are You Sure!

* * * Program Will Be Lost! * * *
F1 - Resume
F4 - Quit
77. Press F4 to return to the Main Menu.
30
LabWave 9000
600066
Rev. 1
IV Operation
General Precautions
CAUTION
Do not operate this instrument if there is any
damage to the instrument cavity, cavity door or
door seal, or the magnetron waveguide assembly.
CAUTION
Do not operate this instrument with any object
placed between the cavity and instrument door.
Do not permit residue to accumulate on the door
sealing surfaces.
CAUTION
Do not tamper with or attempt to defeat the door
safety interlock system.
CAUTION
If the instrument is switched off for an extended
period of time (weekend, holidays, etc.), ensure
that warm-up time is permitted prior to use. Permit the Labwave 9000 to warm up (power switch
on, microwaves not being produced) for at least
45 minutes prior to operation. If the instrument
has not been operated for a period of one hour,
preheat the instrument by operating it empty for
5 minutes at 100% power in the Quick Dry
method.
The LabWave 9000 is designed to measure percent solids and/or moisture of a sample. Following is an overview of the sample analysis procedure:
LabWave 9000
600066
Rev. 1
1.
Program the LabWave 9000 for the appropriate method parameters.
2.
Place two CEM glass fiber sample pads on the balance pan.
3.
Tare the weight of the sample pads.
4.
Remove the sample pads from the balance pan and apply sample
to the pads.
5.
Place the sample pads containing sample on the balance pan.
6.
Press Start.
7.
The LabWave 9000 automatically weighs the sample, controls the

drying process and calculates the results.
31
Sample Analysis
Proper sample preparation and testing are critical to obtaining accuracy and precision. Each sample has a specific characteristic composition; therefore, each sample may require an individual method of
analysis. However, guidelines can be established for analysis of general sample types.
Sample Preparation As with any chemical analysis, a homogeneous sample is critical to obtaining precision and accuracy.
Sample Weight A consistent sample size helps ensure precision and accuracy. Most CEM applications specify a sample size
of 2-5 grams, emphasizing the importance of a homogeneous
sample.
Sample Holders Absorbent pads to which a sample can be
applied are used for most analyses. Glass fiber pads are
recommended because glass fibers do not absorb microwaves.
Other holders include Teflon coated glass fiber mesh, a drying
basket and a thermapad.
Sample Application Most samples should be spread
smoothly, avoiding lumps, peaks or any uneven areas. Sample
spread must be consistent.
Drying Time The drying time is determined by the type of
sample and its microwave absorbency.
Microwave Power The power necessary to dry a sample is
determined by sample composition. A sample should be tested at
the highest possible power without burning or degradation of the
sample.
Sample Preparation
Sample preparation is critical to achieving precise and accurate test
results. The sample should be properly prepared to achieve repeatable
moisture results between duplicate analyses of the same sample. Sample preparation is either a physical or chemical modification of the
sample. Physical modification may be as simple as stirring or shaking
the sample to ensure homogeneity or more complex such as particle
size reduction, dilution or dearation. Chemical modification is the
addition of an enzyme to hydrolyze chemically bound fat. The objective
is to create a homogeneous sample and to improve the correlation of
the test method to standard methods. Some products, such as a beef
emulsion or comminuted poultry, may require no additional preparation. Other materials will require particle size reduction, dilution or
dearation prior to testing. Samples should be kept cool and in sealed
containers to prevent loss of moisture. If repeatable results cannot be
obtained on the same sample, re-blend the sample to improve the
homogeneity and repeat tests. Sample preparation methods include:
1.
32
Mixing of Sample Thoroughly stir or shake sample to

ensure homogeneity.
LabWave 9000
600066
Rev. 1
2.
Particle Size Reduction Many products require particle

size reduction prior to being applied to the glass fiber pad.
Reduction, based on product sample, can be accomplished with
a meat grinder, either an industrial or consumer grade food
processor, a coffee mill or a cheese grater. The meat grinder is
the best choice for all meat products. USDA procedure
specifies three to four passes through a 1/8 or 5/64 blade with
mixing between grinds. A USDA inspector or outside laboratory can make recommendations. An industrial grade food
processor is a good alternative for grinding meat products. A
consumer grade food processor is ideal for grinding frozen
potatoes, breaded products, or dry snack foods such as
cookies, crackers, and chips. A coffee mill can be used to grind
or mix dry snack foods. A cheese grater can be used to grate
small quantities of hard cheese samples or soap.
3.
Dilution Products with a high carbohydrate content are

strong microwave absorbers and have a tendency to burn.
These samples require either a water or salt dilution.
A. Water Dilution A specified amount of sample is diluted
with a specified amount of water and mixed in a blender.
Typical samples include doughs, cheese powders, corn
syrups, dried meat bases and sauces. An external balance
and a blender are required for this procedure.
(1) Interface an external balance with the Moisture/Solids
Analyzer.
(2) Tare the blender cup on the external balance.
(3) Add product sample to the blender cup.
(4) Add water to the product sample in the blender cup.
(5) Blend until a homogeneous mixture is obtained.
(6) Use the diluted sample to perform analysis.
B.
Salt Dilution A specified amount of salt is added to the

product sample prior to analysis. Typical samples include
frozen potatoes and frozen breaded products. This
procedure requires a teflon basket and dry table salt
(sodium chloride).
(1) Line a teflon basket (CEM p.n. 200090) with two
square glass fiber pads.
(2) Place the lined basket and one round glass fiber pad
on the balance of the Moisture/Solids Analyzer. Press
Tare.
(3) Place approximately 8g of salt in the lined basket.
Press Tare.
LabWave 9000
600066
Rev. 1
33
(4) Place the product sample on top of the salt. Press

Start to record the initial weight.
(5) Press Stop.
(6) Thoroughly mix the salt and sample in the basket.
(7) Return the basket to the balance of the Moisture/
Solids Analyzer. Press Start to continue the sample
analysis.
4.
Dearation Frozen dairy and imitation dairy products must

be dearated to remove the excess air in order to provide reproducible test results. This procedure requires a 125 mL
Erlenmeyer flask, a 1 liter beaker, a magnetic stirrer, a 11/2 x
3/8 magnetic stirring bar, and a #5 rubber stopper.
(1) Place 100 mL of sample in a 125 mL Erlenmeyer flask.
(2) Place a 11/2 x 3/8 magnetic stirring bar in the flask. Using
a #5 rubber stopper, loosely cap the flask.
(3) Place flask in a 1 liter beaker containing 250 mL of water
which has been heated to 70C.
(4) Place beaker with flash on a magnetic stirrer. Mix for 5 - 7
minutes.
(5) Cool sample to ambient temperature and thoroughly mix
sample prior to testing.
5.
Enzymatic Hydrolysis The fat in processed cheese and

dairy products is often tightly bound to the protein. In order to
achieve accurate test results, the fat must be released from the
protein prior to the fat extraction process. This can be accomplished by a protease enzymatic hydrolysis of the sample. Note:
The sample must be in a liquid or pourable state for the
enzymatic hydrolysis to be effective.
(1) Thoroughly mix approximately 100g of sample. Heat sample in a water bath at 60C ( 5C) for five minutes.
(2) Add eight (8) drops of CEM Enzyme (p.n. 302630) and mix
well.
(3) Return sample to water bath for five minutes.
Sample Weight
Sample weight can be very critical to the final test result. As with
most analytical procedures, a consistent sample size helps ensure precision and accuracy. Sample sizes can vary, based on type of sample,
from 1 gram on the low end (high percent solids level) to 10-15 grams
on the high end (very low percent solids level). Test procedures documented by CEM and included in this manual, are for specific sample
34
LabWave 9000
600066
Rev. 1
types and suggested sample size. Sample size should remain within
the weight guidelines. CEM has determined that the suggested sample size results in the most consistent drying and test results. Heavier
sample weights may cause sample degradation or burning, resulting
in high moisture results. Lower sample weights may result in underdrying of the sample.
Sample Holders
Sample holders should be transparent to microwave energy.
CEM Square Sample Pad The square pad is the most commonly
used sample holder. Typically, two (2) pads are used with the sample
sandwiched between the pads. For heat sensitive samples, only one
pad is recommended to minimize heat buildup. For low solids samples,
three or four pads are used for absorption.
CEM Round Sample Pad The round pad is used as a collection
pad for fat extraction and is recommended, but not required, for thermapad applications.
Sample Pads CEM glass fiber pads are designed to provide optimum conditions for rapid, thorough and repeatable drying. CEM
Corporation follows strict specifications in the manufacture of sample pads. Specifications include low moisture content and optimum
absorbency, density, porosity, and strength for microwave drying.
Moisture Content Excessive moisture in sample pads will
cause moisture or solids values to be incorrect. Controlling
the moisture ensures that residual moisture is maintained to
very close tolerances.
Absorbency The pad material must be absorbent enough to
form a wick for a liquid sample and to be a sample holder for
more viscous type samples.
Density The sample medium must have uniform density to
guarantee that the moisture will volatilize rapidly and
evenly, without causing residual heating.
Porosity Correct porosity of the pad material ensures maximum surface area for liquid samples in order to increase
volatilization of moisture. Correct porosity helps prevent
sample degradation or burning.
Strength The tensile strength of the medium has a direct
effect on the ability of the sample pad to withstand the stress
imposed during sample application.
Teflon Coated Glass Fiber Mesh The mesh is used as a holder for
fiber samples or as a spacer between multiple sheets of paper samples.
Drying Basket The basket is made of Teflon coated glass fiber
mesh. It is typically lined with two square pads. It is used to hold
large samples and for salt dilutions.
LabWave 9000
600066
Rev. 1
35
Thermapad
The thermapad is used to remove bound moisture from a sample. It
is a round flexible pad which absorbs microwave energy up to a specific temperature which it will then maintain. Available temperature
levels are 120, 150 and 180C. To use, the thermapad is placed on the
internal balance and preheated for 5 minutes prior to performing the
analysis in order to obtain an accurate tare weight. Then the sample is
applied to a round sample pad rather than the standard square sample pad. Typical applications are pharmaceuticals, powders, dry
organic based products, dehydrated food products and inorganic compounds containing bound water.
Sample Application
The viscosity of the sample plays an important role in determining
how the sample is spread onto the pad for analysis. If a sample is thin,
it can be pipetted onto the pad and can be tested at high power levels.
A thin sample spread over a large area permits moisture to evaporate
rapidly with little residual heat buildup. Glass fiber pads may be
stacked for increased absorbency.
High viscosity samples (samples that do not flow well) require a different technique. If the sample can be easily spread across the glass fiber
pad, no dilution is required. A thick sample will tend to puddle and
form a crust, sometimes trapping volatiles within the bubble. Overheating or burning can also occur on thick samples. If repeatable
results cannot be obtained by spreading the sample, a dilution may be
necessary. The sample must be soluble in the diluting agent, and the
diluting agent must be a microwave absorber.
To generate the appropriate amount of heat and achieve optimum
moisture results, different types of samples must be spread to different thicknesses over different areas of the glass fiber sample pad. As a
general guideline, the sample will generate heat in direct proportion
to the thickness of the sample layer on the pad. A sample spread too
thickly can cause sample burning; a sample spread too thinly can
cause insufficient drying. The prepared sample should be applied to a
glass fiber sample pad. Once the sample is properly applied to the
sample pad, it should be covered with a second glass fiber pad to
ensure heat retention and to eliminate splattering.
Liquid samples should be pipetted onto the pad. Solids samples should
be spread onto a pad placed on the edge of a clean, flat surface, such
as a countertop. The spatula should be held level with the pad when
spreading the sample to ensure a smooth, uniform application of sample to the pad surface.
If the sample is an organic solvent-based liquid, special handling is
required. Equipment and method modification may be required. CEM
Corporation recommends that the LabWave 9000 High Volatiles
Instrument be used when analyzing this type of sample.
Non-polar organic solvents do not absorb microwave energy; therefore,
samples containing this type of solvent will not dry unless they are
36
LabWave 9000
600066
Rev. 1
mixed with a diluent which absorbs microwave energy and has a

higher boiling point than the non-polar solvent.
If the sample is a polar organic solvent-based liquid, samples will
absorb microwave energy and dry as readily as a water-based liquid. If
the organic solvent is an alcohol, a ketone, or an ester, samples should
be tested with water-based techniques.
Some base resins are microwave absorbers. Polyester is a known base
resin that is an absorber of microwaves. Titanium dioxide and calcium
carbonate have also been found to be microwave absorbent. If these
materials are present in a sample, usually enough heat is generated to
remove most high boiling non-polar solvents and any other volatiles.
Oils become very hot when placed in the microwave field. Some metal
based samples can be tested. If carbon black is present in a sample, it
will heat very quickly and possibly burn even at low power levels.
It is recommended that CEM Corporation or a local distributor be consulted prior to testing any solvent based sample.
General Sample Application Technique
If the sample is in a paste, semi-solid, or crumb form or a raw or skeletal meat product such as fresh pork, ground beef, or chicken, place
the sample on the end of a spatula and spread it across one end of the
pad. Then spread the sample to a uniform thickness covering approximately 90% of the pad surface area.
LabWave 9000
600066
Rev. 1
Spread Thin Layer Across 90% of Pad
37
If the sample contains bound water such as an all-meat emulsion,

cooked all-meat sausage, semi-dry sausage, or ham, place the sample
on the end of the spatula and apply the sample to the middle of the
pad. Then spread the sample around the pad in a circle, covering
approximately 65% of the pad surface area to generate thermal heat.
Spread Layer Over 65% of Pad
If the sample is cooked sausage with extenders, place the sample on

the end of the spatula and apply the sample to the middle of the pad.
Then spread the sample in a small circle, covering approximately fifty
percent of the pad surface area.
38
Spread Layer Over 50% of Pad
LabWave 9000
600066
Rev. 1
If the sample is a water-based liquid, use a pipette to dispense the

sample onto the pad(s). Sample size should be 2-5 grams, based on
solid content of the sample 2-3 grams for high solids samples, 4-5
grams for samples containing less than 15 percent solids. Samples
containing less than two percent solids may require as much as 10
grams for analysis. Large quantity samples should be pipetted onto
the pads in a thin even layer. Additional glass fiber pads may be used
for increased absorbency. A sufficient number of pads should be used
to ensure that liquid samples do not drip onto the floor of the instrument cavity.
Puddle, Spread with Pipette and Cover
LabWave 9000
600066
Rev. 1
Puddle and Cover
39
Swirl or Zig-Zag Pattern, No Cover
Standard application for heat-sensitive liquids

swirl or zig-zag liquid on glass fiber sample pad
Dot Pattern, No Cover

8 Other
40
LabWave 9000
600066
Rev. 1
Drying Time and Microwave Power

Drying time and microwave power should be appropriate to the sample. Most water-based samples should achieve constant weight in 4-6
minutes. The power level regulates the rate of drying. If the power
level is too low, the analysis will require more time than necessary. If
the power level is too high, the sample may splatter and/or burn. If a
sample contains a strong microwave absorber such as carbohydrates,
the power level will likely have to be adjusted to prevent browning or
burning of the sample. To optimize correlations with the standard reference method, a slight increase or decrease in power may be required.
In most cases, a 10 percent power change will be sufficient. When
developing an analysis method for a new sample, begin testing at 50
percent power and increase or decrease power in 10 percent increments until the optimum power level is determined. Drying time may
have to be increased to compensate for reduced power.
During the initial testing of a new sample, the weight display should
be monitored to ensure that the sample does not ignite and that a
stable weight reading is displayed. Sharp declines in weight indicate
excessive sample heating. If ignition occurs, the weight reading will
fluctuate rapidly.
If the weight does not stabilize in the set time period, either the sample has not reached a constant weight and is not dry or solids degradation is present. If no degradation is noted, additional drying time
should be allowed.
Samples that are strong absorbers of microwave energy should be
diluted or tested at reduced power levels. These products usually contain simple carbohydrates or tightly held moisture that will not readily escape, causing overheating and/or burning and non-reproducible
results. These samples should be tested at a low power. Examples of
heat sensitive samples include powders, paper fibers, candy and black
liquor.
Note: Due to the variance in design factors, results from the LabWave 9000 may not precisely match results from the CEM AVC-80. To
match results more closely, adjustment in power and/or time parameters may be required. If questions arise, contact the CEM Applications Department at (800) 726-3331.
LabWave 9000
600066
Rev. 1
41
Analysis Programs and Options

