Академический Документы
Профессиональный Документы
Культура Документы
Syntesis)
Name
= Correction
The reduction of particle size to the nanometer scale leads to substantial changes
properties of zeolite which make them as promising materials for many applications.
in
Many other researchers reported the success of nanozeolite synthesis which indicate the
interesting and promising prospect of nanozeolite technology.
In preparation of LTA, two typical solutions have been deployed, namely solution-1 and
solution-2. The solution-1 is composed of aluminum tri-isopropoxide(Al(OiPr)3, 99.99%,
Sigma-Aldrich) dispersed in distillated water and sodium hydroxide (NaOH, 1M).
Furthermore, the solution was vigorously stirred for an hour.
Two kind of solution (namely solution1 and solution 2) must be prepared for
LTA. solution 1 is composed of alumunium triisopropoxide (Al(OiPr)3,99,99%,
Sigma-Aldrich) dispersed in distillated water and NaOH 1M, stir the solution
for an hour.
The first investigation result obtained in this report shows that nanocrystalline zeolite A can
be synthesised effectively at temperatures of 80 C-150 C with initial Si/Al ratio of 1.46,
3.06, 4.59 and 6.79.
It can be seen from the pictures that higher crystallization time and Temperature will
result in the increase of average particle size. However, for LTA-6 and LTA-21 the
difference of the average particle size is not significant.
The picture show that temperature and time influence in increasing of average
particle size. Althought, the difference in some matter is not significant.