The analysis program and/or option is selected based on sample type.
Standard The instrument performs a moisture/solids determination.
Modified The fat is extracted from one sample while another sample is dried for moisture analysis, permitting analysis of fat content of
samples in which initial drying may bind the fat molecules.
Dilution The sample is diluted, and a dilution factor is used for the
diluted sample result; therefore, an accurate moisture/solids value for
the undiluted sample is obtained. An interfaced external balance is
required. The dilution program should be used with samples that burn
easily, viscous samples or samples which dry unevenly.
Syringe Weigh Syringe Weigh is utilized when the moisture/solids
instrument cannot accurately record the initial sample weight due to
rapid evaporation. The rapid evaporation can be caused by the sample
being warmer than room temperature or containing a solvent that
evaporates quickly. The instrument internal balance or an interfaced
external balance can be used to calculate the weight of the syringe.
Total Suspended Solids (TSS) A filter is utilized for samples with
low solids concentration. The instrument dries and weighs the solids
obtained on a tared filter from the filtration of a known volume of
sample which is manually entered into the system.
Total Volatile Suspended Solids (TVSS) The moisture/solids
instrument performs a standard analysis on the sample. The dried
sample is then transferreed to an ashing furnace. The ashed sample is
returned to the moisture/solids instrument for weighing of the ashed
sample. Total Suspended Solids and Total Volatile Suspended Solids
are calculated.
% Ash/Volatile Solids The moisture/solids instrument performs a
standard solids analysis on the sample. The dried sample is then
transferred to an ashing furnace. Once the sample is ashed, it is
returned to the moisture/solids instrument and reweighed.
Alternate This program permits drying of one sample in the moisture/solids instrument while another sample is being ashed in the ashing furnace or is being processed in the fat extractor.
Bias Identification
Most samples can be analyzed for percent moisture content with a
CEM drying method, and results will compare precisely with the standard test method. Occasionally, however, all volatiles in a particular
sample cannot be removed with microwave power. Different spread
techniques can be used to eliminate the need for a moisture bias in
most samples. Sometimes browning of the sample in the same manner
as in the air oven will also produce test results comparable to the standard test.
42
LabWave 9000
600066
Rev. 1
If microwave moisture test results are repeatable, but not comparable

to the standard test results, a bias can be identified. With most samples, the bias will amount to only a few tenths of a percent. To determine a moisture bias, prepare a sample for testing, ensuring that the
sample is homogeneous. Test this sample by both a standard method
and the CEM microwave method. Perform at least ten tests by each
method to check repeatability, then figure an average of the ten
results. Subtract the average of the microwave test results from the
average of the standard test results. Enter the resulting number
(moisture bias) into the CEM moisture/solids instrument. Corrected
moisture test results will be displayed and printed. Only positive numbers can be entered as a moisture bias. If the difference in the average
test results is a negative number, the power level should be reduced
and the tests should be repeated.
Some meat and poultry products, whether raw or cooked, show a fat
bias when analyzed with the CEM instruments. Less fat is extracted
by a short solvent extraction than by the longer ether extraction of the
traditional Soxhlet technique. The bias will be a constant for a given
product and should be considered when generating data.
Cooked sausage (i.e. wieners, bolognas, etc. with extenders) and other
cooked products tend to bind fat in the carbohydrate/protein structure
of the cooked product and will generally yield a lower fat value when
extracted in the CEM instrument than when extracted with the Soxhlet.
For proper determination and use of biases, results from the CEM
instrument should be compared with the results from traditional
long or standard methods used by USDA laboratories for compliance
testing. Standard methods consist of an air oven (four hours, 125C)
for moisture and Soxhlet (four hour ether extraction) for fat. USDA
recommends correlation of rapid fat and moisture methods with these
long methods.
USDA Processed Products Inspection Division encourages the use of
rapid methods for fat and moisture analysis to assist in better process
control and compliance. USDA recommends periodic back-up analysis
(one in every 10 - 20 analyses) by standard long methods when rapid
methods are used in approved Total and Partial QC (TQC/PQC) Programs. Backup checks can be performed less frequently as laboratories gain confidence in the established biases. CEM Corporation
also recommends a Quality Assurance Program for establishing and
maintaining biases and to ensure USDA compliance.
Prior to establishing a fat bias for the Fat Analysis System, a laboratory should be confident of obtaining the best possible results for
moisture, since precision of the fat results will depend on the moisture
results. Moisture results should have repeatability between duplicate
analyses of the same sample and a mean or average moisture values
that are close to the values being generated on the same samples by
standard oven. To obtain the best possible results for moisture, and
thus for fat, there are three factors to consider: 1) sample preparation,
2) sample application technique and 3) power and time parameters.
LabWave 9000
600066
Rev. 1
43
After establishing moisture repeatability and achieving moisture

results as close to standard long methods as possible, use the following procedure to identify fat biases for different product categories.
1. Select three or more samples (approximately two pounds each)
from different lots of the same product.
2. Prepare each sample according to standard procedures (3 - 4
passes through a 5/64 blade, with mixing between grinds, or
equivalent).
3. Divide each ground sample in half and package and label subsamples in two separate, air-tight containers.
4. Analyze one set of the sub-samples (from step 3) in duplicate by
standard long methods oven for moisture, Soxhlet for fat. If
facilities and/or personnel are not available for these tests, use
an independent laboratory. Request raw data (individual tests)
from the laboratory, not the mean or average value.
5. After obtaining the results from the standard long methods,
analyze the other set of subsamples in the LabWave 9000 for
moisture only. Adjust power and spread technique until accept
able moisture repeatability is achieved.
6. After obtaining acceptable moisture repeatability, use the Fat
Analysis System and perform 3 - 5 moisture and fat analyses
for each sample. As with moisture, fat results should be repeat
able.
To obtain optimum fat results, use a sufficient redry time. Two minutes is typical, although some samples may require more time. The
sample weight should be stable (<0.2 mg weight change in the last five
seconds). An insufficient redry time will yield artificially low fat
results since the true dry, extracted weight will not be reached.
7. Subtract values obtained from the LabWave 9000 from Soxhlet
values. Average the differences to identify the average bias for
a specific product or product group.
Sample
Average Soxhlet fat
- Average CEM fat

= Bias
(A + B + C)/3 = Average Fat Bias
8. The bias should be relatively less than 2.0% and must be added
to the fat results from the LabWave 9000 to produce results that
correlate closely with official methods. Repeat this process on a
regular basis to confirm that the bias is consistent. Raw meats
and blends will produce smaller biases than cooked products
with extenders.
44
LabWave 9000
600066
Rev. 1
Determining Ash/COH for Processed Meats

For samples that contain salt, sugar, spice, cure or other added components,
ash/carbohydrate (COH) values must be determined by analysis. For purposes of calculating the protein by difference, the specific amount of each
component (salt, spice, bone, etc.) is not important, only the total amount.
To determine ash/COH values for finished products or blends with sugar,
salt, spice, etc., use the following procedure:
1. Collect and prepare three (3) samples from different lots of the same
product. Store the samples in airtight containers until tested.
2. Analyze the 3 samples in duplicate for fat and moisture in the
LabWave 9000 and Fat Analysis System and for protein using long
methods (Kjeldahl). If necessary, an independent laboratory can
provide this analysis.
3. Average the results of the duplicate analyses for each sample, then
total the % Protein + % Fat + % Moisture for each sample.
4. Subtract the sum from 100% to get an Ash/Carbohydrate factor. For
example, if the composition of a sample is:
Moisture
Fat
Protein
Total
52.54%
28.36%
11.25%
92.15%
Ash/COH = 100% - 92.2%

Ash/COH = 7.85%
5. Calculate an average of the the ash/COH values for each of the 3
samples and program that factor into the LabWave 9000.
Check samples periodically to verify the ash/COH values. Variations in the
amount of added constituents (salt, sugar, spice, extenders, etc.) can cause
the ash/COH factor to vary.
7.85%
11.25%
Moisture
Fat
52.54%
Protein
Ash/COH
28.36%
LabWave 9000
600066
Rev. 1
45
Ash Content Of Meats

The following values should be helpful in establishing ash/carbohydrate factors for raw meats. Since the carbohydrate values for these
meats are so low, the ash alone is usually adequate. Obviously, for
meats with added salt, spice, cure, sugars, soy, etc., the ash/COH values will vary. Refer to page 45 for the procedure for determining processed meat ash/carbohydrate factors.
The following values are estimates since composition may vary due to
individual differences in the the meat sources, seasonal variations,
processing, etc.
Moisture
Protein
Fat
Ash
Green Beef Material

Bull Meat
Ship Boneless Beef
Regular Boneless Beef
Boneless Beef Pad. for Ck.
Boneless Bull Chux
Boneless Chux C. & C.
Boneless Ship Chux
Shank Meat
Clods
Sirloin Butts
Star Beef (Dry Saus.)
Spcl. Beef
Spcl. Bf. Trmgs.
Reg. Bf. Trmgs.
Bnls. Plates
Bnls. Flanks
Bnls. Plate Trmgs.
Beef Fat
Beef Fat from Old Cow
Brains
Cheeks
Diaphragm Meat
Gullet Meat
Head Meat
Hearts
Lips
Lungs
Tongues
Tongue Trmgs.
Tripe, Cooked
46
67.90
64.00
70.00
65.70
72.50
70.00
62.10
72.60
72.30
66.60
70.00
69.00
52.50
64.60
43.60
41.90
40.30
11.80
22.20
77.40
70.00
65.79
73.20
68.45
72.40
59.40
78.00
64.25
69.40
81.90
19.40
16.20
20.00
18.30
19.80
19.30
17.55
19.80
20.18
19.40
20.00
19.00
14.60
19.40
13.40
13.10
12.70
5.10
5.60
11.40
19.30
18.21
16.80
18.96
16.55
17.07
18.80
17.75
19.17
15.50
11.70
19.00
9.00
15.00
7.2
9.70
19.35
6.60
6.90
13.00
9.00
11.00
31.90
15.00
42.00
44.00
46.00
82.90
71.80
9.80
9.70
15.60
9.00
11.59
9.80
22.53
2.20
17.00
10.43
2.10
1.00
.80
1.00
1.00
.50
1.00
1.00
1.00
.62
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
.20
.40
1.40
1.00
.50
1.00
1.00
1.25
1.00
1.00
1.00
1.00
.50
LabWave 9000
600066
Rev. 1
Ash Content Of Meats (Continued)

Moisture
Protein
Fat
16.90
17.70
18.40
15.00
17.10
12.70
13.80
12.70
16.60
16.10
13.20
11.30
7.00
9.70
14.40
15.90
22.50
18.00
18.90
17.60
15.00
2.60
5.70
1.30
3.10
1.30
22.80
11.80
15.75
15.75
17.00
16.20
15.25
9.25
17.50
18.73
23.50
17.70
14.61
16.43
13.85
16.25
8.65
21.00
17.50
14.20
20.00
20.10
40.90
36.00
41.00
22.50
25.00
38.50
46.60
67.50
55.00
33.10
25.00
8.00
7.80
15.00
19.00
20.00
84.00
71.70
92.20
84.90
92.9
28.50
9.80
16.00
16.00
13.65
8.00
25.00
57.37
7.00
11.27
3.85
1.80
32.14
23.57
13.50
24.50
64.85
Ash
Green Pork Material

Spiced Ham Trmgs.
Lean Ham Trmgs.
Hamette
Corned Pk. Shldr. Mt.
A Shoulder Trmgs.
B Shoulder Trmgs.
B & F Shldrs. 1/2 Fat
B & F Shldrs. 1 Fat
Lean Picnic Trmgs.
C.T. Butts
Boneless Boston Butts
Bnls. Packer Side Mt. 124-55
Skd. Belly Mt.
Reg. Pk. Trmgs.
Neck Bone Trmgs.
Spec. Lean Trim.
A Pk. Trmgs.
Blade Meat
Picnic Shank Meat
Ham Shank Meat
Pk. Trmgs. Pad for Ck.
Neck Fat Skin Off
Skd. Jowls
Belly Fat Skin Off
Ham Fat Skin Off
Back Fat Skin Off
Gelatin Skins 10% Fat
Brains
Cheeks
Cheeks Pad. for Ck.
Diaphragm Meat
Gullet Mt.
Head Mt.
Head Skins
Hearts
Jaw Mt
Livers
Melts
Snouts
Snout Mt.
Stomachs
Tongues
Tongue Trmgs.
LabWave 9000
600066
Rev. 1
61.10
63.80
66.40
61.80
61.80
45.40
49.20
45.30
59.90
57.90
47.30
41.10
24.80
34.30
51.50
58.10
68.80
73.10
65.30
62.60
64.00
13.00
22.10
6.40
11.80
5.70
47.50
77.40
67.25
67.25
68.20
74.60
58.00
32.40
74.40
69.00
69.80
79.30
52.25
59.00
70.25
58.35
26.50
1.00
1.00
1.00
3.20
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
.70
1.00
1.00
1.00
.60
1.10
.80
.80
1.00
.40
.50
.10
.20
.10
1.20
1.00
1.00
1.00
1.15
1.20
1.75
.98
1.10
1.00
2.85
1.20
1.00
1.00
1.90
1.00
.10
47
Ash Content Of Meats (Continued)

Moisture
Protein
Fat
Ash
18.10
9.20
12.80
14.50
6.00
5.00
8.00
2.30
1.80
38.00
7.70
19.00
43.00
84.50
78.10
85.00
46.50
76.00
74.00
51.00
6.50
1.50
4.00
2.70
2.50
0.00
0.00
0.00
72.25
74.50
76.50
71.70
87.30
19.80
17.21
15.20
19.67
9.00
6.95
7.21
7.30
7.63
3.20
1.00
1.00
1.25
1.00
.50
69.40
67.90
75.00
67.20
90.05
19.17
18.84
15.40
14.90
8.07
10.43
12.26
9.10
14.40
1.40
1.00
1.00
.50
3.50
.48
Cured Pork Material

Clear Fat
DS Fat Backs
Smoked Pk. Skins
Bacon Ends and Pcs.
High Fat Cracklings
Med. Fat Cracklings
Low Fat Cracklings
Green Calf Material
Reg. Bnls. Veal
Cheeks
Gullet Mt.
Hearts
Tripe
Green Sheep Material
Reg. Boneless Mutton
Cheeks
Gullett Mt.
Hearts
Tripe
Methods Development
The CEM Applications Laboratory has developed procedures for various types of samples. These procedures include parameters (program,
power, time, sample preparation, etc.) needed to program the LabWave 9000 and analyze samples in the LabWave 9000 and Fat Analysis System. CEM sample analysis procedures can be requested from
the CEM Applications Laboratory.
If a procedure for a particular sample is not included in the applications list, review all information in this chapter relating to sample
preparation, sample spread technique, time and power parameters,
redry time, and bias identification to develop an application method. If
necessary, call the CEM Applications Laboratory for additional information and assistance (800) 726-3331.
48
1.
Begin testing at 50% power.
2.
If the sample has high solids content (approximately 75% solids),

begin testing with a low sample weight (1 - 2 grams).
3.
Use Mode 2 (AVC-80) or Quick Dry (LabWave 9000) for testing.
LabWave 9000
600066
Rev. 1
LabWave 9000
600066
Rev. 1
4.
Observe weight change closely. The weight should steadily

decline. If weight is erratic (1 mg), the test should be stopped
because the sample is probably burning.
5.
Record final weight result and time. If drying time is excessive,

power should be increased sufficiently to reduce drying time, but
not cause burning of sample solids.
6.
Perform multiple sample tests with determined power and time.

Results should be within 0.2%.
7.
For fat content results, the re-dry power setting should be no

higher than the power setting used to remove moisture.
49
Sample Type
Sample
Preparation
Sample
Spread
Program
Size
Technique
(Grams)
Dry
Dry
%
Time
Power (Min.)
Comments
Food Products
Apple, Dried Chunks
3A
Dilution
30 - 50
Apple Pulp
Asparagus
Bacon Bits
Bacon Bits with Soybean
Bacon, Crumbled
Barbecue Sauce
Batter, Wafer Cookie
Beans, Refried
Beef Concentrate
Beef, Ground
Beef Jerky
Beets, Sugar
Bologna, All-Meat
Brownie, Fudge
Butter, Salted
Butter, Unsalted
Cabbage
Cake, Chocolate with Cream
Filling and Chocolate Icing
Cake, Fudge, Fat Free
Cake Mix
Candy, Caramel
3A
2
2
2
2
1
1
1
3A
2
2
2
2
3A
1
1
3A
3A
3
3
3
3
3
2.5 - 3
2.5
4.5
3
3.5 - 4.5
3.5 - 4.5
4
3.5 - 4.5
3
3-4
3-4
5
4.5
1
3
3
3
3
4
1
2
6
2
3
3
3
1
1
1
4
1
Dilution
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Dilution
Standard
Standard
Standard
Standard
Dilution
Standard
Standard
Dilution
Dilution
70 - 80
70 - 80
65
65
65
50 - 70
40 - 60
60 - 80
30 - 50
80 - 100
70 - 90
70 - 80
60 - 80
40 - 60
70 - 100
70 - 100
100
50 - 70
10
8
10
7
7
6-7
7
3.5
8
4-5
3-5
14
4-5
6
3-4
5-6
5
6
3A
3
3A
3.5
3
3
1
1
6
Dilution
Dilution
Dilution
45 - 65
65
50 - 70
7
8
6
Candy, Licorice
3A
Dilution
50 - 70
Candy, Marzipan (Ground

almond and sugar)
Cardamom
Cheese, American
3A
Dilution
50 - 70
2
2
2.5
4
1
8
Standard
Standard
80 - 100
55 - 65
12
4
Cheese, Cheddar
4.5
Standard
60 - 80
Cheese, Mozzarella
Standard
60 - 80
4.5
Cheese, Muenster
3.5
Standard
40 - 50
Cheese, Parmesan
Standard
40 - 60
4.5
Cheese, Paste
Cheese Puffs
1
2
3
3.5 - 4
8
1
Standard
Standard
40 - 60
50 - 60
3
6
Dilute 25g 1:3 with water
Some browning is normal

Slight browning may occur

Blend sample prior to dilution with water
Dilute 50g 1:1.5 with water, blend
Dilute 1:1 with water
Freeze sample for size reduction, Dilute 25g
1:2 with water
1:2 with water
1:2 with water
Use G-12 Thermapad
Use cheese grater, place sample in center of
pad with all particles touching
50
Sample Type
Sample
Preparation
Sample
Spread
Program
Size
Technique
(Grams)
2
8
Standard
Cheese, Romano
Cheese Sauce
Cheese, Soft and Processed
5
5
4
2.5 - 3.5
1
2
Cherries
Chicken, Mechan. Deboned
Chili Sauce
Cilantro
Cinnamon
Coconut, Shredded
Cookie Mix
Cookies, Brown Sugar with
Cream Filling and Raisins
Cookies, Fig Filled, Non-Fat
Cookies, Sugar
Corn
Corn Chips
Chocolate
3A
2
1
4
1
3
1
3
3A
4
3.5 - 4.5
3
2.5
2.5
2.5
3
3
3A
2
1
2
2
3.5
3.5 - 4
4.5
3.5 - 4
3-4
1
1
3
1
1
3
3.5
3.5
1
2
2
1
1
1
1
1
1
2
2
3B
1
1
3
1
1
2
3.5 - 4
2
3
2.5
2
3
3
3.5
3
2-3
4
3
3
2
3
3
Chocolate Syrup
Cocoa Powder
Cottage Cheese
Crackers, Cheese
Crackers, Wheat
Cream
Cream, Half & Half
Cream, Heavy
Cream Cheese
Creamer, Non-Dairy
Creamer, Low-Fat Non-Dairy
Crust, Pie
Crust, Pie, Frozen
Crust, Pizza, Precooked
Dip, French Onion
Dog Food, Dry
Doughnut
Dressing, Caesar
Dressing, Catalina
1
1
1
1
1
4
4
1
4
4
1
2
8
1
2
1
1
1
Modified
Dilution
or
Modified
Dilution
Standard
Standard
Standard
Standard
Standard
Dilution
Dilution
Dry
Dry
Comments
%
Time
Power (Min.)
40 - 60
4.5
50
4.5
40 - 60
4.5
30 - 50
80 - 100
80
40 - 60
40 - 60
15 - 30
70
50 - 70
6
5-6
5
8
10
10
8
6
Dilution
Standard
Standard
Standard
Standard
40 - 70
40 - 50
55 - 95
50 - 60
7
7
4.5
6
Standard
Standard
80
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Dilution
Modified
Standard
Dilution
Standard
Standard
80 - 100
55
30
80
60 - 80
60 - 80
40 - 60
80
100
40
20 - 40
50 - 70
50 - 70
50 - 70
85
100
60
4
7
4
5
5
5
4.5
4
5
4.5
4.5
7
5
10
10
4.5
5

Slight browning will occur
Separate sample, place in thin layer on pad
Dilute 1:1 with water

Dilute 50g 1:2 with water, blend
Fat content only, no microwave drying,

external balance required
Use 3 square pads
Use 3 square pads, fat content only, no
microwave drying, external balance
required
Use 3 square pads
Use drying basket lined with 2 pads
Dilute 1:1.5 with water
51
Dressing, French
Dressing, Guacamole
Sample Type
1
1
Sample
Preparation
3
1
Standard
4
1
Standard
Sample
Spread
Program
Size
Technique
(Grams)
3
1
Standard
3
4
Standard
2.5
1
Standard
2.5
4
Standard
3
4
Standard
3
1
Standard
Dressing, Honey Sauce

Dressing, Italian
Dressing, Ranch
Dressing, 1000 Island
Eggs, Liquid
Eggs, Powdered
1
1
1
1
1
1
Egg Yolk, with Salt

Egg Yolk, with Sugar
Egg Whites
Eggs, Whole
Fat, Chicken
Fish, Cod
Fish, Haddock
Fish, Pollock
Fish, Surimi
Fish Stick, Breaded
Flavorings, Meat
1
1
1
1
1
2
2
2
2
2
3
3
2
3 - 3.5
2.5 - 3
2
3.5
3.5
3.5
3.5 - 4.5
4
2
2
2
2
2
6
1
1
1
1
1
4
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Dilution
1
3A
3A
1
2
2
1
4
3A
2
1
2
1
1
1
3A
1
1
1
1
1
3
2.5
3
2.5
4
4
2
3.5
3
4
3
4
3-4
3-4
3.5
3
3
3
3
2.5 - 3
2.5 - 3.5
1
6
4
1
2
3
4
4
1
1
1
1
1
1
4
7
1
1
1
1
1
Dilution
Dilution
Dilution
Standard
Standard
Standard
Standard
Modified
Dilution
Standard
Standard
Standard
Standard
Standard
Standard
Dilution
Standard
Modified
Standard
Standard
Standard
Frosting, Cream Cheese

Fructose
Fudge Sauce, Hot
Grits, Corn
Ham, Chopped
Ham, Italian
Ice Cream, Mixes
Ice Cream, Finished Product
Jelly, Strawberry
Knockwurst
Lecithin
Lung, Beef
Margarine, Salted
Margarine, Unsalted
Marinade, Beef Based
Marshmallow
Mayonnaise
Mayonnaise, Low-Fat
Meal, Meat, Poultry, Feather
Meal, Fish
Meat, Canned
100
3.5
80
4
Dry
Dry
Comments
%
Time
Power (Min.)
80
5
100
3
90
5
60
5
100
4
70 - 90
10
Sample must be refrigerated, slight
browning may occur
100
5
Sample must be refrigerated
40
8
100
5
100
4
30 - 50
3
70
4.5
55
4.5
70
4.5
90 - 100 5 - 6
90
4
100
10
Dilute 25g 2:1 with water, slightly
discolored after testing
60 - 80
5
20 - 40
10
35 - 55
6
Dilute 25g 1:1 with water, shake
60 - 80
10
70
4.5
90
4.5
60
4.5
45
5
30 - 50
6
70
5
70 - 90
4
100
5
70 - 100 3 - 4
70 - 100 5 - 6
70
5
40 - 60
4
100
2
100
2
90
10
Thermapad required
75
5
90 - 100 5 - 6 Moisture only, slight browning may occur
52
Milk, Sweetened Condensed

Milk
Molasses
Sample Type
Mushrooms
Noodles, Fried
Onion
Onion Rings, Breaded
Orange Peel
Oregano, Ground
Pancake Mix
Peanut Butter
Peanuts, Raw
Peanuts, Raw Blanched
Pepper, Black, Ground
Pepperoni
Pepper Sauce
Pet Food, Canned
Pie Filling, Cherry, less than
38% solids
Pie Filling, Strawberry
Pimiento Cheese Spread
Pizza Sauce (approx. 15%
solids)
Pork, Fresh
Potato Chips
Potatoes, French Fried
Potted Meat
Protein, Hydrolysate from
Chicken Byproducts (approx.
32% solids)
Protein, Texturized
Vegetable
Pudding, Banana
Pudding, Chocolate
Pudding, Vanilla
Puddings, Finished Product
Puddings, Raw Product
Rice, Precooked
Sausage, All-Meat (Cooked)
Sausage, Fresh
Sausage, Semi-Dry
1
1
3A
Sample
Preparation
2
3
2
2
3B
1
3
1
2
2
3.5
5
Standard
100
4
3.5 - 4.5
2
Standard 80 - 100
4
2.5
6
Dilution
40 - 60
4
Sample
Spread
Program
Dry
Dry
Size
Technique
%
Time
(Grams)
Power (Min.)
3
3
Standard 70 - 80
8
4
4
Dilution
80
6
2
3
Standard 20 - 40
5
2.5 - 3.5
1
Standard 40 - 60
8
4
Standard 60 - 80
7
2
1
1 or 2
1
2.5
3
2.5 - 3
3-5
4
2.5
3
2.5
2.5 - 3.5
1.5
1
1
1
1
1
1
4
5
1
1
Standard
Dilution
Standard
Standard
Standard
Standard
Standard
Standard
Standard
Standard
100
55
40 - 55
50
35
100
80
50 - 70
90 - 100
15 - 25
10
6
7
7
7
10
5
2.5
5-7
5
1
1
1
2.5
3.5
3
4
1
1
Standard
Modified
Standard
15 - 25
70
80 - 100
10
4
2.5
2
2
3B
1
1
4
3.5 - 4
4
3
1.5
1
1
basket
1
1
Standard
Standard
Standard
Standard
Standard
90
50 - 60
50 - 80
95
100
5
6
6-7
6
3
Standard
90
4.5
1
1
1
1
1
2
2
2
2
3.5
2
2
2.5 - 3.5
2.5 - 3
4
3.5 - 4.5
4
3.5
1
1
1
1
1
1
2
1
2
Standard
Standard
Standard
Modified
Standard
Standard
Standard
Standard
Standard
30 - 50
40 - 60
30 - 50
40 - 60
30 - 35
50 - 80
60 - 80
80 - 100
90
5
4
5
4-5
6
6-7
4-5
5
5

Comments
Dilute 25g 1:1.5 with water

Place sample on 1 pad in petri dish
Dilute 4g with 8g salt, use drying basket
lined with 2 pads
Use G-12 thermapad
Dilute with water
Use G-12 thermapad
Slight browning is normal

Use approximately 8g of salt
Do not cover sample with pad
53
Scallops
Silage, Dry
Silage, Wet
Sample Type
Sausage, with Additives
(Cooked)
Sorbitol, Liquid
Sour Cream
Soy Sauce
Supplement, Geriatric
Supplement, Infant
Syrup, Cane
Syrup, Corn
Tea, Instant
Tea , Liquid (Final, Intermediate and Fill Product)
Tea, Slurry (Final, Intermediate and Fill Product)
Tea, Waste Product
Taco Shells, Hard
Taco Shells, Soft
Tartar Sauce
Toast
Tomato Paste, Bulk, approx.
33% solids
Tomato Paste, Canned,
approx. 26% solids
Tortilla Chips
Yeast (70% to 90% water)
Yeast, Dry
Yogurt, Cherry
Yogurt, Grape
Yogurt, Plain (no fruit)
Yogurt, Vanilla
Wiener, All-Meat
Wiener, Turkey
Wiener, with Additives
Whey, Liquid
Whipped Topping, Non-Dairy
(M/S)
Whipped Topping, Non-Dairy
(M/F)
Worcestershire Sauce
2
1
1
Sample
Preparation
2
5
1
Standard
70
4.5
1
Standard 80 - 100
10
3
1
Standard 80 - 100
10
Sample
Spread
Program
Dry
Dry
Comments
Size
Technique
%
Time
(Grams)
Power (Min.)
3.5 - 4.5
3
Standard 30 - 50
4 - 5 Significant browning will occur
3A
1
1
1
1
3A
3A
1
1
3
3
2.5
4
4
2.5
2.5
2
3.5
6
1
5
5
5
6
6
1
5
Dilution
Standard
Standard
Standard
Standard
Dilution
Dilution
Standard
Standard
40 - 50
100
50 - 70
60 - 80
60 - 80
25 - 45
50 - 70
100
90 - 100
6
4
2.5
4.5
4.5
6
6
10
4.5
3.5
Standard
90 - 100
4.5
1
2
2
1
3
3A
3.5
4.5
3.5
3
3-4
3.5
2
1
4
1
1
Standard
Standard
Standard
Standard
Dilution
Dilution
90 - 100
30 - 50
80 - 100
60
100
80 - 100
10
5
10
6
4
4

3A
Dilution
80 - 100
3.5
2
1
1
1
1
1
1
2
2
2
4
2.5
3
2.5
2
2
2.5 - 3.5
2
3.5 - 4.5
4
4
3
3.5
1
2
1
1
1
1
1
3
1
1
2
2
Standard
Standard
Standard
Standard
Standard
Modified
Standard
Standard
Standard
Standard
Standard
Standard
60
80
50
40
50
100
70
60 - 80
80
40
100
100
6
4.5
6
7
6
5
4
4-5
5
5
4
4
Modified
60
Standard
70 - 90

Use G-12 thermapad
54
Sample Type
Non-Food Products
Acrylic Latex (approx. 60%
solids)
Acrylic Resin (approx. 58%
solids)
Acrylic Resin (approx. 49%
solids)
Acrylonitrile Butadiene
Polymer Dispersion
Alumina Chrome Oxide,
Fused White (approx. 6%
volume)
Alumina, Powder, Dry
Alumina, Powder, Slurry
Bauxite, Calcined (approx.
6% volume)
Black Liquor (approx. 62%
solids)
Boric Acid (approx. .2%
volume)
Castor Oil
Cellulose Acetate
Cellulose Nitrate
Clay, Calcined (approx. 3.5%
volume)
Coal
Conditioner, Hair (approx.
5% solids)
Detergent, Dishwasher (dry)
Detergent, Laundry (dry)
Detergent, Dish (liquid)
(approx. 64% solids)
Detergent, Non-Methyl
Glucamine Based (liquid)
Dye, Powder, Yellow (approx.
1.4% volume)
Dye, Press Cake, Yellow
Dye, Suspension, Orange
Sample
Preparation
Sample
Spread
Program
Size
Technique
(Grams)
Dry
%
Power
Dry
Time
(Min.)
Standard
50 - 70
Standard
80 - 100
Standard
80 - 100
1.5
Standard
10 - 30
None
4.5
Standard
80 - 100
None
1
None
10
5
6
1
1
1
Standard
Standard
Standard
80 - 100
80 - 100
80 - 100
2
4
3
3A
Dilution
80 - 100
None
Standard
80 - 100
1
None
2
2.5
5
5
5
4
None
None
4
4
1
1
Standard 15 - 35
Syringe 80 - 100
(Internal)
Standard 80 - 100
Standard 80 - 100
2
1
7
3
1
1
Standard
Standard
60 - 90
90 - 100
8
5
3A
3A
1
3
3
2
6
6
4
Dilution
Dilution
Standard
90 - 100
90 - 100
45 - 65
6
5
2.5
3A
2.5
Dilution
35 - 55
None
Standard
80 - 100
None
1
2.5
2
2
5
Standard
Standard
80 - 100
80 - 100
10
2
Comments
Dilute 50g 1:1 with cold deionized water,

shake
10
3
Use Teflon pad to support pad

55
Sample Type
Sample
Preparation
Emulsification Agent, Silica,

Oil, Water-Based (approx.
80% solids)
Epichlorohydrin Dimethylamine Condensate (approx.
50% solids)
Ethyl Acetate Resin
Suspension
Fiber, Cotton
Finish, Textile (approx. 1%
solids)
Hair Spray
Imidazaline (approx. 50%
solids)
Iron Oxide Dryer Product
(approx. 1% water)
Iron Oxide Press Cake
Iron Oxide Slurry (approx.
3% solids)
Lacquer, Clear
Lacquer, Gloss
Mannich Polyacrylamide,
emulsion form (approx. 50%
solids)
Neoprene in Acetone
Hexane, Toluene & MEK
Neoprene Latex in Water
Nonionic-Anionic Amide
Blend (approx. 61% solids)
Nonyl Phenol
Nylon Fiber, Raw Material
(approx. 31% volume)
Nylon Yarn, (approx. 3%
volume)
Oil, Fatty
Oil-Water Emulsion (<5%
solids)
Paint, Acrylic Based
Paper Cake from Dryer
Paper, Carbon Black Filled
Sample
Spread
Program
Dry
Dry
Size
Technique
%
Time
(Grams)
Power (Min.)
2
3
Standard 80 - 100
4
1.5
Standard
None
1
5
10
8
5
Syringe 80 - 100
(Internal)
Standard 40 - 60
Standard 80 - 100
1
1
1.5
1.5
8
6
Syringe
Syringe
80 - 100
60 - 80
5
5
Standard
80 - 100
1.5
None
Standard
80 - 100
2.5
3.5
Standard
60 - 90
1
1
1
2
2
2.5
5
5
5
Standard
Standard
Standard
55 - 75
80 - 100
80 - 100
10
10
10
Standard
80 - 100
1
1
2
1
4
7
Standard
Standard
80 - 100
20 - 40
3
4
1
See
Comments
See
Comments
1
1
2
2
5
8
Standard
Standard
30 - 50
70 - 90
5
6
Standard
80 - 100
1.5
5
5
5
Standard
Standard
80 - 100
80 - 100
10
8
3
3.5
7
5
2
None
Standard
Standard
Standard
80 - 100
80 - 100
20 - 35
10
12
10
1
2
See
Comments
15 - 35
Comments
5
10
7
Fluff on Teflon screen

3 pads
External balance required
Spread as much as possible, use drying

basket lined with one pad
Cut yarn into strips of <3, use Teflon
screen, fluff loosely on screen
Use Teflon screen, cut into 4 squares
56
Paper Pulp (approx. 1.2%

solids)
Sample Type
Paper Release (approx. 3- 6%
solids)
Paper, Coated (approx. 2.5%
vol.)
Paper, Coating (containing
Kaolin, CACo3, and/or
binder)
Phenolic Resin, Dried
(approx. 4% volume)
Phenolic Resin with
Inorganic Filler
Photoresist (approx. 25%
solids)
Polish, Floor (concentrate)
(approx. 6% solids)
Polish, Nail
Polyamide Resin (approx. 61%
solids)
Polyamide Resin in Water
Solution (approx. 50% solids)
Polydiallyldimehtyl
Ammonium Chloride Solution
Polyester Fiber, Loose
(approx. 0l7% volume)
Polyester Fiber, Raw
Material (approx. 7% volume)
Polyester Yarn, (approx. .5%
volume)
Polyvinyl Acetate, Aqueous
Solution, (approx. 12% solids)
Polyvinyl Acetate in
Methanol (approx. 43%
solids)
Pulp, Lap (approx. 43% solids)
Rayon Fiber, Raw Material
(47% volume)
Rosin Ester Resin Solution
Rubber Suspension in
Toluene
5.5
Syringe 80 - 100
4
(Internal)
Sample
Sample
Spread
Program
Dry
Dry
Comments
Preparation
Size
Technique
%
Time
(Grams)
Power (Min.)
See
5
None
Standard 60 - 80
5
Use Teflon screen, cut paper to size
Comments
See
4.5
None
Standard 70 - 90
10
Cut into 4 squares
Comments
3A
3
1
Standard 80 - 90
3.5
Dilute 50g 1:1 with cold deionized water,
shake
2
Standard
80 - 90
10
2.5
Standard
50 - 70
Standard
50 - 70
12
Standard
80 - 100
1
1
2
1
5
1
Standard
Standard
65 - 85
70 - 90
1
8
Standard
15 - 35
10
Standard
60 - 80
See
Comments
See
Comments
See
Comments
1
20
None
Standard
70 - 90
10
None
Standard
70 - 90
None
Standard
60 - 90
3.5
Standard
80 - 100
2.5
Syringe
(Internal)
60 - 80
2
None
7
2
Standard
Standard
60 - 70
70 - 90
7
6
Standard
80 - 100
2.5
4.5
Standard
20 - 40
Sandwich fluffed sample between 2 Teflon

screens
Fluff loosely onto pad, use drying basket
lined with one pad
Cut yarn into strips of <3, fluff loosely on
Teflon screen
Use Teflon screen to support pads

Fluff loosely onto pad, use drying basket
lined with one pad
57
Sizing, Textile, Water Based

Sludge Cake, WWTP (approx.
20% solids)
Sample Type
Standard
80 - 100
Standard
70 - 90
Sample
Preparation
Sludge, Metallic Hydroxide

Sludge, Oily
Soap, Bar
1
1
2
Soap, Beauty Bar
Soap, Liquid
Sodium Carbonate
Softener, Laundry (liquid)
Starch, Slurry
Urea Formaldehyde Resin
Varnish (contains ethyl
hexanol & mineral spirits)
Wastewater
Wax Blend, Cationic
1
None
1
1
1
Sample
Spread
Program
Dry
Dry
Comments
Size
Technique
%
Time
(Grams)
Power (Min.)
2.5
1
Standard 80 - 100
10
3-4
1
Standard 50 - 80
6
3
8
Standard 30 - 50
4
2
8
Standard 20 - 30
2.5
3
5
Standard 90 - 100
4
8
1
Standard 80 - 100
10
2.5
4
Standard 40 - 60
7
3
5
Standard 80 - 100
8.5
2.5
5
Standard 40 - 60
3.5
Standard
80 - 100
12
100-500
mL
2
None
TSS
80 - 100
Standard
80 - 100
Requires non-cellulose acetate type filter
58
V Quick Dry
Quick Dry permits simple entry of power and time parameters for a
one-time analysis or method development. The Quick Dry method contains two sample analysis procedures Auto Time and Constant
Weight.
Auto Time permits the operator to control the sample analysis
by entering a specified analysis time and power level. At the end
of the specified time, the percent solids and/or moisture of the
sample is calculated and displayed.
Constant Weight permits the operator to dry a sample until a
constant weight is achieved. Dryness is specified by defining a
maximum acceptable weight loss over a specified time interval.
During the specified time interval, when the weight loss is equal
to or less than that which was specified, the analysis stops and
results are calculated. The Constant Weight procedure permits
analysis of a sample without prior knowledge of the required dry
ing time. The time interval can be set for 0 to 59 seconds. The
weight loss differential can be set from 0.0 to 0.9 mg. Typically, a
time interval of approximately 15 seconds and a weight loss
differential of 0.2 - 0.5 mg will be specified.
Auto Time Sample Analysis

MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.
Press F1 to activate the Quick Dry method.

NAME
POWER
TIME
000
00.00
F2 - Case
Up/Dn - Arr
LabWave 9000
600066
Rev. 1
F4 - Quit
Ent - Run
F3 - End (Const. Wt.)
2.
Using the numeric keys, enter a procedure name or number. (Procedure name or number is optional in the Quick Dry method.)
3.
Press the down arrow key to position the cursor for entering
power. Using the numeric keys, enter the desired power level
(1 - 100%). (Example: To enter 80% power, press 8 and 0.)
59
4.
time. Using the numeric keys, enter the desired sample drying
time. (Example: To enter 1 minute, 30 seconds, press 1, 3 and 0.)
5.
To edit an entered parameter of the procedure (name, power and

time), use the up and down arrow keys to position the cursor
for entering corrections. To edit name, press F1 to erase name
and enter new data. To edit power and time, enter new data.
6.
Press Enter to perform the analysis procedure.
Note: Press F3 for the Constant Weight procedure, page 42.

TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID -XXXXXXXX
POWER
MOISTURE
XXX%
UNDER
F1 - EDIT
F3 - M/S
F2 - DATA 0 - I D
F4 - EXIT
5 - BAL SP
Wt. X.XXXXg
Note: Press 6 to edit power and/or dry time. Press F1 to edit name,
power and/or dry time.
Open the instrument door, lift the air shield, and place two glass
Press Tare.
TARE
8.
<* * *W A I T* * *>
Wait for the instrument to zero the weight of the sample pads.
The Quick Dry screen will reappear when the tare function is
complete.
TIME
XX:XX xx
DRY TIME
XX:XX
F1 - EDIT
F3 - M/S
XXXXXXXX
F2 - DATA
F4 - EXIT
0 - ID
5 - BAL SP
UNDER
T
ID -XXXXXXXX
POWER
MOISTURE
XXX%
7.
Wt. X.XXXXg
60
LabWave 9000
600066
Rev. 1
Note: Press F3 to change % moisture, % solids or % dry weight display. Press F4 to exit the procedure. Press 0 to enter or edit a sample identification number and/or name. Press 5 to change graph
weight range and/or to enter a moisture bias.
Note: The graph weight range (graph line on right side of display) is
designed to provide a visual representation of initial sample weight.
The LabWave 9000 defaults to a minimum of 2 and a maximum of 4
grams. However, based on sample size, minimum graph weight can be
set as low as 0, and maximum graph weight can be set as high as 50.0.
Refer to CEM Application Procedures for recommended sample
weight. To enter graph weights other than default settings, press 5
to activate the Balance Set Points screen.
Balance Set Points
Min Graph Wt: 02.00

Max Graph Wt: 04.00
F1 - Clr
Up - Arr
Dn - Arr
ENT - Exit
Note: If graph weight range requires no change, but a moisture bias is

necessary, press Enter to proceed to the Moisture Bias screen.
9.
Use the up and down arrow keys to select minimum or maximum graph weight. Press F1 to clear entered data. Using the
numeric keys, enter desired graph weight (minimum and maxi
mum). Press Enter to exit to the Moisture Bias screen.
% MOISTURE BIAS
Moisture Bias
Ent - Accept
0.00
F2 - (+/)F
4 - Exit
Note: If a moisture bias is not necessary, press F4 to exit to the

Quick Dry screen.
10. If applicable, use the numeric keys to enter a moisture bias. Press
Enter to accept the moisture bias and exit to the Quick Dry
screen.
LabWave 9000
600066
Rev. 1
61
XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
UNDER
T
ID - XXXXXXXX
POWER
MOISTURE
XXX%
F1 - EDIT
F3 - M/S
F2 - DATA
F4 - EXIT
0 - ID
5 - BAL SP
Wt. X.XXXXg
11. Remove the sample pads from the balance pan. Apply sample in a
thin, even layer to one of the sample pads. Quickly place the
sample pads back on the balance pan and position the air shield.
12. Close the instrument door. Press Start.
XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
XXX.XX%
F3 - M/S
STOP
Wt X.XXXX g
to beginning analysis. As analysis begins, the sample weight
F3 key may be pressed to alternate between displaying % moisture, % solids or % dry weight. The dry time displayed will begin
counting down. When drying time is complete, five short beeps
will be heard, and the Data Results screen will appear displaying
applicable results.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID
F3 - PRN GRAPH
F4 - EXIT
Note: To review initial weight, final weight and weight differential,

press F1. To return to Data Results screen, press any key. Press
F2 to activate a visual graph of data results on the display. Press
F3 to print a graph of data results. (To print a graph of data results,
print graph, Select Print Form, page 14, must be in the on position.)
62
LabWave 9000
600066
Rev. 1
XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
ID -XXXXXXXX
POWER
MOISTURE
XXX%
F1 - EDIT F2 - DATA 0 - I D
F3 - M/S F4 - EXIT
5 - BAL SP
Wt. X.XXXXg
15. To analyze additional samples using the same time and power,
press Tare, and repeat procedures outlined in steps 7 through
14. To analyze additional samples with modified time and power,
press 6 to edit parameters. To analyze additional samples with
a different name and modified time and power, press F1 to edit
parameters. Repeat procedures outlined in steps 5 through 14.
16. To end the Quick Dry program, press F4.
Are You Sure!

F1 - Resume
F4 - Quit
Note: Press F1 to resume Quick Dry program.

17. Press F4 to return to the Main Menu. All entered data and
parameters will be lost if the Quick Dry program is exited.
LabWave 9000
600066
Rev. 1
63
Constant Weight Sample Analysis

Constant Weight analysis may be used when analyzing an unfamiliar
sample or samples that vary in moisture. This procedure permits drying of samples until a constant weight is achieved. Perform the sample
analysis as follows:
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.
Press F1 to activate the Quick Dry method.

NAME
POWER
TIME
000
00:00
F2 - Case
Up/Dn - Arr
2.
Press F3 to activate the Constant Weight screen.

NAME
POWER
TIME
WEIGHT
MAX TIME
F2 - Case
Up/Dn - Arr
64
F4 - Quit
Ent - Run
F3 - End (Const. Wt.)
000
00
0.0
00
F4 - Quit
F3 - End (Time)
Ent - Run
3.
Using the numeric keys, enter a procedure name or number. (Procedure name or number is optional in the Quick Dry method.)
4.
power. Using the numeric keys, enter the desired power level
(1 - 100%). (Example: To enter 80% power, press 8 and 0.)
5.
Press the down arrow key to position the cursor for entering the
time interval. The differential time interval can be set for 0 to 59
seconds. Normally, a value of 15 seconds is used. Using the
numeric keys, enter the desired differential time interval.
(Example: To enter 15 seconds, press 1 and 5.)
6.
weight loss differential. Weight loss differential can be set from
LabWave 9000
600066
Rev. 1
0.0 to 0.9 mg. Normally, a value of 0.2 - 0.5 mg is used. Using the
numeric keys, enter the desired weight loss differential.
(Example: To enter 0.4 milligrams, press 4.)
7.
maximum run time. Using the numeric keys, enter the desired
maximum run time. (Example: To enter 10 minutes, press 1 and
0.)
Note: Maximum Run Time is the amount of time the instrument will
operate prior to shutdown if a constant weight has not been reached. A
maximum run time must be entered or the program will be invalid. If
the instrument shuts down due to maximum run time, parameters
should be adjusted prior to repeating analysis.
8.
Press Enter.
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID -XXXXXXXX
POWER
MOISTURE
XXX%
XXX.XX%
UNDER
F1 - EDIT
F3 - M/S
F2 - DATA 0 - I D
F4 - EXIT
5 - BAL SP
Wt X.XXXX g
Note: If necessary to edit any of the above entered parameters, press

6 or F1. Use the up and down arrow keys to position the cursor.
Use the numeric keys to enter correct parameters.
9.
Press Tare.
TARE
<* * *W A I T* * *>
10. Wait for the instrument to zero the weight of the sample pads.
The Quick Dry screen will reappear when the tare function is
complete.
LabWave 9000
600066
Rev. 1
65
XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
ID - XXXXXXXX
POWER
MOISTURE
80%
UNDER
F1 - EDIT
F3 - M/S
F2 - DATA 0 - I D
F4 - EXIT
5 - BAL SP
Wt 0.0000 g
Note: Press F3 to change % moisture, % solids or % dry weight display. Press F4 to exit the procedure. Press 0 to enter or edit a sample identification number and/or name. Press 5 to change graph
weight range and/or to enter a moisture bias.
The LabWave 9000 defaults to a minimum of 2 and a maximum of 4
grams. However, based on sample size, minimum graph weight can be
set as low as 0, and maximum graph weight can be set as high as 50.0.
Refer to CEM Application Procedures for recommended sample
Balance Set Points
Min Graph Wt:

Max Graph Wt:
F1 - Clr
02.00
04.00
Up - Arr
Dn - Arr
ENT - Exit
Note: If graph weight range requires no change, but a moisture bias is

necessary, press Enter to proceed to the Moisture Bias screen.
11. Use the up and down arrow keys to select minimum or maximum graph weight. Press F1 to clear entered data. Using the
numeric keys, enter desired graph weight (minimum and maximum). Press Enter to exit to the Moisture Bias screen.
% MOISTURE BIAS
Moisture Bias
Ent - Accept
66
000
F2 - (+/)
F4 - Exit
LabWave 9000
600066
Rev. 1
12. If applicable, use the numeric keys to enter a moisture bias. Press
Enter to accept the moisture bias and exit to the Quick Dry
screen.
XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
ID - XXXXXXXX
POWER
MOISTURE
80%
UNDER
F1 - EDIT
F3 - M/S
F2 - DATA
F4 - EXIT
0 - ID
5 - BAL SP
Wt 0.0000 g
13. Remove the sample pads from the balance pan. Apply 2 - 5 grams
of sample in a thin, even layer to one of the sample pads. Quickly
and gently place the sample pads back on the balance pan and
position the air shield.
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
XX.XX%
F3 - M/S
Wt 0.0000 g
STOP
decreases as the moisture is removed. During drying time, the
F3 key may be pressed to display % moisture, % solids or % dry
weight. The dry time displayed will begin counting up. When the
weight loss is equal to or less than that which was specified, five
short beeps will be heard, and the Data Results screen will
appear displaying applicable data results.
DATA RESULTS
LabWave 9000
600066
Rev. 1
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID XXXXXXXX
F3 - PRN GRAPH
F4 - EXIT
67
16. To review initial weight, final weight and weight differential,

press F1. To return to Data Results screen, press any key. Press
F2 to activate a visual graph of data results on the display.
Press F3 to print a graph of data results.
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
XXX.XX%
F1 - EDIT F2 - DATA
F3 - M/S F4 - EXIT
0 - ID
5 - BAL SP
UNDER
TIME
XX:XX xx
DRY TIME
01:30
Wt 0.0000 g
18. To analyze additional samples using the same method parameters

(power, time interval, weight loss differential and maximum run
time), press Tare, and repeat procedures outlined in steps 9
through 17.
19. To analyze additional samples with modified method parameters
(power, time interval, weight loss differential and maximum run
time), press 6 to edit parameters. To analyze additional samples
with a different name and different parameters, press F1.
Repeat procedures outlined in steps 3 through 17.
Note: Once time and power parameters are established for a sample,
operation in Auto Time sample analysis is recommended unless the
sample is hydroscopic.
20. To end the Quick Dry program, press F4.
Are You Sure!

F1 - Resume
F4 - Quit
Note: Press F1 to resume Quick Dry program.

21. Press F4 to return to the Main Menu. All entered data and
parameters will be lost if the Quick Dry program is exited.
68
LabWave 9000
600066
Rev. 1
VI
Program/Edit/Run Method
The Program/Edit/Run Method permits entry and storage of analysis

programs for a variety of different sample types (40 program capacity)
and sample analysis using the stored programs. To enter, store and
edit programs, follow procedures outlined below (pages 69 through 75).
To perform analysis, follow procedures outlined on pages 76 through
145.
Program/Edit Method
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.
Press F2 to activate the Program/Edit/Run Method.

SELECT PROGRAM
FILE
01
PGMS
XX
PGM NAME
F1 - NEW
En - RUN
2.
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
Press F1 to enter and store a new program in memory.
Note: PressF2 to activate the program directory for a listing of available programs.
CREATE PROGRAM
NAME
OPERATOR
ANALYSIS
Up/Dn - Arr
F3 - HELP
3.
LabWave 9000
600066
Rev. 1
Moisture/Solids
>
F4 - EXIT
0 -Analysis
ENT - NEXT SCRN
Using the numeric keyboard, enter the selected program name

(16 letters, numbers and/or spaces maximum). (Example: For the
program Milk LF, press 5 two times, 3 four times and 4 four
times; press the right arrow key; press 4 three times; press the
dot key twice for space; press 4 four times and 2 four times.
69
4.
If an operator name or number is desired, press the down arrow

key to position the curser for entering operator information. Using
the numeric keyboard, enter the desired operator information (16
letters, numbers and/or spaces maximum).
5.
The LabWave 9000 system software defaults to Moisture/Solids

analysis. If a different type analysis is desired, press the down
arrow key to position the curser on analysis type. Press 0 to
select desired type of analysis Moisture/Solids (page 70),
Moisture/Fat (page 72) or Moisture/Fat/Protein (page 73).
6.
Press Enter to proceed to the next screen.
Moisture/Solids Analysis
SELECT PROGRAM OPTIONS
STANDARD
% ASH
% ASH ALT
SYRINGE WEIGH
DILUTIONS
TSS
TSS/TVSS
TSS/TVSS ALT
Up - Arr
Dn - Arr
ENT - Nxt
F4 - Exit
1.
Using the up and down arrow keys, select the program option
desired Standard (Moisture/Solids), TSS (Total Suspended
Solids), TSS/TVSS (Total Volatile Suspended Solids), TSS/TVSS
ALT (Total Volatile Suspended Solids in Alternate Mode), % Ash,
% Ash Alternate, Syringe Weigh, or Dilution. Refer to page 2 for
descriptions of available programs and pages 76 through 120 for
operation procedures.
2.
Press Enter.
END METHOD TIME
% Power
Run Time
000
00:00
END METHOD CONSTANT WT.
Time
00 sec
Up - Arr
3.
70
Weight
0.0 mg
Dn - Arr
Max Tm
00 min
ENT - Nxt
F4 - Exit
Using the up and down arrow keys, position the cursor to

enter parameters for either Auto Time (power and time) or Con
stant Weight (power, time interval, weight loss differential and
maximum run time) sample analysis. Using the numeric keys,
enter analysis parameters. Press Enter to proceed to the next
screen.
LabWave 9000
600066
Rev. 1
% MOISTURE BIAS
0.00
Moisture Bias
Ent - Accept
4.
F2 - (+/)
F4 -Exit
If applicable, use the numerical keys to enter a moisture bias.

Press F2 to change the moisture bias from a + to a - or vice
versa. Press Enter to proceed to the next screen.
Balance Set Points
Min Graph Wt:

Max Graph Wt:
F1 - Clr
02.00
04.00
Up - Arr
Dn - Arr
ENT - Exit
The LabWave 9000 is defaulted for a minimum of 2 and a maximum of
4 grams. However, based on sample size, minimum graph weight can
be set as low as 0, and maximum graph weight can be set as high as
50.0. Refer to CEM Application Procedures for recommended sample
weight.
5.
To change the minimum and/or maximum graph weight, use the

up and down arrow keys to select minimum or maximum
graph weight. Press F1 to clear entered data. Using the numeric
keys, enter desired graph weight (minimum and maximum).
Press Enter to exit. (If default settings of 2 and 4 are to be used,
simply press Enter to exit to the Select Program screen.
FILE
01
PGM NAME
F1 - NEW
En - RUN
6.
LabWave 9000
600066
Rev. 1
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
To perform program analysis, follow procedures outlined on pages

76 through 120.
71
Moisture/Fat Analysis
Note: Ensure that steps 1 through 6, pages 69 and 70, have been performed.
STANDARD
ALTERNATE
DILUTIONS
MODIFIED FAT
Up - Arr
1.
Dn - Arr
ENT - Nxt
F4 - Exit
desired Standard, Alternate, Dilutions or Modified Fat. Press
Enter.
SET PROGRAM CONSTANTS
Run Time
% Power
% Bias
M 00:00
F 00:00
M 000
F 000
M 00.00
F 00.00
Up - Arr
Dn - Arr
ENT - Nxt
F4 - Exit
2. Using the arrow keys, position the cursor to enter parameters for
sample analysis. Using the numeric keys, enter analysis
parameters (run time, % power and, if applicable, % bias for both
moisture and fat procedures) in accordance with analytical
method. Press Enter.
Balance Set Points
Min Graph Wt:

Max Graph Wt:
F1 - Clr
02.00
04.00
Up - Arr
Dn - Arr
ENT - Exit
72
LabWave 9000
600066
Rev. 1
3.

simply press Enter to exit to Select Program screen.
SELECT PROGRAM
FILE
01
PGM NAME
F1 - NEW
En - RUN
4.
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR

121 through 145.
Moisture/Fat/Protein Analysis
Note: Ensure that steps 1 through 6, pages 69 and 70, have been performed.
STANDARD
ALTERNATE
DILUTIONS
MODIFIED FAT
Up - Arr
1.
Dn - Arr
ENT - Nxt
F4 - Exit
desired Standard, Alternate, Dilutions or Modified Fat. Press
Enter.
SET PROGRAM CONSTANTS
Run Time
% Power
M 00:00
F 00:00
M 000
F 000
Up - Arr
Dn - Arr
% Bias
M 00.00
F 00.00
A + C 00.00
ENT - Nxt
F4 - Exit
2. Using the arrow keys, position the cursor to enter parameters for
sample analysis. Using the numeric keys, enter analysis
parameters (run time, % power and, if applicable, % bias for both
moisture and fat procedures) in accordance with analytical
method. Press Enter.
LabWave 9000
600066
Rev. 1
73
Balance Set Points
Min Graph Wt:

Max Graph Wt:
F1 - Clr
02.00
04.00
Up - Arr
Dn - Arr
ENT - Exit
3.

simply press Enter to exit to Select Program screen.
SELECT PROGRAM
FILE
01
PGM NAME
F1 - NEW
En - RUN
4.
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR

121 through 145.
Moisture/Fat/Protein Parameters
To perform the Moisture/Fat and Moisture/Fat/Protein analyses, enter
parameters of run time and % power for both moisture (M) and fat (F)
determinations. If necessary, based on bias identification, enter % bias
for moisture and/or fat. For Moisture/Fat/Protein analysis, if required,
enter % ash and carbohydrate factor (A + C).
74
LabWave 9000
600066
Rev. 1
Program Deletion
To delete a program which has been stored in the Program/Edit/Run
Method, proceed as follows:
SELECT PROGRAM
FILE
01
PGM NAME
F1 - NEW
En - EDIT
1.
PGMS
03
XXXXXXXX
F2 - DIR
0 - Edit
F3 - ERA
1 - PRN
F4 - EXIT
Up - Arr
Press F3 to delete (erase) a program.

DELETE PROGRAM
Enter File Number to Delete.
See Dir for File Number.
Delete File
00
F2 - DIR
F4 - EXIT
Note: Press F2 for directory to determine file number to be deleted.

2.
Using the numeric keys, enter the file number to be deleted from
the directory.
3.
Press Enter.
Erase File XX
Are You Sure?
F1 - YES
F4 - NO
4.
Press F1 to delete selected file.
File Deleted.
5.
LabWave 9000
600066
Rev. 1
Press F4.
Press F4 to return to Select Program screen.

75
Run Method
The Program/Edit/Run Method permits sample analysis using the programs previously stored.
Note: The Program/Edit/Run Method cannot be utilized for analysis
unless one or more programs have been properly entered and stored
(pages 69 through 74).
Moisture/Solids Standard
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

SELECT PROGRAM
FILe
01
PGM NAME
F1 - NEW
En - RUN
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
Note: The LabWave 9000 defaults to the first file of the program
directory.
2.
Press down (up) arrow key to select the desired program.
Note: Press 0 to edit program parameters. Press F2 to view the

program directory. Press 1 to print a hard copy of the selected program, all programs or the program directory. F1 permits entry of a
new program. F3 permits deletion (erasure) of an entered program.
3.
76
Press Enter to perform the selected analysis.
LabWave 9000
600066
Rev. 1
TIME
XX:XX xx
DRY TIME
XX:XX
F3 - M/S
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
F2 - DATA
F4 - EXIT
0 - ID
Wt X.XXXX g
UNDER
-
Note: Press 6 to edit program parameters. Press 0 to enter or edit

an analysis identification number. Press F3 to change moisture/
solids/dry weight display. Press F4 to exit the procedure.
4.
Press Tare.
TARE
5.
<* * *W A I T* * *>
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
UNDER
-
F3 - M/S
LabWave 9000
600066
Rev. 1
F2 - DATA
F4 - EXIT
0 - ID
Wt X.XXXX g
6.
Remove the sample pads from the balance pan. Apply sample in a
sample back on the balance pan and position the air shield.
7.
Close the instrument door. Press Start.
77
XXXXXXXX
TIME
XX:XX xx
ID - XXXXXXXX
DRY TIME
XX:XX
POWER
XXX%
MOISTURE
XX.XX%
F3 - M/S
Wt - X.XXXX g
Stop
8.
The instrument will record the initial weight of the sample prior
F3 key may be pressed to alternate between displaying mois
ture, solids and dry weight. The dry time will begin counting.
When drying time is complete, five short beeps will be heard, and
the Data Results screen will appear displaying applicable results.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F3 - PRN GRAPH
F4 - EXIT
Press F1 to review weight data. To return to Data Results

screen, press any numeric key. Press F2 to activate a visual
graph of data results on the display. Press F3 to print a graph of
data results. To end analysis, press F4.
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
9.
F2-GRAPH
SAMPLE ID XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
UNDER
F3 - M/S
F2 - DATA
F4 - EXIT
0 - ID
Wt - X.XXXX g
10. To analyze additional samples using the same program, repeat

procedures outlined in steps 4 through 9. To edit program
parameters prior to analyzing additional samples, press 6.
11. To exit program, press F4.
78
LabWave 9000
600066
Rev. 1
Are You Sure!

Test Results Will Be Lost!
F1 - Resume
F4 - Quit
Note: Press F1 to resume program.

12. Press F4 to exit (quit) program.
FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
LabWave 9000
600066
Rev. 1
79
Moisture/Solids - TSS (Total Suspended Solids)

This procedure is used to determine the total suspended solids content
of a sample using the initial liquid volume as the initial weight. It is
recommended that a minimum of 250 ml of liquid be filtered to achieve
a representative level of solids after drying. For very low levels of TSS,
50 - 100 mg/liter, the volume will need to be increased to 500 or 1000
ml.
Required Equipment:
1 liter graduated cylinder
Whatman glass microfibre filters or equivalent
7 - 11 cm Buchner funnel
2000 ml filtering flask with side arm
Vacuum pump, aspirator or other vacuum source
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

3.
80
LabWave 9000
600066
Rev. 1
TSS MODE
Enter number of samples
to process. XX
Num - Keys
Ent - Accept
F4 - Exit
4.
Using the numeric keys, enter the correct number of samples to

be processed during analysis.
5.
Press Enter.
UNDER
-
TIME
X XXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
INIT. LIQ. VOL. (ML) 250
NO. OF SAMPLES XX
0 - ID
F 3 - M / S F4 - EXIT 1 - VOL
6.
F2 - Data
Wt X.XXXX g
If necessary, press 1 to position the cursor for changing initial

liquid volume. Using the numeric keys, enter the volume of liquid
measured (default value of 250 ml). Press Enter to store the new
volume of liquid.

7.
Press Tare.
TSS MULTIPLE TARE
Place Sample Pad #01 on
Balance and Press TARE.
PADS TARED = 00
F4 - End TARE
8.
LabWave 9000
600066
Rev. 1
Open the instrument door, lift the air shield, and place the first
Whatman filter on the balance pan. Reposition the air shield, and
close the instrument door.
81
Note: If the instrument door is not properly closed, the following

screen will appear. Ensure that the door is closed.
Door Must be Closed.
9.
Press Tare.
TSS MULTIPLE TARE
TARE <* * * WAIT * * *>
PADS TARED = 00
F4 - End TARE
10. Wait for the LabWave 9000 to zero the weight of the filter.
TSS MULTIPLE TARE
PADS TARED = 01
F4 - End TARE
Note: If only one sample is to be analyzed, the above screen will not
appear.
11. Open the instrument door, remove the first filter from the balance
pan. Place the second pad on the balance pan, position the air
shield, and close the instrument door.
12. Press Tare.
TSS MULTIPLE TARE
TARE <* * * WAIT * * *>
PADS TARED = 01
F4 - End TARE
82
LabWave 9000
600066
Rev. 1
13. Continue the tare process until filters for the total number of samples to be analyzed have been tared.
Note: Filters must be kept in the order in which they are tared for
sample analysis.
XXXXXXXX
TIME
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
INIT. LIQ. VOL. (ML) XXX
PROCESSING X OF X
UNDER
F2 - Data 0 - ID
F 3 - M / S F4 - EXIT 1 - VOL
Wt X.XXXX g
14. Place the first filter for which the weight was tared in the Buchner funnel. With the vacuum source operating, pour the sample
into the funnel. When all the sample has been filtered, remove the
filter from the funnel.
15. Open the instrument door, lift the air shield, and place the wet filter on the balance pan. Lower the air shield, and close the instru
ment door.
16. Press Start.
XXXXXXXX
POWER
XXX%
MOISTURE
XX.XX%
TIME
XX:XX xx
DRY TIME
XX:XX
PROCESSING X OF X
F3 - M/S
Stop
Wt X.XXXX g
17. As analysis begins, the sample weight decreases as the moisture
is removed. During drying time, the F3 key may be pressed to
display moisture, solids or dry weight. The dry time displayed will
begin counting. When the analysis is complete, five short beeps
will be heard, and the Data Results screen will appear.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
F1-WEIGHTS
LabWave 9000
600066
Rev. 1
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F2-GRAPH
SAMPLE ID
MG/LITER
SAMPLE
INITIAL LIQ. VOL.
F3 - PRN GRAPH
XXXXXXXX
XX
XX
XXX
F4 - EXIT
83
18. Press F1 to review weights. To return to Data Results screen,

press any numeric key. Press F2 to activate a visual graph of
data results on the display. Press F3 to print a graph of data
results. (To print a graph of data results, print graph, Select Print
Form, page 14, must be in the on position.) Press F4 to exit to
TSS screen to continue sample analyses.
TIME
XXXXXXXX
XX:XX xx
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
UNDER
INIL. LIQ. VOL. (ML) XXX
NO. OF SAMPLES XX
F2 - Data 0 - ID
F3 - M/S F4 - Exit
1 - VOL
Wt X.XXXXg
19. If necessary, press 6 to edit program parameters or 1 to

change the initial liquid volume.
20. Repeat steps 14 through 19 using consecutive filter pads until
each analysis has been completed. Filters must be used in the
order in which they were tared until final analysis is complete.
21. Press F4.
Are You Sure!

F1 - Resume
F4 - Quit

22. Press F4 to exit program.
FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
84
LabWave 9000
600066
Rev. 1
Moisture/Solids - TSS/TVSS (Total Volatile Suspended Solids)

This procedure is used to determine the total volatile suspended solids
content of a sample using the initial liquid volume as the initial
weight. It is recommended that a minimum of 250 ml of liquid be filtered to achieve a representative level of solids after drying. For very
low levels of TVSS, 50 - 100 mg/liter, the volume will need to be
increased to 500 or 1000 ml.
Required Equipment:
CEM MAS-7000 Microwave Muffle Furnace or other ashing
furnace
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

SELECT PROGRAM
FILE
01
PGM NAME
F1 - NEW
En - RUN
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

3.
LabWave 9000
600066
Rev. 1
85
UNDER
-
XXXXXXXX
TIME
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
F3 - M/S
4.
F2 - Data 0 - ID
F4 - EXIT 1 - VOL
Wt - X.XXXX g

measured (minimum of 250 ml).
Note: Press 6 to edit program parametrs. Press 0 to enter or edit

5.
Open the instrument door, lift the air shield, and place a Whatman filter on the balance pan. Reposition the air shield, and close
the instrument door.
6.
Press Tare.
TARE
7.
<* * *W A I T* * *>
Wait for the LabWave 9000 to zero the weight of the filter.
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
INIT. LIQ. VOL. (ml) XXX
UNDER
T
F3 - M/S
F2 - Data
F4 - EXIT
0 - ID
1 - VOL
WT X.XXXX g
8.
Open the instrument door, remove the filter from the balance pan
and place it in the Buchner funnel. With the vacuum source
operating, pour the sample into the funnel. When all the sample
has been filtered, remove the filter from the funnel.
9.
Open the instrument door, lift the air shield, and place the wet filter on the balance pan. Lower the air shield, and close the instrument door.
10. Press Start.
86
LabWave 9000
600066
Rev. 1
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
XX.XX%
F3 - M/S
Stop
Wt X.XXXX g
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID
MG/LITER TSS
MG/LITER TVSS
INIT. LIQ. VOL.
F3 - PRN GRAPH
XXXXXXXX
X
X
XXX
F4 - EXIT
12. Press F1 to review weights. Press F2 to activate a visual graph

of data results on the display. Press F3 to print a graph of data
results. Press F4 to exit to TVSS screen to continue sample
analyses.
XXXXXXXX
TIME
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
REWEIGH SAMPLE
UNDER
F3 - M/S
F2 - Data
F4 - EXIT
Wt X.XXXX g
13. Open the instrument, lift the air shield, and remove the sample
filter with the dried sample from the balance pan.
14. Fold the filter, place it in an ashing crucible, and place the crucible in the ashing furnace. Ash the sample by the appropriate
method.
15. Remove the sample from the ashing furnace, and place it back on
the LabWave 9000 balance pan. Lower the air shield, and close
LabWave 9000
600066
Rev. 1
87
16. Press Start.
UNDER
-
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
REWEIGHING SAMPLE
F3 - M/S
F2 - Data
F4 - EXIT
Wt X.XXXX g
17. The LabWave 9000 reweighs the sample and calculates the total
volatile suspended solids content.
Note: The straight line in the microwave indicator box indicates that
microwaves are not being produced during sample reweigh.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID
MG/LITER TSS
MG/LITER TVSS
INITL. LIQ. VOL.
F3 - PRN GRAPH
XXXXXXXX
X
X
XXX
F4 - EXIT

results. Press F4 to exit to TVSS screen to continue sample
analyses.
UNDER
-
TIME
XXXXXXXX
XX:XX xx
ID-XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
INIT. LIQ. VOL. (ML) XXX
F2 - Data 0 - ID
F4 - EXIT 1 - VOL
F3 - M/S
Wt X.XXXX g
19. Press F4.
Are You Sure!

F1 - RESUME
88
F4 - QUIT
LabWave 9000
600066
Rev. 1

20. Press F4 to exit (quit) the program.
FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
01
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
LabWave 9000
600066
Rev. 1
89
Moisture/Solids - TSS/TVSS (Total Volatile Suspended Solids)

Alternate Mode
The TVSS procedure is used to determine the total volatile suspended
solids content of a sample using the initial liquid volume as the initial
weight. It is recommended that a minimum of 250 ml of liquid be filtered to achieve a representative level of solids after drying. For very
low levels of TVSS, 50 - 100 mg/liter, the volume will need to be
increased to 500 or 1000 ml.
Required Equipment:
CEM MAS-7000 Microwave Muffle Furnace or other ashing furnace
The alternate mode permits drying of one sample in the LabWave 9000
while ashing another sample in the ashing furnace or drying all samples to be ashed and later reweighed. This method requires a sample
identification for each sample to ensure proper test results.
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

3.
90

LabWave 9000
600066
Rev. 1
XXXXXXXX
ID - XXXXXXXX
MOISTURE
F1 - REWEIGH F 2 - D A T A 0 - I D
F3 - M/S
F4 - EXIT 1 - VOL
UNDER
TIME
XX:XX xx
DRY TIME
POWER
XX:XX
XXX%
Wt X.XXXX g
Note: Press 6 to edit program parameters. Press F3 to change

moisture/solids/dry weight display. Press F4 to exit the procedure.
4.

measured (minimum of 250 ml).
5.
Press 0 to enter a sample identification name and/or number.
Note: An identification name and/or number must be entered to perform an analysis in the alternate mode.
EDIT SAMPLE ID
SAMPLE ID
Ent - Accept
F4 - Exit
6.
Using the numeric keyboard, enter a sample identification (8

numbers, letters and/or spaces maximum).
7.
Press Enter.
FILE
XX
PGM NAME
PGMS
XX
XXXXXXXX
F2 - Directory
Enter - Accept
8.
Up/Dn Arr - Sel
Ensure that the program name displayed is the selected program.

Press Enter to accept the sample identification into the
program.
Note: If necessary, use the up and down arrow keys to select the
appropriate program.
LabWave 9000
600066
Rev. 1
91
ID - XXXXXXXX
MOISTURE
F3 - M/S
F4 - EXIT 1 - VOL
9.
UNDER
-
XXXXXXXX
TIME
XX:XX xx
DRY TIME
POWER
XX:XX
XXX%
Wt X.XXXX g
Open the instrument door, lift the air shield, and place a Whatman filter on the balance pan. Reposition the air shield, and close
10. Press Tare.
TARE
<* * *W A I T* * *>
11. Wait for the LabWave 9000 to zero the weight of the filter.
F3 - M/S
F4 - EXIT 1 - VOL
UNDER
T
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
Wt X.XXXX g
12. Open the instrument door, remove the filter from the balance pan
and place it in the Buchner funnel. With the vacuum source
operating, pour the sample into the funnel. When all the sample
has been filtered, remove the filter from the funnel.
13. Open the instrument door, lift the air shield, and place the wet filter on the balance pan. Lower the air shield, and close the
instrument door.
14. Press Start.
Note: If a sample identification has not been entered, the instrument
will not begin the sample analysis. An Invalid Sample ID screen will
appear. A sample identification must be entered prior to proceeding
with the analysis.
92
LabWave 9000
600066
Rev. 1
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
XX.XX%
INIT. LIQ. VOL. (ml) XXX
F3 - M/S
Stop
Wt X.XXXX g
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID
MG/LITER TSS
MG/LITER TVSS
INITL. LIQ. VOL.
F3 - PRN GRAPH
XXXXXXXX
X
X
XXX
F4 - EXIT

results. Press F4 to exit and continue sample analysis.
TIME
XXXXXXXX
XX:XX xx
ID DRY TIME
POWER
MOISTURE
XX:XX
XXX%
INITIAL LIQ. VOL. (ml) XXX
UNDER
F1 - REWEIGH
F3 - M/S
F2 - DATA 0 - I D
F4 - EXIT 1 - VOL
Wt X.XXXX g
17. Open the instrument door; lift the air shield; and remove the filter pad (with the dried sample) from the balance pan.
18. To ash the dried sample, fold the filter; place it in an ashing crucible; and place the crucible in the ashing furnace. Ash the sample
by the defined method.
19. To dry additional samples, follow procedures outlined in steps 4
through 16, ensuring that each sample is properly labeled with
the sample identification in order to enter the proper identification for reweighing.
LabWave 9000
600066
Rev. 1
93
20. To reweigh an ashed sample, press F1 from the previous screen.

The following screen will appear.
EDIT SAMPLE ID
SAMPLE ID
Ent - Accept
F4 - Exit
21. Using the numeric keyboard, enter the identification name and/or
number to be reweighed.
22. Press Enter.
UNDER
-
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
REWEIGHING SAMPLE
F3 - M/S
F4 - EXIT
Wt X.XXXX g
23. Press Start. The instrument weighs the ashed sample and calculates the data results.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID
MG/LITER TSS
MG/LITER TVSS
INITL. LIQ. VOL.
F3 - PRN GRAPH
XXXXXXXX
X
X
XXX
F4 - EXIT

results. Press F4 to exit.
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
INITIAL LIQ. VOL. (ml) XXX
UNDER
F1 - REWEIGH
F3 - M/S
94
F2 - DATA 0 - I D
F4 - EXIT
Wt X.XXXX g
LabWave 9000
600066
Rev. 1
25. To reweigh additional samples, follow procedures outlined in

steps 20 through 24.
26. When the final sample has been reweighed, press F4 to end the
program.
NOTE
Ensure that all samples have been reweighed. All data
and weight results will be deleted upon exiting the program.
Are You Sure!

F1 - RESUME
F4 - QUIT

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
28. Press F4 to exit to the Main Menu.
LabWave 9000
600066
Rev. 1
95
Moisture/Solids Percent Ash/Volatile Solids

This procedure is used to determine the ash and volatile solids content
of a sample.
Required equipment:
CEM MAS-7000 Microwave Muffle Furnace or other ashing
furnace
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

3.

TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
UNDER
F3 - M/S
96
F2 - Data 0 - ID
F4 - EXIT
Wt X.XXXX g
LabWave 9000
600066
Rev. 1
Note: Press 6 to edit program parameters. Press 0 to enter an

analysis identification number. Press F3 to change moisture/solids/
dry weight display. Press F4 to exit the procedure. Press F2 to
review program data.
4.
fiber sample pads on the balance pan. Reposition the air shield,
and close the instrument door.
5.
Press Tare.
TARE
6.
<* * *W A I T* * *>
Wait for the LabWave 9000 to zero the weight of the pads.
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID MOISTURE
POWER
XXX%
UNDER
F3 - M/S
F2 - Data
F4 - EXIT
0 - ID
Wt X.XXXX g
7.
Remove the sample pads from the balance pan. Apply sample in a
8.
Close the instrument door. Press Start.

TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
POWER
XXX%
MOISTURE
XX.XX%
F3 - M/S
Stop
Wt X.XXXX g
LabWave 9000
600066
Rev. 1
97
9.
F3 key may be pressed to alternate between displaying moisture, solids or dry weight. The dry time will begin counting. When
drying time is complete, five short beeps will be heard, and the
Data Results screen will appear, displaying applicable results.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID XXXXXXXX
F3 - PRN GRAPH
F4 - EXIT
10. Press F1 to review weight data. Press F2 to activate a visual

data results. Press F4 to exit.
TIME
XX:XX xx
DRY TIME
POWER
XX:XX
XXX%
REWEIGH SAMPLE
XXXXXXXX
ID - XXXXXXXX
MOISTURE
UNDER
F3 - M/S
F2 - Data
F4 - EXIT
Wt X.XXXX g
pads with the dried sample from the balance pan.
12. Fold the pads, place them in an ashing crucible, and place the crucible in the ashing furnace. Ash the sample by the appropriate
method.
13. Remove the pads with the sample from the ashing furnace, and
place them back on the LabWave 9000 balance pan. Lower the air
shield, and close the instrument door.
14. Press Start.
TIME
XX:XX xx
DRY TIME
POWER
XX:XX
XXX%
REWEIGHING SAMPLE
XXXXXXXX
ID - XXXXXXXX
MOISTURE
UNDER
F3 - M/S
98
F2 - Data
F4 - EXIT
Wt X.XXXX g
LabWave 9000
600066
Rev. 1
Note: The straight line in the microwave indicator box indicates that
microwaves are not being produced during sample reweigh.
15. The LabWave 9000 reweighs the sample and calculates the percent ash.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
F1-WEIGHTS
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F2-GRAPH
SAMPLE ID
ASH
VOL. SOLIDS
F3 - PRN GRAPH
XXXXXXXX
XX.XX%
XX.XX%
F4 - EXIT

results. Press F4 to exit.
TIME
XX:XX xx
DRY TIME
XX:XX
POWER
XXX%
UNDER
-
XXXXXXXX
ID - XXXXXXXX
MOISTURE
F3 - M/S
F2 - Data 0 - ID
F4 - EXIT
Wt X.XXXX g
Note: To analyze additional samples using the same program, repeat

procedures outlined in steps 4 through 16.
17. Press F4 to exit the program.
Are You Sure!

F1 - RESUME
F4 - QUIT

LabWave 9000
600066
Rev. 1
99
FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
100
LabWave 9000
600066
Rev. 1
Moisture/Solids Percent Ash Alternate

The percent ash with alternate mode permits drying of one sample in
the LabWave 9000 while another sample is being ashed in the ashing
furnace or drying of all samples to be ashed and later reweighed.
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.
Note: Press 0 to enter or edit program parameters. Press F2 to

view the program directory. Press 1 to print a hard copy of the
selected program, all programs or the program directory. F1 permits
entry of a new program. F3 permits deletion (erasure) of an entered
program.
3.

TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
POWER
XXX%
ID - XXXXXXXX
MOISTURE
UNDER
F3 - M/S
F4 - EXIT
Wt X.XXXX g

moisture/solids/dry weight display. Press F2 to review program data.
Press F4 to exit the procedure.
LabWave 9000
600066
Rev. 1
101
4.
EDIT SAMPLE ID
SAMPLE ID
Ent - Accept
F4 - Exit
5.

6.
Press Enter.
FILE
XX
PGM NAME
PGMS
XX
XXXXXXXX
F2 - Directory
Enter - Accept
7.
Up/Dn Arr - Sel

Press Enter. to accept the sample identification into the
program.
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
POWER
XXX%
ID - XXXXXXXX
MOISTURE
UNDER
F3 - M/S
F4 - EXIT
102
Wt X.XXXX g
8.
9.
Press Tare.
LabWave 9000
600066
Rev. 1
TARE
<* * *W A I T* * *>
10. Wait for the LabWave 9000 to zero the weight of the pads.
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
POWER
XXX%
ID - XXXXXXXX
MOISTURE
UNDER
F3 - M/S
F4 - EXIT
Wt X.XXXX g
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
POWER
XXX%
ID - XXXXXXXX
MOISTURE
XX.XX%
F3 - M/S
Stop
Wt X.XXXX g
13. The instrument will record the initial weight of the sample prior to
beginning analysis. As analysis begins, the sample weight
F3 key may be pressed to alternate between displaying moisture,
solids or dry weight. The dry time will begin counting. When dry
ing time is complete, five short beeps will be heard, and the Data
Results screen will appear, displaying applicable results.
LabWave 9000
600066
Rev. 1
103
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
F1-WEIGHTS
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F2-GRAPH
SAMPLE ID XXXXXXXX
F3 - PRN GRAPH
F4 - EXIT

TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
POWER
XXX%
ID - XXXXXXXX
MOISTURE
UNDER
F3 - M/S
F4 - EXIT
Wt X.XXXX g
pads with the dried sample from the balance pan.
16. To ash the dried sample, fold the pads, place them in an ashing
crucible, and place the crucible in the ashing furnace. Ash the
sample by the appropriate method.
the sample identification in order to enter the proper identification for reweighing.
18. To reweigh an ashed sample, press F1 from the previous screen.
The following screen will appear.
EDIT SAMPLE ID
SAMPLE ID
Ent - Accept
F4 - Exit
20. Press Enter.
104
LabWave 9000
600066
Rev. 1
TIME
XX:XX xx
DRY TIME
POWER
XX:XX
XXX%
REWEIGHING SAMPLE
UNDER
-
XXXXXXXX
ID - XXXXXXXX
MOISTURE
F3 - M/S
F4 - EXIT
Wt X.XXXX g
21. Press Start. The instrument weighs the ashed sample and calculates the data results.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
F1-WEIGHTS
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
SAMPLE ID
ASH
VOL. SOLIDS
F2-GRAPH
F3 - PRN GRAPH
XXXXXXXX
XX.XX%
XX.XX%
F4 - EXIT

TIME
XX:XX xx
DRY TIME
POWER
XX:XX
XXX%
REWEIGHING SAMPLE
XXXXXXXX
ID - XXXXXXXX
MOISTURE
UNDER
F3 - M/S
F4 - EXIT
Wt X.XXXX g
23. To reweigh additional samples, follow procedures outlined in

steps 19 through 22.
24. When the final sample has been reweighed, press F4 to end the
program.
NOTE
LabWave 9000
600066
Rev. 1
105
Are You Sure!

F1 - Resume
F4 - Quit

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
106
LabWave 9000
600066
Rev. 1
Moisture/Solids Syringe Weigh

This procedure is used for samples that, due to rapid evaporation, cannot achieve a stable initial weight with the standard moisture/solids
application. The instrument internal balance or an external balance
can be used for calculating the weight of the syringe.
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

program.
3.
Note: To perform syringe weigh using the internal balance, follow procedures outlined on pages 108 through 111. To perform syringe weigh
using an external balance, follow procedures outlined on pages 112
through 115. To utilize an external balance, the balance type must be
selected in system setup, page 16. Refer to External Balance Setup,
page 10, for proper settings of balance.
LabWave 9000
600066
Rev. 1
107
Internal Balance Syringe Weigh

TIME
XX:XX xx
DRY TIME
XX:XX
UNDER
-
XXXXXXXX
ID POWER
XXX%
MOISTURE
F 2 - D a t a F1 - EX SYR
F3 - M/S F4 - EXIT 0 - ID
Wt X.XXXX g

solids/dry weight display. Press F2 to review program data. F1
exits to external balance syringe weigh. Press F4 to exit the procedure.
1.
2.
Press Tare.
TARE
3.
<* * *W A I T* * *>
INTERNAL BALANCE (SYRINGE)
Remove Sample Pads.
Place Filled Syringe on
Balance and Press F1.
F4 - Exit
108
4.
Remove sample pads from balance pan. Place syringe containing

sample on balance pan. Position air shield and close instrument
door.
5.
Press F1.
LabWave 9000
600066
Rev. 1
WAIT!
Weighing Syringe
F4 - EXIT
Dispense Sample on Pads.
Place Syringe back on
Balance and Press F1.
F4 - EXIT
6.
Dispense sample from syringe on tared sample pads.
7.
Place the empty syringe back on the instrument balance pan.

Position the air shield, and close the instrument door.
8.
Press F1.
WAIT!
Reweighing Syringe
Remove Syringe
Place Sample on Balance.
Press Any Key, then START.
9.
Remove the syringe from the balance pan. Place the sample pads
with sample on the balance pan. Position the air shield, and close
10. Press any numeric key.
LabWave 9000
600066
Rev. 1
109
TIME
XX:XX xx
DRY TIME
XX:XX
UNDER
-
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
Wt X.XXXX g
11. Press Start.

TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
XX.XX%
F3 - M/S
Stop
Wt X.XXXX g
is removed. During the drying time, the F3 key may be pressed
to alternate between displaying moisture, solids or dry weight.
The dry time will begin counting. When drying time is complete,
five short beeps will be heard, and the Data Results screen will
appear, displaying applicable results.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID XXXXXXXX
F3 - PRN GRAPH
F4 - EXIT
13. Press F1 to review weight data. To return to Data Results

data results.Press F4 to exit.
110
LabWave 9000
600066
Rev. 1
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
Wt X.XXXX g

procedures outlined in steps 1 through 13 of Internal Balance Syringe
Weigh.
Are You Sure!

F1 - RESUME
F4 - QUIT

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
01
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
LabWave 9000
600066
Rev. 1
111
External Balance Syringe Weigh

1.
Ensure that steps 1 through 3 of Syringe Weigh, page 107, have

been performed.
TIME
XX:XX xx
DRY TIME
XX:XX
UNDER
-
XXXXXXXX
ID POWER
XXX%
MOISTURE
Wt X.XXXX g

solids/dry weight display. Press F2 to review program data. Press
F4 to exit the procedure.
2.
Press F1 to exit to external balance syringe weigh.

EXTERNAL BALANCE (SYRINGE)
PLACE CLEAN PADS ON INTERNAL

BALANCE. PRESS TARE.
F4 - Exit
3.
4.
Press Tare.
TARE
5.
112
<* * *W A I T* * *>
LabWave 9000
600066
Rev. 1

CLEAR EXTERNAL BALANCE PAN.
PRESS TARE.
F4 - Exit
6.
Ensure that external balance pan is clear of any weight.
7.
Press Tare.
PLACE FILLED SYRINGE ON
EXTERNAL BALANCE. LET
STABILIZE, THEN PRESS F1.
F4 - Exit
8.
Place syringe containing sample on external balance pan. Wait for

the weight to stabilize.
9.
Press F1.
REMOVE SYRINGE. DISPENSE
SAMPLE ON PADS, RETURN
SYRINGE TO EXTERNAL BALANCE.
LET STABILIZE, THEN PRESS F1.
F4 - Exit
10. Remove sample pads from instrument balance pan. Dispense

sample from syringe on sample pad in accordance with application.
11. Place empty syringe on external balance pan. Wait for the weight
to stabilize.
12. Press F1.
LabWave 9000
600066
Rev. 1
113

SAMPLE WT.
XX.XXXX
PLACE SAMPLE ON INTERNAL

BALANCE, PRESS F4 THEN START.
F4 - Exit
13. Place the sample pads with sample on the internal balance pan.
Position the air shield, and close the instrument door.
14. Press F4.
TIME
XX:XX xx
DRY TIME
XX:XX
UNDER
-
XXXXXXXX
ID POWER
XXX%
MOISTURE
Wt X.XXXX g
15. Press Start.

TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID POWER
XXX%
MOISTURE
XX.XX%
F3 - M/S
Stop
Wt X.XXXX g
DATA RESULTS
114
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID XXXXXXXX
F3 - PRN GRAPH
F4 - EXIT
LabWave 9000
600066
Rev. 1

TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
Wt X.XXXX g

Are You Sure!

F1 - RESUME
F4 - QUIT

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
01
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
LabWave 9000
600066
Rev. 1
115
Moisture/Solids Dilution
This procedure is used for viscous samples or samples that dry unevenly. The dilution is accomplished by using a volatile diluent such as
water, methyl ethyl ketone or methyl isobutyl ketone. The diluent
must be miscible with the sample. The LabWave 9000 performs calculations to correct for the dilution.
Required Equipment:
External Balance
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

program.
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
DILUTION RATIO
XX.XXXX
F1 - DIL
F3 - M/S
116
F2 - DATA 0 - I D
F4 - EXIT 1 - RATIO
UNDER
3.
Wt X.XXXX g
LabWave 9000
600066
Rev. 1

solids/dry weight display. Press F4 to exit the procedure. Press F2
to review program data. Press 1 for ratio.
4.
Press F1 to exit to external balance for dilution.

EXTERNAL BALANCE (DILUTIONS)
PLACE EMPTY CONTAINER ON

EXTERNAL BALANCE, PRESS TARE.
F4 - Exit
5.
Place an empty container suitable for sample and diluent on

external balance. Wait for the weight to stabilize.
6.
Press Tare.
ADD SAMPLE TO CONTAINER,

PRESS F1.
F4 - Exit
7.
Place sample in container on external balance pan. Wait for the

weight to stabilize.
Note: The LabWave 9000 records the weight of the sample.

8.
Press F1.
SAMPLE WT.
XX.XXXX
ADD DILUENT TO CONTAINER,

PRESS F1.
F4 - Exit
9.
Add diluent to sample in container on external balance. Wait for

10. Press F1.
LabWave 9000
600066
Rev. 1
117

SAMPLE WT.
SAMPLE + DIL. WT.
DILUTION RATIO.
XX.XXXX
XX.XXXX
X.XXXX
F4 - Exit
11. Press F4.
UNDER
-
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
DILUTION RATIO
XX.XXXX
F2 - DATA 0 - I D
F4 - EXIT 1 - RATIO
F1 - DIL
F3 - M/S
Wt X.XXXX g
12. Open the instrument door, lift the air shield, and place two glass
13. Press Tare.
TARE
<* * *W A I T* * *>
F1 - DIL
F3 - M/S
F2 - DATA 0 - I D
F4 - EXIT 1 - RATIO
UNDER
T
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
DILUTION RATIO
XX.XXXX
Wt X.XXXX g
15. Remove the sample pads from the balance pan. Apply diluted
sample in a thin, even layer to one of the sample pads. Place the
sample pads back on the balance pan and position the air shield.
118
LabWave 9000
600066
Rev. 1
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
XX.XX%
DILUTION RATIO
XX.XXXX
Stop
F3 - M/S
Wt - X.XXXX g
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY WT.
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID XXXXXXXX
F3 - PRN GRAPH
F4 - EXIT

F1 - DIL
F3 - M/S
F2 - DATA 0 - I D
F4 - EXIT 1 - RATIO
UNDER
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
DILUTION RATIO
XX.XXXX
Wt - X.XXXX g

LabWave 9000
600066
Rev. 1
119
Are You Sure!

F1 - RESUME
F4 - QUIT

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
120
LabWave 9000
600066
Rev. 1
Moisture/Fat or Moisture/Fat/Protein Standard
Moisture/Fat and Moisture/Fat/Protein analyses require the CEM Fat

Extraction System. Refer to the Fat Extraction System Operation
Manual for operating instructions for the system.
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

program.
3.

XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
POWER
XXX%
MOISTURE
F2 - DATA 0 - I D
F3 - M/S F4 - EXIT
LabWave 9000
600066
Rev. 1
UNDER
-
ID - XXXXXXXX
Wt X.XXXX g
121

analysis identification number. Press F3 to change moisture/solids
display. Press F4 to exit the procedure.
4.
Open the instrument door, lift the air shield, and place one round
and two square glass fiber sample pads on the balance pan (round
pad on bottom). Reposition the air shield. Close the instrument
door. Press Tare.
TARE
5.
<* * *W A I T* * *>
XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
UNDER
T
ID - XXXXXXXX
POWER
XXX%
MOISTURE
F2 - DATA 0 - I D
F3 - M/S F4 - EXIT
Wt X.XXXX g
6.
Remove the square sample pads from the balance pan. Apply
sample in a thin, even layer to one of the sample pads and cover
the sample with the second pad. With the round pad still on the
balance pan, quickly place the square sample pads back on the
balance pan and position the air shield. Close the instrument
door.
7.
Press Start.
M / F STD
TIME
XX:XX xx
DRY TIME
XX:XX
ID - XXXXXXXX
POWER
XXX%
MOISTURE
XX.XX%
F3 - M/S
Stop
Wt X.XXXX g
122
LabWave 9000
600066
Rev. 1
8.
F3 key may be pressed to alternate between displaying mois
ture and solids. The dry time will begin counting. When drying
time is complete, five short beeps will be heard, and the Data
Results screen will appear displaying applicable results.
DATA RESULTS
SAMPLE ID XXXXXXXX
MOISTURE
SOLIDS
DRY TIME
F1-WEIGHTS
9.
XX.XX%
XX.XX%
XX:XX
F2-GRAPH
F3 - PRN GRAPH
F4 - EXIT
Press F1 to review weight data. To return to Data Results

TIME
XXXXXXXX
XX:XX xx
REDRY TIME
XX:XX
ID - XXXXXXXX
POWER
XXX%
MOISTURE
F2 - DATA
F3 - M/S F4 - EXIT
UNDER
-
Wt X.XXXX g
10. Open the instrument door and remove the sample pads with the
dried sample from the balance pan.
11. Fold the square pads in half and place them in the extraction
chamber of the Fat Extraction System. Place the round pad
(smooth side up) in the recess at the top of the extraction cham
ber, and close and latch the lid.
WARNING
Failure to insert or properly position the round
filter pad in the recess at the top of the extraction chamber could result in operator exposure to
solvent due to leakage or possible spraying and/
or damage to the Fat Extraction System, resulting from solid matter entering the distillation
system.
LabWave 9000
600066
Rev. 1
123
12. Press the Run/Stop button on the Extractor to start the extraction
cycle. When the extraction is complete, the extractor cup will be
inverted, a beep tone will sound, and the light in the Run/Stop
button will flash. While the extractor cup is still in the inverted
position, unlatch the lid and remove the round sample pad on
which the chopped square pads and extracted and dried sample
have been deposited. Latch the cup lid. The extractor cup will
automatically rotate 180 degrees to the upright position.
13. Open the LabWave 9000 door, lift the air shield, and place the
round pad with extracted sample on the balance pan. Position the
air shield and close the instrument door.
14. Press Start.
TIME
XXXXXXXX
XX:XX xx
ID - XXXXXXXX
REDRY
XX:XX
F3 - M/S
POWER
XXX%
FAT
XXX.XX%
Stop
Wt X.XXXX g
15. The instrument will record the weight of the sample prior to
F3 key may be pressed to alternate between displaying moisture
and solids. The redry time will begin counting. When redrying
DATA RESULTS
MOISTURE
SOLIDS
DRY TIME
F1 - Weights
XX.XX%
XX.XX%
XX:XX
SAMPLE ID XXXXXXXX
FAT
XX.XX%
REDRY TM
XX.XX
F2 - GRAPH
F3 - PRN GRAPH
F4 - E x i t

124
LabWave 9000
600066
Rev. 1
XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
UNDER
-
ID - XXXXXXXX
POWER
XXX%
MOISTURE
F2 - DATA 0 - I D
F3 - M/S F4 - EXIT
Wt X.XXXX g

Are You Sure!

F1 - Resume
F4 - Quit

SELECT PROGRAM
FILE
01
PGM NAME
F1 - NEW
En - RUN
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
LabWave 9000
600066
Rev. 1
125
Moisture/Fat or Moisture/Fat/Protein Alternate

Moisture/Fat and Moisture/Fat/Protein analyses require the CEM Fat
Extraction System. Refer to the Fat Extraction System Operation
Manual for operating instructions for the system.
The alternate mode permits drying of one sample in the LabWave
9000 while another sample is being processed in the Extractor or drying of all samples to be extracted and later reweighed.
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

program.
3.

TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
XXX%
MOISTURE
F1 - REDRY F 2 - D A T A 0 - I D
F3 - M/S
F4 - EXIT 9 - DEL
126
UNDER
Wt X.XXXX g
LabWave 9000
600066
Rev. 1
4.
EDIT SAMPLE ID
SAMPLE ID
Ent - Accept
F4 - Exit
5.

6.
Press Enter.
FILE
XX
PGM NAME
PGMS
XX
XXXXXXXX
F2 - Directory
Enter - Accept
7.
Up/Dn Arr - Sel

Press Enter. to accept the sample identification into the pro
gram.
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
XXX%
MOISTURE
F3 - M/S
F4 - EXIT 9 - DEL
UNDER
Wt X.XXXX g

moisture/solids display. Press F4 to exit the procedure. Press 9 to
delete an identification number.
8.
LabWave 9000
600066
Rev. 1
pad on bottom). Reposition the air shield. Close the instrument
door. Press Tare.
127
TARE
9.
<* * *W A I T* * *>
TIME
XX:XX xx
DRY TIME
XX:XX
UNDER
-
XXXXXXXX
ID - XXXXXXXX
POWER
XXX%
MOISTURE
F3 - M/S
F4 - EXIT 9 - DEL
Wt X.XXXX g
10. Remove the square sample pads from the balance pan. Apply
door.
11. Press Start.
TIME
XX:XX xx
DRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
XXX%
MOISTURE
XX.XX%
F3 - M/S
Stop
Wt X.XXXX g
and solids. The dry time will begin counting. When drying time is
screen will appear displaying applicable results.
128
LabWave 9000
600066
Rev. 1
DATA RESULTS
SAMPLE ID XXXXXXXX
MOISTURE
SOLIDS
DRY TIME
F1-WEIGHTS
XX.XX%
XX.XX%
XX:XX
F2-GRAPH
F3 - PRN GRAPH
F4 - EXIT

TIME
XX:XX xx
REDRY TIME
XX:XX
XXXXXXXX
ID - XXXXXXXX
POWER
XXX%
FAT
F1 - END F2 - DATA 0 - I D
F3 - M/S F4 - EXIT
9 - DEL
UNDER
Wt - X.XXXX g
the sample identification in order to enter the proper identification for redrying.
16. To extract fat from sample, fold the square pads with dried sample in half and place them in the extraction chamber of the Fat
Extraction System. Place the round pad (smooth side up) in the
recess at the top of the extraction chamber, and close and latch
the lid. Press the Run/Stop button on the Extractor to start the
extraction cycle.
WARNING
system.
17. To redry samples, press F1 from the previous screen. The following screen will appear.
LabWave 9000
600066
Rev. 1
129
EDIT SAMPLE ID
SAMPLE ID
Ent - Accept
F4 - Exit
19. Press Enter.
Note: If a sample identification has not been entered, the instrument
will not begin the sample analysis. An Invalid Sample ID screen will
appear. A sample identification must be entered prior to proceeding
with the analysis.
TIME
XX:XX xx
REDRY
XX:XX
UNDER
-
XXXXXXXX
ID - XXXXXXXX
POWER
XXX%
FAT
F3 - M/S F4 - EXIT
9 - DEL
Wt X.XXXX g
round pad with extracted sample on the balance pan for redrying.
Position the air shield and close the instrument door.
21. Press Start.
XXXXXXXX
TIME
XX:XX xx
REDRY
XX:XX
POWER
XXX%
FAT
XX.XX%
F3 - M/S
Stop
Wt X.XXXX g
22. When redrying time for sample is complete, five short beeps will
be heard, and the Data Results screen will appear, displaying
applicable results.
130
LabWave 9000
600066
Rev. 1
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY TIME
F1-WEIGHTS
XX.XX%
XX.XX%
XX.XX%
XX:XX
SAMPLE ID
FAT
REDRY Tm.
F2-GRAPH
F3 - PRN GRAPH
XXXXXXXX
XX.XX
XX:XX
F4 - EXIT

TIME
XX:XX xx
REDRY TIME
XX:XX
UNDER
-
XXXXXXXX
ID - XXXXXXXX
POWER
XXX%
FAT
F3 - M/S F4 - EXIT
9 - DEL
Wt X.XXXX g
24. To redry additional samples, follow procedures outlined in steps

17 through 23.
25. When the final sample has been redried, press F4 to exit the
program.
NOTE
Are You Sure!

F1 - Resume
F4 - Quit

LabWave 9000
600066
Rev. 1
131
FILE
01
PGM NAME
F1 - NEW
En - RUN
SELECT PROGRAM
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
132
LabWave 9000
600066
Rev. 1
Moisture/Fat or Moisture/Fat/Protein Dilutions

Some types of samples require dilution prior to extraction of the fat.
This procedure combines the dilution option with the fat analysis procedure.
Required Equipment:
External Balance
Fat Extraction System
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

SELECT PROGRAM
FILE
01
PGM NAME
F1 - NEW
En - RUN
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

program.
3.

XXXXXXXX
ID - XXXXXXXX
TIME
XX:XX xx
DRY TIME
POWER
XX:XX
XXX%
MOISTURE
DILUTION RATIO
XX.XXXX
F1 - DIL F2 - DATA 0 - I D
F3 - M/S F4 - EXIT
1 - RATIO
LabWave 9000
600066
Rev. 1
UNDER
Wt X.XXXX g
133

display. Press F4 to exit the procedure. Press F2 to review program
data. Press 1 for dilution ratio. If dilution ratio is altered, press
Enter to store the new parameter.
4.
Press F1 to exit to external balance for dilution.

PLACE EMPTY CONTAINER ON

EXTERNAL BALANCE, PRESS TARE.
F4 - Exit
5.
Place an empty container suitable for sample and diluent on

external balance. Wait for the weight to stabilize.
6.
Press Tare.
ADD SAMPLE TO CONTAINER,

PRESS F1.
F4 - Exit
7.
Place sample in container on external balance pan. Wait for the

weight to stabilize.
Note: The LabWave 9000 records the weight of the sample.

8.
Press F1.
SAMPLE WT.
XX.XXXX
ADD DILUENT TO CONTAINER,

PRESS F1.
F4 - Exit
9.
Add diluent to sample in container on external balance. Wait for

10. Press F1.
134
LabWave 9000
600066
Rev. 1

SAMPLE WT.
SAMPLE + DIL. WT.
DILUTION RATIO
XX.XXXX
XX.XXXX
X.XXXX
F4 - Exit
11. Press F4.
XXXXXXXX
MOISTURE
UNDER
TIME
XX:XX xx
DRY TIME
POWER
XX:XX
XXX%
DILUTION RATIO
XX.XXXX
F3 - M/S F4 - EXIT
1 - RATIO
Wt. X. XXXX g
12. Open the instrument door, lift the air shield, and place one round
pad on bottom). Reposition the air shield, and close the instrument door.
13. Press Tare.
TARE
<* * *W A I T* * *>
XXXXXXXX
MOISTURE
F3 - M/S F4 - EXIT
1 - RATIO
UNDER
TIME
XX:XX xx
DRY TIME
POWER
XX:XX
XXX%
DILUTION RATIO
XX.XXXX
Wt. X.XXXX g
15. Remove the square sample pads from the balance pan. Apply
diluted sample in a thin, even layer to one of the sample pads and
cover the sample with the second pad. With the round pad still on
the balance pan, place the square sample pads back on the bal
ance pan and position the air shield. Close the instrument door.
LabWave 9000
600066
Rev. 1
135
16. Press Start.

XXXXXXXX
TIME
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
XX.XX%
DILUTION RATIO
XX.XXXX
Stop
F3 - M/S
Wt X.XXXX g
to alternate between displaying moisture and solids. The dry time
will begin counting. When drying time is complete, five short
beeps will be heard, and the Data Results screen will appear,
displaying applicable results.
DATA RESULTS
MOIST. BIAS
MOISTURE
SOLIDS
DRY TIME
XX.XX%
XX.XX%
XX.XX%
XX:XX
F1-WEIGHTS
F2-GRAPH
SAMPLE ID XXXXXXXX
F3 - PRN GRAPH
F4 - EXIT

F1 - DIL F2 - Data
F3 - M/S F4 - EXIT
UNDER
XXXXXXXX
TIME
XX:XX xx
ID - XXXXXXXX
REDRY
POWER
FAT
XX:XX
XXX%
DILUTION RATIO
XX.XXXX
Wt X.XXXX g
(smooth side up) in the recess at the top of the extraction
chamber, and close and latch the lid.
136
LabWave 9000
600066
Rev. 1
WARNING
system.
cycle. When the extraction is complete, the extractor cup will be
inverted, a beep tone will sound, and the light in the Run/Stop
button will flash. While the extractor cup is still in the inverted
position, unlatch the lid and remove the round sample pad on
which the chopped square pads and extracted and dried sample
have been deposited. Latch the cup lid. The extractor cup will
round pad with extracted sample on the balance pan. Position the
air shield and close the instrument door.
23. Press Start.
REDRY Tm
POWER
XX:XX
XXX%
DILUTION RATIO
XX.XXXX
F3 - M/S
UNDER
-
XXXXXXXX
TIME
XX:XX xx
FAT
XXX.XX%
Stop
Wt X.XXXX g
Results screen will appear, displaying applicable results.
DATA RESULTS
MOISTURE
SOLIDS
DRY TIME
F1 - Weights
LabWave 9000
600066
Rev. 1
XX.XX%
XX.XX%
XX:XX
F2 - GRAPH
SAMPLE ID
FAT
REDRY TM
F3 - PRN GRAPH
XXXXXXXX
XX.XX%
XX.XX
F4 - E x i t
137

data results.Press F4 to exit.
F3 - M/S F4 - EXIT
1 - RATIO
UNDER
XXXXXXXX
TIME
XX:XX xx
ID - XXXXXXXX
DRY TIME
POWER
MOISTURE
XX:XX
XXX%
DILUTION RATIO
XX.XXXX
Wt. X.XXXX g

Are You Sure!

F1 - RESUME
F4 - QUIT

SELECT PROGRAM
FILE
01
PGM NAME
F1 - NEW
EN - RUN
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - PRN
F4 - EXIT
UP/DN - ARR
138
LabWave 9000
600066
Rev. 1
Moisture/Fat or Moisture/Fat/Protein Modified Fat

With the modified procedure, the fat is extracted from one sample
while another sample is dried for moisture analysis. This procedure
permits determination of fat content of samples in which initial drying
of sample may bind the fat molecules in the sample matrix.
Required Equipment:
External Balance
Fat Extraction System
MAIN MENU
F1: QUICK DRY
F3: SYSTEM SETUP
1.

SELECT PROGRAM
FILE
01
PGM NAME
F1 - NEW
En - RUN
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
directory.
2.

program.
3.

XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
ID - XXXXXXXX
POWER
XXX%
MOISTURE
F2 - DATA 0 - I D
F3 - M/S F4 - EXIT
LabWave 9000
600066
Rev. 1
UNDER
Wt X.XXXX g
139

display. Press F2 to review program data. Press F4 to exit the procedure.
4.
pad on bottom). Reposition the air shield, and close the instrument door.
5.
Press Tare.
TARE
6.
<* * *W A I T* * *>
MODIFIED FAT
Spread Sample on Pads.
Place Sample with Pads
on Balance and Press F1.
F4 - Quit
7.
Remove the square sample pads from the balance pan. Apply
door.
8.
Press F1.
MODIFIED FAT
WAIT Weighing Sample.
F4 - Quit
Note: The LabWave 9000 weighs and records the weight of sample 1.
140
LabWave 9000
600066
Rev. 1
MODIFIED FAT
Place Sample 1 in Fat
Extractor Chamber.
Place Sample 2 Pads on
Sample #1 Wt. = XX.XXXX
F4 - Quit
9.
Open the instrument door and remove the sample pads with the
weighed sample from the balance pan.
(smooth side up) in the recess at the top of the extraction chamber, and close and latch the lid.
WARNING
system.
cycle.
12. Place two square glass fiber filter pads on the balance pan of the
LabWave 9000.
13. Press Tare.
TARE
<* * *W A I T* * *>
Note: Wait for the LabWave 9000 to zero the weight of the pads.
MODIFIED FAT
Spread Sample on Pads.
Place Sample with Pads
on Balance. Press any Key
to Exit, then START.
F4 - Quit
LabWave 9000
600066
Rev. 1
141
thin, even layer to one of the sample pads and cover the sample
with the second pad. Quickly place the square sample pads back
on the balance pan and position the air shield. Close the instrument door.
15. Press any numerical key to exit.
XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
ID - XXXXXXXX
POWER
XXX%
MOISTURE
F2 - DATA 0 - I D
F3 - M/S F4 - EXIT
Wt X.XXXX g
16. Press Start.

XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
ID - XXXXXXXX
POWER
MOISTURE
XXX%
XX.XX%
F3 - M/S
Stop
Wt X.XXXX g
and solids. The dry time will begin counting. When drying time is
screen will appear displaying applicable results.
DATA RESULTS
SAMPLE ID XXXXXXXX
MOISTURE
SOLIDS
DRY TIME
F1-WEIGHTS
142
XX.XX%
XX.XX%
XX:XX
F2-GRAPH
F3 - PRN GRAPH
F4 - EXIT
LabWave 9000
600066
Rev. 1

data results. (To print a graph of data results, print graph, Select
Print Form, page 14, must be in the on position.) Press F4 to
exit.
TIME
XX:XX xx
REDRY
XX:XX
XXXXXXXX
UNDER
-
ID - XXXXXXXX
POWER
XXX%
FAT
F2 - DATA
F3 - M/S F4 - EXIT
Wt X.XXXX g
19. Open the instrument door and remove the sample pads with dried
sample no. 2 from the balance pan. This sample can now be
discarded.
20. When the extraction of sample no. 1 is complete, the extractor cup
will be inverted, a beep tone will sound, and the light in the Run/
Stop button will flash. While the extractor cup is still in the
inverted position, unlatch the lid and remove the round sample
pad on which the chopped square pads and extracted sample have
been deposited. Latch the cup lid. The extractor cup will
21. Place the round pad with extracted sample no. 1 on the LabWave
9000 balance pan. Position the air shield and close the instrument
door.
22. Press Start. The LabWave 9000 will redry the extracted sample
to remove any residual solvent or moisture.
TIME
XX:XX xx
REDRY
XX:XX
F3 - M/S
UNDER
-
XXXXXXXX
ID - XXXXXXXX
POWER
XXX%
FAT
XXX.XX%
Stop
Wt X.XXXX g
LabWave 9000
600066
Rev. 1
143
DATA RESULTS
MOISTURE
SOLIDS
DRY TIME
F1-WEIGHTS
SAMPLE ID XXXXXXXX
FAT
XX.XX%
REDRY Tm. XX:XX
XX.XX%
XX.XX%
XX:XX
F2-GRAPH
F3 - PRN GRAPH
F4 - EXIT
Note: The LabWave 9000 will store the final weight of the fatextracted sample. Based on the weight of sample no. 1 prior to extraction, the weight prior to redry, and the final weight after redry plus
the weights of sample no. 2 prior to and following the drying process,
the instrument will compute and display fat and, if applicable, protein
analysis results.
XXXXXXXX
TIME
XX:XX xx
DRY TIME
XX:XX
ID - XXXXXXXX
POWER
XXX%
MOISTURE
F2 - DATA 0 - I D
F3 - M/S F4 - EXIT
UNDER
Wt X.XXXX g

144
LabWave 9000
600066
Rev. 1
Are You Sure!

F1 - Resume
F4 - Quit

SELECT PROGRAM
FILE
01
PGM NAME
F1 - NEW
En - RUN
PGMS
XX
XXXXXXXX
F2 - DIR
0 - EDIT
F3 - ERA
1 - Prn
F4 - EXIT
Up/Dn - ARR
LabWave 9000
600066
Rev. 1
145
146
LabWave 9000
600066
Rev. 1
VII
Maintenance, Troubleshooting and

Service
This chapter covers routine maintenance and basic troubleshooting.

For detailed instructions concerning service and repair, contact CEM
Corporation Service Department or your local distributor.
Cleaning Recommendations
Clean the door seals and interior of the LabWave 9000 cavity with
warm, soapy water applied with a soft cloth. Do not use abrasive
cleaners or solvents because they could scratch the cavity coating.
Rinse and thoroughly dry all cleaned areas.
Routine Maintenance
A monthly preventive maintenance program is recommended to
ensure optimum performance of the LabWave 9000. Check the following items:
1. Door, Seals, and Lock Carefully inspect the door, door seals,
and door interlock to verify that they are clean and working
properly. Ensure that there is no loosening of or damage to the
door hinges or latch. Ensure that the door closes securely.
2. Balance Check balance calibration using procedures outlined
in Chapter III, Setup, pages 20 and 21, procedures 36 through
42.
3. Air Shield Inspect the air shield for damage or degradation.
4. Microwave Leakage Measurement and Microwave Power
Measurement Follow procedures outlined below.
Microwave Leakage Measurement

The door and cavity of the LabWave 9000 are designed for durability
and reliable operation under severe laboratory conditions. External
radiation checks are performed on the instrumeNt at several points in
the manufacturing process to ensure that microwave leakage is only a
fraction of that permitted by U.S. law (5 mW/cm2).
The door of the LabWave 9000 is equipped with a safety interlock system (figures 10 and 11, pages 159 and 160) which stops the generation
of microwave energy when the instrument door is ajar. If the interlock
system fails, a monitoring mechanism will blow the fuse through
which power is supplied to the magnetron, rendering the microwave
power system inoperable if the interlock system fails.
To verify that door seals and interlock system are working properly,
the LabWave 9000 should be tested for microwave leakage. To test for
microwave leakage, operate the LabWave 9000 at 100% power for 5
minutes. While it is operating, use a federally approved microwave
leakage detector such as the Holaday Model HI-1500 and measure the
microwave leakage around the door seal, at the louvres in the cover,
LabWave 9000
600066
Rev. 1
147
and at the fan grills in the cover. Leakage should not exceed 5 mW/
cm2. If the instrument shows excessive microwave leakage, do not
attempt further operation. Contact the CEM Corporation Service
Department or your local distributor.
Microwave test meters are available from CEM Corporation. CEM
does not recommend use of inexpensive meters available in electronics
stores because they lack the necessary sensitivity to properly test an
instrument for microwave leakage.
Microwave Power Measurement

The LabWave 9000 has a microwave power output of approximately
630 watts at 100% power. Use the following procedures to determine
power output.
MAIN MENU
F1: QUICK DRY
F2: PROGRAM/EDIT/RUN METHOD
F3: SYSTEM SETUP
1.
Press F1 to activate the Quick Dry program.

NAME
POWER
TIME
F2 - Case
Up/Dn - Arr
000
00:00
F4 - Quit
Ent - Run
CAUTION
If the LabWave 9000 has not been operated for a
period of one hour, preheat the instrument by
operating it empty for 5 minutes at 100% power
in the Quick Dry program.
148
2.
Press the down arrow key to move the cursor to power. Using
the numeric keys, enter 100% power by pressing 1, 0, 0. Press
the down arrow key to move the selector to time. Enter 2
minutes of time by pressing 2, 0, 0.
3.
Press Enter.
LabWave 9000
600066
Rev. 1
TIME
XX :XX xx
DRY TIME
0 2 : 0 0
XXXXXXXX
ID POWER
1 0 0 %
MOISTURE
UNDER
F 3 - M / S F4 - EXIT 5 - BAL SP
Wt. X.XXXXg
4.
Press Tare.
TARE
5.
<* * *W A I T* * *>
Wait for the Quick Dry screen to reappear.

TIME
XX :XX xx
XXXXXXXX
DRY TIME
POWER
0 2 : 0 0
1 0 0 %
UNDER
T
ID -
MOISTUR E
Wt. X.XXXXg
LabWave 9000
600066
Rev. 1
6.
Pour 1000 ml of room temperature water into a 1000 ml glass or

polypropylene beaker. Using a thermometer with 0.1 degree C
gradations, stir the water and measure its temperature. Record
this temperature as the initial water temperature (Ti). Remove
the thermometer from the beaker.
7.
Open the instrument door. Remove the balance pan and stem.
Carefully place the beaker in the left rear corner of the cavity.
Gently close the door to avoid spilling the water.
8.
Press Start.
149
XXXXXXXX
ID POWER
100%
TIME
XX :XX xx
DRY TIME
0 2 : 0 0
MOISTURE
XXX.XX%
F3 - M/S
Wt. X.XXXXg
STOP
Note: The flashing wavy line in the microwave indicator box indicates
that microwaves are being produced.
9.
At the end of the 2 minute period, five short beeps will sound, and
the Data Results screen will appear.
DATA RESULTS
MOISTURE BIAS
MOISTURE
SOLIDS
100.00%
100.00%
00.00%
DRY WT
00.00%
DRY TIME
02:00
F1 - Weights
F2 - GRAPH
SAMPLE ID XXXXXXXX
F3 - PRN GRAPH
F 4 - Exi t
10. Remove the beaker from the instrument cavity. Using the thermometer, stir the water for 30 seconds. Measure and record the
peak temperature reading. This is the final water temperature
(Tf).
11. Press F4.
TIME
XX :XX xx
DRY TIME
0 2 : 0 0
XXXXXXXX
ID POWER
1 0 0 %
MOISTURE
UNDER
Wt. X.XXXXg
12. Calculate microwave power output as follows:

Power in Watts = 35 (Tf - Ti)
13. If the measured power is below 580 watts, repeat the power measurement test by performing steps 4 through 12. If the measured
power remains below 580W, contact the CEM Corporation Service
Department or your local distributor.
14. Press F4 to exit program.
150
LabWave 9000
600066
Rev. 1
Are You Sure!

F1 - Resume
F4 - Quit
Error Messages
Due to improper system operation or component failure, the following
error messages can appear on the display:
Receive Time Out Error!

Check Balance Cables,
Power, Stability, etc.
F1 - Retry
F4 - Abort
Framing Error.
F1 - RETRY
F4 - ABORT
The above error messages appear as an indication of a communication

error with the external balance during syringe weigh or dilutions analyses. Press F1 to retry analysis. If error message displays again,
abort the test by pressing F4. Check external balance to ensure that
it is properly connected to an appropriate power outlet and to the
external balance port of the LabWave 9000. Verify the stability of the
external balance. If error message continues to appear, contact the
CEM Corporation Service Department or the local distributor.
LabWave 9000
600066
Rev. 1
151
Calibration Error. Aborting

Err 08
Press Any Key
The balance error messages above appears when the instrument is

turned on prior to installation of the balance stem and pan or if weight
is applied to the balance prior to turning the instrument on. To clear
this message, turn the instrument off and ensure that the balance
stem and pan are installed and that no weight is being applied to the
balance prior to turning the instrument on.
Stack Overflow
Contact Factory
Op Code Error
SP XXXX
Illegal Int Error

SP XXXX
The three error messages above indicate component failure. If any of

these error messages appear on the display, turn the LabWave 9000
off. Do not attempt further operation. Call the CEM Corporation
Service Department or your local distributor for service assistance.
152
LabWave 9000
600066
Rev. 1
Troubleshooting
WARNING
The LabWave 9000 utilizes high voltage and
microwave radiation. Instrument service and
repair must be undertaken only by technicians
trained in the repair and maintenance of high
voltage and microwave power systems.
The most important principle in troubleshooting the LabWave 9000 is
to check each component of the system separately and trace any malfunction to its source.
Verify each of these factors:
Balance Calibration (page 20)
Microwave Power (page 148)
Standard Solution (page 25)
Analytical Method (Verify method of analysis.) If necessary, contact CEM Corporation or your local distributor for assistance.
In most cases, an analysis of the symptoms will lead to the area in
which a defect is located. For example, if no microwave power is being
produced, check the following components which affect microwave
production:
15A fuses in 120V instruments or 8A fuses in 240V instruments
Door interlock switches
High voltage and filament transformers, high voltage capacitor,
magnetron and associated wiring
Thermal switches
Mode stirrer
Control Boards
LabWave 9000
600066
Rev. 1
153
Troubleshooting Guide
Symptom
Possible Cause/Remedy
LabWave 9000 inoperative.
Ensure that instrument is

properly connected to power outlet
and that instrument is switched on.
Check fuses and replace if nec
essary.
Balance will not tare.
Balance overloaded; use less

sample.
Balance not opearting.
Check 0.5A fuse in instrument

pedestal and replace if necessary.
No microwave drying.
Door not closed properly.

Check 15A fuses (8A fuses for 240V
units) and replace if necessary.
Sample burning.
Sample too large and/or unevenly

applied to pad. Sample not homo
geneous. Power level too high.
Results not reproducible.
Sample applied unevenly to pad.

Sample not homogeneous and
absorbs microwaves unevenly.
Keep sample container closed when
not extracting sample. Work quickly
when applying sample to pads and
placing on balance pan.
Incorrect results.
Verify proper sample handling and

method parameters.
At the end of the test, the

display reads Data Results
Invalid.
Final weight greater than

initial weight. Repeat test.
Check balance calibration
Door Open Message
Ensure that instrument door is

properly closed.
A qualified service technician, using the schematics located in the

Appendix and standard troubleshooting techniques, should be able to
identify and resolve operational problems. If a problem persists, call
the CEM Corporation Service Department or your local distributor for
assistance.
154
LabWave 9000
600066
Rev. 1
Service and Repair

WARNING
The LabWave 9000 utilizes high voltage and
microwave radiation. Instrument service and
repair must be undertaken only by technicians
trained in the repair and maintenance of high
voltage and microwave power systems.
If damage to the LabWave 9000 is detected, do not attempt further
instrument operation. Contact the CEM Corporation Service Department or your local distributor.
CEM Corporation
Service Department
3100 Smith Farm Road
P.O. Box 200
Matthews, NC 28106-0200
Within the United States
(800) 726-5551
(704) 821-7015
FAX (704) 821-4368
Outside the United States
(704) 821-7015
FAX (704) 821-4368
E-mail: service@cemx.com
CEM Ltd.
2 Middle Slade
Buckingham Ind. Park
Buckingham MK18 1WA
United Kingdom
Tel: (44) 1-280-822873
Fax: (44) 1-280-822342
CEM GmbH
Carl-Friedrich-Gauss-Str. 9
47475 Kamp-Lintfort
Germany
Tel: (49) 2842-96440
Fax: (49) 2842-964411
CEM S.r.l.
Via DellArtigianato, 6/8
24055 Cologno al Serio (Bg)
Italy
Tel: (39) 35-896224
Fax: (39) 35-891661
It is recommended that service and repair by the user be limited to

identifying and replacing defective sub-system modules such as
printed circuit boards, transformers, fans, lamps, or motors. The user
may find it convenient to stock an assortment of replacement parts to
facilitate service procedures. A list of recommended spare parts is provided on page 161.
WARNING
To avoid possible electrical shock or exposure to
microwave energy, disconnect instrument from
electrical outlet prior to any disassembly procedures.
LabWave 9000
600066
Rev. 1
155
To remove the cover of the LabWave 9000 for service to the high voltage components, remove the screws located along the bottom of the
sides and back of the cover. Pull back and lift up on the cover to
remove it from the instrument cavity.
WARNING
Prior to troubleshooting or replacement of any
component in the high voltage section of the LabWave 9000, the instrument must be switched off
and unplugged from the electrical outlet. Permit
instrument to sit idle for at least two minutes.
Using a well insulated screwdriver, touch the
end of the screwdriver between terminals of the
high voltage capacitor (illustrated in figure 6) to
discharge all residual voltage from the instrument.
Prior to replacement of the cover, visually check the components to
ensure the integrity of electrical connections. Install the cover carefully to avoid damage to wiring or internal components.
After performing any service to or inspection of the LabWave 9000
which requires removal of the cover or replacement of components in
the instrument door, interlock assemblies, or microwave generation
system, perform a microwave leakage measurement, page 147, prior to
instrument operation.
Figure 6. Discharge of Residual Voltage from High Voltage

Capacitor
156
LabWave 9000
600066
Rev. 1
Transformer
(149900)
(240V, 50 Hz only)
Power Supply
(115270)
0.5A Fuse
(188350)
Balance
(003022)
Pedestal
Access
PC Board
(532000-RA-P)
Sub-D
Assembly
Board
(203180-P)
(Not Shown)
Figure 7. LabWave 9000 with Cover Removed and Cavity Hinged

for Service of Pedestal Components
LabWave 9000
600066
Rev. 1
157
Exhaust
Fan
(184860)
Magnetron
Thermal
Switch (142020)
Magnetron
(111280)
Magnetron
Cooling Fan
(184900)
High Voltage
Rectifier (189702)
AC/DC
Control Board
(532010)
High Voltage
Capacitor (103010)
High Voltage
Transformer
120V - (149230)
240V - (149310)
Line
Filter
(230293)
On/Off
Switch
(142000)
Transformer
Cooling Fan
(184900)
Fuses
15A - 120V
(188320)
8A - 240V
(188331)
Power Cord
Receptacle
(251460)
Filament
Transformer
(149910)
Triac
(150261)
Figure 8. LabWave 9000 with Cover Removed

for Service in High Voltage Section
158
LabWave 9000
600066
Rev. 1
Front of
Instrument
Keyboard (500811-P)
Display
Control
Board
(203170-P)
Display
LCD Board
(304025)
Secondary
Interlock
Assembly
(500740)
(See figure 10)
Mode
Stirrer
Motor
(304011)
Isolator
Thermal Switch
(143100)
Figure 9. LabWave 9000 Front Panel (from rear of unit)
Front of
Instrument
Adjustment Screw
Interlock Switch
Door Arm
Interlock Switch
Adjustment Screw
Figure 10. Secondary Interlock Assembly
LabWave 9000
600066
Rev. 1
159
Adjustment
Screw
Interlock
Switches
Adjustment
Screw
Figure 11. Primary Interlock Assembly
ABC
DEF
GHI
JKL
MNO
PQR
STU
VWX
YZ
SPACE
SYMBOL
START
STOP
ENTER
Innovators in
Microwave Technology
Balance Pan
(004120)
Balance Stem
(003670)
RF Stub
(016540)
;;;;;;;;;;;;;;;;;;;;;;;;;;;;;
;;;;;;;;;;;;;;;;;;;;;;;;;;;;;
Figure 12. Balance Pan and Balance Stem
160
LabWave 9000
600066
Rev. 1
VIII Ordering Information

Use a copy of this page as an order form when ordering spare parts
listed below. Mail, call or fax your order to CEM Corporation.
CEM Corporation
P.O. Box 200
(800) 726-3331 (704) 821-7015 FAX (704) 821-6314
Part No.
003670
004120
004150
500200
188320
188331
200150
203400
300500
302001
302150
302860
302600
Description
Balance Stem
Balance Pan, Plastic
Balance Pan, Glass, 3 Diameter
Balance Air Shield
15A Fuse (120V Instrument)
8A Fuse (240V Instrument)
Glass Fiber Sample Pads, Square, Box of 400*
Thermapad, G120
Microwave Test Meter, Holaday
Teflon Coated Spatula
Disposable Pipettes
Starter Accessory Kit
Standard Test Solution
*Blanket orders for sample pads ensure a continuous supply.
When placing an order, please provide the following information:

Company Name
Shipping Address (Street, City, State, Zip Code)
Billing Address (Street or P.O. Box, City, State, Zip Code)
Ship to the Attention of:
Your Name and Telephone No.
Purchase Order No.
LabWave 9000
600066
Rev. 1
161
162
LabWave 9000
600066
Rev. 1
IX Specifications
Moisture/Solids Range:
0.01% to 99.99% in Liquids, Solids and

Slurries. 0.01% Resolution
Balance Capacity:
50 Grams
0.1 mg. Readability
Microwave Power:
0 to 100% Power (630 50 watts) in 1%

Increments
Program Storage:
40 Methods
Protected by Password Against
Unauthorized Usage
Data Entry:
Alphanumeric Keypad
Display:
High Resolution Backlit LCD

Graphics Display
Printer Port:
25-PIN, Parallel Type
Computer Port:
RS-232, 9-PIN, IBM AT Compatible
External Balance Port:
RS-232, 9-PIN
Electrical Requirements:
108/125 VAC, 60 Hz, 15 Amps

220/250 VAC, 50 Hz, 8 Amps
Instrument Dimensions:
21.4 in. x 18.1 in. x 22.5 in.

54.4 cm. x 46.0 cm. x 57.2 cm.
Weight:
110 lbs.
50 kg.
Emission and Safety Approvals
78355
Conforms to UL Std. 3101
Emissions Complies with FCC part 18 (47 CFR part 18

Industrial, scientific and Medical Equipment).
Safety ETL* approved to UL standard 3101 (Laboratory
Equipment).
CSA** approved to standard CAN/CSA C22.2 No. 1010.1
(Laboratory Equipment).
European Community
Certified to
CAN/CSA C22.2 No. 1010.1
CE
LabWave 9000
600066
Rev. 1
U.S. and Canada
Emissions Conforms to EC standard EN 55011 (Emissions for

Industrial, Scientific and Medical Equipment).
Conforms to EC standard EN50082-2 (Electromagnetic
Compatability).
Safety Conforms to EC standard IEC 1010-1 (Safety
Requirements for Electrical equipment for measurement,
control and laboratory use - Part 1).
*ETL and UL are equivalent NRTLs (Nationally Recognized Testing
Laboratories)
**CSA is approved testing laboratory by the Standards Council of Canada
163
164
LabWave 9000
600066
Rev. 1
Warranty
What Is Covered:
CEM Corporation warrants that the instrument will be free from any defect
in parts or workmanship and will, at its option, replace or repair any defec
tive part (excluding consumables) or instrument.
For How Long:
This warranty remains in effect for 365 days from date of delivery to the
original purchaser.
What Is Not Covered:
This warranty does not cover parts or workmanship which have been damaged due to:
Neglect, abuse or misuse,
Damage caused by or to test samples,
Damage incurred during instrument relocation,
Damage caused by or to any attached equipment,
Use of incorrect line voltages or fuses,
Fire, flood, acts of God, or other contingencies beyond the control of
CEM Corporation,
Improper or unauthorized repair, or
Any other damage caused by purchaser or its agents.
Responsibilities of Purchaser:
To ensure warranty coverage, purchaser must:
Use the instrument according to directions
Connect the instrument properly to a power supply of proper voltage
Replace blown fuses
Replace consumables, and
Clean the instrument as required.
How to Get Service:
Purchaser should contact the Service Department of CEM Corporation or
your distributor for return authorization and for proper crating and
shipping instructions to return instrument, freight prepaid, for service.
On-site repairs by an authorized service technician are available through
the CEM Service Department. Travel costs will be charged to the purchaser
for on-site repairs.
Within the U.S.:
CEM Corporation
3100 Smith Farm Rd.
(800) 726-5551
Fax: (704) 821-4368
Outside the U.S.:

CEM Corporation
3100 Smith Farm Rd.
(704) 821-7015
Fax: (704) 821-4368
Warranty Disclaimer:
CEM Corporation hereby excludes and disclaims any warranty of merchantibility or fitness for any particular purpose. No warranty, express or implied,
extends beyond the face hereof. CEM Corporation shall not be liable for loss of
use of instrument or other incidental or consequential costs, expenses or dam
ages incurred by the purchaser or any other user.
Purchasers Rights under State Law:
This warranty gives the purchaser specific legal rights, and the purchaser
may also have other rights which vary from state to state.
LabWave 9000
600066
Rev. 1
165
Customer Support Service Contacts

For customer support in the areas of service, applications or sales,
call the following toll-free numbers.
Service Assistance (800) 726-5551
Applications Assistance (800) 726-3331
Sales Assistance (800) 726-3331
166
LabWave 9000
600066
Rev. 1

CEM Labwave 9000

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Operation Manual

Copyright 1999 by CEM Corporation

FAX: (704) 821-7894

To the best of our knowledge, the information contained herein is

Warnings, Cautions and Notes

Table of Contents (Continued)

Maintenance, Troubleshooting and Service

VIII Ordering Information

The CEM LabWave 9000 Moisture/Solids Analyzer is an analytical

Figure 2. Front View

Start/Stop Press to begin or stop sample analysis. Microwave

Figure 4. Rear View

Magnetron Cooling Fan draws air through the magnetron.

Personal Computer or Serial Printer Setup (Port J2)

External Balance Installation

External Balance Setup (Port J1)

2. Press F3 to activate the System Setup screen.

ANY KEY - MAIN MENU

3. Press F1 to set date/time format.

4. Hour Format can be set for either 12 hour or 24 hour format.

ANY KEY - MAIN MENU

8. Press F2 to activate the Set System Parameters screen.

SET SYSTEM PARAMETERS

Any Key - Exit

Press F1 to activate the Select Printer/Balance screen.

Any Key - Exit

10. Press F1 to activate the Select Printer screen.

Up/Dn Arr - Sel

Any Key - Exit

12. Press F2 to activate the Select Print Style screen.

Any Key - Exit

15. Press F3 to activate the Select Print Form screen.

F 1 - Print Data in Rows

16. Print form can be set to print data in rows or columns. If

Example: Data Results Screen

Note: Press F2 for display of graph.

17. Press Enter to exit to the Select Printer/Balance screen.

Any Key - Exit

18. Press F4 to activate Select External Balance screen.

Up/Dn Arr - Sel

19. Available external balances include Denver Instrument,

Any Key - Exit

Any Key - Exit

21. Press F2 to activate the Utilities screen.

Set Display Contrast

Any Key - Exit

22. Press F1 to activate the Set Display Contrast screen.

USE UP and DOWN ARROWS

Set Display Contrast

Any Key - Exit

25. Press any numeric key to exit.

Any Key - Exit

26. Press F3 to activate System Info screen.

Any Key - Exit

27. Press F1 to activate System Data screen.

28. Press F4 to exit.

Any Key - Exit

29. Press F2 to activate Print Profile Data screen.

Profile Data to Prn

Any Key - Exit

Note: Profile data is time and weight readings transmitted through

31. PC line termination is based on the PC software. Press F1 to

Any Key - Exit

32. Press F3 to activate Software Version screen.